JPH0570949A - Evaporation rate detector of arc ion plating device - Google Patents

Evaporation rate detector of arc ion plating device

Info

Publication number
JPH0570949A
JPH0570949A JP23641691A JP23641691A JPH0570949A JP H0570949 A JPH0570949 A JP H0570949A JP 23641691 A JP23641691 A JP 23641691A JP 23641691 A JP23641691 A JP 23641691A JP H0570949 A JPH0570949 A JP H0570949A
Authority
JP
Japan
Prior art keywords
cathode
target
ion plating
electrode
detection electrode
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
JP23641691A
Other languages
Japanese (ja)
Inventor
Kunihiko Tsuji
邦彦 辻
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Kobe Steel Ltd
Original Assignee
Kobe Steel Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Kobe Steel Ltd filed Critical Kobe Steel Ltd
Priority to JP23641691A priority Critical patent/JPH0570949A/en
Publication of JPH0570949A publication Critical patent/JPH0570949A/en
Pending legal-status Critical Current

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  • Measuring Volume Flow (AREA)
  • Physical Vapour Deposition (AREA)

Abstract

PURPOSE:To easily and surely detect a change in the evaporation rate of a target material by connecting a detecting electrode to a DC power source in such a manner that the electrode has a more negative potential than cathode and detecting the current flowing in the detecting electrode by an electrode detector. CONSTITUTION:The target 14 is mounted on the cathode 12. Arc ion plating is executed by generating an arc discharge between an anode 11 and the target 14 within a vacuum vessel 10 and forming the film of the target on the surfaces of objects 16 for vapor deposition. The detecting electrode 18 is, thereupon, provided in front of the cathode 12. The detecting electrode 18 is so connected to the DC electrode 19 as to attain the more negative potential than the cathode 12. The current flowing in the detecting electrode 18 is detected by a current detector 20. The operating conditions of the arc ion plating device are corrected in this way.

Description

【発明の詳細な説明】Detailed Description of the Invention

【0001】[0001]

【産業上の利用分野】本発明は、アークイオンプレーテ
ィング装置における蒸発量検出装置に関するものであ
る。
BACKGROUND OF THE INVENTION 1. Field of the Invention The present invention relates to an evaporation amount detecting device in an arc ion plating device.

【0002】[0002]

【従来の技術】図2は従来のアークイオンプレーティン
グ装置の概要を示す。図2において、1 は金属製の真空
容器で、この真空容器1 の壁面に一対の陽極2 と陰極3
とが取付けられている。なお、真空容器の壁面を陽極と
して使用することも可能である。そして、陽極2 はアー
ク電源4 の+側に、陰極3 はその−側に夫々電気的に接
続されている。また陰極3 には、一般に金属等からなる
蒸発材料、即ちターゲット5 が取付けられている。
2. Description of the Related Art FIG. 2 shows an outline of a conventional arc ion plating apparatus. In FIG. 2, reference numeral 1 is a metal vacuum container, and a pair of an anode 2 and a cathode 3 are provided on the wall surface of the vacuum container 1.
And are installed. It is also possible to use the wall surface of the vacuum container as the anode. The anode 2 is electrically connected to the + side of the arc power source 4, and the cathode 3 is electrically connected to the-side thereof. Further, the cathode 3 is attached with an evaporation material generally made of metal or the like, that is, a target 5.

【0003】真空容器1 の底面には回転台6 が回転自在
に設けられ、この回転台6 は真空容器1 に対して所定の
負電位となるようにバイアス電源7 に接続されている。
このアークイオンプレーティング装置において、今、回
転台6 上に被蒸着物8を置き、図外の真空装置により真
空容器1 内を所定の真空度まで排気した後、陽極2 と陰
極3 に装着したターゲット5 の間でアーク放電を発生さ
せる。するとターゲット5 の材料が蒸発・イオン化し、
被蒸着物8 の表面にターゲット材料の皮膜が形成され
る。この時、金属容器1 内に所定量の反応ガス (窒素ガ
ス、炭化水素ガス、酸素等) を導入することにより、金
属窒化物、炭化物、酸化物の皮膜が形成できる。
A rotary table 6 is rotatably provided on the bottom surface of the vacuum container 1, and the rotary table 6 is connected to a bias power source 7 so as to have a predetermined negative potential with respect to the vacuum container 1.
In this arc ion plating device, the deposition object 8 is now placed on the rotary table 6, the inside of the vacuum container 1 is evacuated to a predetermined vacuum degree by a vacuum device (not shown), and then attached to the anode 2 and the cathode 3. An arc discharge is generated between the targets 5. Then, the target 5 material evaporates and ionizes,
A film of the target material is formed on the surface of the object to be vapor-deposited 8. At this time, by introducing a predetermined amount of reaction gas (nitrogen gas, hydrocarbon gas, oxygen, etc.) into the metal container 1, a metal nitride, carbide, or oxide film can be formed.

【0004】[0004]

【発明が解決しようとする課題】この種の装置では、一
般的にはアーク電流とターゲット材料の蒸発量は比例関
係にある。しかし、ターゲット5 の消耗によりターゲッ
ト厚さが減じると、同一のアーク電流に対して蒸発量が
低下し、同じ運転条件で運転すれば、被蒸着物8に形成
される皮膜の厚さが減少し、操業管理上、問題がある。
In this type of device, the arc current and the evaporation amount of the target material are generally in a proportional relationship. However, when the target thickness decreases due to the consumption of the target 5, the evaporation amount decreases for the same arc current, and if operating under the same operating conditions, the thickness of the film formed on the deposition object 8 decreases. There is a problem in operation management.

【0005】そこで、従来は定期的にテストピースを入
れ、そのテストピースに形成される皮膜の厚さを実測し
て対処しているが、これは作業が非常に煩雑であり、ま
た操業率の低下を招くという問題がある。本発明は、か
かる従来の課題に鑑み、ターゲット材料のイオン電流を
計測して蒸発量の変化を容易かつ確実に検出できるよう
にすることを目的とする。
Therefore, conventionally, a test piece is put in periodically and the thickness of the film formed on the test piece is actually measured to deal with it. However, this is very complicated and the operation rate There is a problem of causing a decrease. In view of the above conventional problems, it is an object of the present invention to measure the ion current of a target material and to easily and surely detect a change in the evaporation amount.

【0006】[0006]

【課題を解決するための手段】本発明は、陰極12にター
ゲット14を装着し、真空容器10内で陽極11とターゲット
14間でアーク放電を発生させて、被蒸着物16の表面にタ
ーゲット材料の皮膜を形成するようにしたアークイオン
プレーティング装置において、陰極12の前方に検出電極
18を設けると共に、この検出電極18を陰極12よりも負電
位となるように直流電源19に接続し、この検出電極18に
流れる電流を検出する電流検出器20を設けたものであ
る。
According to the present invention, a target 12 is attached to a cathode 12, and an anode 11 and a target are placed in a vacuum container 10.
In an arc ion plating device in which an arc discharge is generated between 14 to form a film of the target material on the surface of the deposition object 16, a detection electrode is provided in front of the cathode 12.
18 is provided, the detection electrode 18 is connected to a DC power source 19 so as to have a negative potential than the cathode 12, and a current detector 20 for detecting a current flowing through the detection electrode 18 is provided.

【0007】[0007]

【作用】陰極12前方の検出電極18が陰極12に対して負電
位となっているので、検出電極18にターゲット材料から
のイオン電流が流れる。このターゲット材料のイオン化
の割合は金属材料によって一定の値を持っているので、
イオン電流を電流検出器20で検出することにより蒸発量
を知ることができる。
Since the detection electrode 18 in front of the cathode 12 has a negative potential with respect to the cathode 12, an ionic current from the target material flows through the detection electrode 18. Since the ionization rate of this target material has a certain value depending on the metal material,
The amount of evaporation can be known by detecting the ion current with the current detector 20.

【0008】[0008]

【実施例】以下、本発明の実施例を図面に基づいて詳述
する。図1において、10は金属製の真空容器で、壁面に
は一対の陽極11と陰極12が取付けられている。陽極11は
アーク電源13の+側に、陰極12はその−側に夫々接続さ
れ、また陰極12にはターゲット14が取付けられている。
Embodiments of the present invention will now be described in detail with reference to the drawings. In FIG. 1, 10 is a vacuum container made of metal, and a pair of anode 11 and cathode 12 are attached to the wall surface. The anode 11 is connected to the + side of the arc power source 13, the cathode 12 is connected to the-side thereof, and the cathode 12 is attached with the target 14.

【0009】15は回転台で、真空容器10内の底面側に回
転自在に設けられており、この回転台15上に被蒸着物16
が載置されている。17はバイアス電源で、回転台15を真
空容器10に対して負電位に保っている。18は検出電極で
あって、陰極12の前方でかつ被蒸着物16の邪魔にならな
い位置に固定されている。検出電極18は真空容器10との
間に介装された直流電源19の−側に接続され、20〜50V
程度の陰極12よりも十分に負電位の電圧が印加されてい
る。20は検出電極18に流れる電流を検出する電流検出器
で、検出電極18と直流電極19との間に介装されている。
Reference numeral 15 denotes a turntable, which is rotatably provided on the bottom surface side in the vacuum container 10.
Is placed. Reference numeral 17 denotes a bias power source, which keeps the rotary table 15 at a negative potential with respect to the vacuum container 10. Reference numeral 18 denotes a detection electrode, which is fixed in front of the cathode 12 and at a position where it does not interfere with the material 16 to be deposited. The detection electrode 18 is connected to the negative side of a DC power source 19 that is interposed between the detection electrode 18 and the vacuum container 10 and has a voltage of 20 to 50 V
A voltage of a negative potential is applied sufficiently more than the cathode 12 of a certain degree. A current detector 20 detects the current flowing through the detection electrode 18, and is interposed between the detection electrode 18 and the DC electrode 19.

【0010】このように独立した専用の検出電極18を設
け、これに電流検出器20を接続しておけば、ターゲット
14の蒸発量を正確に知ることができる。即ち、アーク蒸
発現象ではターゲット材料が高度にイオン化されてい
る。このイオン化の割合は金属材料によって一定の値を
持っており、イオン電流を計測することによって蒸発量
を知ることができる。従って、バイアス電源17に流れる
電流の傾向として現われるが、被蒸着物16の量、形状、
真空圧力により大きく影響され、正確に蒸発量の変化を
把えることは難しい。
As described above, by providing the independent dedicated detection electrode 18 and connecting the current detector 20 thereto, the target
The evaporation amount of 14 can be known accurately. That is, in the arc evaporation phenomenon, the target material is highly ionized. This ionization rate has a constant value depending on the metal material, and the evaporation amount can be known by measuring the ion current. Therefore, although appearing as a tendency of the current flowing in the bias power source 17, the amount, shape, and
It is greatly affected by the vacuum pressure, and it is difficult to accurately grasp the change in the evaporation amount.

【0011】しかし、検出電極18を設けておけば、陰極
12に対して十分負電位であるため、この検出電極18への
電子の流入を防ぎつつイオン電流が流れるので、その電
流を検出することによって、計測時の真空圧力、アーク
電流を一定にしておく限り、被蒸着物16の影響を受けず
に、正確にターゲット14の蒸発量の変化を知ることがで
きる。即ち、電流検出器20にはターゲット材料の蒸発量
に比例した信号が得られる。従って、この電流検出器20
の信号を制御用として利用して、運転条件を補正するこ
とが可能である。
However, if the detection electrode 18 is provided, the cathode
Since the potential is sufficiently negative with respect to 12, an ionic current flows while preventing the inflow of electrons to the detection electrode 18, so that the vacuum pressure and arc current during measurement are kept constant by detecting the current. As long as it is, the change in the evaporation amount of the target 14 can be accurately known without being affected by the deposition object 16. That is, the current detector 20 can obtain a signal proportional to the evaporation amount of the target material. Therefore, this current detector 20
It is possible to correct the operating conditions by using the signal of 1 for control.

【0012】この時の補正法としては、具体的にはアー
ク電流を補正することが最も望ましい。例えば、ターゲ
ットの厚さの減少によりイオン電流が10%減っていれ
ば、アーク電流を10%増加させることにより、当初のイ
オン電流、即ち、当初の蒸発量を得ることができ、当初
設定した条件を再現させることが可能となる。なお、こ
の補正動作は、真空度が十分に高い状態 (1×10-4Torr
以下程度) で行えば正確であり、通常、コーティングサ
イクルの最初に行えば良いが、コーティング中に時々真
空度を上げて入っても良い。
As the correction method at this time, specifically, it is most desirable to correct the arc current. For example, if the ion current is reduced by 10% due to the reduction of the target thickness, the initial ion current, that is, the initial evaporation amount can be obtained by increasing the arc current by 10%. Can be reproduced. Note that this correction operation is performed when the degree of vacuum is sufficiently high (1 × 10 -4 Torr
It is more accurate if it is performed (about the following), and usually, it may be performed at the beginning of the coating cycle, but the vacuum degree may be occasionally increased during coating.

【0013】[0013]

【発明の効果】本発明によれば、陰極12にターゲット14
を装着し、真空容器10内で陽極11とターゲット14間でア
ーク放電を発生させて、被蒸着物16の表面にターゲット
材料の皮膜を形成するようにしたアークイオンプレーテ
ィング装置において、陰極12の前方に検出電極18を設け
ると共に、この検出電極18を陰極12よりも負電位となる
ように直流電源19に接続し、この検出電極18に流れる電
流を検出する電流検出器20を設けているので、ターゲッ
ト材料のイオン電流を計測して蒸発量の変化を容易かつ
確実に検出できる。
According to the present invention, the cathode 12 and the target 14 are
Mounted, by generating an arc discharge between the anode 11 and the target 14 in the vacuum container 10, in the arc ion plating apparatus to form a film of the target material on the surface of the deposition object 16, the cathode 12 of Since the detection electrode 18 is provided on the front side, the detection electrode 18 is connected to the DC power source 19 so as to have a negative potential than the cathode 12, and the current detector 20 for detecting the current flowing through the detection electrode 18 is provided. By measuring the ion current of the target material, the change in the evaporation amount can be detected easily and reliably.

【図面の簡単な説明】[Brief description of drawings]

【図1】本発明の一実施例を示す構成図である。FIG. 1 is a configuration diagram showing an embodiment of the present invention.

【図2】従来例を示す構成図である。FIG. 2 is a configuration diagram showing a conventional example.

【符号の説明】[Explanation of symbols]

10 真空容器 11 陽極 12 陰極 14 ターゲット 16 被蒸着物 18 検出電極 19 直流電源 20 電流検出器 10 Vacuum container 11 Anode 12 Cathode 14 Target 16 Deposition object 18 Detection electrode 19 DC power supply 20 Current detector

Claims (1)

【特許請求の範囲】[Claims] 【請求項1】 陰極(12)にターゲット(14)を装着し、真
空容器(10)内で陽極(11)とターゲット(14)間でアーク放
電を発生させて、被蒸着物(16)の表面にターゲット材料
の皮膜を形成するようにしたアークイオンプレーティン
グ装置において、陰極(12)の前方に検出電極(18)を設け
ると共に、この検出電極(18)を陰極(12)よりも負電位と
なるように直流電源(19)に接続し、この検出電極(18)に
流れる電流を検出する電流検出器(20)を設けたことを特
徴とするアークイオンプレーティング装置における蒸発
量検出装置。
1. A target (14) is attached to a cathode (12), an arc discharge is generated between an anode (11) and a target (14) in a vacuum container (10), and a target material (16) is deposited. In an arc ion plating device that forms a film of target material on the surface, a detection electrode (18) is provided in front of the cathode (12), and this detection electrode (18) is at a negative potential than the cathode (12). A vaporization amount detection device in an arc ion plating device, characterized in that a current detector (20) for detecting a current flowing through the detection electrode (18) is provided by being connected to a DC power source (19).
JP23641691A 1991-09-17 1991-09-17 Evaporation rate detector of arc ion plating device Pending JPH0570949A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP23641691A JPH0570949A (en) 1991-09-17 1991-09-17 Evaporation rate detector of arc ion plating device

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP23641691A JPH0570949A (en) 1991-09-17 1991-09-17 Evaporation rate detector of arc ion plating device

Publications (1)

Publication Number Publication Date
JPH0570949A true JPH0570949A (en) 1993-03-23

Family

ID=17000434

Family Applications (1)

Application Number Title Priority Date Filing Date
JP23641691A Pending JPH0570949A (en) 1991-09-17 1991-09-17 Evaporation rate detector of arc ion plating device

Country Status (1)

Country Link
JP (1) JPH0570949A (en)

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO1999022397A1 (en) * 1997-10-24 1999-05-06 Filplas Vacuum Technology Pte Ltd. Arc monitoring
CN104498884A (en) * 2014-12-04 2015-04-08 南京工业大学 Method and device for detecting ionization rate of coating material particles
CN110042349A (en) * 2019-04-28 2019-07-23 吉林大学 A kind of multi-arc ion coating cathode assembly

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO1999022397A1 (en) * 1997-10-24 1999-05-06 Filplas Vacuum Technology Pte Ltd. Arc monitoring
CN104498884A (en) * 2014-12-04 2015-04-08 南京工业大学 Method and device for detecting ionization rate of coating material particles
CN110042349A (en) * 2019-04-28 2019-07-23 吉林大学 A kind of multi-arc ion coating cathode assembly

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