JPH09272516A - Manufacture of hot-filled drink to be packed in container - Google Patents

Manufacture of hot-filled drink to be packed in container

Info

Publication number
JPH09272516A
JPH09272516A JP8111316A JP11131696A JPH09272516A JP H09272516 A JPH09272516 A JP H09272516A JP 8111316 A JP8111316 A JP 8111316A JP 11131696 A JP11131696 A JP 11131696A JP H09272516 A JPH09272516 A JP H09272516A
Authority
JP
Japan
Prior art keywords
beverage
pressure
treated
feeding
heat exchanger
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
JP8111316A
Other languages
Japanese (ja)
Other versions
JP3643172B2 (en
Inventor
Koji Hashimoto
浩二 橋本
Masami Matsunaga
正見 松長
Shigeki Matsuura
茂樹 松浦
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Daiwa Can Co Ltd
Original Assignee
Daiwa Can Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Daiwa Can Co Ltd filed Critical Daiwa Can Co Ltd
Priority to JP11131696A priority Critical patent/JP3643172B2/en
Publication of JPH09272516A publication Critical patent/JPH09272516A/en
Application granted granted Critical
Publication of JP3643172B2 publication Critical patent/JP3643172B2/en
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

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  • Filling Of Jars Or Cans And Processes For Cleaning And Sealing Jars (AREA)
  • Food Preservation Except Freezing, Refrigeration, And Drying (AREA)

Abstract

PROBLEM TO BE SOLVED: To sufficiently deaerate drink to be processed in high-temperature short-time sterilization for manufacturing without losing color and flavor at the time of mixing the drink by preheating the drink to the vicinity of its boiling point, then deaerating under a normal pressure, and further sufficiently sterilizing it at a high temperature with pressure applied thereafter. SOLUTION: When drink to be processed is rapidly heated to the vicinity of its boiling point by a preheating means 32 under an approximately normal pressure, dissolved oxygen appears as bubbles. When it reaches a temporary reservoir 34 of a deaerating means, oxygen in the drink is discharged into a head space for removing head space gas, thereby discharging the oxygen in the drink from the temporary reservoir 34. The deoxidized drink is supplied by a pressure-feeding means 36 with pressure applied and sterilized in a short time at a high temperature of 100 deg.C or higher with pressure applied by a sterilizing means 38. The sterilizing means 38 for sterilizing at a high temperature with pressure applied heats the deaerated drink, thereby improving heating efficiency.

Description

【発明の詳細な説明】Detailed Description of the Invention

【0001】[0001]

【発明の属する技術分野】本発明は容器詰め熱間充填飲
料の製造方法及び装置、特に高温短時間殺菌処理におけ
る脱気機構の改良に関する。
BACKGROUND OF THE INVENTION 1. Field of the Invention The present invention relates to a method and an apparatus for producing a hot-filled beverage packed in a container, and more particularly to improvement of a deaeration mechanism in a high temperature short time sterilization process.

【0002】[0002]

【従来の技術】缶詰、瓶詰等の飲料については、貯蔵中
の腐敗を避けるため殺菌処理を行うことが必須である。
この殺菌処理には、ごく特殊な例ではフィルターなどを
用いた非加熱殺菌を採用することもあるが、通常は加熱
殺菌が行われる。飲料の加熱殺菌法としては、飲料を
缶、瓶等に充填、密封した後に加熱するレトルト殺菌
法、飲料を高温状態で缶などに充填し高温状態のまま直
ちに密封する熱間充填法、及び充填前に飲料を例えば百
数十℃で短時間(数十秒程度)維持して殺菌する高温短
時間殺菌法がある。
2. Description of the Related Art Beverages such as canned and bottled products must be sterilized in order to avoid spoilage during storage.
For this sterilization treatment, non-heat sterilization using a filter may be adopted in a very special case, but usually heat sterilization is performed. As the heat sterilization method for beverages, a retort sterilization method in which beverages are filled into cans, bottles, etc., sealed and then heated, a hot filling method in which beverages are filled into cans in a high temperature state and immediately sealed in a high temperature state, and filling Before that, there is a high-temperature short-time sterilization method in which a beverage is maintained at, for example, one hundred and several tens of degrees Celsius for a short time (about several tens of seconds) and sterilized.

【0003】前記レトルト殺菌法は、缶詰状態で殺菌さ
れるため、充填時に多少の菌汚染が生じたとしてもレト
ルト殺菌中に死滅することから、充填前後における工程
管理が容易であるという利点がある。しかしながら、殺
菌終了後に缶詰、瓶詰という比較的容量の大きい容器中
の高温の飲料を急速に冷却することは極めて困難であ
り、飲料が比較的長時間(数十分間)にわたり高温に維
持され、味、香りが変わるなどの欠点がある。
Since the retort sterilization method is sterilized in a canned state, even if some bacterial contamination occurs during filling, it is killed during retort sterilization, so that there is an advantage that process control before and after filling is easy. . However, it is extremely difficult to rapidly cool a hot beverage in a container having a relatively large capacity such as canned and bottled after sterilization is completed, and the beverage is maintained at a high temperature for a relatively long time (tens of minutes), There are drawbacks such as changes in taste and aroma.

【0004】一方、高温短時間殺菌法及び熱間充填法
は、飲料を細管式熱交換器、プレート式熱交換器などに
通し、短時間で高温にし、容器に充填・密封して、充填
・密封後のレトルト殺菌をなくすことにより味、香りの
よい飲料缶詰が得られるという利点を有し、最近の飲料
缶詰の殺菌法として注目されている。特に、ウーロン
茶、紅茶、緑茶等の茶類飲料には抗菌物質であるカテキ
ン類が含まれているため、近年は、レトルト殺菌を行わ
ずに高温短時間殺菌後90−95℃で熱間充填する方法
がとられている。また、従来は、その高酸性を有するた
め、比較的緩和な条件で殺菌されていた果実飲料も、海
外からの原料輸入の結果、高温耐性を持つ細菌が発見さ
れている。この場合も高温短時間殺菌後90−95℃で
熱間充填されている。
On the other hand, in the high-temperature short-time sterilization method and the hot filling method, the beverage is passed through a thin tube heat exchanger, a plate heat exchanger, etc., heated to a high temperature in a short time, filled / sealed in a container, and filled / filled. By eliminating the retort sterilization after sealing, it has the advantage that a canned beverage with a good taste and aroma can be obtained, and it has attracted attention as a recent sterilization method for beverage canning. In particular, tea beverages such as oolong tea, black tea, and green tea contain catechins that are antibacterial substances, so in recent years, hot refilling at 90-95 ° C. is performed without sterilization by retort after hot sterilization. The method is taken. Further, as for the fruit drink, which has been conventionally sterilized under relatively mild conditions due to its high acidity, bacteria having high temperature resistance have been discovered as a result of importing raw materials from abroad. Also in this case, hot filling at 90 to 95 ° C. is performed after high temperature short time sterilization.

【0005】[0005]

【発明が解決しようとする課題】一方、飲料の変質は加
熱時間だけでなく、溶存酸素濃度にも大きく依存してお
り、例えば容器詰め茶飲料は、溶存酸素によって経時的
に変色するため、加熱殺菌時間と共に溶存酸素の低減が
強く要望されている。一般に溶液の温度が上がることに
より溶存酸素量は低下するため、前記熱間充填法にあっ
ては、飲料を充填する前に高温槽中に滞留させることに
より脱気できるが、高温短時間殺菌法にあっては加圧下
に高温処理されるため殺菌中での脱気は行われず、溶存
酸素に起因する色素、香気成分などの酸化変性が大きな
問題となっている。
On the other hand, the deterioration of the beverage is largely dependent not only on the heating time but also on the dissolved oxygen concentration. For example, a packaged tea beverage changes its color with time due to dissolved oxygen. There is a strong demand for reduction of dissolved oxygen with sterilization time. In general, the amount of dissolved oxygen decreases as the temperature of the solution rises, so in the hot filling method, it can be degassed by staying in a high temperature tank before filling the beverage, but the high temperature short time sterilization method In this case, since high-temperature treatment is performed under pressure, deaeration is not performed during sterilization, and oxidative modification of pigments, aroma components, etc. due to dissolved oxygen is a serious problem.

【0006】従来より、例えば特開平1−317586
号に示されるように原料水の脱気は行われているが、飲
料調合時に酸素が再度とけ込む可能性がある。ところ
が、調合済み飲料の脱気は行われておらず、また、特に
茶飲料など、酸化による変色が生じやすい飲料において
は、溶存酸素2ppm以下程度が品質保持のため要望され
ている。しかし、前記従来の一般的な減圧脱気法ではこ
の要望を達成することは到底不可能であった。また、果
実飲料にあっても、その本来有する香味、色素は酸化に
より容易に劣化するため、低酸素濃度下での短時間での
殺菌が望まれている。本発明は前記従来技術の課題に鑑
みなされたものであり、その目的は高温短時間殺菌法に
おいて脱気効率の高い容器詰め熱間充填飲料の製造方法
及び装置を提供することにある。
Conventionally, for example, Japanese Patent Laid-Open No. 1-317586
Although the raw water is degassed as shown in No. 6, the oxygen may melt again when the beverage is prepared. However, a prepared beverage has not been deaerated, and particularly in a beverage such as a tea beverage, which is susceptible to discoloration due to oxidation, a dissolved oxygen content of about 2 ppm or less is required to maintain quality. However, it has been impossible to achieve this demand by the conventional general vacuum degassing method. Further, even in fruit drinks, the inherent flavors and pigments thereof are easily deteriorated by oxidation, so sterilization in a short time under low oxygen concentration is desired. The present invention has been made in view of the above-mentioned problems of the prior art, and an object thereof is to provide a method and an apparatus for producing a packaged hot-filled beverage in a container having high degassing efficiency in a high-temperature short-time sterilization method.

【0007】[0007]

【課題を解決するための手段】前記目的を達成するため
に本発明にかかる容器詰め熱間充填飲料の製造方法は、
被処理飲料を略常圧下で送給する送給手段と、該送給手
段で送給する被処理飲料を狭路中で熱交換によりその沸
点近傍の温度まで急速加熱する予熱工程と、上部にヘッ
ドスペースを有する一時貯留槽内に前記予熱工程で予熱
された被処理飲料を常圧下に短時間保持し、そのヘッド
スペースガスを除去する脱気工程と、該脱気工程で脱気
された被処理飲料を圧送する圧送工程と、該圧送工程に
より圧送される被処理飲料を狭路中で熱交換により10
0℃以上の高温、加圧下で短時間殺菌処理する殺菌工程
と、殺菌が終了した被処理飲料を直ちに95℃乃至90
℃の熱間充填温度まで急速冷却する冷却工程と、前記熱
間充填温度に冷却された被処理飲料を、少なくとも内面
側を洗浄済みの容器に充填し、実質的に酸素との接触を
絶ちつつ密封する充填工程と、を備えたことを特徴とす
る。
In order to achieve the above object, a method for producing a packaged hot-filled beverage according to the present invention comprises:
A feeding means for feeding the beverage to be treated under substantially normal pressure, a preheating step for rapidly heating the beverage to be fed by the feeding means to a temperature near its boiling point by heat exchange in a narrow path, and an upper portion In the temporary storage tank having a head space, the beverage to be treated preheated in the preheating step is held under normal pressure for a short time, and a deaeration step of removing the headspace gas, and a deaeration step deaerated in the deaeration step The pressure-feeding step of pressure-feeding the treated beverage, and the beverage to be treated pressure-fed by the pressure-feeding step are performed by heat exchange in a narrow path.
A sterilization step of sterilizing at a high temperature of 0 ° C or higher and under pressure for a short time, and the treated beverage after sterilization is immediately heated to 95 ° C to 90 ° C.
A cooling step of rapidly cooling to a hot filling temperature of ℃, the beverage to be treated cooled to the hot filling temperature, at least the inner surface side is filled in a washed container, while substantially interrupting the contact with oxygen And a filling step of sealing.

【0008】また、本発明にかかる装置は、被処理飲料
を略常圧下で送給する送給手段と、該送給手段により送
給される被処理飲料をその沸点近傍の温度まで急速加熱
する熱交換器と、加熱された被処理飲料をヘッドスペー
ス部を保持した状態で短時間貯留し得る一時貯留槽と、
該貯留槽のヘッドスペース部から排気を行う手段とから
成る脱気手段と、該脱気手段により脱気された被処理飲
料を圧送する圧送手段と、該圧送手段により圧送される
被処理飲料を加圧下100℃以上で高温短時間殺菌処理
する熱交換器と、殺菌済みの被処理飲料を95℃乃至9
0℃熱間充填温度まで急速冷却する熱交換器と、前記熱
間充填温度の被処理飲料を、少なくとも内面側を洗浄済
みの容器に充填し、実質的に酸素との接触を絶ちつつ密
封する充填装置及び密封装置とから構成される充填手段
と、を備えたことを特徴とする。
Further, the apparatus according to the present invention rapidly feeds the beverage to be treated under a substantially normal pressure and the beverage to be treated fed by the feeder to a temperature near its boiling point. A heat exchanger, a temporary storage tank capable of storing a heated beverage to be treated for a short time while holding the head space portion,
A deaeration means comprising a means for exhausting air from the head space of the storage tank, a pressure feeding means for pressure-fed the beverage to be treated deaerated by the deaeration means, and a beverage to be pressure-fed by the pressure feeding means. A heat exchanger that sterilizes at a high temperature for a short time at a temperature of 100 ° C or more under pressure and a sterilized beverage to be treated at 95 ° C to 9 ° C.
A heat exchanger that rapidly cools to a hot filling temperature of 0 ° C. and a beverage to be treated at the hot filling temperature are filled in a container that has been cleaned at least on the inner surface side and sealed while substantially cutting off contact with oxygen. And a filling device including a filling device and a sealing device.

【0009】[0009]

【発明の実施の形態】本発明にかかる容器詰め熱間充填
飲料の製造方法及び装置は、前述したように予熱手段に
より略常圧下で被処理飲料をその沸点近傍まで急速加熱
する。この状態で被処理飲料中の溶存酸素の溶解度は急
激に低下し、過飽和ないし場合により気泡として出現す
る。そして、脱気手段の一時貯留槽に至ると、前記飲料
中酸素はヘッドスペース部分に放出され、該ヘッドスペ
ースガスが除去されることにより飲料中酸素は一時貯留
槽から放出される。そして、脱酸素が行われた被処理飲
料は圧送手段により加圧状態で送給され、殺菌手段によ
り加圧下に100℃以上の高温下で短時間に殺菌が行わ
れる。
BEST MODE FOR CARRYING OUT THE INVENTION As described above, the method and apparatus for producing a hot-packed beverage packed in a container according to the present invention rapidly heats the beverage to be treated to a temperature near its boiling point under substantially normal pressure by the preheating means. In this state, the solubility of dissolved oxygen in the beverage to be treated drops sharply and appears as supersaturation or in some cases bubbles. Then, when reaching the temporary storage tank of the degassing means, the oxygen in the beverage is released to the headspace portion, and the oxygen in the beverage is released from the temporary storage tank by removing the headspace gas. Then, the deoxidized beverage to be processed is fed in a pressurized state by the pressure feeding means, and sterilized in a short time at a high temperature of 100 ° C. or higher under pressure by the sterilizing means.

【0010】なお、一時貯留槽に貯留される時間は短時
間、すなわち、数秒〜十数秒程度である。従って、予熱
手段、脱気手段、及び殺菌手段で被処理飲料が高温に維
持される時間は短く、この間の被処理液の変性は最小限
に抑えられる。しかも、高温、加圧下に殺菌処理する殺
菌手段においては、脱気された被処理飲料が加熱対象で
あるので、加熱効率がよい。以下、図面に基づき本発明
の好適な実施態様について説明する。図1は本発明の一
実施態様にかかる容器詰め熱間充填飲料の製造装置の概
略構成が示されている。同図に示す容器詰め熱間充填飲
料製造装置10は、飲料調合装置12と、飲料の脱気・
殺菌・充填・密封装置14とからなる。
The time of storage in the temporary storage tank is short, that is, several seconds to ten and several seconds. Therefore, the preheating means, the deaerating means, and the sterilizing means maintain the beverage to be treated at a high temperature for a short period of time, and the denaturation of the liquid to be treated during this period is minimized. Moreover, in the sterilizing means for performing sterilization treatment under high temperature and pressure, the degassed beverage to be treated is an object to be heated, so that the heating efficiency is good. Hereinafter, preferred embodiments of the present invention will be described with reference to the drawings. FIG. 1 shows a schematic configuration of an apparatus for producing a container-filled hot-filled beverage according to an embodiment of the present invention. The hot-filled beverage production apparatus 10 for container filling shown in FIG.
It comprises a sterilization / filling / sealing device 14.

【0011】そして、前記飲料調合装置12は、イオン
交換水が貯留された密閉脱気槽16と、密閉脱気槽16
を減圧下に置く真空ポンプ18と、前記密閉脱気槽16
に貯留されたイオン交換水を送給するサニタリーポンプ
20と、サニタリーポンプ20により送給される脱気イ
オン交換水を切換弁21を介して、一方の脱気イオン交
換水を50〜80℃に加温する熱交換器22と、熱交換
器22から送給される加温イオン交換水が送給される茶
葉抽出装置23と、茶葉抽出装置23で抽出された濃厚
茶葉抽出液が貯留された原液タンク26と、前記切換弁
21を介した他方の脱気イオン交換水が送給される脱気
イオン交換水を貯留する調合タンク24とを含む。そし
て、調合タンク24には脱気されたイオン交換水と濃厚
茶葉抽出液が順次供給され、所望の濃度の茶飲料が調整
される。
The beverage preparation device 12 has a closed degassing tank 16 in which ion-exchanged water is stored and a closed degassing tank 16
A vacuum pump 18 for placing the air under reduced pressure and the closed deaeration tank 16
Of the degassed ion-exchanged water sent to the sanitary pump 20 and the degassed ion-exchanged water sent from the sanitary pump 20 through the switching valve 21 to 50 to 80 ° C. A heat exchanger 22 for heating, a tea leaf extractor 23 to which warm ion-exchanged water sent from the heat exchanger 22 was sent, and a concentrated tea leaf extract solution extracted by the tea extractor 23 was stored. It includes a stock solution tank 26 and a preparation tank 24 for storing the degassed ion exchanged water to which the other degassed ion exchanged water is fed via the switching valve 21. Then, the degassed ion-exchanged water and the concentrated tea leaf extract are sequentially supplied to the mixing tank 24 to adjust a tea beverage having a desired concentration.

【0012】一方、本発明において特徴的な容器詰め飲
料の脱気・殺菌・充填・密封装置14は、送給手段を構
成する送給ポンプ30と、予熱手段を構成する第1プレ
ート式熱交換器32と、脱気手段を構成する一時貯留槽
34と、圧送手段を構成する圧送ポンプ36と、殺菌手
段を構成する第2プレート式熱交換器38と、冷却手段
を構成する第3プレート式熱交換器40と、圧力制御弁
42と、充填手段を構成する充填装置及び密封装置とか
ら成る充填・密封装置44とを含む。そして、前記送給
ポンプ30は、調合タンク24に貯留された調合済み茶
飲料を略常圧下で第1プレート式熱交換器32へ送給す
る。
On the other hand, the deaeration / sterilization / filling / sealing device 14 of the container-packed beverage, which is a characteristic of the present invention, has a feed pump 30 constituting a feed means and a first plate type heat exchange constituting a preheating means. 32, a temporary storage tank 34 that constitutes deaeration means, a pressure feed pump 36 that constitutes pressure feed means, a second plate heat exchanger 38 that constitutes sterilization means, and a third plate type that constitutes cooling means. It includes a heat exchanger 40, a pressure control valve 42, and a filling / sealing device 44 including a filling device and a sealing device that form a filling means. Then, the feed pump 30 feeds the prepared tea beverage stored in the preparation tank 24 to the first plate heat exchanger 32 under substantially normal pressure.

【0013】第1プレート式熱交換器32は、送給ポン
プ30より送給される茶飲料を狭路中で熱交換によりそ
の沸点近傍の温度まで急速加熱する。ここで、茶飲料の
場合には例えば95℃程度まで加熱することが好適であ
り、熱交換器32での加熱は沸点以下であるので、加圧
を行う必要はなく常圧のまま昇温すればよい。
The first plate heat exchanger 32 rapidly heats the tea beverage fed from the feed pump 30 to a temperature near its boiling point by heat exchange in a narrow path. Here, in the case of a tea beverage, for example, it is preferable to heat it up to about 95 ° C., and since the heating in the heat exchanger 32 is below the boiling point, it is not necessary to pressurize and the temperature can be raised at normal pressure. Good.

【0014】また、前記一時貯留槽34はヘッドスペー
スを有するタンクよりなり、貯留槽34には前記熱交換
器32で予熱された茶飲料が常圧下に短時間保持され
る。そして、貯留槽34のヘッドスペースガスは図示を
省略した吸引ポンプ等により貯留槽34内が常圧よりも
高圧にならないように除去される。なお、貯留槽34へ
の茶飲料の滞留時間は数秒〜十数秒であることが好適で
あり、数十秒ないし数分貯留させるように構成すると貯
留槽34の必要容量が大きくなるばかりでなく、茶飲料
が高温に維持される時間がそれだけ長くなり、茶飲料の
変質が進む原因ともなる。一方、貯留槽34の容量が余
りに小さいと、圧送ポンプ36の送給量と熱交換器32
からの供給量のバランスが崩れた場合にオーバーフロー
を生じたりあるいは熱交換器38へ空気が進入してしま
う等の不具合を生じるおそれがある。
The temporary storage tank 34 is composed of a tank having a head space, and the tea beverage preheated by the heat exchanger 32 is held in the storage tank 34 under normal pressure for a short time. Then, the head space gas in the storage tank 34 is removed by a suction pump or the like (not shown) so that the pressure inside the storage tank 34 does not become higher than normal pressure. In addition, it is preferable that the retention time of the tea beverage in the storage tank 34 is several seconds to several tens of seconds, and not only the required capacity of the storage tank 34 becomes large when configured to store several tens of seconds to several minutes, The tea beverage is maintained at a high temperature for a longer period of time, which causes deterioration of the tea beverage. On the other hand, when the capacity of the storage tank 34 is too small, the feed amount of the pressure feed pump 36 and the heat exchanger 32 are reduced.
When the balance of the supply amount from the air is lost, there is a possibility that an overflow may occur or air may enter the heat exchanger 38.

【0015】圧送ポンプ36は、貯留槽34に貯留され
た予熱茶飲料を加圧下に第2プレート式熱交換器38へ
送給する。該交換器38では茶飲料の殺菌に必要な温
度、例えば140℃で数秒ないし数十秒保持するように
構成されている。この交換器38を経た殺菌済茶飲料は
直ちに第3プレート式熱交換器40により95℃乃至9
0℃まで急速冷却される。従って、茶飲料が百数十度の
高温にさらされる時間は長くても数十秒であり、すでに
十分に脱酸素された状態で短時間高温にさらされるのみ
であるので、茶飲料の香気成分あるいは色素成分に与え
る影響は極めて小さいものとなる。
The pressure feed pump 36 feeds the preheated tea beverage stored in the storage tank 34 to the second plate heat exchanger 38 under pressure. The exchanger 38 is configured to maintain the temperature necessary for sterilizing the tea beverage, for example, 140 ° C. for several seconds to several tens seconds. The sterilized tea beverage that has passed through the exchanger 38 is immediately heated to 95 ° C to 9 ° C by the third plate heat exchanger 40.
It is rapidly cooled to 0 ° C. Therefore, the tea beverage is exposed to a high temperature of hundreds of tens of degrees for several tens of seconds at the longest, and it is only exposed to a high temperature for a short time in a state of being sufficiently deoxidized. Alternatively, the effect on the pigment component is extremely small.

【0016】前記熱交換器40を経た熱間充填温度の茶
飲料は熱交換器38,40内の圧力を高圧に維持する圧
力制御弁42を介して充填・密封装置44に供給され
る。この充填装置44は、圧力制御弁42を介して供給
される熱間充填温度に冷却された茶飲料を容器に充填
し、その後実質的に無酸素雰囲気下で密封する。缶詰の
場合には、缶に茶飲料を充填した後、缶蓋の巻締めを行
う。むろん、茶飲料が充填される前に少なくとも缶胴の
内面側は洗浄されている。ここで、缶を密封する際の無
酸素雰囲気を形成するには、窒素ガス、炭酸ガス等の不
活性ガスを単独又は混合して使用するのが好ましく、こ
れらのガスとスチームとの混合ガスも使用できる。
The tea beverage having the hot filling temperature, which has passed through the heat exchanger 40, is supplied to the filling / sealing device 44 via a pressure control valve 42 which maintains the pressure in the heat exchangers 38, 40 at a high pressure. The filling device 44 fills the container with the tea beverage cooled to the hot filling temperature supplied via the pressure control valve 42, and then seals the container in a substantially oxygen-free atmosphere. In the case of canned food, the can lid is closed after filling the can with tea beverage. Of course, at least the inner surface side of the can body is cleaned before being filled with the tea beverage. Here, in order to form an oxygen-free atmosphere at the time of sealing the can, it is preferable to use an inert gas such as nitrogen gas or carbon dioxide alone or in combination, and a mixed gas of these gases and steam is also used. Can be used.

【0017】次に実質的な無酸素雰囲気形成手段として
は、缶に缶蓋を巻締める際に窒素ガスによるアンダーカ
バーガッシングを行って、缶のヘッドスペース部の空気
を窒素ガスで置換する方法、充填装置から缶蓋巻締装置
の間の飲料充填済み缶搬送コンベア上方を覆うと共にそ
の側壁が少なくとも缶の開口部よりも下方に垂れ下がっ
ているように缶の通路を覆うカバー(又はトンネル)を
設け、カバー(又はトンネル)で囲まれた部分に窒素ガ
スを導入して上方から缶の開口部に向けて窒素ガスを吹
き込んで缶のヘッドスペースの空気を窒素ガスで置換し
た後、アンダーカバーガッシングを行う方法、これらの
手段に加えて缶蓋巻締装置をカバーで囲み、その中に窒
素ガスを導入して巻締めを窒素ガス雰囲気で行う方法、
及び缶蓋巻締装置をカバーで囲み、この中を窒素ガス雰
囲気にすると共にアンダーカバーガッシングをする方法
がある。
As a means for forming a substantially oxygen-free atmosphere, undercover gassing with nitrogen gas is performed when the can lid is wound around the can to replace the air in the headspace of the can with nitrogen gas. , A cover (or tunnel) that covers the top of the beverage-filled can conveyor between the filling device and the can lid wrapping device and covers the passage of the can so that its side wall hangs at least below the opening of the can. After introducing the nitrogen gas into the area surrounded by the cover (or tunnel) and blowing the nitrogen gas from above toward the opening of the can to replace the air in the head space of the can with the nitrogen gas, A method of performing singing, a method of enclosing a can lid winding device with a cover in addition to these means, and introducing nitrogen gas into the device to perform winding in a nitrogen gas atmosphere,
Also, there is a method in which the can lid wrapping device is surrounded by a cover, the inside of which is made a nitrogen gas atmosphere, and undercover gassing is performed.

【0018】アンダーカバーガッシングするだけでも、
缶のヘッドスペース部の酸素量を0.2ml/缶以下に
まで減少させることができ、また缶蓋巻締装置までの缶
搬送コンベア上方及び側方を覆うカバーを設けてこの中
に窒素ガスを導入し、上方から缶の開口部に向けて窒素
ガスを吹き付けた後、缶蓋巻締め時にアンダーカバーガ
ッシングを行うと、缶のヘッドスペース部の酸素量を
0.1ml/缶以下に削減でき、これらに加えて缶蓋巻
締装置をカバーで囲むと共にその中を窒素ガス雰囲気に
すると、缶のヘッドスペース部の酸素量をほぼゼロにす
ることができる。また、缶蓋巻締装置をカバーで囲み、
その中に窒素ガスを導入して巻締めをする部分を窒素ガ
ス雰囲気にすると共にアンダーカバーガッシングをする
ことにより、缶にヘッドスペース部の酸素量0.1ml
/缶以下にすることができる。
Even under-cover gassing,
The amount of oxygen in the headspace of the can can be reduced to 0.2 ml / can or less, and a cover for covering the upper and side of the can transporting conveyor to the can lid wrapping device is provided to allow nitrogen gas to enter into the can. After introducing and blowing nitrogen gas from above toward the opening of the can, undercover gassing when tightening the can lid can reduce the oxygen amount in the headspace of the can to 0.1 ml / can or less. In addition to these, by surrounding the can lid wrapping device with a cover and creating a nitrogen gas atmosphere therein, the amount of oxygen in the head space of the can can be reduced to almost zero. Also, surround the can lid winding device with a cover,
Oxygen amount of 0.1 ml in the head space of the can was obtained by introducing nitrogen gas into the can and tightening the part to be tightened with nitrogen gas and performing undercover gassing.
/ Can be less than or equal to a can.

【0019】いずれの方法も、単に熱間充填をするだけ
のもの(ヘッドスペース部の酸素量約2.0ml/缶)
よりもヘッドスペース部の酸素量を非常に少なくでき
る。どの方法を選択するかは、缶詰を製造する工場の設
備やその飲料がどれくらい酸素によって劣化され易いか
を考慮して決定する。尚、窒素ガスの代わりに、炭素ガ
ス、窒素ガスと炭酸ガスの混合ガス、炭酸ガスとスチー
ムとの混合ガス、窒素ガスとスチームとの混合ガス等を
使うことができるのは上述したとおりである。
In any of the methods, only hot filling is performed (oxygen amount in head space is about 2.0 ml / can)
The amount of oxygen in the headspace can be made much smaller than that. The choice of method depends on the equipment of the canning plant and how much the beverage is susceptible to deterioration by oxygen. As described above, carbon gas, a mixed gas of nitrogen gas and carbon dioxide, a mixed gas of carbon dioxide and steam, a mixed gas of nitrogen gas and steam, and the like can be used instead of nitrogen gas. .

【0020】次に、図2および図3を参照して本実施態
様に用いられるプレート式交換器について簡単に説明す
る。図2にはプレート式交換器32の概念図が示されて
いる。同図より明らかなように、茶飲料は流路50を介
して流れ、一方スチーム等の熱媒体は流路52を介して
流れている。また、両流路50,52の間には、熱伝導
率の高い伝熱プレート54が介在している。
Next, the plate type exchanger used in this embodiment will be briefly described with reference to FIGS. 2 and 3. FIG. 2 shows a conceptual diagram of the plate type exchanger 32. As is clear from the figure, the tea beverage flows through the flow path 50, while the heat medium such as steam flows through the flow path 52. Further, a heat transfer plate 54 having high thermal conductivity is interposed between the flow paths 50 and 52.

【0021】そして、熱媒体流路52を流れる高温熱媒
体より伝熱プレート54を介して茶飲料流路ルート50
を流れる茶飲料に熱交換が行われ、熱媒体流路52の出
口からは温度の下がった熱媒体が、また茶飲料流路50
の出口からは昇温された茶飲料がそれぞれ流出する。図
3には本実施態様に用いられる熱交換器のより詳細な構
造が示されている。同図より明らかなように、茶飲料は
流路入口50aより熱交換器32内に流入し、流路出口
50bより流出する。
Then, the high temperature heat medium flowing through the heat medium flow passage 52 is passed through the heat transfer plate 54 to the tea beverage flow passage route 50.
The heat exchange is performed on the tea beverage flowing through, and the heat medium whose temperature has dropped from the outlet of the heat medium flow passage 52 is regenerated.
The heated tea beverages respectively flow out from the outlets of. FIG. 3 shows a more detailed structure of the heat exchanger used in this embodiment. As is clear from the figure, the tea beverage flows into the heat exchanger 32 through the flow path inlet 50a and flows out through the flow path outlet 50b.

【0022】一方、高温スチームは熱媒体流路入口52
aより熱交換器32内に進入し、流路出口52bから吐
き出される。そして、熱交換器32は微細な間隔をあけ
て密閉配置された伝熱プレート54が多数配置されてお
り、例えば伝熱プレート54a,54bの間隙で形成さ
れる狭路には下部の入口側茶飲料流路より茶飲料が供給
され、該茶飲料は狭路を図中上方に流れ、上部の出口側
茶飲料流路に流れ込む。一方、該伝熱プレート54b
と、その反対側に隣接した伝熱プレート54cの間にも
狭い間隙が形成されており、この狭路には上部の入口側
熱媒体流路52より高温熱媒体が供給され、該高温熱媒
体は狭路を図中下方に流れ、出口側熱媒体流路52bに
流れ込む。
On the other hand, the high temperature steam is the heat medium flow path inlet 52.
It enters into the heat exchanger 32 from a and is discharged from the flow path outlet 52b. Further, the heat exchanger 32 is provided with a large number of heat transfer plates 54 which are hermetically arranged at a fine interval, and for example, a narrow passage formed by a gap between the heat transfer plates 54a and 54b has a lower inlet side tea. A tea beverage is supplied from the beverage flow channel, the tea beverage flows upward in the drawing in the narrow path, and flows into the outlet-side tea beverage flow channel in the upper portion. On the other hand, the heat transfer plate 54b
And a narrow gap is also formed between the heat transfer plates 54c adjacent to the opposite side, and the high temperature heat medium is supplied from the upper inlet side heat medium flow passage 52 to the narrow path, and the high temperature heat medium is supplied. Flows through the narrow path downward in the figure and flows into the outlet-side heat medium flow path 52b.

【0023】従って、茶飲料と熱媒体は薄い伝熱プレー
ト54bにより隔てられているのみであり、茶飲料と熱
媒体が伝熱プレート54bを介して熱交換しつつ逆方向
に進行することとなる。本実施態様において用いられる
熱交換器は、前述したように茶飲料が流れる狭路と熱媒
体が流れる狭路が交互に多数配置された構造となってお
り、大量の茶飲料について短時間で均一かつ効率的な昇
温を行わせることができる。本実施態様に係る容器詰め
熱間充填飲料の製造装置は概略以上のように構成されて
おり、これらを次のように運転して容器詰め熱間充填飲
料を製造する。
Therefore, the tea beverage and the heat medium are only separated by the thin heat transfer plate 54b, and the tea beverage and the heat medium travel in opposite directions while exchanging heat via the heat transfer plate 54b. . The heat exchanger used in the present embodiment has a structure in which a large number of narrow passages through which the tea beverage flows and narrow passages through which the heat medium flows are alternately arranged as described above, and a large amount of tea beverage can be uniformly distributed in a short time. In addition, the temperature can be raised efficiently. The manufacturing apparatus of the hot-packed beverage packed in a container according to the present embodiment is roughly configured as described above, and these are operated as follows to manufacture a hot-packed beverage packed in a container.

【0024】前述したように、本実施態様に係る容器詰
め熱間充填飲料の製造方法は、第1プレート式熱交換器
32により被処理飲料をその沸点近傍の温度にまで急速
に加熱する。この際、水溶液中における気体の溶解度は
温度の上昇とともに減少するため、熱交換器32による
加熱により溶存酸素のほとんどが過飽和ないし微細気泡
の状態となる。この状態の茶飲料が一時貯留槽34へ放
出されることにより、前記液中酸素が該貯留槽34上部
のヘッドスペース部分に放出される。従って、該ヘッド
スペースガスを除去することにより、茶飲料中の溶存酸
素のほとんどが除去されることとなる。例えば、図4に
はイオン交換水の溶存酸素と温度の関係が示されてい
る。
As described above, in the method for producing a packaged hot-filled beverage according to the present embodiment, the beverage to be treated is rapidly heated to a temperature near its boiling point by the first plate heat exchanger 32. At this time, since the solubility of the gas in the aqueous solution decreases as the temperature rises, most of the dissolved oxygen becomes supersaturated or in the form of fine bubbles due to the heating by the heat exchanger 32. When the tea beverage in this state is released to the temporary storage tank 34, the oxygen in the liquid is released to the head space portion above the storage tank 34. Therefore, most of the dissolved oxygen in the tea beverage will be removed by removing the headspace gas. For example, FIG. 4 shows the relationship between the dissolved oxygen and the temperature of ion-exchanged water.

【0025】同図より明らかなように、20℃で9ppm
程度の溶存酸素が存在していたものが、温度60℃では
5ppm 、温度95℃では溶存酸素濃度が1ppm 程度とな
る。従って、調合タンク24内の茶飲料の温度が60℃
であると溶存酸素が5ppm であったのが、熱交換器32
中で茶飲料が95℃まで昇温されると溶存可能酸素が1
ppm となるのであるから、差分4ppm の余剰溶存酸素は
過飽和ないし微細気泡状となる。溶存酸素2ppm 以下は
茶類缶詰の品質上大きな意義をもっており、特に1ppm
以下というのは例えば茶飲料等においても長期にわたり
変質が極めて生じにくく、保存性向上に非常に効果的な
酸素濃度である。この状態で一時貯留槽34に注入され
ると、前記余剰溶存酸素は該貯留槽34のヘッドスペー
ス部分に放出される。
As is clear from the figure, 9 ppm at 20 ° C.
Although there was a degree of dissolved oxygen, the dissolved oxygen concentration was about 5 ppm at a temperature of 60 ° C and about 1 ppm at a temperature of 95 ° C. Therefore, the temperature of the tea beverage in the mixing tank 24 is 60 ° C.
Therefore, the dissolved oxygen was 5 ppm, which means that the heat exchanger 32
When the temperature of the tea drink is raised to 95 ℃, the amount of oxygen that can be dissolved becomes 1
Since it becomes ppm, the excess dissolved oxygen with a difference of 4 ppm becomes supersaturated or in the form of fine bubbles. Dissolved oxygen of 2ppm or less has great significance in the quality of canned tea, especially 1ppm.
The following is an oxygen concentration that is extremely effective for improving shelf life, for example, even in a tea beverage or the like, deterioration is extremely unlikely to occur. When injected into the temporary storage tank 34 in this state, the excess dissolved oxygen is released to the head space portion of the storage tank 34.

【0026】一方、一時貯留槽34内には窒素ボンベ6
0からフィルターで除菌された無菌の窒素ガスが供給さ
れており、前記ヘッドスペース部分へ茶飲料中から放出
された空気(酸素)は窒素ガスとともに開口34aから
系外へ排出される。そして、溶存酸素が例えば2ppm 以
下まで低減された調合液は、圧送ポンプ36により第2
プレート式熱交換器38に送給される。熱交換器38は
前記第1プレート式熱交換器32と同様の熱交換器から
構成されるが、調合液を常圧沸点以上の高温とするた
め、ポンプ36は調合液が沸騰しないように加圧を行っ
ている。
On the other hand, the nitrogen tank 6 is placed in the temporary storage tank 34.
Aseptic nitrogen gas, which has been sterilized by a filter, is supplied from 0, and the air (oxygen) released from the tea beverage to the headspace portion is discharged from the system through the opening 34a together with the nitrogen gas. Then, the mixed solution whose dissolved oxygen is reduced to, for example, 2 ppm or less is second
It is fed to the plate heat exchanger 38. The heat exchanger 38 is composed of the same heat exchanger as the first plate type heat exchanger 32, but the pump 36 is heated so as not to boil the preparation liquid in order to raise the preparation liquid to a high temperature above the atmospheric pressure boiling point. I'm doing pressure.

【0027】以上のようにして得られた溶存酸素濃度2
ppm 以下の茶飲料は、直ちに第3プレート式熱交換器4
0により熱間充填温度まで冷却された後、圧力制御弁4
2を介して充填・密封装置44に供給される。充填・密
封装置44は充填装置及び密封装置で構成され、容器に
茶飲料を充填・密封する。なお、充填・密封装置44に
も窒素ガスが供給されており、茶飲料は缶に充填された
後、実質的に酸素との接触が絶たれた状態で缶蓋により
密封される。以上説明したように、本実施態様に係る容
器詰め熱間充填飲料の製造方法によれば、常圧下で被処
理飲料をその沸点近傍で滞留させ、この間に脱気を行
い、さらに加圧、高圧下で十分な殺菌を行うため、充填
・密封装置44により充填される調合液は十分に殺菌、
脱気されたものとなる。
Dissolved oxygen concentration 2 obtained as described above
For tea beverages below ppm, immediately use the third plate heat exchanger 4
After being cooled to the hot filling temperature by 0, the pressure control valve 4
2 to the filling / sealing device 44. The filling / sealing device 44 includes a filling device and a sealing device, and fills and seals the tea beverage in the container. Nitrogen gas is also supplied to the filling / sealing device 44, and after the tea beverage is filled in the can, the tea beverage is sealed by the can lid in a state where the contact with oxygen is substantially cut off. As described above, according to the method for manufacturing a container-packed hot-filled beverage according to the present embodiment, the beverage to be treated is allowed to stay near its boiling point under normal pressure, and deaeration is performed during this, further pressurization and high pressure. In order to perform sufficient sterilization below, the preparation liquid filled by the filling / sealing device 44 is sufficiently sterilized,
It will be degassed.

【0028】なお、本実施態様においては窒素ガスは一
時貯留槽34のヘッドスペース部分に供給されたが、例
えば一時貯留槽34内でバブリングすることも好適であ
る。また、より脱気の完全を図るために、本実施態様に
おいては窒素ガスを調合タンク24内にも供給してい
る。また、本実施態様においては一時貯留槽34および
充填・密封装置44に酸素濃度計64を設け、各工程に
おける酸素濃度が一定以上とならないように窒素ガス供
給量を制御することにより、さらに安定した脱気効果を
得ている。なお、本実施態様において一時貯留槽34と
しては例えば図5に示すような構造のものを用いること
が好適である。
In the present embodiment, the nitrogen gas was supplied to the head space portion of the temporary storage tank 34, but it is also preferable to bubble in the temporary storage tank 34, for example. Further, in order to achieve more complete degassing, nitrogen gas is also supplied into the mixing tank 24 in this embodiment. Further, in the present embodiment, the oxygen concentration meter 64 is provided in the temporary storage tank 34 and the filling / sealing device 44, and the nitrogen gas supply amount is controlled so that the oxygen concentration in each step does not exceed a certain level, thereby further stabilizing. It has a degassing effect. In this embodiment, as the temporary storage tank 34, it is preferable to use one having a structure as shown in FIG. 5, for example.

【0029】すなわち、同図に示す一時貯留槽34は、
貯留槽34下部に流入路70、およびその反対側の下部
に流出路72を設け、両流路70,72の間には隔壁7
4が設けられている。このため、流入路70から流入す
る飲料は隔壁74に妨げられて一度液面(ヘッドスペー
スとの接触面)に至り、十分な脱気が行われたのち流出
路72から第2プレート式熱交換器38へ送給される。
このため、一時貯留槽34内部で液溜まりが生じること
なく、しかも脱気効率も高くなる。
That is, the temporary storage tank 34 shown in FIG.
An inflow passage 70 is provided in the lower portion of the storage tank 34, and an outflow passage 72 is provided in the lower portion on the opposite side thereof, and a partition wall 7 is provided between the flow passages 70, 72.
4 are provided. Therefore, the beverage flowing from the inflow passage 70 is blocked by the partition wall 74 and once reaches the liquid surface (contact surface with the head space), and after sufficient deaeration is performed, the second plate heat exchange is performed from the outflow passage 72. It is delivered to the container 38.
Therefore, liquid is not accumulated inside the temporary storage tank 34, and the degassing efficiency is increased.

【0030】[0030]

【実施例】以下、図6に基づき本発明の一実施例として
煎茶缶詰製造工程について説明する。同図に示す実施例
においては、溶存酸素濃度0.9ppm のイオン交換水に
煎茶を1.25%添加し、70℃で5分間抽出処理を行
った後、濾過、冷却、重曹およびL−アスコルビン酸の
添加を行って茶飲料が調合される。この調合済茶飲料
は、脱気イオン交換水を使ったにも拘わらず、溶存酸素
濃度は6.0ppm となっている。
EXAMPLE A canned green tea can manufacturing process will be described below as an example of the present invention with reference to FIG. In the example shown in the figure, 1.25% of green tea was added to ion-exchanged water having a dissolved oxygen concentration of 0.9 ppm, and the mixture was subjected to extraction treatment at 70 ° C. for 5 minutes, followed by filtration, cooling, baking soda and L-ascorbin. A tea beverage is prepared by adding acid. This prepared tea beverage has a dissolved oxygen concentration of 6.0 ppm, despite using deaerated ion-exchanged water.

【0031】これに対して、従来一般的に用いられてい
る飲料缶詰の製法であるホットパック後にレトルト殺菌
法を用いて殺菌を行った場合(従来技術1)には、ホッ
トパツク(充填温度90℃)時の溶存酸素濃度は1.6
ppm 、さらにレトルト殺菌(121℃×10分)の後の
溶存酸素濃度は0.4ppm であった。また、前記調合済
茶飲料をそのまま高温短時間殺菌し常温充填した場合
(従来技術2)には、充填後の溶存酸素濃度は5.1pp
m であり、溶存酸素濃度が極めて高く保存中の酸化が予
想される。
On the other hand, in the case where sterilization is performed using the retort sterilization method after hot packing, which is a conventionally commonly used method for canning beverages (prior art 1), a hot pack (filling temperature 90 ° C.) is used. ) Hour, the dissolved oxygen concentration is 1.6
ppm, and the dissolved oxygen concentration after retort sterilization (121 ° C. × 10 minutes) was 0.4 ppm. When the prepared tea beverage is sterilized at high temperature for a short time and is filled at room temperature (prior art 2), the dissolved oxygen concentration after filling is 5.1 pp.
m, and the dissolved oxygen concentration is extremely high, and oxidation during storage is expected.

【0032】一方、前記調合済茶飲料を、本発明に係る
方法で缶に充填し、充填装置から缶蓋巻締装置への缶搬
送路を覆っているカバー内で缶の開口部に向けて窒素ガ
スを吹き付け、更に、カバーで囲い、その内部を窒素ガ
ス雰囲気にしてある缶蓋巻締装置によりアンダーカバー
ガッシングして缶のヘッドスペース部の空気を窒素ガス
で置換しながら密封した場合、一時貯留槽34における
溶存酸素濃度は1.9ppm 、さらに高温・高圧殺菌を行
い熱間充填、冷却した後の溶存酸素濃度は0.9ppm で
あった。
On the other hand, the prepared tea beverage is filled into a can by the method according to the present invention, and is directed toward the opening of the can in the cover covering the can conveying path from the filling device to the can lid winding device. When nitrogen gas is blown and further covered with a cover, and the inside of the can is closed by a can lid wrapping device that is in a nitrogen gas atmosphere to seal air while replacing the air in the head space of the can with nitrogen gas, The dissolved oxygen concentration in the temporary storage tank 34 was 1.9 ppm, and the dissolved oxygen concentration was 0.9 ppm after hot sterilization and hot filling and cooling.

【0033】以上の様にして製造した茶飲料について、
a値およびL−アスコルビン酸の変化量をそれぞれ調合
時(殺菌前)、製造時(殺菌後)、室温1カ月保存時、
室温3カ月保存時に調査した。その結果を次の表1〜表
2に示す。
Regarding the tea beverage produced as described above,
The a value and the amount of change in L-ascorbic acid were measured at the time of preparation (before sterilization), at the time of production (after sterilization), at room temperature for 1 month, and
It was investigated when stored at room temperature for 3 months. The results are shown in Tables 1 and 2 below.

【0034】[0034]

【表1】 なお、a値はLab測色系で、色相(赤−緑)を表し、
a値が増加することにより褐変度合いが増加したことを
示している。
[Table 1] The a value is a Lab colorimetric system and represents hue (red-green),
It shows that the degree of browning increased as the value a increased.

【0035】[0035]

【表2】 [Table 2]

【0036】[0036]

【表3】 *** :危険率0.1%で有意差有り。 ** :危険率1.0%で有意差有り。 * :危険率5.0%で有意差有り。[Table 3] ***: There is a significant difference with a risk rate of 0.1%. **: There is a significant difference with a risk rate of 1.0%. *: There is a significant difference at a risk rate of 5.0%.

【0037】なお、官能検査は発明者の所属する研究所
の日常的に訓練された研究員20人で1人3回繰り返し
テストを行った。前記表1および表2より明らかなよう
に、レトルト殺菌法を用いた従来技術1はa値およびL
−アスコルビン酸の変化量とも極めて大きく、さらに前
記表3に示すとおりフレーバーテストの結果によっても
著しく飲料の劣化が進んでいることが明らかとなった。
なお、前記図6を参照すると、従来技術1においては殺
菌、冷却後の溶存酸素濃度が0.4ppm とかなり低い
が、これは溶存酸素が殆どレトルト殺菌中に反応・消費
されたことを示唆するものであり、さらに充填直後の溶
存酸素が少ないにもかかわらず貯蔵中の変質が急速に進
むことが明らかとなった。
The sensory test was carried out by repeating the test three times by 20 researchers who were routinely trained at the institute to which the inventor belongs. As is clear from Tables 1 and 2, the prior art 1 using the retort sterilization method has a value and L
-The amount of change in ascorbic acid was also extremely large, and as shown in Table 3 above, it was revealed from the results of the flavor test that the beverage was significantly deteriorated.
In addition, referring to FIG. 6, the dissolved oxygen concentration after sterilization and cooling in the prior art 1 is 0.4 ppm, which is considerably low. This suggests that most of the dissolved oxygen was reacted and consumed during the retort sterilization. Furthermore, it was revealed that the deterioration during storage proceeded rapidly even though the amount of dissolved oxygen immediately after filling was small.

【0038】一方、従来技術2においては、a値の変化
を見ると、前記従来技術1ほどの大幅な変化量は示さな
いが、図6に示したように充填直後の溶存酸素濃度が著
しく高いことから貯蔵中におけるL−アスコルビン酸の
消費が著しく、またa値も漸増することが理解される。
これらの従来技術1,2に対して本発明は充填・密封
し、冷却直後の溶存酸素濃度も低く、さらにa値および
L−アスコルビン酸の変化量共に前記従来技術に比較し
て著しく小さく、品質の大幅な改善および維持が図られ
ていることが明らかである。
On the other hand, in the prior art 2, looking at the change in the a value, although the amount of change is not as large as that in the prior art 1, the dissolved oxygen concentration immediately after filling is extremely high as shown in FIG. Therefore, it is understood that the consumption of L-ascorbic acid during storage is remarkable, and the a value is gradually increased.
In contrast to these prior arts 1 and 2, the present invention is filled and sealed, the dissolved oxygen concentration immediately after cooling is low, and further, the a value and the change amount of L-ascorbic acid are significantly smaller than those of the prior art, and the quality is improved. It is clear that significant improvements and maintenance of

【0039】次に、図7に基づき本発明の他の実施例と
してオレンジストレート100%果汁製造工程について
説明する。同図に示す実施例においては、溶存酸素濃度
8.3ppm のオレンジストレート100%果汁を対象と
する。これに対して、従来一般的に用いられている熱間
充填法を用いて殺菌充填を行った場合(従来技術3)に
は、充填巻締め(充填温度90℃)時の溶存酸素濃度は
1.1ppm 、さらに30℃冷却の後の溶存酸素濃度は
0.8ppm であった。
Next, an orange straight 100% fruit juice production process will be described as another embodiment of the present invention with reference to FIG. In the embodiment shown in the figure, 100% orange straight fruit juice having a dissolved oxygen concentration of 8.3 ppm is targeted. On the other hand, when sterilization filling is performed using the hot filling method that has been generally used in the past (conventional technique 3), the dissolved oxygen concentration during filling and tightening (filling temperature 90 ° C.) is 1 0.1 ppm, and the dissolved oxygen concentration after cooling at 30 ° C. was 0.8 ppm.

【0040】一方、前記オレンジストレート100%果
汁を、本発明に係る方法で缶に充填した(密封時の実質
的無酸素雰囲気形成手段は、前記の煎茶缶詰の場合と同
じである。)場合、一時貯留槽34における溶存酸素濃
度は0.9ppm 、さらに高温・高圧殺菌を行い熱間充填
・密封し、冷却した後の溶存酸素濃度は0.7ppm であ
った。以上の様にして製造したオレンジストレート10
0%果汁について、a値およびL−アスコルビン酸の変
化量をそれぞれ調合時(殺菌前)、製造時(冷却後)、
室温1カ月保存時、室温3カ月保存時に調査した。その
結果を次の表4〜表6に示す。
On the other hand, in the case where the orange straight 100% fruit juice is filled in a can by the method according to the present invention (the means for forming a substantially oxygen-free atmosphere at the time of sealing is the same as in the above-mentioned canned sencha), The dissolved oxygen concentration in the temporary storage tank 34 was 0.9 ppm, and the dissolved oxygen concentration was 0.7 ppm after hot sterilization, hot filling, sealing, and cooling. Orange straight 10 produced as described above
Regarding 0% fruit juice, the a value and the change amount of L-ascorbic acid were measured at the time of preparation (before sterilization), at the time of production (after cooling), and
Investigations were conducted at room temperature for 1 month and at room temperature for 3 months. The results are shown in Tables 4 to 6 below.

【0041】[0041]

【表4】 なお、a値は色相(赤−緑)を表し、a値が増加するこ
とにより褐変度合いが増加したことを示している。
[Table 4] The a value represents a hue (red-green), and shows that the degree of browning increases as the a value increases.

【0042】[0042]

【表5】 [Table 5]

【0043】[0043]

【表6】 *** :危険率0.1%で有意差有り。 ** :危険率1.0%で有意差有り。 * :危険率5.0%で有意さ有り。[Table 6] ***: There is a significant difference with a risk rate of 0.1%. **: There is a significant difference with a risk rate of 1.0%. *: Significant with a risk rate of 5.0%.

【0044】なお、官能検査は当研究所の日常的に訓練
された研究員20人で1人3回繰り返しテストを行っ
た。また、官能検査は前記煎茶缶詰と同様行った。前記
表4および表5より明らかなように、通常の熱間充填を
用いた従来技術3はa値およびL−アスコルビン酸の変
化量とも極めて大きく、さらに前記表6に示すとおりフ
レーバーテストの結果によっても著しく飲料の劣化が進
んでいることが明らかとなった。この従来技術3に対し
て本発明は充填後の溶存酸素濃度も低く、さらにa値お
よびL−アスコルビン酸の変化量共に前記従来技術に比
較して著しく小さく、品質の大幅な改善および維持が図
られていることが明らかである。
The sensory test was carried out by repeating the test three times by 20 daily trained researchers of the Institute. The sensory test was performed in the same manner as the canned green tea. As is clear from Tables 4 and 5, the conventional technique 3 using ordinary hot filling has extremely large a value and the amount of change in L-ascorbic acid, and as shown in Table 6, the results of the flavor test show that It became clear that the deterioration of the beverage was significantly advanced. Compared with the prior art 3, the present invention has a low dissolved oxygen concentration after filling, and the a value and the amount of change in L-ascorbic acid are significantly smaller than those of the prior art, and thus the quality can be greatly improved and maintained. It is clear that

【0045】なお、前記実施態様および実施例において
は茶飲料を例に取り説明したが、本発明はこれに限られ
るものではなく、コーヒー(ブラック)、茶類飲料(煎
茶、ウーロン茶、紅茶)等の現在レトルト殺菌の対象と
なっている飲料、さらには果実飲料、スポーツ飲料、殺
菌乳酸菌飲料、トマト・野菜ジュース等の高温短時間殺
菌および熱間充填法の対象となっている缶詰飲料や瓶詰
飲料やプラスチック容器詰め飲料及び紙やプラスチック
や金属箔等から成る複合容器詰め飲料についても適用可
能であることは言うまでもない。さらに、前記実施態様
においては熱交換器としてプレート式熱交換器を用いた
が、例えば細管式熱交換器を用いることも可能である。
In the above-mentioned embodiments and examples, tea beverages have been described as an example, but the present invention is not limited to this, and coffee (black), tea beverages (sencha, oolong tea, black tea), etc. Beverages that are currently subject to retort sterilization, as well as canned beverages and bottled beverages that are subject to high-temperature short-time sterilization and hot filling methods such as fruit beverages, sports beverages, sterilized lactic acid bacteria beverages, tomato and vegetable juices It goes without saying that it is also applicable to plastic packaged beverages and plastic packaged beverages made of paper, plastic, metal foil and the like. Furthermore, although the plate heat exchanger is used as the heat exchanger in the above-described embodiment, it is also possible to use, for example, a capillary heat exchanger.

【0046】[0046]

【発明の効果】以上説明したように本発明に係る容器詰
め熱間充填飲料の製造方法によれば、被処理飲料の沸点
近傍まで予熱した後常圧下に保持して脱気し、さらにそ
の後高温、加圧下に十分な殺菌を行うこととしたので、
高温短時間殺菌において十分な脱気を行うことが可能と
なる。従って、本発明方法により飲料の調合時の色調、
フレーバーを殆ど損なわずに製造でき、また容器詰め熱
間充填飲料の貯蔵中においても溶存酸素が少ないため上
記の成分を安定して保存することが可能となる。また、
本発明に係る容器詰め熱間充填飲料の製造装置によれ
ば、調合時の色調、フレーバーを殆ど損なわずに容器詰
め熱間充填飲料が製造できる。
As described above, according to the method for producing a packaged hot-filled beverage according to the present invention, it is preheated to near the boiling point of the beverage to be treated, degassed by being kept under normal pressure, and then at a high temperature. Since it was decided to perform sufficient sterilization under pressure,
It becomes possible to perform sufficient deaeration in high temperature short time sterilization. Therefore, according to the method of the present invention, the color tone during the preparation of the beverage,
The flavor can be produced with almost no damage, and the above components can be stably stored even during storage of the hot-filled beverage packed in a container because the dissolved oxygen is small. Also,
According to the manufacturing apparatus for a hot-packed beverage packed in a container according to the present invention, a hot-packed beverage packed in a container can be manufactured with almost no loss of color tone and flavor during preparation.

【図面の簡単な説明】[Brief description of drawings]

【図1】本発明の一実施態様に係る容器詰め熱間充填飲
料の製造方法に用いられる飲料缶詰製造装置の概略構成
図である。
FIG. 1 is a schematic configuration diagram of a beverage canning production apparatus used in a method for producing a container-filled hot-filled beverage according to an embodiment of the present invention.

【図2】図1に示す予熱手段、殺菌手段、冷却手段に用
いられる熱交換器の概念の説明図である。
FIG. 2 is an explanatory view of the concept of a heat exchanger used in the preheating means, sterilization means, and cooling means shown in FIG.

【図3】図1に示した装置に用いられるプレート式熱交
換器の説明図である。
FIG. 3 is an explanatory view of a plate heat exchanger used in the device shown in FIG.

【図4】イオン交換水の温度と溶存酸素濃度の関係の説
明図である。
FIG. 4 is an explanatory diagram of a relationship between a temperature of ion-exchanged water and a dissolved oxygen concentration.

【図5】図1に示した装置に用いられる一時貯留槽の説
明図である。
5 is an explanatory view of a temporary storage tank used in the apparatus shown in FIG.

【図6】本発明と従来技術の煎茶缶詰製造工程および溶
存酸素濃度の比較図である。
FIG. 6 is a comparison diagram of the manufacturing process of canned green tea and the dissolved oxygen concentration of the present invention and the prior art.

【図7】本発明と従来技術のオレンジストレート100
%果汁缶詰製造工程および溶存酸素濃度の比較図であ
る。
FIG. 7: Orange straight 100 of the present invention and prior art
FIG. 3 is a comparison diagram of a% juice canned manufacturing process and a dissolved oxygen concentration.

【符号の説明】[Explanation of symbols]

14 飲料脱気・殺菌・充填・密封装置 30 送給ポンプ(送給手段) 32 第1プレート式熱交換器(予熱手段) 34 一時貯留槽(脱気手段) 36 圧送ポンプ(圧送手段) 38 第2プレート式熱交換器(殺菌手段) 40 第3プレート式熱交換器(冷却手段) 44 充填・密封装置(充填手段) 14 Beverage Deaeration / Sterilization / Filling / Sealing Device 30 Feed Pump (Feeding Means) 32 First Plate Heat Exchanger (Preheating Means) 34 Temporary Storage Tank (Deaerating Means) 36 Pressure Feeding Pump (Pressing Means) 38th 2 plate type heat exchanger (sterilizing means) 40 3rd plate type heat exchanger (cooling means) 44 filling / sealing device (filling means)

Claims (2)

【特許請求の範囲】[Claims] 【請求項1】 被処理飲料を略常圧下で送給する送給工
程と、 該送給工程で送給する被処理飲料を狭路中で熱交換によ
りその沸点近傍の温度まで急速加熱する予熱工程と、 上部にヘッドスペースを有する一時貯留槽内に、前記予
熱工程で予熱された被処理飲料を常圧下に短時間保持
し、そのヘッドスペースガスを除去する脱気工程と、 該脱気工程により脱気された被処理飲料を圧送する圧送
工程と、 該圧送工程で圧送される被処理飲料を狭路中で熱交換に
より100℃以上の高温、加圧下で短時間殺菌処理する
殺菌工程と、 殺菌が終了した被処理飲料を直ちに95℃乃至90℃の
熱間充填温度まで急速冷却する冷却工程と、 前記熱間充填温度に冷却された被処理飲料を、少なくと
も内面側を洗浄済みの容器に充填し、実質的に酸素との
接触を絶ちつつ密封する充填工程と、 を備えたことを特徴とする容器詰め熱間充填飲料の製造
方法。
1. A feeding step of feeding a beverage to be treated under substantially normal pressure, and preheating for rapidly heating the beverage to be treated fed in the feeding step to a temperature near its boiling point by heat exchange in a narrow path. And a degassing process for holding the beverage to be treated preheated in the preheating process under normal pressure for a short time in a temporary storage tank having a headspace at the upper part, and removing the headspace gas thereof, And a sterilization step of sterilizing the beverage to be processed that is pressure-fed in the pressure-feeding step by heat exchange in a narrow path at a high temperature of 100 ° C. or higher for a short time under pressure. A container in which at least the inner surface of the beverage to be treated which has been sterilized is rapidly cooled to a hot filling temperature of 95 ° C. to 90 ° C. Filled with and substantially contact with oxygen A method for producing a packaged hot-filled beverage, comprising:
【請求項2】 被処理飲料を略常圧下で送給する送給手
段と、 該送給手段により送給される被処理飲料をその沸点近傍
の温度まで急速加熱する熱交換器と、 加熱された被処理飲料をヘッドスペース部を保持した状
態で短時間貯留し得る貯留槽と、 該貯留槽のヘッドスペース部から排気を行う手段とから
成る脱気手段と、 該脱気手段により脱気された被処理飲料を圧送する圧送
手段と、 該圧送手段により圧送される被処理飲料を加圧下100
℃以上で高温短時間殺菌処理する熱交換器と、 殺菌済みの被処理飲料を95℃乃至90℃の熱間充填温
度まで急速冷却する熱交換器と、 前記熱間充填温度の被処理飲料を少なくとも内面側を洗
浄済みの容器に充填し、実質的に酸素との接触を絶ちつ
つ密封する充填装置及び密封装置とから構成される充填
手段と、 を備えたことを特徴とする容器詰め熱間充填飲料の製造
装置。
2. A feeding means for feeding the beverage to be treated under substantially normal pressure, a heat exchanger for rapidly heating the beverage to be treated fed by the feeding means to a temperature near its boiling point, and a heat exchanger. And a degassing means comprising a storage tank capable of storing the beverage to be treated while holding the headspace portion for a short time, and a means for exhausting the headspace portion of the storage tank, and degassing by the degassing means. A pressure-feeding means for pressure-feeding the beverage to be treated and a beverage to be treated pressure-fed by the pressure-feeding means under pressure 100
A heat exchanger for sterilization at a high temperature for a short time at a temperature of ℃ or more; a heat exchanger for rapidly cooling a sterilized beverage to be hot-filled at 95 ° C to 90 ° C; At least an inner surface side is filled in a washed container, and a filling device configured to include a filling device and a sealing device that substantially seals the container while cutting off contact with oxygen; Filled beverage manufacturing equipment.
JP11131696A 1996-04-08 1996-04-08 Method and apparatus for producing hot-packed beverages in containers Expired - Fee Related JP3643172B2 (en)

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JP11131696A JP3643172B2 (en) 1996-04-08 1996-04-08 Method and apparatus for producing hot-packed beverages in containers

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JPH09272516A true JPH09272516A (en) 1997-10-21
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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2011255952A (en) * 2010-06-11 2011-12-22 Suntory Holdings Ltd Heating sterilization system
CN109843782A (en) * 2016-09-12 2019-06-04 克朗斯股份公司 For carrying out heat treatment and filling canning line to liquid
JP2019180287A (en) * 2018-04-09 2019-10-24 花王株式会社 Method for filling packed beverage

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111559730B (en) * 2020-05-07 2022-05-24 杭州娃哈哈集团有限公司 Energy-saving beverage filling cold bottle system

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS60179193U (en) * 1984-05-10 1985-11-28 凸版印刷株式会社 Microwave heating sterilizer
JPS6384466A (en) * 1986-09-30 1988-04-15 Toyo Seikan Kaisha Ltd Canning method
JPH07123962A (en) * 1993-11-01 1995-05-16 Hitachi Techno Eng Co Ltd Continuously sterilizing device

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS60179193U (en) * 1984-05-10 1985-11-28 凸版印刷株式会社 Microwave heating sterilizer
JPS6384466A (en) * 1986-09-30 1988-04-15 Toyo Seikan Kaisha Ltd Canning method
JPH07123962A (en) * 1993-11-01 1995-05-16 Hitachi Techno Eng Co Ltd Continuously sterilizing device

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2011255952A (en) * 2010-06-11 2011-12-22 Suntory Holdings Ltd Heating sterilization system
CN109843782A (en) * 2016-09-12 2019-06-04 克朗斯股份公司 For carrying out heat treatment and filling canning line to liquid
JP2019180287A (en) * 2018-04-09 2019-10-24 花王株式会社 Method for filling packed beverage

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