JPH0922665A - X-ray image pickup tube and manufacture thereof - Google Patents

X-ray image pickup tube and manufacture thereof

Info

Publication number
JPH0922665A
JPH0922665A JP16980695A JP16980695A JPH0922665A JP H0922665 A JPH0922665 A JP H0922665A JP 16980695 A JP16980695 A JP 16980695A JP 16980695 A JP16980695 A JP 16980695A JP H0922665 A JPH0922665 A JP H0922665A
Authority
JP
Japan
Prior art keywords
plate
image pickup
face plate
target electrode
pickup tube
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
JP16980695A
Other languages
Japanese (ja)
Inventor
Kazuyuki Nagatsuma
一之 長妻
Tadaaki Hirai
忠明 平井
Kazutaka Tsuji
和隆 辻
Kenji Samejima
賢二 鮫島
Kenichi Mogi
謙一 茂木
Norio Okamura
憲伯 岡村
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Hitachi Denshi KK
Hitachi Ltd
Original Assignee
Hitachi Denshi KK
Hitachi Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Hitachi Denshi KK, Hitachi Ltd filed Critical Hitachi Denshi KK
Priority to JP16980695A priority Critical patent/JPH0922665A/en
Publication of JPH0922665A publication Critical patent/JPH0922665A/en
Pending legal-status Critical Current

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  • Measurement Of Radiation (AREA)
  • Image-Pickup Tubes, Image-Amplification Tubes, And Storage Tubes (AREA)

Abstract

PROBLEM TO BE SOLVED: To provide an X-ray image pickup tube having high sensitivity and high quality of image without generating the white-spot-like image defect and dark current even in the high electric field by adhering a first and a second insulating surface plates, which are respectively formed integrally with a part of a target electrode pin, to each other. SOLUTION: A BN plate 4 and a glass plate 2 are adhered to each other so as to correspond a Mo target electrode pin 1 welded to the glass plate 2 to a through hole provided in the BN plate 4. The hole of the plate 4 is filled with the silver epoxy resin, and after heating it, both the surfaces are polished, and after washing both the surfaces, the plate 2 side is flattened and smoothed by ion etching so as to form the surface plate. An A film as a target electrode film 6, a CeO2 film as a positive hole filling hindering layer, and a Se film as a photoconductive film 7 are formed in order by vacuum-deposition on the surface plate, and furthermore, a Sb2 S3 porous film is formed so as to form an electron filling hindering layer. A glass plate 5 having a rectangular X-ray transmitting window and an electrode ejecting through hole at the center thereof is adhered, and the through hole is filled with the silver epoxy resin 3 so as to form a target part of an image pickup tube.

Description

【発明の詳細な説明】Detailed Description of the Invention

【0001】[0001]

【産業上の利用分野】本発明は、X線撮像管に係り、特
に、高感度のターゲット部を有するX線撮像管及びその
製造方法に関するものである。
BACKGROUND OF THE INVENTION 1. Field of the Invention The present invention relates to an X-ray image pickup tube, and more particularly to an X-ray image pickup tube having a highly sensitive target portion and a method for manufacturing the same.

【0002】[0002]

【従来の技術】X線撮像管は、通常、X線やγ線(以
下、単にX線と呼ぶ)を透過しやすい面板上に、ターゲ
ット電極膜と光導電膜とを積層した撮像管ターゲット部
と、真空を介し上記光導電膜に対向して設けられた走査
電子ビーム発生部とからなり、入射X線を上記光導電膜
に吸収させて電荷に変換し、これを走査電子ビームによ
り直接電気信号として取り出す。X線撮像管は、実時間
での観測ができ、高い解像度が得られることなどから、
半導体IC等の非破壊検査や、生体内部の診断、結晶解
析、材料分析などに有効であって、産業、計測、学術等
の分野で広く利用されている。
2. Description of the Related Art An X-ray image pickup tube is usually a target portion of an image pickup tube in which a target electrode film and a photoconductive film are laminated on a face plate which easily transmits X-rays and γ-rays (hereinafter, simply referred to as X-rays). And a scanning electron beam generator provided to face the photoconductive film via a vacuum, the incident X-ray is absorbed by the photoconductive film and converted into an electric charge, which is directly converted by the scanning electron beam. Take out as a signal. The X-ray image pickup tube enables real-time observation and provides high resolution.
It is effective for nondestructive inspection of semiconductor ICs, diagnosis inside living bodies, crystal analysis, material analysis, etc., and is widely used in fields such as industry, measurement, and academic fields.

【0003】X線撮像管のターゲット部の面板として
は、従来、X線を最も透過しやすい固体材料である金属
Be(ベリリュウム)板が多く利用されてきたが、近
年、X線透過性はBeほど良くないものの、毒性がな
く、機械加工性が良好で、絶縁性の固体材料であるBN
(窒化硼素)板を用いたX線撮像管も使用されている
(特願平2‐230658、特願平5‐89646、テ
レビジョン学会技術報告IPU’93‐63、1〜6
頁、1993年、等)。
As a face plate of a target portion of an X-ray image pickup tube, a metal Be (beryllium) plate, which is a solid material most easily transmitting X-rays, has been conventionally used in many cases, but in recent years, X-ray transparency is Be. BN, which is not as good, but is a non-toxic, machinable, insulating solid material
An X-ray image pickup tube using a (boron nitride) plate is also used (Japanese Patent Application No. 2-230658, Japanese Patent Application No. 5-89646, Television Engineering Society Technical Report IPU'93-63, 1-6).
P., 1993, etc.).

【0004】BN板面板の平滑化方法としては、精密研
磨後、(1)BN板自体をイオンエッチングする(特願
平2‐072054)、(2)BN板に他の材料を積層
する(特願平2‐051694、特願平5‐8964
6、特願平7‐1722、等)、(3)BN板に他の材
料を積層し、さらにその材料をイオンエッチング等によ
り平滑化する(特願平2‐072054)、等の方法が
開示されている。
As a smoothing method for the BN plate face plate, after precision polishing, (1) the BN plate itself is ion-etched (Japanese Patent Application No. 2-072054), and (2) another material is laminated on the BN plate (special feature). Japanese Patent Application No. 2-051694, Japanese Patent Application No. 5-8964
(6, Japanese Patent Application No. 7-1722, etc.), (3) Laminating another material on a BN plate, and further smoothing the material by ion etching or the like (Japanese Patent Application No. 2-072054). Has been done.

【0005】BN板を使用し、ターゲット電極膜6の形
状を電子ビームの走査領域にほぼ対応する部分に限定し
て形成する従来のX線撮像管における、電極の取り出し
に関するターゲット構造例を、図2(a)〜(c)に、
具体的な概略断面図として示す(特願平2‐23065
8、テレビジョン学会技術報告IPU’93‐63、1
〜6頁、1993年)。ここで、7は、入射X線を吸収
して表面に電荷パターンを形成する光導電膜である。
An example of a target structure relating to electrode extraction in a conventional X-ray image pickup tube in which a BN plate is used and the shape of the target electrode film 6 is limited to a portion substantially corresponding to an electron beam scanning region is shown in FIG. 2 (a)-(c),
Shown as a specific schematic cross-sectional view (Japanese Patent Application No. 2-23065)
8. Television Society Technical Report IPU '93 -63, 1
~ 6, 1993). Here, 7 is a photoconductive film that absorbs incident X-rays and forms a charge pattern on the surface.

【0006】まず、図2(a)は、X線を通過させる開
口部を有する絶縁板5とBN薄板4とが接着され、これ
らを貫通する電極ピン1と、真空蒸着などにより面板上
に形成された金属膜13とがハンダ14等により接合・
封止された構造である。次に、図2(b)は、BN薄板
4に貫通孔が、絶縁板5にX線通過用の開口部が開けら
れており、それらの内面および近傍の両表面に金属膜1
3が付けられ、それらが導電性樹脂3および絶縁性樹脂
15により接着・封止された構造である。図2(c)
は、X線通過用の開口部を有する絶縁板5として、電極
ピン1が融着されたガラス板が使用され、これと電極ピ
ンに対応する位置に貫通孔が開けられたBN薄板4とが
接着され、貫通孔内部に導電性樹脂3が充填・封止され
た構造である。
First, as shown in FIG. 2 (a), an insulating plate 5 having an opening for passing X-rays and a BN thin plate 4 are adhered to each other, and an electrode pin 1 penetrating them is formed on a face plate by vacuum vapor deposition or the like. The metal film 13 is joined by solder 14 or the like.
It is a sealed structure. Next, in FIG. 2B, a through hole is formed in the BN thin plate 4 and an opening for X-ray passage is formed in the insulating plate 5, and the metal film 1 is formed on the inner surface and both surfaces in the vicinity thereof.
3 is attached, and they are adhered and sealed by the conductive resin 3 and the insulating resin 15. Figure 2 (c)
The glass plate having the electrode pin 1 fused is used as the insulating plate 5 having an opening for X-ray passage, and the BN thin plate 4 having a through hole at a position corresponding to the electrode pin is used. This is a structure in which the conductive resin 3 is adhered and the inside of the through hole is filled and sealed.

【0007】X線撮像管の光導電膜7には、一般に、P
bO,Si,Se,CdTe等が用いられている。このう
ち、特に非晶質Seは、高電界を印加すると内部で電荷
のアバランシェ増倍現象が起こるので、高感度用の撮像
管材料として使用される。
The photoconductive film 7 of the X-ray image pickup tube is generally made of P.
bO, Si, Se, CdTe, etc. are used. Among them, especially amorphous Se is used as a high sensitivity image pickup tube material because an avalanche multiplication phenomenon of charges occurs inside when a high electric field is applied.

【0008】[0008]

【発明が解決しようとする課題】しかし、一般に、アバ
ランシェ増倍現象を利用するX線撮像管では、面板表面
にわずかでも凹凸が存在すると、高電界下で光導電膜に
不均一電界が印加され、局所的に白点状画面欠陥が発生
し、また、暗電流が増加してしまう。このため、面板表
面の凹凸を少なくとも±0.1μm以下に平滑化する必
要があり、かつ、この平滑化面に異物が付着して洗浄性
が損なわれないように、充分に配慮する必要がある。
However, in general, in an X-ray image pickup tube utilizing the avalanche multiplication phenomenon, if a slight unevenness exists on the face plate surface, a nonuniform electric field is applied to the photoconductive film under a high electric field. However, white dot-shaped screen defects locally occur, and dark current increases. For this reason, it is necessary to smooth the irregularities on the surface of the face plate to at least ± 0.1 μm or less, and to prevent foreign matter from adhering to the smoothed surface and impairing the cleaning performance. .

【0009】上記図2(a)〜(c)に示した構造のタ
ーゲットでは、その製造工程において、いずれも、電極
取り出しのため、金属膜の形成作業、ハンダ付け作業、
樹脂充填作業のいずれかの作業が必要となる。これらの
作業は、通常、面板準備工程のBN板4(または、BN
板4上の接合材料)の表面の平滑化処理工程の後に行わ
れるため、これらの作業で微小な異物が平滑化面に付着
して、面板表面に局所的な凹凸をもたらし、白点状画面
欠陥発生の原因となりやすい。一方、図2(b)および
(c)に示した構造のターゲット製造工程では、BN板
4(または、場合によってはBN板4とその上の接合材
料)の貫通孔に導電性樹脂等を充填した後、研磨加工
し、イオンエッチング法等により平滑化処理をする工程
も考えられるが、平滑化処理工程で導電性樹脂等の微粒
子が発生して、BN薄板4の平滑化面上を汚染しやす
く、白点状画面欠陥の原因となりやすい。
In the manufacturing process of the targets having the structures shown in FIGS. 2A to 2C, in order to take out the electrodes, a metal film forming operation, a soldering operation,
Either of the resin filling work is required. These operations are normally performed on the BN plate 4 (or BN plate) in the face plate preparation process.
Since it is performed after the surface smoothing process of the bonding material on the plate 4), a minute foreign substance adheres to the smoothed surface in these operations and causes local unevenness on the surface of the face plate, resulting in a white dot screen. It is easy to cause defects. On the other hand, in the target manufacturing process of the structure shown in FIGS. 2B and 2C, the through holes of the BN plate 4 (or, in some cases, the BN plate 4 and the bonding material thereon) are filled with a conductive resin or the like. After that, a step of polishing and performing a smoothing treatment by an ion etching method or the like can be considered. However, fine particles such as a conductive resin are generated in the smoothing treatment step and contaminate the smoothed surface of the BN thin plate 4. It is easy to cause white spot-like screen defects.

【0010】本発明は、このような課題を解決するため
になされたもので、アバランシェ増倍現象が生じる程の
高電界下でも、白点状画面欠陥の発生や暗電流の増加な
しに、SN比の高い高感度、高画質画像が得られるX線
撮像管、およびその製造方法を提供することを目的とす
る。
The present invention has been made in order to solve such a problem. Even under a high electric field such that an avalanche multiplication phenomenon occurs, SN can be generated without occurrence of white dot-like screen defects and dark current. It is an object of the present invention to provide an X-ray imaging tube having a high ratio and high sensitivity and capable of obtaining a high quality image, and a manufacturing method thereof.

【0011】[0011]

【課題を解決するための手段】この目的を達成するため
に、本発明においては、X線撮像管のターゲット部を、
第1の絶縁性面板と、片面を平滑化した第2の絶縁性面
板と、この第1および第2の絶縁性面板を貫通して設け
られたターゲット電極ピンと、該ターゲット電極ピンお
よび第2の絶縁性面板上に積層されたターゲット電極膜
と光導電膜とで構成し、第2の絶縁性面板内のターゲッ
ト電極ピンを、予め第2の絶縁性面板に融着等により一
体化した金属製の電極ピンとする。ここで、第1の絶縁
性面板をBN板で、第2の絶縁性面板をSiO2で構成
し、第1の絶縁性面板内のターゲット電極ピンを、第2
の絶縁性面板内の金属製の電極ピンと異なる組成の導電
性物質、たとえば、樹脂などで形成する。また、光導電
膜をSeを主体とする非晶質材料で構成し、これらの光
導電膜に、X線の入射により発生した電荷がアバランシ
ェ増倍現象が生じる程の高電界を印加する。
In order to achieve this object, in the present invention, the target portion of the X-ray image pickup tube is
A first insulating face plate, a second insulating face plate having one surface smoothed, a target electrode pin penetrating the first and second insulating face plates, the target electrode pin and the second insulating face plate. It is composed of a target electrode film and a photoconductive film laminated on the insulating face plate, and the target electrode pins in the second insulating face plate are integrated with the second insulating face plate in advance by fusion or the like. And the electrode pin. Here, the first insulating face plate is made of a BN plate, the second insulating face plate is made of SiO 2 , and the target electrode pin in the first insulating face plate is
The insulating face plate is formed of a conductive material having a different composition from that of the metal electrode pin, for example, resin. Further, the photoconductive film is made of an amorphous material mainly composed of Se, and a high electric field is applied to these photoconductive films such that charges generated by the incidence of X-rays cause an avalanche multiplication phenomenon.

【0012】また、上記のX線撮像管の製造方法におい
て、金属製ターゲット電極ピンを融着等により一体化し
た第2の絶縁性面板と、上記電極ピンに対応する位置に
貫通孔を開けた第1の絶縁性面板とを接着する第1の工
程と、第2の絶縁性面板と金属製ターゲット電極ピンと
を薄く研磨加工する第2の工程とを順次行う。また、上
記の第1と第2の工程との間に、第1の絶縁性面板の貫
通孔に導電性物質を充填する工程を設け、さらに、上記
の第2の工程の後に、第2の絶縁性面板表面を、イオン
エッチング法により平滑化する処理を行う。そして、そ
の平滑化された面上にターゲット電極膜と光導電膜とを
順次形成して、ターゲット部を構成する。
Further, in the above-mentioned method for manufacturing an X-ray image pickup tube, a second insulating face plate in which metal target electrode pins are integrated by fusion or the like and a through hole is formed at a position corresponding to the electrode pin. The first step of adhering the first insulating face plate and the second step of thinly polishing the second insulating face plate and the metal target electrode pin are sequentially performed. Further, a step of filling the through hole of the first insulating face plate with a conductive substance is provided between the first and second steps, and further, a second step is performed after the second step. The surface of the insulating face plate is smoothed by an ion etching method. Then, a target electrode film and a photoconductive film are sequentially formed on the smoothed surface to form a target portion.

【0013】[0013]

【作用】本発明に係る上記のX線撮像管及びその製造方
法においては、ターゲット部のターゲット電極膜が形成
される面板として、金属製のターゲット電極ピンの一部
が予め融着等により一体化された第2の絶縁性面板(S
iO2薄板)と第1の絶縁性面板(BN板)とが接着して
使用されているため、上記の電極引き出しのための、従
来技術における金属膜の形成作業、ハンダ付け作業、樹
脂充填作業などが全て不要となる。また、第2の絶縁性
面板に融着等により一体化された金属製の電極ピンは緻
密であるため、平滑化処理の際に、白点状画面欠陥の原
因となる微粒子を発生することもない。
In the X-ray image pickup tube and the method of manufacturing the same according to the present invention, a part of the target electrode pin made of metal is previously integrated by fusion or the like as the face plate on which the target electrode film of the target portion is formed. Second insulating face plate (S
Since the iO 2 thin plate) and the first insulating face plate (BN plate) are used by being adhered to each other, the metal film forming work, the soldering work, and the resin filling work in the prior art for the above-mentioned electrode extraction are performed. Etc. are all unnecessary. In addition, since the metal electrode pin integrated with the second insulating face plate by fusion bonding or the like is dense, fine particles that cause white dot-like screen defects may be generated during the smoothing process. Absent.

【0014】したがって、本発明に係るX線撮像管にお
いては、アバランシェ増倍現象が生じる程の高電界下で
も、画面に白点状の像欠陥や暗電流が発生することが抑
えられるので、SN比の高い高感度、高画質のX線画像
が得られる。
Therefore, in the X-ray image pickup tube according to the present invention, it is possible to suppress the generation of white dot-like image defects and dark current on the screen even under a high electric field such that the avalanche multiplication phenomenon occurs. A high-sensitivity, high-quality X-ray image having a high ratio can be obtained.

【0015】[0015]

【実施例】【Example】

(実施例1)図1は、本発明に係るX線撮像管の基本構
造を示す図で、(a)は撮像管ターゲット部近傍の概略
断面図、(b)は、(a)のX‐X′線で切断した場合
のターゲット表面を電子ビーム走査側(A方向)から見
た平面図である。1はターゲット電極ピンの一部である
金属製ターゲット電極ピン、2は第2の絶縁性面板であ
るガラス薄板、3は導電性樹脂、4は第1の絶縁性面板
であるBN薄板、5は補強用絶縁板、6はターゲット電
極膜、7は光導電膜、8は走査電子ビームの走査領域、
9は金属リング、10はインジュウムリング、11はメ
ッシュ電極、12はガラス外管である。
(Embodiment 1) FIG. 1 is a view showing a basic structure of an X-ray image pickup tube according to the present invention. (A) is a schematic sectional view in the vicinity of an image pickup tube target portion, (b) is an X-ray of (a). FIG. 6 is a plan view of the target surface when cut along the line X ′ as seen from the electron beam scanning side (direction A). 1 is a metal target electrode pin which is a part of the target electrode pin, 2 is a glass thin plate which is a second insulating face plate, 3 is a conductive resin, 4 is a BN thin plate which is a first insulating face plate, and 5 is A reinforcing insulating plate, 6 is a target electrode film, 7 is a photoconductive film, 8 is a scanning electron beam scanning region,
Reference numeral 9 is a metal ring, 10 is an indium ring, 11 is a mesh electrode, and 12 is a glass outer tube.

【0016】金属製ターゲット電極ピン1は予めガラス
薄板2に融着等により一体化されている。BN薄板4に
は金属製ターゲット電極ピン1に対応する位置に貫通孔
が開けられ、内部に導電性樹脂3が充填されている。補
強用絶縁板5には走査電子ビームの走査領域8に対応し
たX線通過用の開口部、および金属製ターゲット電極ピ
ン1に対応した貫通孔が開けられ、貫通孔内には導電性
樹脂3が充填され、金属製ターゲット電極ピン1と共
に、ターゲット電極ピンが形成されている。ガラス薄膜
2、BN薄板4、補強用絶縁板5は、接着剤で接着され
ている。ガラス薄板2および金属製ターゲット電極ピン
1に密着して、ターゲット電極膜6および光導電膜7
が、図に示すように形成されている。ここで、光導電膜
7には、非晶質Seを用いることが望ましく、また、正
孔注入阻止層(例えば、CeO2膜)および電子注入阻止
層(例えば、Sb23膜)を非晶質Seの膜の両側に配置
することがより望ましい。 なお、上記金属製ターゲッ
ト電極ピンと第2の絶縁性面板の表面は、必ずしも同一
表面である必要は無く、ターゲット電極膜とターゲット
電極ピンとが低抵抗で接続されさえすれば、これらの接
続部に多少の凹凸が存在しても差し支えない。 また、
上記金属製ターゲット電極ピンと第2の絶縁性面板を一
体化する方法としては、第2の絶縁性面板としてSiO2
ガラスを使用する場合は、SiO2ガラスを融解して、そ
の中にターゲット電極ピンを埋め込んだ後、徐冷して一
体化する融着法が適当と考えられるが、その他、接着剤
や埋込樹脂を使用する方法も考えられ、これらによって
もなんら差し支えない。
The metal target electrode pin 1 is previously integrated with the thin glass plate 2 by fusion or the like. Through holes are formed in the BN thin plate 4 at positions corresponding to the metal target electrode pins 1, and the conductive resin 3 is filled inside. An opening for X-ray passage corresponding to the scanning area 8 of the scanning electron beam and a through hole corresponding to the metal target electrode pin 1 are opened in the reinforcing insulating plate 5, and the conductive resin 3 is provided in the through hole. And the target electrode pin 1 is formed together with the metal target electrode pin 1. The glass thin film 2, the BN thin plate 4, and the reinforcing insulating plate 5 are bonded with an adhesive. The target electrode film 6 and the photoconductive film 7 are in close contact with the thin glass plate 2 and the metallic target electrode pin 1.
Are formed as shown in the figure. Here, it is desirable to use amorphous Se for the photoconductive film 7, and the hole injection blocking layer (for example, CeO 2 film) and the electron injection blocking layer (for example, Sb 2 S 3 film) are not used. It is more desirable to dispose on both sides of the crystalline Se film. The surface of the metal target electrode pin and the surface of the second insulating face plate do not necessarily have to be the same surface, and as long as the target electrode film and the target electrode pin are connected with low resistance, they may be slightly connected to these connection parts. There is no problem even if there is unevenness. Also,
As a method of integrating the metal target electrode pin and the second insulating faceplate, SiO 2 as the second insulating faceplate
When glass is used, a fusion method in which SiO 2 glass is melted, the target electrode pin is embedded in the glass, and then gradually cooled to be integrated is considered appropriate. A method of using a resin is also conceivable, and there is no problem even with these methods.

【0017】図3に、図1の撮像管構造のSe光導電膜
におけるX線吸収率の計算結果例を示す。図3では、面
板として、0.5mm厚のBe板、BN板、SiO2板を単
独で使用する場合、およびBN板と平滑化材料のSiO2
薄膜を重ね合わせて使用する場合の、Se光導電膜25
μmにおけるX線吸収率(X線利用率)の計算結果を示
している。図3から、BN板使用の場合、Be板使用の
場合ほどSe膜でのX線吸収率は大きくないものの、5
〜13keV程度の低エネルギー帯域でも使用可能であ
ること、平滑化のためのSiO2薄板の厚さは薄い方が望
ましいことがわかる。
FIG. 3 shows an example of the calculation result of the X-ray absorptance in the Se photoconductive film having the image pickup tube structure shown in FIG. In FIG. 3, when a 0.5 mm thick Be plate, a BN plate, and a SiO 2 plate are used alone as the face plate, and when the BN plate and the smoothing material SiO 2 are used.
Se photoconductive film 25 when thin films are stacked and used
The calculation result of the X-ray absorption rate (X-ray utilization rate) in μm is shown. From FIG. 3, when the BN plate is used, the X-ray absorptivity of the Se film is not as great as when the Be plate is used, but 5
It can be seen that it can be used even in a low energy band of about 13 keV and that the thin SiO 2 plate for smoothing is preferably thin.

【0018】図4に、本発明に係るX線撮像管の基本的
な製造工程のフロー図を示す。製造工程は、(1)BN
板4の孔開け、(2)ガラス板2・BN板4の接着、
(3)導電性樹脂3の充填、(4)ガラス板2の研磨、
(5)洗浄・イオンエッチング、(6)ターゲット電極
膜6の蒸着、(7)光導電膜7の蒸着、(8)補強用絶
縁板5の接着、(9)補強用絶縁板5の電極加工、(1
0)撮像管の組立て、の各工程で構成されている。
FIG. 4 shows a flow chart of a basic manufacturing process of the X-ray image pickup tube according to the present invention. The manufacturing process is (1) BN
Drilling holes in plate 4, (2) Adhesion of glass plate 2 and BN plate 4,
(3) Filling with conductive resin 3, (4) Polishing of glass plate 2,
(5) cleaning / ion etching, (6) vapor deposition of the target electrode film 6, (7) vapor deposition of the photoconductive film 7, (8) adhesion of the reinforcing insulating plate 5, (9) electrode processing of the reinforcing insulating plate 5. , (1
0) Assembling of the image pickup tube.

【0019】上記工程のうち、(8)および(9)工程
は、(4)工程の次に、順次行われても良い。また、補
強用絶縁板5が不要の時は、(8)工程および(9)工
程は省略される。さらにまた、(2)工程以前に(4)
工程を行う工程順では、ガラス板2単独での取扱いが難
しい上、(2)工程で研磨、清浄面を汚染する心配があ
り、不適当である。
Of the above steps, steps (8) and (9) may be sequentially performed after step (4). Further, when the reinforcing insulating plate 5 is unnecessary, the steps (8) and (9) are omitted. Furthermore, before step (2), (4)
In the order of steps, the glass plate 2 is not suitable because it is difficult to handle the glass plate 2 alone, and there is a risk of contaminating the polished and cleaned surfaces in the step (2).

【0020】なお、金属製ターゲット電極ピン1を予め
融着したガラス板2を単独でX線撮像管として用いるこ
とも考えられるが、強度の点から、ガラス薄板の板厚は
あまり薄くできず、そのため、図3の曲線Cから推定さ
れるように、適用X線エネルギー帯域が限定されてしま
う。
It is possible to use the glass plate 2 having the metal target electrode pins 1 fused in advance as an X-ray image pickup tube alone, but from the viewpoint of strength, the glass thin plate cannot be made so thin. Therefore, as estimated from the curve C in FIG. 3, the applied X-ray energy band is limited.

【0021】次に、上記X線撮像管の製造手順を、さら
に詳細に説明する。
Next, the manufacturing procedure of the X-ray image pickup tube will be described in more detail.

【0022】まず、厚さ0.5mm、直径26mmのB
N板4の中心から8.5mmの位置に、直径1.5mmの
貫通孔を超音波加工により開ける。つぎに、中心から
8.5mmの位置に直径0.8mmのMo製のターゲット
電極ピン1が予め融着されている厚さ1.0mm、直径
26mmのガラス板2と前記BN板4とを、ターゲット
電極ピン1と貫通孔とが対応するように接着剤を用いて
接着する。この時、ターゲット電極ピン1の表面に接着
剤が付着しないように注意する。つぎに、BN板4の貫
通孔内に銀エポキシ樹脂3を充填し、加熱硬化する。さ
らに、銀エポキシ樹脂充填側を一旦軽く研磨して、BN
板4表面と銀エポキシ樹脂3表面を同一平面とした後、
ガラス板2表面側を、ガラス板2の厚さが50μmとな
るまで機械研磨により、研磨加工する。この接合板を充
分洗浄した後、高周波スパッタリング装置でArガスを
用いて、ガラス薄板2側表面をイオンエッチング法によ
り平滑化してX線撮像管用の面板を得る。
First, B having a thickness of 0.5 mm and a diameter of 26 mm
A through hole having a diameter of 1.5 mm is formed by ultrasonic processing at a position 8.5 mm from the center of the N plate 4. Then, a glass plate 2 having a thickness of 1.0 mm and a diameter of 26 mm and a BN plate 4 having a target electrode pin 1 made of Mo and having a diameter of 0.8 mm fused in advance at a position of 8.5 mm from the center, The target electrode pin 1 and the through hole are bonded with an adhesive so that they correspond to each other. At this time, be careful that the adhesive does not adhere to the surface of the target electrode pin 1. Next, the silver epoxy resin 3 is filled in the through holes of the BN plate 4 and heat cured. Furthermore, lightly polish the side filled with silver epoxy resin to remove BN.
After making the surface of the plate 4 and the surface of the silver epoxy resin 3 flush with each other,
The surface side of the glass plate 2 is polished by mechanical polishing until the thickness of the glass plate 2 becomes 50 μm. After sufficiently cleaning this bonded plate, the surface of the glass thin plate 2 side is smoothed by an ion etching method using Ar gas in a high frequency sputtering apparatus to obtain a face plate for an X-ray image pickup tube.

【0023】つぎに、真空蒸着装置を用いて、上記面板
上に、10.5mm×13.7mmの長方形部と金属性タ
ーゲット電極ピン1への接続部とを有する、図1(b)
に示した形状で、厚さ30nmのAl膜をターゲット電極
膜6として形成し、その上に、直径20mm、厚さ20
nmのCeO2膜を正孔注入阻止層とし、厚さ8μmのSe
膜を光導電膜7として、順次真空蒸着する。さらに、そ
の上に、同一装置を用い、0.4TorrのArガス雰囲気
内で、Sb23多孔質膜を厚さ約0.1μmの電子注入阻
止層として形成する。
Next, using a vacuum vapor deposition apparatus, a rectangular portion of 10.5 mm × 13.7 mm and a connecting portion to the metallic target electrode pin 1 are provided on the face plate, as shown in FIG. 1 (b).
An Al film having a thickness of 30 nm and having a shape shown in FIG. 2 is formed as a target electrode film 6, and a target electrode film 6 has a diameter of 20 mm and a thickness of 20 nm.
8 nm thick SeO 2 film is used as the hole injection blocking layer.
The film is used as the photoconductive film 7 and is sequentially vacuum-deposited. Further, using the same device, an Sb 2 S 3 porous film is formed as an electron injection blocking layer having a thickness of about 0.1 μm in an Ar gas atmosphere of 0.4 Torr.

【0024】真空蒸着装置から取り出した面板に、図1
に示すように、中心部に11mm×14mmの長方形の
X線通過用の開口窓と、中心から8.5mmの位置に直
径2.5mmの電極取り出し用の貫通孔を、超音波加工
で開けた厚さ2.0mm、直径26mmの補強用のガラ
ス板5を接着した後、貫通孔に室温硬化型の銀エポキシ
樹脂3を充填し、撮像管のターゲット部が完成する。
The face plate taken out from the vacuum vapor deposition apparatus is shown in FIG.
As shown in Fig. 5, an 11 mm x 14 mm rectangular opening window for X-ray passage was formed in the center, and a through hole for electrode extraction of 2.5 mm diameter was formed at a position 8.5 mm from the center by ultrasonic processing. After adhering a reinforcing glass plate 5 having a thickness of 2.0 mm and a diameter of 26 mm, the through hole is filled with a room temperature curing type silver epoxy resin 3 to complete the target portion of the image pickup tube.

【0025】以上により得られた撮像管ターゲット部
を、電子銃を内蔵した撮像管筐体であるガラス外管12
にインジュウムリング10、金属リング9を介して圧着
し、内部を排気して真空封止し、X線撮像管を完成す
る。
The target portion of the image pickup tube obtained as described above is used as a glass outer tube 12 which is an image pickup tube housing containing an electron gun.
Then, the inner ring 10 and the metal ring 9 are pressure-bonded to each other, and the inside is evacuated and vacuum-sealed to complete the X-ray imaging tube.

【0026】得られたX線撮像管を、カメラに組み込ん
で、インジュウムリング10をカソード電位とし、ター
ゲット電極6に100〜900Vの電圧を印加して動作
させた。その結果、白点状画面欠陥の発生や暗電流の増
加無しに、SN比の高い高感度、高画質のX線画像が得
られた。
The obtained X-ray image pickup tube was incorporated into a camera, and the indium ring 10 was operated at a cathode potential and a voltage of 100 to 900 V was applied to the target electrode 6. As a result, a high-sensitivity, high-quality X-ray image with a high SN ratio was obtained without the occurrence of white dot-shaped screen defects and an increase in dark current.

【0027】(実施例2)本発明に係るX線撮像管の、
他の実施例におけるターゲット部近傍の概略断面図を、
図5に示す。図5と前記図1とを比べると、補強用ガラ
ス板5の電極取り出し用の貫通孔内の構成が異なってい
るのと、ターゲット面板およびインジュウムリング10
に接して、電極16が新たにもうけられていることがわ
かる。この電極16は、発明者等がシールド電極、ある
いはガード電極と呼んでいるもので、走査電子ビームの
走査領域外の光導電膜7表面の電位をカソード電位とす
ることによって、さざ波現象や画像反転現象等の、画像
異常現象を抑制する効果を有するものである(特願平5
‐89646)。
(Embodiment 2) The X-ray image pickup tube according to the present invention,
A schematic cross-sectional view of the vicinity of the target portion in another embodiment,
As shown in FIG. Comparing FIG. 5 with FIG. 1, the structure inside the through hole for taking out the electrode of the reinforcing glass plate 5 is different, the target face plate and the indium ring 10 are different.
It can be seen that the electrode 16 is newly provided by contacting with. The electrode 16 is called a shield electrode or a guard electrode by the inventors, and when the potential of the surface of the photoconductive film 7 outside the scanning region of the scanning electron beam is set to the cathode potential, ripples and image inversion occur. It has an effect of suppressing image abnormal phenomenon such as a phenomenon (Japanese Patent Application No.
-89646).

【0028】実施例1と同様に、厚さ0.5mm、直径
26mmのBN板4の中心から8.5mmの位置に、直
径1.5mmの貫通孔を超音波加工により開ける。つぎ
に、中心から8.5mmの位置に直径0.8mmのMo製
のターゲット電極ピン1が予め融着されている厚さ1.
0mm、直径26mmのガラス板2と前記BN板4と
を、ターゲット電極ピン1と貫通孔が対応するように接
着剤を用いて接着する。つぎに、BN板4の貫通孔内に
銀エポキシ樹脂3を充填し、加熱硬化する。さらに、銀
エポキシ樹脂充填側を一旦軽く研磨して、BN板4表面
と銀エポキシ樹脂3表面を同一平面とした後、ガラス板
2表面側を、ガラス板2の厚さが50μmとなるまで機
械研磨により、研磨加工する。
As in the first embodiment, a through hole having a diameter of 1.5 mm is formed by ultrasonic machining at a position 8.5 mm from the center of the BN plate 4 having a thickness of 0.5 mm and a diameter of 26 mm. Next, a target electrode pin 1 made of Mo and having a diameter of 0.8 mm is pre-fused at a position of 8.5 mm from the center and has a thickness of 1.
The glass plate 2 having a diameter of 0 mm and a diameter of 26 mm is bonded to the BN plate 4 with an adhesive so that the target electrode pin 1 and the through hole correspond to each other. Next, the silver epoxy resin 3 is filled in the through holes of the BN plate 4 and heat cured. Further, the side filled with the silver epoxy resin is lightly polished once to make the surface of the BN plate 4 and the surface of the silver epoxy resin 3 flush with each other, and then the surface of the glass plate 2 is machined until the thickness of the glass plate 2 becomes 50 μm. Polishing is performed by polishing.

【0029】つぎに、実施例1と同一のX線通過用の開
口窓、および電極取り出し用の貫通孔を開けた補強用の
ガラス板5を接着する。引き続き、貫通孔内に、主たる
部分の直径が0.3mmで頭部の直径が0.8mmの金属
製の電極ピン17を銀エポキシ樹脂3を用いて接着、硬
化した後、さらに絶縁性樹脂(エポキシ樹脂)15を用
いて補強する。さらに、充分洗浄後、実施例1と同様
に、高周波スパッタリング装置でガラス薄板2側表面を
イオンエッチング法により平滑化してX線撮像管用の面
板を得る。
Next, the same opening window for X-ray passage and the reinforcing glass plate 5 having through holes for taking out electrodes as in Example 1 are bonded. Subsequently, a metal electrode pin 17 having a main portion having a diameter of 0.3 mm and a head portion having a diameter of 0.8 mm is adhered and cured using a silver epoxy resin 3 in the through hole, and then an insulating resin ( Reinforce with (epoxy resin) 15. Further, after thoroughly washing, the surface of the glass thin plate 2 side is smoothed by an ion etching method with a high frequency sputtering device in the same manner as in Example 1 to obtain a face plate for an X-ray image pickup tube.

【0030】つぎに、真空蒸着装置を用いて、上記面板
上に、10.5mm×13.7mmの長方形部とターゲッ
ト電極ピン1への接続部とを有する、厚さ30nmのAl
膜をターゲット電極膜6として形成し、その上に、直径
20mm、厚さ20nmのCeO2膜を正孔注入阻止層と
して、また、厚さ25μmのSe膜を光導電膜7とし
て、順次真空蒸着する。さらにその上に、同一装置で、
0.3TorrのArガス雰囲気内で厚さ約0.1μmのSb2
3多孔質膜を電子注入阻止層として形成する。
Next, using a vacuum vapor deposition apparatus, a 30 nm thick Al having a rectangular portion of 10.5 mm × 13.7 mm and a connecting portion to the target electrode pin 1 was formed on the face plate.
A film is formed as a target electrode film 6, on which a CeO 2 film having a diameter of 20 mm and a thickness of 20 nm is used as a hole injection blocking layer, and a Se film having a thickness of 25 μm is used as a photoconductive film 7, which are sequentially vacuum-deposited. To do. Furthermore, on the same device,
Sb 2 with a thickness of about 0.1 μm in an Ar gas atmosphere of 0.3 Torr
The S 3 porous film is formed as an electron injection blocking layer.

【0031】以上により得られた撮像管ターゲット部と
シールド電極16とを、図5に示すように、電子銃を内
蔵した撮像管筐体のガラス外管12にインジュウムリン
グ10、金属リング9を介して圧着し、内部を排気して
真空封止し、X線撮像管を完成する。
As shown in FIG. 5, the image pickup tube target portion and the shield electrode 16 obtained as described above are provided with an indium ring 10 and a metal ring 9 on a glass outer tube 12 of an image pickup tube housing containing an electron gun. Then, the inside is evacuated and vacuum-sealed to complete an X-ray imaging tube.

【0032】得られたX線撮像管を、カメラに組み込ん
で、インジュウムリング10およびシールド電極16を
カソード電位とし、ターゲット電極6に200〜255
0Vの電圧を印加して動作させた。その結果、白点状画
面欠陥の発生や暗電流の増加、および画面異常現象なし
に、SN比の高い高感度、高画質のX線画像が得られ
た。
The obtained X-ray image pickup tube was incorporated into a camera, the indium ring 10 and the shield electrode 16 were set to the cathode potential, and the target electrode 6 was set to 200 to 255.
It was operated by applying a voltage of 0V. As a result, a high-sensitivity and high-quality X-ray image with a high SN ratio was obtained without the occurrence of white dot-shaped screen defects, an increase in dark current, and a screen abnormal phenomenon.

【0033】(実施例3)本発明に係るX線撮像管の、
他の実施例におけるターゲット部近傍の概略断面図を、
図6に示す。図6と前記図5とを比べると、図6には、
補強用ガラス板5がなく、BN板4の形状が異なり、B
N板4が補強板の役目も果たす構成となっているのがわ
かる。
(Embodiment 3) An X-ray image pickup tube according to the present invention,
A schematic cross-sectional view of the vicinity of the target portion in another embodiment,
As shown in FIG. Comparing FIG. 6 with FIG. 5, FIG.
There is no reinforcing glass plate 5, the shape of the BN plate 4 is different, and
It can be seen that the N plate 4 is configured to also serve as a reinforcing plate.

【0034】厚さ2.5mm、直径26mmのBN板4
の中心部に、断面積が11mm×14mmで、深さ2.
0mmの直方体のX線通過用の開口窓と、中心から8.
5mmの位置に直径2.5mmの貫通孔を、超音波加工
により開ける。このBN板4に、中心から8.5mmの
位置に直径0.8mmのMo製のターゲット電極ピン1
が、予め融着されている厚さ1.0mm、直径26mm
のガラス板2を、ターゲット電極ピン1と貫通孔とを対
応させて接着し、BN板4の貫通孔内に銀エポキシ樹脂
3を充填して加熱硬化する。
BN plate 4 having a thickness of 2.5 mm and a diameter of 26 mm
The cross-sectional area is 11mm x 14mm and the depth is 2.
A 0 mm rectangular parallelepiped opening window for X-ray passage and 8.
A through hole having a diameter of 2.5 mm is formed at a position of 5 mm by ultrasonic processing. On this BN plate 4, a target electrode pin 1 made of Mo and having a diameter of 0.8 mm was placed at a position 8.5 mm from the center.
Is pre-fused with a thickness of 1.0 mm and a diameter of 26 mm
The glass plate 2 is bonded so that the target electrode pin 1 and the through hole correspond to each other, and the silver epoxy resin 3 is filled in the through hole of the BN plate 4 and heat-cured.

【0035】つぎに、BN板4の開口窓に、研磨時の補
強用として、開口窓とほぼ同一形状のBN板を一時的に
接着、充填した後、ガラス板2表面側を、ガラス板2の
厚さが50μmとなるまで、機械研磨により精密研磨す
る。
Next, after temporarily adhering and filling the opening window of the BN plate 4 with a BN plate having substantially the same shape as that of the opening window for reinforcement during polishing, the front surface side of the glass plate 2 is attached to the glass plate 2. Precision polishing by mechanical polishing until the thickness becomes 50 μm.

【0036】つぎに、充分洗浄し、高周波スパッタリン
グ装置でガラス薄板2側表面をイオンエッチング法によ
り平滑化して、X線撮像管用の面板を得る。
Next, after thoroughly washing, the surface of the glass thin plate 2 side is smoothed by an ion etching method with a high frequency sputtering device to obtain a face plate for an X-ray image pickup tube.

【0037】この撮像管面板上に、真空蒸着装置を用い
て、10.5mm×13.7mmの長方形部とターゲット
電極ピン1への接続部とを有する、厚さ25nmのIT
O膜を、1×10~2TorrのO2雰囲気中で、ターゲット
電極膜6として形成する。その上に、真空中で直径20
mm、厚さ20nmのCeO2膜と、厚さ25μmのSe
膜7を蒸着する。さらに、同一装置で、0.3TorrのA
rガス雰囲気内で厚さ約0.1μmのSb23多孔質膜を
電子注入阻止層として形成し、X線撮像管ターゲット部
を完成する。
A 25 nm thick IT having a rectangular portion of 10.5 mm × 13.7 mm and a connecting portion to the target electrode pin 1 was formed on this imaging tube face plate using a vacuum vapor deposition apparatus.
The O film is formed as the target electrode film 6 in an O 2 atmosphere of 1 × 10 to 2 Torr. On top of that, a diameter of 20
mm, 20 nm thick CeO 2 film and 25 μm thick Se
The film 7 is deposited. Furthermore, with the same device, A of 0.3 Torr
A Sb 2 S 3 porous film having a thickness of about 0.1 μm is formed as an electron injection blocking layer in an r gas atmosphere to complete an X-ray image pickup tube target portion.

【0038】以上により得られた撮像管ターゲット部と
シールド電極16とを、図6に示すように、電子銃を内
蔵した撮像管筐体のガラス外管12にインジュウムリン
グ10、金属リング9を介して圧着し、内部を排気して
真空封止し、X線撮像管を完成する。
As shown in FIG. 6, the image pickup tube target portion and the shield electrode 16 obtained as described above are provided with an indium ring 10 and a metal ring 9 on a glass outer tube 12 of an image pickup tube housing containing an electron gun. Then, the inside is evacuated and vacuum-sealed to complete an X-ray imaging tube.

【0039】得られたX線撮像管を、カメラに組み込ん
で、インジュウムリング10およびシールド電極16を
カソード電位とし、ターゲット電極6に200〜255
0Vの電圧を印加して動作させた。その結果、実施例2
と同様に、白点状画面欠陥の発生や暗電流の増加、およ
び画面異常現象なしに、SN比の高い高感度、高画質の
X線画像が得られた。
The obtained X-ray image pickup tube was incorporated in a camera, the indium ring 10 and the shield electrode 16 were set to the cathode potential, and the target electrode 6 was set to 200 to 255.
It was operated by applying a voltage of 0V. As a result, Example 2
Similarly to the above, a high-sensitivity and high-quality X-ray image with a high SN ratio was obtained without occurrence of white dot-shaped screen defects, increase in dark current, and screen abnormal phenomenon.

【0040】[0040]

【発明の効果】以上説明したように、本発明に係るX線
撮像管及びその製造方法においては、金属性のターゲッ
ト電極ピンを予め融着した第2の絶縁性面板を第1の面
板に接着して研磨加工することにより、撮像管のターゲ
ット面板の平滑化ならびに洗浄性に優れ、高電界下で
も、白点状画面欠陥の発生や暗電流の増加なしに、SN
比の高い高感度・高画質のX線画像が得られ、産業面だ
けではなく、医学や学術研究上においても、極めて利用
価値の高いX線撮像管が得られた。
As described above, in the X-ray image pickup tube and the method of manufacturing the same according to the present invention, the second insulating face plate having the metallic target electrode pins fused in advance is bonded to the first face plate. By polishing and polishing the target surface plate of the image pickup tube, the SN is excellent in smoothing and cleaning, and even under a high electric field, there is no occurrence of white dot-shaped screen defects or increase in dark current, and SN
A high-sensitivity, high-quality X-ray image having a high ratio was obtained, and an X-ray image pickup tube having an extremely high utility value was obtained not only in industrial aspects but also in medical and academic research.

【図面の簡単な説明】[Brief description of drawings]

【図1】本発明に係るX線撮像管の基本構造を示す図で
あり、(a)はターゲット部近傍の概略断面図、(b)
はターゲット表面を電子ビーム走査側から見た平面図で
ある。
FIG. 1 is a diagram showing a basic structure of an X-ray image pickup tube according to the present invention, in which (a) is a schematic sectional view in the vicinity of a target portion, and (b).
FIG. 4 is a plan view of the target surface as seen from the electron beam scanning side.

【図2】従来のBN板を用いたX線撮像管のターゲット
部の電極取り出し方法を示す図である。
FIG. 2 is a diagram showing a method of extracting electrodes from a target portion of an X-ray image pickup tube using a conventional BN plate.

【図3】本発明に係るX線撮像管のSe光導電膜におけ
るX線吸収率の計算結果を示す図である。
FIG. 3 is a diagram showing a calculation result of X-ray absorptance in a Se photoconductive film of an X-ray image pickup tube according to the present invention.

【図4】本発明に係るX線撮像管の基本的な製造工程を
示すフロー図である。
FIG. 4 is a flowchart showing a basic manufacturing process of an X-ray image pickup tube according to the present invention.

【図5】本発明に係るX線撮像管の実施例2におけるタ
ーゲット部近傍の構成を示す概略断面図である。
FIG. 5 is a schematic cross-sectional view showing a configuration in the vicinity of a target portion in Embodiment 2 of the X-ray imaging tube according to the present invention.

【図6】本発明に係るX線撮像管の実施例3におけるタ
ーゲット部近傍の構成を示す概略断面図である。
FIG. 6 is a schematic cross-sectional view showing a configuration in the vicinity of a target portion in Embodiment 3 of the X-ray imaging tube according to the present invention.

【符号の説明】[Explanation of symbols]

1…金属製ターゲット電極ピン 2…ガラス薄板 3…導電性樹脂 4…BN薄板 5…補強用絶縁板 6…ターゲット電極膜 7…光導電膜 8…走査電子ビームの走査領域 9…金属リング 10…インジュウムリング 11…メッシュ電極 12…ガラス外管 13…金属膜 14…ハンダ 15…絶縁性樹脂 16…シールド電極 17…金属製の電極ピン DESCRIPTION OF SYMBOLS 1 ... Metal target electrode pin 2 ... Glass thin plate 3 ... Conductive resin 4 ... BN thin plate 5 ... Reinforcement insulating plate 6 ... Target electrode film 7 ... Photoconductive film 8 ... Scanning electron beam scanning region 9 ... Metal ring 10 ... Indium ring 11 ... Mesh electrode 12 ... Glass outer tube 13 ... Metal film 14 ... Solder 15 ... Insulating resin 16 ... Shield electrode 17 ... Metal electrode pin

フロントページの続き (72)発明者 辻 和隆 東京都国分寺市東恋ケ窪1丁目280番地 株式会社日立製作所中央研究所内 (72)発明者 鮫島 賢二 東京都国分寺市東恋ケ窪1丁目280番地 株式会社日立製作所中央研究所内 (72)発明者 茂木 謙一 東京都小平市御幸町32番地 日立電子株式 会社小金井工場内 (72)発明者 岡村 憲伯 山梨県北巨摩郡小渕沢町上笹尾3434−1 日立電子株式会社小渕沢工場内Front page continuation (72) Inventor Kazutaka Tsuji, 1-280, Higashi Koikekubo, Kokubunji, Tokyo, Central Research Laboratory, Hitachi, Ltd. (72) Inventor, Kenji Samejima 1-280, Higashi Koikeku, Kokubunji, Tokyo Hitachi Research Center Co., Ltd. In-house (72) Kenichi Mogi, 32 Miyuki-cho, Kodaira-shi, Tokyo Inside Koganei Plant, Hitachi Electronics Co., Ltd. (72) Inori, Noriaki Okamura 3434-1, Kamisasao, Obuchizawa-machi, Kitakoma-gun, Yamanashi Hitachi Electronics Co., Ltd. Obuchizawa Plant Within

Claims (9)

【特許請求の範囲】[Claims] 【請求項1】第1の絶縁性面板と、該第1の絶縁性面板
上に積層配置された第2の絶縁性面板と、該第2の絶縁
性面板上に積層配置されたターゲット電極膜と、該ター
ゲット電極膜上に積層配置されたX線を電気信号に変換
するための光導電膜と、上記第1の絶縁性面板を貫通し
た導電性物質から成るターゲット電極ピンと、上記第2
の絶縁性面板を貫通して、上記ターゲット電極ピンと上
記ターゲット電極膜とを接続する上記導電性物質とは異
なる組成よりなる金属製ターゲット電極ピンとを有し、
上記第2の絶縁性面板の上記ターゲット電極膜側の面が
平滑化されている撮像管ターゲット部を有することを特
徴とするX線撮像管。
1. A first insulating face plate, a second insulating face plate laminated on the first insulating face plate, and a target electrode film laminated on the second insulating face plate. A photoconductive film for converting the X-rays laminated on the target electrode film into an electric signal; a target electrode pin made of a conductive material penetrating the first insulating face plate;
Through the insulating face plate, having a target electrode pin made of metal having a composition different from that of the conductive substance connecting the target electrode pin and the target electrode film,
An X-ray image pickup tube having an image pickup tube target portion in which a surface of the second insulating face plate on the side of the target electrode film is smoothed.
【請求項2】上記第1の絶縁性面板がBN板であること
を特徴とする請求項1に記載のX線撮像管。
2. The X-ray image pickup tube according to claim 1, wherein the first insulating face plate is a BN plate.
【請求項3】上記第2の絶縁性面板がSiO2板であるこ
とを特徴とする請求項1または2に記載のX線撮像管。
3. The X-ray image pickup tube according to claim 1, wherein the second insulating face plate is a SiO 2 plate.
【請求項4】上記導電性物質が樹脂であることを特徴と
する請求項1から3までのいずれかの項に記載のX線撮
像管。
4. The X-ray image pickup tube according to claim 1, wherein the conductive substance is a resin.
【請求項5】上記光導電膜がSeを主体とする非晶質材
料から成ることを特徴とする請求項1から4までのいず
れかの項に記載のX線撮像管。
5. The X-ray image pickup tube according to any one of claims 1 to 4, wherein the photoconductive film is made of an amorphous material mainly containing Se.
【請求項6】上記光導電膜の内部で、入射X線を吸収し
て発生した電荷がアバランシェ増倍現象を起こす程の高
電界を印加することを特徴とする請求項1から5までの
いずれかの項に記載のX線撮像管。
6. A high electric field is applied to the inside of the photoconductive film such that charges generated by absorbing incident X-rays cause an avalanche multiplication phenomenon. The X-ray imaging tube according to the section.
【請求項7】貫通孔を開けた第1の絶縁性面板と、金属
製ターゲット電極ピンと一体化した第2の絶縁性面板と
を、上記金属製ターゲット電極ピンと上記貫通孔とが対
応するように接着する第1の工程と、該第1の工程後に
上記第2の絶縁性面板と上記金属製ターゲット電極ピン
とを薄く研磨加工する第2の工程と、該第2の工程後に
上記第2絶縁性面板の研磨加工面を平滑化処理する第3
の工程と、該第3の工程後に上記第2絶縁性面板の平滑
化処理面および上記金属製ターゲット電極ピンの端面の
上にターゲット電極膜を形成する第4の工程と、該ター
ゲット電極膜上にX線を電気信号に変換するための光導
電膜を形成する第5の工程とを有する製造方法により作
製した撮像管ターゲット部を用いることを特徴とするX
線撮像管の製造方法。
7. A first insulative face plate having a through hole and a second insulative face plate integrated with a metal target electrode pin are arranged such that the metal target electrode pin and the through hole correspond to each other. A first step of adhering, a second step of thinly polishing the second insulating face plate and the metal target electrode pin after the first step, and a second insulating property after the second step The third to smooth the polished surface of the face plate
And a fourth step of forming a target electrode film on the smoothed surface of the second insulating face plate and the end surface of the metal target electrode pin after the third step, and on the target electrode film. And a fifth step of forming a photoconductive film for converting an X-ray into an electric signal, and an image pickup tube target portion manufactured by a manufacturing method is used.
Method for manufacturing a line image pickup tube.
【請求項8】上記第1の工程と第2の工程との間に、上
記第1の絶縁性面板の貫通孔に導電性物質を充填する第
6の工程を行なうことを特徴とする請求項7に記載のX
線撮像管の製造方法。
8. A sixth step of filling a through hole of the first insulating face plate with a conductive substance between the first step and the second step. X described in 7
Method for manufacturing a line image pickup tube.
【請求項9】上記平滑化処理は、イオンエッチング法を
用いて行なうことを特徴とする請求項7または8に記載
のX線撮像管の製造方法。
9. The method of manufacturing an X-ray image pickup tube according to claim 7, wherein the smoothing process is performed by using an ion etching method.
JP16980695A 1995-07-05 1995-07-05 X-ray image pickup tube and manufacture thereof Pending JPH0922665A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP16980695A JPH0922665A (en) 1995-07-05 1995-07-05 X-ray image pickup tube and manufacture thereof

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP16980695A JPH0922665A (en) 1995-07-05 1995-07-05 X-ray image pickup tube and manufacture thereof

Publications (1)

Publication Number Publication Date
JPH0922665A true JPH0922665A (en) 1997-01-21

Family

ID=15893248

Family Applications (1)

Application Number Title Priority Date Filing Date
JP16980695A Pending JPH0922665A (en) 1995-07-05 1995-07-05 X-ray image pickup tube and manufacture thereof

Country Status (1)

Country Link
JP (1) JPH0922665A (en)

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