JPH07270297A - Industrial analyzer - Google Patents

Industrial analyzer

Info

Publication number
JPH07270297A
JPH07270297A JP5924994A JP5924994A JPH07270297A JP H07270297 A JPH07270297 A JP H07270297A JP 5924994 A JP5924994 A JP 5924994A JP 5924994 A JP5924994 A JP 5924994A JP H07270297 A JPH07270297 A JP H07270297A
Authority
JP
Japan
Prior art keywords
heating furnace
container
sample
analysis
lid
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
JP5924994A
Other languages
Japanese (ja)
Other versions
JP2721797B2 (en
Inventor
Yoshiro Yuasa
芳郎 湯浅
Susumu Izumitani
進 泉谷
Shoji Seike
捷二 清家
Chikafumi Ihara
爾史 井原
Toshihiko Nakagawa
敏彦 中川
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
NGK Insulators Ltd
Kansai Electric Power Co Inc
Original Assignee
NGK Insulators Ltd
Kansai Electric Power Co Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by NGK Insulators Ltd, Kansai Electric Power Co Inc filed Critical NGK Insulators Ltd
Priority to JP5924994A priority Critical patent/JP2721797B2/en
Publication of JPH07270297A publication Critical patent/JPH07270297A/en
Application granted granted Critical
Publication of JP2721797B2 publication Critical patent/JP2721797B2/en
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

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  • Investigating Or Analyzing Materials Using Thermal Means (AREA)
  • Sampling And Sample Adjustment (AREA)

Abstract

PURPOSE:To improve the accuracy of both analyses by preventing the influence of oxygen when analyzing a volatile matter and achieving a complete combustion by fully supplying oxygen when analyzing ash content in an industry analysis device for analyzing volatile matter content by a heating oven and then analyzing ash content. CONSTITUTION:A lid body-removing mechanism 40 is provided in the front part of a heating oven 13 on a transfer path of an arm 24b of a transfer mechanism 20 within a case 11. A lid body v1 for covering the upper opening of a sample storage container V1 carried from the heating oven 13 after a volatile matter is analyzed is removed from the lid body-removing mechanism 40, thus carrying in the container V1 into the heating oven 13 again.

Description

【発明の詳細な説明】Detailed Description of the Invention

【0001】[0001]

【産業上の利用分野】本発明は、石炭、コークス等鉱物
の分析用試料を容器に収容した状態で加熱炉内で所定の
加熱条件で加熱処理して同分析用試料の加熱処理後の重
量を測定し、同分析用試料の加熱処理前後の測定重量か
ら、水分、揮発分、灰分等所定の成分量を測定するため
の工業分析装置に関する。
BACKGROUND OF THE INVENTION The present invention relates to a weight of a sample for analysis of minerals such as coal and coke, which is heat-treated under a predetermined heating condition in a heating furnace in a state of being contained in a container. And an industrial analyzer for measuring the amount of a predetermined component such as water, volatile matter, and ash from the measured weights of the analytical sample before and after the heat treatment.

【0002】[0002]

【従来の技術】一般に、この種形式の工業分析装置は1
基の加熱炉を備えたもので、試料を収容した容器をセツ
トした加熱炉内を第1の加熱処理条件に設定して第1の
加熱処理を行い、次いで加熱炉内を第2の加熱処理条件
に設定して第2の加熱処理を行い、さらに加熱炉内を第
3の加熱処理条件に設定して第3の加熱処理を行うとい
う各加熱処理を順次行うようになっている。これらの一
連の加熱処理においては、第1の加熱処理終了後加熱炉
から試料収容容器を一旦取出して所定時間冷却してその
重量の測定を行い、次いで加熱炉内を第2の加熱処理条
件に設定して試料収容容器をセットして第2の加熱処理
を行い、加熱処理後上記と同様に試料収容容器を加熱炉
から取出して冷却して重量の測定を行うという作業を順
次繰り返す。これらの各加熱処理条件および冷却工程の
条件は、JIS規格(M8812−1984)に規定さ
れている。
2. Description of the Related Art Generally, this type of industrial analyzer has one
The first heating treatment is performed by setting the inside of the heating furnace in which the container containing the sample is set to the first heating treatment condition, and then performing the second heating treatment in the heating furnace. The second heat treatment is performed under the set conditions, and the third heat treatment is performed under the third heat treatment condition in the heating furnace, so that the respective heat treatments are sequentially performed. In the series of heat treatments, after the first heat treatment is completed, the sample container is once taken out from the heating furnace, cooled for a predetermined time and its weight is measured, and then the inside of the heat furnace is set to the second heat treatment condition. The operation of setting and setting the sample storage container and performing the second heat treatment, and after the heat treatment, taking out the sample storage container from the heating furnace, cooling it, and measuring the weight is repeated in the same manner as above. These heat treatment conditions and cooling process conditions are specified in JIS standard (M8812-1984).

【0003】このように、この種形式の工業分析装置に
おいては、1基の加熱炉で1個の分析用試料を1加熱処
理条件で加熱処理し、一旦冷却工程に付して重量測定を
行うという作業を各分析項目毎にそれぞれ行うことか
ら、分析項目および分析用試料の個数が多い場合には分
析作業に長時間を要する。かかる問題を解決するため、
本出願人は下記の工業分析装置を開発し、かつ当該工業
分析装置を特許出願している。当該工業分析装置の第1
の分析装置は、熱天秤を有する加熱炉を備えるととも
に、分析用試料を収容する容器を待機位置から前記加熱
炉内に搬入しかつ同加熱炉内から加熱処理後の試料収容
容器を前記待機位置に搬出する搬送機構を備え、前記加
熱炉内に搬入された試料を同加熱炉内の雰囲気を酸化状
態および非酸化状態に切り替えて互いに異なる条件で加
熱処理を行って、異なる種類の成分量を分析する工業分
析装置である。また、当該工業分析装置の第2の分析装
置は、上記した構成の工業分析装置において、前記加熱
炉を高温加熱炉に構成するとともに、同高温加熱炉の左
右の一側に所定の間隔を保持して低温加熱炉を並列した
構成のものである。
As described above, in this type of industrial analyzer, one analysis sample is heat-treated under one heat-treatment condition in one heating furnace, and once subjected to the cooling step, the weight is measured. Since such work is performed for each analysis item, a long time is required for the analysis work when the number of analysis items and the number of analysis samples is large. To solve this problem,
The applicant has developed the following industrial analyzer and applied for a patent for the industrial analyzer. First of the industrial analyzer
The analysis apparatus of, including a heating furnace having a thermobalance, the container for storing the sample for analysis is carried into the heating furnace from the standby position and the sample storage container after the heat treatment is carried out from the inside of the heating furnace to the standby position. The sample carried into the heating furnace is switched to an oxidizing state and a non-oxidizing state in the heating furnace, and heat treatment is performed under different conditions to obtain different kinds of component amounts. It is an industrial analyzer for analysis. The second analyzer of the industrial analyzer is the same as the industrial analyzer of the above-mentioned configuration, in which the heating furnace is a high-temperature heating furnace and a predetermined interval is maintained on one side of the high-temperature heating furnace. Then, the low temperature heating furnaces are arranged in parallel.

【0004】これらの工業分析装置のうち、第1の工業
分析装置においては、1基の加熱炉内の雰囲気を酸化状
態および非酸化状態に切り換えて各加熱処理を行うもの
であり、これらの加熱処理後においては試料収容容器を
加熱処理状態のまま熱天秤で重量測定するものであるこ
とから、冷却工程を廃止することかできる。このため、
従来の各加熱処理後の冷却工程に要する時間を短縮し得
て、分析作業の時間を大幅に短縮することが可能とな
る。また、上記した第2の工業分析装置においては、加
熱炉を熱天秤を有する高温加熱炉と低温加熱炉の2基の
加熱炉を並列して備えていることから、温度の異なる条
件での加熱処理を同時に行うことができて、冷却工程の
廃止ととともに分析作業の一層の時間短縮を図ることが
できる。
Of these industrial analyzers, the first industrial analyzer is one in which the atmosphere in one heating furnace is switched between an oxidized state and a non-oxidized state to carry out each heat treatment. After the treatment, the sample storage container is weighed with a thermobalance in the heat-treated state, so that the cooling step can be omitted. For this reason,
The time required for the conventional cooling process after each heat treatment can be shortened, and the time for analysis work can be shortened significantly. Further, in the above-mentioned second industrial analyzer, since the heating furnace is provided with two heating furnaces, a high-temperature heating furnace having a thermobalance and a low-temperature heating furnace, in parallel, heating under different temperature conditions is performed. Since the treatments can be performed simultaneously, the cooling process can be eliminated and the analysis work can be further shortened.

【0005】[0005]

【発明が解決しようとする課題】本発明の第1の目的
は、当該形式の工業分析装置において、1基の加熱炉内
の雰囲気を酸化状態および非酸化状態に切り換えて各加
熱処理を行う場合、非酸化状態の雰囲気での加熱処理で
は試料収容容器の上端開口部を蓋体で覆蓋することによ
り、加熱炉内に存在しまたは加熱炉の開閉時に侵入する
酸素の影響を防止し、また酸化状態の雰囲気での加熱処
理では同容器の上端開口部から蓋体を取外して開放状態
にすることにより容器内を十分に酸化状態として、これ
らの加熱処理での分析の精度を向上させることにある。
さらに、本発明の第2の目的は、当該形式の工業分析装
置において、各加熱炉に対して容器を搬入し、また搬出
する搬送機構の構造および配置を考慮することにより、
2基の加熱炉を備えた工業分析装置の小型化を図ること
にある。
A first object of the present invention is to perform each heat treatment in an industrial analyzer of this type by switching the atmosphere in one heating furnace to an oxidizing state and a non-oxidizing state. In the heat treatment in a non-oxidized atmosphere, the upper opening of the sample container is covered with a lid to prevent the influence of oxygen existing in the heating furnace or entering the opening / closing of the heating furnace. In the heat treatment in the state atmosphere, the lid is removed from the upper end opening of the container to make it open, so that the inside of the container is sufficiently oxidized and the accuracy of analysis in these heat treatments is improved. .
Further, the second object of the present invention is to consider the structure and arrangement of the transfer mechanism for loading and unloading the container to and from each heating furnace in the industrial analyzer of the type,
It is intended to reduce the size of an industrial analyzer equipped with two heating furnaces.

【0006】[0006]

【課題を解決するための手段】本発明の第1の発明は、
熱天秤を有する加熱炉を備えるとともに、分析用試料を
収容する容器を待機位置から前記加熱炉内に搬入しかつ
同加熱炉内から加熱処理後の試料収容容器を前記待機位
置に搬出する搬送機構を備え、前記加熱炉内に搬入され
た試料を同加熱炉内の雰囲気を酸化状態および非酸化状
態に切り替えて互いに異なる条件で加熱処理を行って、
異なる種類の成分量を分析する工業分析装置であり、前
記加熱炉と前記容器の待機位置間にて同容器の搬送路
に、前記容器の上端開口部を覆蓋する蓋体を同容器から
取外す蓋体取外し機構を設けたことを特徴とするもので
ある。
The first invention of the present invention is as follows:
A transport mechanism that includes a heating furnace having a thermobalance and that carries a container for storing an analysis sample into the heating furnace from a standby position and carries out a sample storage container after heat treatment from the inside of the heating furnace to the standby position. The sample carried into the heating furnace is heated under different conditions by switching the atmosphere in the heating furnace to an oxidized state and a non-oxidized state,
An industrial analyzer for analyzing the amounts of different kinds of components, a lid for covering the upper end opening of the container from the container in the conveyance path of the container between the standby position of the heating furnace and the container. It is characterized in that a body removing mechanism is provided.

【0007】また、本発明の第2の発明は、当該工業分
析装置において、前記加熱炉を高温加熱炉に構成すると
ともに、同高温加熱炉の左右の一側に所定の間隔を保持
して低温加熱炉を並列して配設し、かつ前記搬送機構に
前記両加熱炉に対して容器を搬入、搬出するアームを一
対設けて、同搬送機構を前記両加熱炉間に配設したこと
を特徴とするものである。
A second aspect of the present invention is the industrial analyzer, wherein the heating furnace is a high-temperature heating furnace, and a low temperature is maintained by keeping a predetermined interval on one side of the high-temperature heating furnace. The heating furnaces are arranged side by side, and a pair of arms for loading and unloading the container with respect to the heating furnaces are provided in the transport mechanism, and the transport mechanism is disposed between the heating furnaces. It is what

【0008】[0008]

【発明の作用・効果】このように構成した工業分析装置
のうち、第1の発明に係る工業分析装置においては蓋体
取外し機構により、加熱炉から搬出途中の容器の上端開
口部を覆蓋する蓋体を同容器から取外すことができると
ともに、上端開口部を開放した試料収容容器をさらに加
熱炉内に搬入することができる。このため、加熱炉内に
おいて非酸化状態の雰囲気で加熱処理する場合には、容
器の上端開口部を蓋体で覆蓋して加熱炉内に存在する酸
素、または加熱炉の開閉時に侵入する酸素の試料に対す
る影響を防止することができて、かかる加熱処理による
分析時の酸素の影響を防止してその精度を向上させるこ
とができる。また、酸化状態での加熱処理においては、
容器の上端開口部を覆蓋する蓋体を取外して開放状態で
加熱処理することができるため、かかる加熱処理におけ
る非酸化状態の局部的な発生を防止し得て、その分析精
度を向上させることができる。
In the industrial analyzer according to the first aspect of the present invention, the lid removing mechanism covers the upper end opening of the container being unloaded from the heating furnace. The body can be removed from the container, and the sample storage container with the upper end opening opened can be further carried into the heating furnace. Therefore, when heat treatment is performed in a non-oxidizing atmosphere in the heating furnace, oxygen existing in the heating furnace by covering the upper opening of the container with a lid or oxygen entering the opening / closing of the heating furnace It is possible to prevent the influence on the sample, prevent the influence of oxygen at the time of analysis by such heat treatment, and improve the accuracy. Further, in the heat treatment in the oxidized state,
Since the lid that covers the upper opening of the container can be removed and heat treatment can be performed in an open state, it is possible to prevent local occurrence of a non-oxidized state in such heat treatment and improve the analysis accuracy. it can.

【0009】一方、本発明の第2の発明に係る工業分析
装置においては、加熱炉として高温加熱炉と低温加熱炉
の2基の加熱炉が存在しているため、高温での加熱処理
と低温での加熱処理とを同時に行うことができ、この点
で試料の分析作業時間を一層短縮することがてきるとと
もに、両加熱炉に対して試料収容容器を搬入および搬出
する搬送機構をこれら両加熱炉間に配設しているため、
同搬送機構を分析装置の前側へ配設する場合に比較して
分析装置を小型化することができる。
On the other hand, in the industrial analyzer according to the second aspect of the present invention, since two heating furnaces, a high-temperature heating furnace and a low-temperature heating furnace, exist as heating furnaces, heat treatment at high temperature and low temperature In this respect, the sample analysis work time can be further shortened, and the transfer mechanism for loading and unloading the sample storage container to and from both heating furnaces can be used for both heating processes. Since it is placed between the furnaces,
The analyzer can be downsized as compared with the case where the transport mechanism is arranged on the front side of the analyzer.

【0010】[0010]

【実施例】以下、本発明を実施例に基づいて説明する
に、図1には本発明の一実施例に係る工業分析装置が示
されている。当該工業分析装置は、石炭の水分、揮発分
および灰分を分析するための自動式工業分析装置であ
り、ケース11の内部に熱天秤12を内蔵する高温加熱
炉13と、熱天秤14を内蔵する低温加熱炉15が配設
されているとともに、容器の搬送機構20が配設されて
おり、またケース11の外部正面には容器を収納する収
納機構30が配設されている。
DESCRIPTION OF THE PREFERRED EMBODIMENTS The present invention will be described below based on embodiments. FIG. 1 shows an industrial analyzer according to an embodiment of the present invention. The industrial analyzer is an automatic industrial analyzer for analyzing water content, volatile matter and ash content of coal, and has a high temperature heating furnace 13 having a thermobalance 12 inside a case 11 and a thermobalance 14. A low temperature heating furnace 15 is provided, a container transport mechanism 20 is provided, and a storage mechanism 30 for storing the container is provided on the outer front surface of the case 11.

【0011】高温加熱炉13は石炭の揮発分と灰分を分
析するものでカンタル線ヒータを備え、最高温度が約1
000℃まで維持できるように構成されている。揮発分
の分析では、高温加熱炉13内を窒素雰囲気として図1
および図2に示すように、試料を容器V1に収容した状
態で高温加熱炉13内に臨む熱天秤12の上皿12a上
に乗せて所定の高温で所定時間加熱処理して行い、また
これに引き続いてなされる灰分の分析では、高温加熱炉
13内を酸素雰囲気に切り替え引続き同温度で所定時間
加熱して行う。低温加熱炉15は石炭の水分を分析する
もので遠赤外線ヒータを備え、水分の分析では低温加熱
炉15内を空気雰囲気として、試料を容器V2に収容し
た状態で低温加熱炉15内に臨む熱天秤14の上皿14
a上に乗せて所定の低温で所定時間加熱処理して行う。
The high-temperature heating furnace 13 analyzes the volatile content and ash content of coal and is equipped with a Kanthal wire heater, and the maximum temperature is about 1
It is configured so that it can be maintained up to 000 ° C. In the analysis of volatile matter, the inside of the high-temperature heating furnace 13 was set to a nitrogen atmosphere, and FIG.
As shown in FIG. 2 and FIG. 2, the sample is placed in the container V1 and placed on the upper plate 12a of the thermobalance 12 facing the high temperature heating furnace 13 and heat-treated at a predetermined high temperature for a predetermined time. In the subsequent analysis of ash, the inside of the high temperature heating furnace 13 is switched to an oxygen atmosphere and subsequently heated at the same temperature for a predetermined time. The low-temperature heating furnace 15 is for analyzing the moisture content of coal and is provided with a far infrared heater. In the moisture analysis, the low-temperature heating furnace 15 is placed in an air atmosphere and the heat entering the low-temperature heating furnace 15 with the sample accommodated in the container V2. Top plate 14 of balance 14
It is placed on a and heat-treated at a predetermined low temperature for a predetermined time.

【0012】これらの加熱炉13,15は左右に所定間
隔を保持して配設されており、図1〜図3に示すよう
に、高温加熱炉13においては駆動モータ16aの駆動
により昇降部材16bを昇降させて、昇降部材16bに
連結している高温加熱炉13の周囲の炉壁13aを昇降
させ、低温加熱炉15においては高温加熱炉13の炉壁
13aの昇降に連動して開閉扉15aを昇降させるよう
に構成されている。高温加熱炉13の炉壁13aおよび
低温加熱炉15の開閉扉15aを上昇させる場合は、両
加熱炉13,15を開放させて各容器V1,V2を両加熱
炉13,15に同時に搬入させ、または両加熱炉13,
15から同時に搬出させる場合であり、また高温加熱炉
13の炉壁13aおよび低温加熱炉15の開閉扉15a
を降下させる場合は、両加熱炉13,15内で同時にま
たはいずれか一方で加熱処理を行う場合である。
These heating furnaces 13 and 15 are arranged at right and left at a predetermined interval, and as shown in FIGS. 1 to 3, in the high temperature heating furnace 13, a drive motor 16a drives the lifting member 16b. To elevate and lower the furnace wall 13a around the high temperature heating furnace 13 connected to the elevating member 16b. In the low temperature heating furnace 15, the opening / closing door 15a is interlocked with the elevating and lowering of the furnace wall 13a of the high temperature heating furnace 13. Is configured to move up and down. When raising the furnace wall 13a of the high-temperature heating furnace 13 and the opening / closing door 15a of the low-temperature heating furnace 15, both heating furnaces 13 and 15 are opened and the respective containers V1 and V2 are carried into both heating furnaces 13 and 15 at the same time. Or both heating furnaces 13,
15 at the same time, and also the furnace wall 13a of the high temperature heating furnace 13 and the opening / closing door 15a of the low temperature heating furnace 15
In the case of lowering the heat treatment, the heat treatment is performed in both the heating furnaces 13 and 15 at the same time or one of them.

【0013】搬送機構20は図1、図4および図5に示
すように、第1駆動モータ21a、第2駆動モータ21
b、回転スクリュー22a、ガイドシャフト22b、ナ
ット部材23a、昇降部材23b、連結部材24aで互
いに連結された左右一対のアーム24b,24cを備
え、回転スクリュー22aが両加熱炉13,15の間に
配設した支持台25に回転可能に支持され、かつガイド
シャフト22bが支持台25に回転スクリュー22aと
並列して支持されている。当該搬送機構20において
は、連結部材24aが昇降部材23bに固定されてお
り、昇降部材23bはナツト部材23aに昇降可能に組
付けられている。また、ナット部材23aは回転スクリ
ュー22a上に進退可能に螺合し、かつガイドシャフト
22b上に軸方向へ摺動可能に嵌合している。各アーム
24b,24cは下面側に開口する断面略コ字状のもの
で、両下端部が内側へ突出する掛止部に形成されてお
り、各熱天秤12,14の上皿12a,14aに対向し
ている。当該搬送機構20においては、第1駆動モータ
21aの駆動により回転スクリュー22aが回転してナ
ット部材23aを前後方向へ移動させ、かつ第2駆動モ
ータ21bの駆動により昇降部材23bを昇降させる。
これにより、両アーム24b,24cは前後方向および
上下方向に移動する。
As shown in FIGS. 1, 4 and 5, the transport mechanism 20 includes a first drive motor 21a and a second drive motor 21.
b, a rotating screw 22a, a guide shaft 22b, a nut member 23a, an elevating member 23b, and a pair of left and right arms 24b and 24c connected to each other by a connecting member 24a. The rotating screw 22a is disposed between the heating furnaces 13 and 15. The guide shaft 22b is rotatably supported by the provided support base 25, and is also supported by the support base 25 in parallel with the rotary screw 22a. In the transport mechanism 20, the connecting member 24a is fixed to the elevating member 23b, and the elevating member 23b is assembled to the nut member 23a so as to be able to ascend and descend. The nut member 23a is screwed onto the rotary screw 22a so as to be able to move forward and backward, and is fitted onto the guide shaft 22b so as to be slidable in the axial direction. Each of the arms 24b, 24c has a substantially U-shaped cross-section that opens to the lower surface side, and both lower ends are formed in a hooking portion projecting inward. Facing each other. In the transport mechanism 20, the rotation screw 22a is rotated by the drive of the first drive motor 21a to move the nut member 23a in the front-rear direction, and the elevating member 23b is moved up and down by the drive of the second drive motor 21b.
As a result, both arms 24b and 24c move in the front-rear direction and the up-down direction.

【0014】収納機構30は図1、図6および図7に示
すように、枠状の棚31、回転スクリュー32、駆動モ
ータ33、ナット部材34を備えている。棚31を構成
する枠部31aには、その左右の内側に多数の棚部31
b,31cが上下方向に設けられているとともに、その
上部の中央にナット部材34が固定されている。かかる
棚31においては、枠部31aの左右の両側に設けたガ
イドシャフト31dをケース11の前側の左右に設けた
ガイド部材11aに嵌合させて上下方向に摺動可能に支
持されているとともに、ナット部材34をケース11の
前側の中央に回転可能に固定した回転スクリュー32に
螺合して支持されている。各棚部31b,31cのう
ち、図示左側の棚部31bは搬送機構30のアーム24
bに対向し、かつ図示右側の棚部31cは搬送機構30
のアーム24cに対向するもので、これらの各棚部31
bには試料を収容された容器V1,V2が収納される。
As shown in FIGS. 1, 6 and 7, the storage mechanism 30 includes a frame-shaped shelf 31, a rotary screw 32, a drive motor 33, and a nut member 34. The frame portion 31a that constitutes the shelf 31 includes a large number of shelf portions 31 on the inside of the left and right sides thereof.
b and 31c are provided in the vertical direction, and a nut member 34 is fixed to the center of the upper part thereof. In the shelf 31, the guide shafts 31d provided on both the left and right sides of the frame portion 31a are fitted to the guide members 11a provided on the left and right sides of the front side of the case 11 and supported slidably in the vertical direction. A nut member 34 is screwed and supported by a rotary screw 32 that is rotatably fixed to the center of the front side of the case 11. Of the shelves 31b and 31c, the shelf 31b on the left side of the drawing is the arm 24 of the transport mechanism 30.
The shelf portion 31c on the right side in the drawing facing the b is the transport mechanism 30.
Which opposes the arm 24c of each of the shelves 31
Containers V1 and V2 containing the sample are stored in b.

【0015】当該収納機構30においては、駆動モータ
33の駆動により回転スクリュー32が回転してナット
部材34を上下方向に移動させ、ナット部材34と一体
の棚31を上下方向へ間欠的に移動させるもので、これ
により各棚部31b,31cはケース11の前面に設け
たスリット状開口部11bに間欠的に対向する。搬送機
構20の各アーム24b,24cはかかるスリット状開
口部11bを進退するもので、各棚部31bに収納され
ている各容器V1,V2を受承して前進して各加熱炉1
3,15へ搬入し、かつ各加熱炉13,15内の各容器
V1,V2を受承して後退して各棚部31b,31cへ搬
出する。
In the storage mechanism 30, the drive motor 33 drives the rotating screw 32 to rotate the nut member 34 in the vertical direction, and the rack 31 integrated with the nut member 34 is intermittently moved in the vertical direction. As a result, each of the shelves 31b and 31c intermittently faces the slit-shaped opening 11b provided on the front surface of the case 11. The arms 24b and 24c of the transfer mechanism 20 move forward and backward through the slit-shaped opening 11b. The arms 24b and 24c receive the containers V1 and V2 stored in the shelves 31b and move forward to move the heating furnace 1
Then, the container V3 is carried into the heating furnace 3,15, and the containers V1 and V2 in the heating furnaces 13 and 15 are received and retracted to be carried out to the shelves 31b and 31c.

【0016】しかして、当該工業分析装置においては、
図1および図8に示すように、ケース11内の高温加熱
炉13の前部に蓋体取外し機構40aが配設されてい
る。当該蓋体取外し機構40aは支柱41の上端部に固
定した受承板42からなるもので、支柱41は高温加熱
炉13の正面に立設されている。受承板42は四角形の
平板であり、平板部42aの中央部には高温加熱炉13
側に開口する略U字状の凹溝42bが形成されている。
受承板42は搬送機構20のアーム24b内を通過可能
な大きさに形成されていて、アーム24bの搬送路上に
位置している。
However, in the industrial analyzer,
As shown in FIG. 1 and FIG. 8, a lid removing mechanism 40 a is arranged in the front part of the high temperature heating furnace 13 in the case 11. The lid removing mechanism 40a is composed of a receiving plate 42 fixed to the upper end of the support column 41, and the support column 41 is erected in front of the high temperature heating furnace 13. The receiving plate 42 is a rectangular flat plate, and the high temperature heating furnace 13 is provided at the center of the flat plate portion 42a.
A substantially U-shaped concave groove 42b that opens to the side is formed.
The receiving plate 42 is formed in a size that can pass through the arm 24b of the transfer mechanism 20 and is located on the transfer path of the arm 24b.

【0017】なお、当該工業分析装置においては、水分
の分析には図9に示す容器V2が使用され、揮発分の分
析には図10に示す容器V1が使用され、また灰分の分
析には同図に示す容器V1と蓋体v1とが使用される。
In the industrial analyzer, the container V2 shown in FIG. 9 is used for moisture analysis, the container V1 shown in FIG. 10 is used for volatile content analysis, and the same is used for ash content analysis. The container V1 and lid v1 shown in the figure are used.

【0018】このように構成した工業分析装置において
は、高温加熱炉13において揮発分、および灰分の分析
を行い、また低温加熱炉15において水分の分析を行
う。揮発分の分析においては、高温加熱炉13内を窒素
雰囲気として、試料を収容した容器V1をその上端開口
部を蓋体v1で覆蓋した状態で搬送機構20により高温
加熱炉13内に搬入して熱天秤12の上皿12a上に乗
せ、例えば815℃で7分間加熱処理して行い、これに
引き続いて灰分の分析を行う。灰分の分析では、高温加
熱炉13内を酸素雰囲気に切り替え引続き同温度で13
分間加熱して行うが、揮発分の分析を終了した試料収容
容器V1から蓋体取外し機構40により蓋体v1を取外し
て搬送機構20により高温加熱炉13内に再度搬入して
上皿12a上にセットし、容器V1の上端開口部を開放
した状態で行う。一方、水分の分析においては、低温加
熱炉15内を空気雰囲気として、試料を容器V2に収容
した状態で搬送機構20により低温加熱炉15内に搬入
して熱天秤14の上皿14a上に乗せ、例えば75℃で
20分間加熱処理して行う。これらの各分析の終了時に
は、各熱天秤12,14にて加熱処理後の試料を容器V
1,V2毎重量測定する。
In the industrial analyzer constructed as described above, the high temperature heating furnace 13 analyzes the volatile matter and the ash, and the low temperature heating furnace 15 analyzes the water content. In the analysis of the volatile matter, the inside of the high-temperature heating furnace 13 is brought into a nitrogen atmosphere, and the container V1 containing the sample is carried into the high-temperature heating furnace 13 by the transfer mechanism 20 with its upper end opening covered with the lid v1. It is placed on the upper plate 12a of the thermobalance 12 and heat-treated at 815 ° C. for 7 minutes, for example, and subsequently, ash analysis is performed. In the ash analysis, the inside of the high-temperature heating furnace 13 was switched to an oxygen atmosphere and the temperature was kept at 13
Although heating is performed for a minute, the lid v1 is removed by the lid removing mechanism 40 from the sample container V1 after the analysis of the volatile components, and the carrying mechanism 20 again carries the lid v1 into the high temperature heating furnace 13 and places it on the upper plate 12a. The container V1 is set and the upper end opening of the container V1 is opened. On the other hand, in the analysis of water, with the inside of the low temperature heating furnace 15 as an air atmosphere, the sample is stored in the container V2 and carried into the low temperature heating furnace 15 by the transfer mechanism 20 and placed on the upper plate 14a of the thermobalance 14. For example, heat treatment is performed at 75 ° C. for 20 minutes. At the end of each of these analyses, the heat-treated sample is placed in a container V in each thermobalance 12, 14.
1. Weigh every V2.

【0019】当該工業分析装置においては、上記した各
種の分析を行うに際して、収容機構30の各棚部31
b,31cに所定の試料を一定量収容した重量測定済み
の容器V1,V2を必要な個数だけ収納し、棚31を例え
ば最上段に位置させておく。この状態においては、最上
段の各棚部31b,31cの各容器V1,V2がスリット
状開口部11bに対向し、各容器V1,V2は同開口部1
1bを通して後退して搬送機構20の各アーム24b,
24cに受承されて、各アーム24b,24cの前進に
より各加熱炉13,15内に搬入される。また、加熱処
理後においては、各アーム24b,24cが各加熱炉1
3,15内に侵入して各容器V1,V2を受承して取出
し、スリット状開口部11bを通して後退して、元の棚
部31b,31cに搬出する。その後、収納機構30の
棚31を1段づつ下降させて、上記した動作を繰り返し
行い、必要個数の試料の分析を完了する。
In the industrial analyzer, each shelf 31 of the storage mechanism 30 is used when performing the above-mentioned various analyzes.
The required number of weighed containers V1 and V2 containing a predetermined amount of a predetermined sample are stored in b and 31c, and the shelf 31 is placed at the uppermost position, for example. In this state, the containers V1 and V2 of the uppermost shelves 31b and 31c face the slit-shaped opening 11b, and the containers V1 and V2 have the same opening 1
Each arm 24b of the transport mechanism 20 is retracted through 1b,
It is received by 24c and is carried into each heating furnace 13, 15 by the advance of each arm 24b, 24c. After the heat treatment, the arms 24b and 24c are connected to the heating furnace 1
The containers V1 and V2 are received by the inside of the container 3,15, taken out, retracted through the slit-shaped opening 11b, and carried out to the original shelves 31b and 31c. Then, the shelf 31 of the storage mechanism 30 is lowered step by step, and the above-described operation is repeated to complete the analysis of the required number of samples.

【0020】しかして、当該工業分析装置においては、
揮発分の分析用の試料を収容している容器V1は上端開
口部を蓋体v1で覆蓋した状態で棚部31bに収納され
ていて、覆蓋された状態で高温加熱炉13内に搬入され
て所定の条件で加熱処理され、その後試料収容容器V1
は一旦高温加熱炉13から搬出されて蓋体取外し機構4
0aにて蓋体v1を取外され、試料収容容器V1は上端開
口部を開放された状態で再度高温加熱炉13内に搬入さ
れる。図11には、かかる蓋体v1付きの試料収容容器
V1の高温加熱炉13内からの搬出、および同容器V1か
ら蓋体v1を取外して同容器V1を再度高温加熱炉13内
へ搬入する動作を説明する模式図であり、図11(a)
は当該工業分析装置の模式的な正面図、同図(b)は同
平面図、同図(c)は高温加熱炉13と蓋体取外し機構
40間でのアーム24bの移動状態を矢線で示す側面図
である。
In the industrial analyzer, however,
The container V1 containing the sample for analysis of volatile components is stored in the shelf portion 31b with the upper end opening covered with the lid v1, and is carried into the high temperature heating furnace 13 in the covered state. Heat-treated under predetermined conditions, then sample container V1
Is once discharged from the high temperature heating furnace 13 and the lid removing mechanism 4
The lid v1 is removed at 0a, and the sample container V1 is again loaded into the high-temperature heating furnace 13 with the upper end opening opened. FIG. 11 shows the operation of carrying out the sample container V1 with the lid v1 from the inside of the high temperature heating furnace 13 and the operation of removing the lid v1 from the container V1 and carrying the vessel V1 back into the high temperature heating furnace 13. 11A is a schematic diagram for explaining FIG.
Is a schematic front view of the industrial analyzer, FIG. 8B is a plan view thereof, and FIG. 8C is a diagram showing the movement state of the arm 24b between the high temperature heating furnace 13 and the lid removing mechanism 40 by an arrow. It is a side view shown.

【0021】図11(b),(c)に示す符号イ〜ホは
アーム24bの移動位置を示しており、イ位置は高温加
熱炉13内の熱天秤12の上皿12aに対応する位置、
ロ位置は高温加熱炉13の外側の同加熱炉13と蓋体取
外し機構40の中間の位置、ハ位置は蓋体取外し機構4
0の受承板42上に対応する位置、ニ位置は待機位置、
ホ位置は容器V1の収納位置を示している。揮発分の分
析においては、アーム24bがニ位置からホ位置に後退
し、ホ位置にて上端開口部を蓋体v1で覆蓋された試料
収容容器V1を受承し、同図(c)に1点鎖線で示すよ
うに、蓋体取外し機構40の受承板42の上方を前進し
て加熱炉13内に侵入し、熱天秤12の上皿12aに降
下して蓋体付き容器V1を上皿12a上に載置し、その
後ロ位置まで水平方向に移動して上昇し、さらに水平方
向へ移動してニ位置に至り、揮発分の分析が終了するま
でニ位置にて待機する。
The symbols a to h shown in FIGS. 11B and 11C indicate the moving position of the arm 24b, and the position a corresponds to the upper plate 12a of the thermobalance 12 in the high temperature heating furnace 13,
The position b is an intermediate position between the heating furnace 13 outside the high temperature heating furnace 13 and the lid removing mechanism 40, and the position c is the lid removing mechanism 4
0 is the corresponding position on the receiving plate 42, D is the standby position,
The position E indicates the storage position of the container V1. In the analysis of the volatile matter, the arm 24b is retracted from the two position to the E position, and at the E position, the sample container V1 whose upper end opening is covered with the lid v1 is received, and in FIG. As shown by the dashed line, the lid removing mechanism 40 is advanced above the receiving plate 42 to enter the heating furnace 13, and is lowered to the upper plate 12a of the thermobalance 12 to put the container V1 with the lid on the upper plate. It is placed on 12a, then moves horizontally to the position b and rises, further moves horizontally to position d, and waits at position d until the analysis of volatile components is completed.

【0022】揮発分の分析終了後、ニ位置で待機してい
たアーム24bは蓋体取外し機構40の上方を1点鎖線
に沿って前進してロ位置に至り、実線で示すように、同
位置にて下降して水平に前進して高温加熱炉13内に侵
入し、イ位置にて熱天秤12の上皿12a上に位置して
いる蓋体v1で覆蓋されている試料収容の容器V1を受承
して上昇する。その後、水平に後退して高温加熱炉13
から外部へ移動してロ位置に至り、同位置にて中間位置
まで下降してハ位置まで水平に後退する。ハ位置におい
ては、蓋体取外し機構40aの受承板42がアーム24
b内に侵入していて、アーム24bを下降させることに
より受承されている容器V1が受承板42の凹溝42b
を下方へ通過するとともに、蓋体v1が凹溝42bの周
縁部に掛止されて容器V1から取外される。アーム24
bは、その後さらに実線に沿って水平にイ位置まで移動
して高温加熱炉13内の熱天秤12の上皿12a上に至
り、上端開口部を開放された試料収容容器V1を上皿1
2a上に載置して、2点鎖線で示すようにニ位置まで後
退して、灰分の分析が終了するまで待機する。なお、灰
分分析が終了した後の容器V1の高温加熱炉13からの
搬出は、アーム24bを2点鎖線で示すように移動させ
てなされ、収納機構30の所定の棚部31b上に載置さ
れる。
After the end of the analysis of the volatile matter, the arm 24b waiting at the second position advances above the lid removing mechanism 40 along the alternate long and short dash line to reach the low position, as shown by the solid line. At the position a, the container V1 for storing the sample covered with the lid v1 located on the upper plate 12a of the thermobalance 12 is moved downward and horizontally advanced to enter the high-temperature heating furnace 13. Accept and rise. After that, it retreats horizontally and moves to the high temperature heating furnace 13
To the outside position, descends to the intermediate position and horizontally retreats to the c position. In the C position, the receiving plate 42 of the lid removing mechanism 40a is connected to the arm 24.
The container V1 that has entered the inside of b and is received by lowering the arm 24b is the concave groove 42b of the receiving plate 42.
The lid v1 is hooked on the peripheral edge of the concave groove 42b and is removed from the container V1 while passing downward. Arm 24
After that, b is further moved horizontally along the solid line to the position a and reaches the upper plate 12a of the thermobalance 12 in the high temperature heating furnace 13, and the sample container V1 having the upper end opening is opened.
Place on 2a, retract to the two position as shown by the chain double-dashed line, and wait until the analysis of ash is completed. After the ash content analysis is completed, the container V1 is carried out of the high temperature heating furnace 13 by moving the arm 24b as shown by the chain double-dashed line and placed on the predetermined shelf 31b of the storage mechanism 30. It

【0023】このように、当該工業分析装置において
は、蓋体取外し機構40により、高温加熱炉13から搬
出された試料収容容器V1から蓋体v1を取外して、上端
開口部を開放した状態で高温加熱炉13内へ再度搬入し
て加熱処理に付することができる。このため、試料収容
容器V1の上端開口部を蓋体v1で一旦覆蓋した状態で高
温加熱炉13内で加熱処理して揮発分の分析を行うこと
ができるとともに、揮発分の分析終了後に試料収容容器
V1の上端開口部を開放した状態で高温加熱炉13内で
加熱処理して灰分の分析を行うことができる。従って、
揮発分の分析時には高温加熱炉13内に存在する酸素、
または同加熱炉13の開閉時に侵入する酸素の試料に対
する影響を防止することができて、揮発分の分析に対す
る酸素の影響を防止して分析精度を向上させることがで
きるとともに、灰分の分析時には容器V1内の試料に対
して十分に酸素を供給することができて、灰分の分析精
度を向上させることができる。
As described above, in the industrial analyzer, the lid removing mechanism 40 removes the lid v1 from the sample container V1 carried out from the high-temperature heating furnace 13 and opens it at a high temperature with the upper end opening opened. It can be carried into the heating furnace 13 again and subjected to heat treatment. Therefore, while the upper end opening of the sample storage container V1 is once covered with the lid v1, the volatile component can be analyzed by heat treatment in the high temperature heating furnace 13, and the sample storage can be performed after the volatile component analysis is completed. The ash content can be analyzed by heating in the high temperature heating furnace 13 with the upper end opening of the container V1 open. Therefore,
Oxygen present in the high-temperature heating furnace 13 during the analysis of volatile components,
Alternatively, it is possible to prevent the influence of oxygen invading when the heating furnace 13 is opened and closed on the sample, prevent the influence of oxygen on the analysis of volatile components, and improve the analysis accuracy. Oxygen can be sufficiently supplied to the sample in V1, and the ash content analysis accuracy can be improved.

【0024】また、当該工業分析装置においては、加熱
炉として高温加熱炉13と低温加熱炉15の2基の加熱
炉が存在しているため、高温での加熱処理と低温での加
熱処理とを同時に行うことができ、この点で試料の揮発
分分析、灰分析および水分分析の分析時間を一層短縮す
ることがてきるとともに、両加熱炉13,15に対して
試料収容容器V1,V2を搬入および搬出する搬送機構2
0をこれら両加熱炉13,15間に配設しているため、
搬送機構20を分析装置の前側へ配設する場合に比較し
て分析装置を小型化することができる。
Further, in the industrial analyzer, since there are two heating furnaces, the high-temperature heating furnace 13 and the low-temperature heating furnace 15, as heating furnaces, the heating processing at high temperature and the heating processing at low temperature are performed. This can be performed simultaneously, and in this respect, the analysis time for volatile content analysis, ash analysis, and moisture analysis of the sample can be further shortened, and the sample storage containers V1 and V2 can be carried into both heating furnaces 13 and 15. And a transport mechanism 2 for unloading
Since 0 is arranged between these heating furnaces 13 and 15,
The analyzer can be downsized as compared with the case where the transport mechanism 20 is arranged on the front side of the analyzer.

【0025】図12には、当該工業分析装置における蓋
体取外し機構の変形例が示されている。変形例に係る蓋
体取外し機構40bは回動アーム43と,把持手段44
と、駆動モータ45からなり、駆動モータ45は高温加
熱炉13の前部に立設した支持壁17に固定され、同駆
動モータ45の回転軸に回動アーム43の基端部が固定
されており、また回動アーム43の先端部に把持手段4
4が組付けられている。把持手段44は一対のハンド4
4a,44bを備え、これら両ハンド44a,44bは
回動アーム43の先端部に互いに対向して進退可能に組
付けられ、図示しないアクチュエータにて互いに進退す
るように構成されている。
FIG. 12 shows a modification of the lid removing mechanism in the industrial analyzer. The lid removing mechanism 40b according to the modified example includes a rotating arm 43 and a gripping means 44.
And a drive motor 45. The drive motor 45 is fixed to a support wall 17 standing upright at the front of the high-temperature heating furnace 13, and the base end of the rotating arm 43 is fixed to the rotary shaft of the drive motor 45. And the gripping means 4 at the tip of the rotating arm 43.
4 is assembled. The gripping means 44 is a pair of hands 4
4a and 44b are provided, and these hands 44a and 44b are assembled to the distal end of the rotating arm 43 so as to face each other so as to be able to move forward and backward, and to move forward and backward mutually by an actuator (not shown).

【0026】当該蓋体取外し機構40bを採用する場合
には、ケース11内に容器を受承する受承台18を搬送
機構20のアーム24bの搬送路上にて、回動アーム4
3の先端部の回動軌跡上に立設しておく。受承台18に
は、高温加熱路13から搬出された試料収容の蓋体v1
付き容器V1が受承され、この際駆動モータ45の駆動
により回動アーム43を2点鎖線で示すように下方へ略
90度回動して蓋体v1を両ハンド44a,44b間に
位置させ、両ハンド44a,44bを互いに前進させて
蓋体v1を把持する。この状態で回動アーム43を上方
へ回動させれば、容器V1の上端開口部から蓋体v1を取
外すことができる。また、当該蓋体取外し機構40bを
採用する場合、搬送機構20を構成するアームの一方を
図13に示すアーム24dのごとく構成すれば、受承台
18を省略することができる。同アーム24dは上方が
開口する受け皿状を呈しており、回動アーム43の下方
への回動時に両ハンド44a,44bがアーム24d内
に嵌合して、アーム24dに受承されている容器V1の
上端開口部を覆蓋する蓋体v1を両ハンド45a,45
b間に位置させ、両ハンド45a,45bが互いに前進
して蓋体v1を把持し、回動アーム43の上方への回動
により蓋体v1を容器V1から取外すことができる。図1
4は当該蓋体取外し機構40bを採用した工業分析装置
の模式的な平面図であり、同図(a)はケース11内に
受承台18を立設した装置、同図(b)は搬送機構20
の一方のアームとしてアーム24dを採用した装置であ
る。
When the lid removing mechanism 40b is employed, the receiving base 18 for receiving the container in the case 11 is disposed on the transport path of the arm 24b of the transport mechanism 20 and the rotating arm 4 is provided.
It is provided upright on the rotation locus of the tip portion of 3. The receiving table 18 has a lid v1 for containing the sample carried out from the high temperature heating path 13.
The attached container V1 is received, and at this time, the rotating arm 43 is rotated downward by approximately 90 degrees as shown by the chain double-dashed line by driving the drive motor 45 to position the lid body v1 between the hands 44a and 44b. , Both hands 44a and 44b are advanced to grip the lid v1. By rotating the rotating arm 43 upward in this state, the lid v1 can be removed from the upper end opening of the container V1. Further, when the lid removing mechanism 40b is adopted, the receiving base 18 can be omitted by constructing one of the arms constituting the transport mechanism 20 like the arm 24d shown in FIG. The arm 24d has a saucer shape with an upper opening, and when the rotating arm 43 is rotated downward, both hands 44a and 44b are fitted in the arm 24d and received by the arm 24d. The lid body v1 for covering the upper opening of V1 is attached to both hands 45a, 45.
Both hands 45a and 45b are moved forward to grip the lid body v1 and the lid body v1 can be removed from the container V1 by rotating the rotating arm 43 upward. Figure 1
4 is a schematic plan view of an industrial analyzer that employs the lid removing mechanism 40b. FIG. 4A is a device in which a receiving stand 18 is erected inside the case 11, and FIG. Mechanism 20
The device adopts the arm 24d as one arm.

【図面の簡単な説明】[Brief description of drawings]

【図1】本発明の一実施例に係る工業分析装置の一部切
欠き斜視図である。
FIG. 1 is a partially cutaway perspective view of an industrial analyzer according to an embodiment of the present invention.

【図2】同分析装置を構成する加熱炉および熱天秤の一
部縦断正面図である。
FIG. 2 is a partially longitudinal front view of a heating furnace and a thermobalance that constitute the analyzer.

【図3】同加熱炉の平面図である。FIG. 3 is a plan view of the heating furnace.

【図4】同分析装置を構成する搬送機構の平面図であ
る。
FIG. 4 is a plan view of a transport mechanism that constitutes the analyzer.

【図5】同搬送機構の部分正面図である。FIG. 5 is a partial front view of the transport mechanism.

【図6】同分析装置を構成する収納機構の正面図であ
る。
FIG. 6 is a front view of a storage mechanism that constitutes the analyzer.

【図7】同収納機構の平面図である。FIG. 7 is a plan view of the storage mechanism.

【図8】同分析装置を構成する蓋体取外し機構の斜視図
である。
FIG. 8 is a perspective view of a lid removing mechanism that constitutes the analyzer.

【図9】同分析装置で使用する水分分析用の容器の一部
縦断正面図(a)、および平面図(b)である。
FIG. 9 is a partial vertical front view (a) and a plan view (b) of a container for moisture analysis used in the analyzer.

【図10】同分析装置で使用する揮発分分析および灰分
分析用の容器の一部縦断正面図(a)、および揮発分分
析用の蓋体の一部縦断正面図(b)である。
FIG. 10 is a partial vertical front view of a container for volatile content analysis and ash content analysis used in the same analyzer (a) and a partial vertical front view of a lid for volatile content analysis (b).

【図11】同分析装置の模式的な正面図(a)、同平面
図(b)、および高温加熱炉と蓋体取外し機構間でのア
ームの移動状態を矢印で示す側面図(c)である。
FIG. 11 is a schematic front view (a), a plan view (b), and a side view (c) showing an arm moving state between a high temperature heating furnace and a lid removing mechanism of the analyzer by arrows. is there.

【図12】蓋体取外し機構の変形例を示す斜視図であ
る。
FIG. 12 is a perspective view showing a modified example of the lid removing mechanism.

【図13】搬送機構のアームの変形例を示す部分斜視図
である。
FIG. 13 is a partial perspective view showing a modified example of the arm of the transport mechanism.

【図14】同分析装置の一変形例に係る模式的平面図
(a)、および同他の変形例に係る模式的平面図(b)
である。
FIG. 14 is a schematic plan view according to a modification of the analyzer (a) and a schematic plan view according to another modification (b).
Is.

【符号の説明】[Explanation of symbols]

11…ケース、12,14…熱天秤、13,15…加熱
炉、18…受承台、20…搬送機構、24b,24c,
24d…アーム、30…収納機構、31…棚、31b,
31c…棚部、40a,40b…蓋体取外し機構、42
…受承板、43…回動アーム、45a,45b…ハン
ド。
11 ... Case, 12, 14 ... Thermobalance, 13, 15 ... Heating furnace, 18 ... Receiving stand, 20 ... Transfer mechanism, 24b, 24c,
24d ... Arm, 30 ... Storage mechanism, 31 ... Shelf, 31b,
31c ... Shelf, 40a, 40b ... Lid removing mechanism, 42
... Receiving plate, 43 ... Rotating arm, 45a, 45b ... Hand.

───────────────────────────────────────────────────── フロントページの続き (72)発明者 清家 捷二 愛知県名古屋市瑞穂区須田町2番56号 日 本碍子株式会社内 (72)発明者 井原 爾史 愛知県名古屋市瑞穂区須田町2番56号 日 本碍子株式会社内 (72)発明者 中川 敏彦 愛知県名古屋市瑞穂区須田町2番56号 日 本碍子株式会社内 ─────────────────────────────────────────────────── ─── Continuation of the front page (72) Inventor Seiji Koji 2-56 Sudamachi, Mizuho-ku, Nagoya, Aichi Prefecture Insulator Nihon Higashi Co., Ltd. No. 56 Nihon Insulator Co., Ltd. (72) Inventor Toshihiko Nakagawa No. 56 Sudamachi, Mizuho-ku, Aichi Prefecture Nagoya City No. 56 Nihon Insulator Co., Ltd.

Claims (2)

【特許請求の範囲】[Claims] 【請求項1】熱天秤を有する加熱炉を備えるとともに、
分析用試料を収容する容器を待機位置から前記加熱炉内
に搬入しかつ同加熱炉内から加熱処理後の試料収容容器
を前記待機位置に搬出する搬送機構を備え、前記加熱炉
内に搬入された試料を同加熱炉内の雰囲気を酸化状態お
よび非酸化状態に切り替えて互いに異なる条件で加熱処
理を行って、異なる種類の成分量を分析する工業分析装
置であり、前記加熱炉と前記容器の待機位置間にて同容
器の搬送路に、前記容器の上端開口部を覆蓋する蓋体を
同容器から取り外す蓋体取外し機構を設けたことを特徴
とする工業分析装置。
1. A heating furnace having a thermobalance is provided,
A container for storing a sample for analysis is loaded from the standby position into the heating furnace, and a transport mechanism for transporting the sample storage container after the heat treatment from the heating furnace to the standby position, and is loaded into the heating furnace. The sample is an industrial analyzer that analyzes the amounts of components of different types by performing heat treatment under different conditions by switching the atmosphere in the same heating furnace to the oxidizing state and the non-oxidizing state, and the heating furnace and the container. An industrial analyzer, characterized in that a lid removing mechanism for removing a lid covering the upper end opening of the container from the container is provided in the conveyance path of the container between the standby positions.
【請求項2】請求項1に記載の工業分析装置において、
前記加熱炉を高温加熱炉に構成するとともに、同高温加
熱炉の左右の一側に所定の間隔を保持して低温加熱炉を
並列して配設し、かつ前記搬送機構に前記両加熱炉に対
して容器を搬入、搬出するアームを一対設けて、同搬送
機構を前記両加熱炉間に配設したことを特徴とする工業
分析装置。
2. The industrial analyzer according to claim 1, wherein
The heating furnace is configured as a high-temperature heating furnace, and the low-temperature heating furnaces are arranged in parallel at one side of the same high-temperature heating furnace at a predetermined distance, and the transfer mechanism is provided in both heating furnaces. An industrial analyzer characterized in that a pair of arms for loading and unloading a container is provided, and the transport mechanism is arranged between the heating furnaces.
JP5924994A 1994-03-29 1994-03-29 Industrial analyzer Expired - Fee Related JP2721797B2 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP5924994A JP2721797B2 (en) 1994-03-29 1994-03-29 Industrial analyzer

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP5924994A JP2721797B2 (en) 1994-03-29 1994-03-29 Industrial analyzer

Publications (2)

Publication Number Publication Date
JPH07270297A true JPH07270297A (en) 1995-10-20
JP2721797B2 JP2721797B2 (en) 1998-03-04

Family

ID=13107929

Family Applications (1)

Application Number Title Priority Date Filing Date
JP5924994A Expired - Fee Related JP2721797B2 (en) 1994-03-29 1994-03-29 Industrial analyzer

Country Status (1)

Country Link
JP (1) JP2721797B2 (en)

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP1500918A1 (en) * 2003-07-25 2005-01-26 Waters Investments Limited Thermogravimetrical analyzer with a sample pan unsealing system
JP2008201632A (en) * 2007-02-21 2008-09-04 Mitsubishi Materials Corp Pretreatment method for measuring of combustibility, estimation method of fuel, and method for producing cement
CN106840956A (en) * 2017-03-31 2017-06-13 周学成 Cold and hot two-chamber evaporation residue analyzer
CN107345949A (en) * 2017-09-13 2017-11-14 长沙开元仪器股份有限公司 A kind of industrial analysis instrument of follow-on test
CN108956364A (en) * 2018-06-11 2018-12-07 鹰牌陶瓷实业(河源)有限公司 A kind of detection method of the calorific value characteristic of raw material fire coal

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP1500918A1 (en) * 2003-07-25 2005-01-26 Waters Investments Limited Thermogravimetrical analyzer with a sample pan unsealing system
JP2008201632A (en) * 2007-02-21 2008-09-04 Mitsubishi Materials Corp Pretreatment method for measuring of combustibility, estimation method of fuel, and method for producing cement
CN106840956A (en) * 2017-03-31 2017-06-13 周学成 Cold and hot two-chamber evaporation residue analyzer
CN106840956B (en) * 2017-03-31 2023-07-21 周学成 Cold and hot double-cavity evaporation residue tester
CN107345949A (en) * 2017-09-13 2017-11-14 长沙开元仪器股份有限公司 A kind of industrial analysis instrument of follow-on test
CN108956364A (en) * 2018-06-11 2018-12-07 鹰牌陶瓷实业(河源)有限公司 A kind of detection method of the calorific value characteristic of raw material fire coal

Also Published As

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