JPH0552787A - Device for measuring dissolved gas within oil - Google Patents

Device for measuring dissolved gas within oil

Info

Publication number
JPH0552787A
JPH0552787A JP29672491A JP29672491A JPH0552787A JP H0552787 A JPH0552787 A JP H0552787A JP 29672491 A JP29672491 A JP 29672491A JP 29672491 A JP29672491 A JP 29672491A JP H0552787 A JPH0552787 A JP H0552787A
Authority
JP
Japan
Prior art keywords
oil
gas
sensor
concentration
air
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
JP29672491A
Other languages
Japanese (ja)
Other versions
JP2748751B2 (en
Inventor
Yoshihisa Tanaka
義久 田中
Masaru Kanba
勝 神庭
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Nissin Electric Co Ltd
Original Assignee
Nissin Electric Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Nissin Electric Co Ltd filed Critical Nissin Electric Co Ltd
Priority to JP3296724A priority Critical patent/JP2748751B2/en
Publication of JPH0552787A publication Critical patent/JPH0552787A/en
Application granted granted Critical
Publication of JP2748751B2 publication Critical patent/JP2748751B2/en
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

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  • Testing Electric Properties And Detecting Electric Faults (AREA)
  • Sampling And Sample Adjustment (AREA)
  • Investigating Or Analysing Materials By Optical Means (AREA)
  • Investigating Or Analyzing Materials By The Use Of Electric Means (AREA)

Abstract

PURPOSE:To enable a local overheating and an abnormality due to a discharge phenomenon to be detected simultaneously and a diagnosis performance of an oil electrical equipment to be improved by installing a hydrogen gas sensor and an acetylene gas sensor and by measuring a concentration of hydrogen gas and that of acetylene gas simultaneously in a circulation bubbling process. CONSTITUTION:A sample oil 2 is taken into a gas extraction container 1, an air pump 5 is driven for allowing air to be fed to a circulation system containing the container 1, and then the sample oil 2 is subjected to bubbling, thus enabling an air bubble to be generated from an air bubble generation portion 3, hydrogen gas and acetylene gas within the sample oil 2 to be discharged into air within the container 1, and this procedure to be continued for a specified amount of time for bringing a concentration of an air liquid closer to a balanced value. This balanced value is measured by a hydrogen gas sensor 7 and an acetylene gas sensor 8, is converted to a gas concentration within oil, and is displayed at indicators 11 and 12. When the measurement is completed, a solenoid valve 4 is released and the air pump 5 is driven and then an extracted gas within oil is discharged, thus enabling an inside of the system to be cleaned and an indication value of each sensor to be returned to an initial value.

Description

【発明の詳細な説明】Detailed Description of the Invention

【0001】[0001]

【産業上の利用分野】本発明は油中溶存ガス測定装置に
関する。
BACKGROUND OF THE INVENTION 1. Field of the Invention The present invention relates to an apparatus for measuring dissolved gas in oil.

【0002】[0002]

【従来の技術】従来油入電気機器の異常を検出する手段
として、その電気機器内から採取した絶縁油を試料油と
して、これに空気を導入して循環バブリングを行い、こ
れからその試料油中に溶存している水素ガスの濃度を水
素ガス測定器によって検出し、その検出濃度から油入電
気機器の異常を検出することが行われている。
2. Description of the Related Art Conventionally, as means for detecting an abnormality in an oil-filled electric device, insulating oil taken from the electric device is used as a sample oil, air is introduced into the sample oil to perform circulation bubbling, and then the sample oil is introduced into the oil. The concentration of dissolved hydrogen gas is detected by a hydrogen gas measuring instrument, and the abnormality of oil-filled electrical equipment is detected from the detected concentration.

【0003】ところで、油入電気機器の異常発生とし
て、経験的に局部過熱と、放電現象が挙げられる。局部
過熱が発生すると、絶縁油、絶縁紙が熱分解し、水素ガ
スの他にCH4,C2H4,CO,CO2が発生する。
また放電の発生時には、主として水素ガスの他にアセチ
レンガスが発生する。したがって水素ガス測定器によれ
ば、過熱、放電現象の発生を検出することができるが、
微小放電の発生によって生ずる水素ガスの濃度は低いた
め、これによる異常の判別は困難であった。
By the way, as an abnormal occurrence of the oil-filled electrical equipment, empirically, local overheating and discharge phenomenon can be mentioned. When local overheating occurs, insulating oil and insulating paper are thermally decomposed, and CH4, C2H4, CO, and CO2 are generated in addition to hydrogen gas.
When electric discharge occurs, acetylene gas is mainly generated in addition to hydrogen gas. Therefore, the hydrogen gas measuring device can detect the occurrence of overheating and discharge phenomenon.
Since the concentration of hydrogen gas generated by the occurrence of minute discharges is low, it is difficult to determine the abnormality due to this.

【0004】[0004]

【発明が解決しようとする課題】本発明は、局部過熱と
放電現象による異常を、採取した試料油から同時に測定
可能とし、もって油入電気機器の診断性能の向上を図る
ことを目的とする。
SUMMARY OF THE INVENTION It is an object of the present invention to make it possible to simultaneously measure anomalies due to local overheating and discharge phenomena from sampled oil samples, thereby improving the diagnostic performance of oil-filled electrical equipment.

【0005】[0005]

【課題を解決するための手段】本発明は、循環バブリン
グによる油中溶存ガス手段を用いた油中溶存ガス測定装
置において、バブリングの循環経路中に、水素ガスセン
サーと、アセチレンガスセンサーの両方を設置し、前記
両センサーによって前記循環バプリングの過程で水素ガ
スの濃度と、アセチレンガスの濃度の両方を同時に検出
するようにしたことを特徴とする。
Means for Solving the Problems The present invention is an apparatus for measuring dissolved gas in oil using means for dissolved gas in oil by circulating bubbling, wherein both a hydrogen gas sensor and an acetylene gas sensor are provided in the bubbling circulation path. It is characterized in that both sensors are installed and the concentration of hydrogen gas and the concentration of acetylene gas are simultaneously detected by the both sensors during the circulation bubbling.

【0006】[0006]

【実施例】本発明の実施例を図によって説明する。図1
において、1は油入電気機器から採取した絶縁油を試料
油2として入れるガス抽出容器、3は気泡発生部、4は
吸排気用の電磁弁、5はエアーポンプ、6はセンサーチ
ャンバー、7は水素ガスセンサー、8はアセチレンガス
センサー、9、10は増幅器、11、12は指示計であ
る。各センサーからの出力は、それぞれの増幅器9,1
0により増幅され、それぞれの指示計11,12に濃度
が指示されるようになっている。
Embodiments of the present invention will be described with reference to the drawings. Figure 1
In the figure, 1 is a gas extraction container for containing insulating oil sampled from oil-filled electrical equipment as sample oil 2, 3 is a bubble generating part, 4 is a solenoid valve for intake and exhaust, 5 is an air pump, 6 is a sensor chamber, 7 is A hydrogen gas sensor, 8 is an acetylene gas sensor, 9 and 10 are amplifiers, and 11 and 12 are indicators. The output from each sensor is the respective amplifier 9, 1
It is amplified by 0, and the concentration is instructed to the respective indicators 11, 12.

【0007】図2にセンサーチャンバー6の詳細例を示
す。水素センサチャンバー61には水素ガスセンサー7
が設置されている。ここでは水素ガスセンサー7として
半導体センサー、例えばSnO2系の半導体センサーを
用いている。
FIG. 2 shows a detailed example of the sensor chamber 6. The hydrogen gas sensor 7 is installed in the hydrogen sensor chamber 61.
Is installed. Here, a semiconductor sensor, for example, a SnO 2 based semiconductor sensor is used as the hydrogen gas sensor 7.

【0008】アセチレンセンサーとして、非分散型(波
長13.7μm)赤外線検知装置13を用いている。赤
外線放射源14として、セラミックヒーター(500°
K)を、分光フィルタ15として、ZnSe系のフィル
タで、13.7μm±0.1μmの分光特性で、透過率
60%のものを、受光素子16として焦電型赤外線セン
サーを、またチョッパー17として、チョッパー周波数
が1Hzのものを、それぞれ用いた。18は測定対象の
ガスが導入されるガスセルである。
As the acetylene sensor, a non-dispersion type (wavelength 13.7 μm) infrared detector 13 is used. As the infrared radiation source 14, a ceramic heater (500 °
K) as a spectral filter 15, a ZnSe type filter having a spectral characteristic of 13.7 μm ± 0.1 μm and a transmittance of 60%, a pyroelectric infrared sensor as the light receiving element 16, and a chopper 17. , And those having a chopper frequency of 1 Hz were used. Reference numeral 18 is a gas cell into which the gas to be measured is introduced.

【0009】最初に試料油2をガス抽出容器1内に入
れ、エアーポンプ5を駆動してガス抽出容器1を含む循
環系に空気を送り込み、試料油2をバブリングする。こ
れによって気泡発生部3から気泡が発生し、試料油2中
の水素ガス、アセチレンガスがガス抽出容器1内の空気
中に放出される。これを所定時間にわたって継続するこ
とにより、気液の濃度が平衡値に達する。
First, the sample oil 2 is put into the gas extraction container 1, the air pump 5 is driven, and air is sent into the circulation system including the gas extraction container 1 to bubble the sample oil 2. As a result, bubbles are generated from the bubble generator 3, and hydrogen gas and acetylene gas in the sample oil 2 are released into the air in the gas extraction container 1. By continuing this for a predetermined time, the concentration of gas-liquid reaches an equilibrium value.

【0010】その平衡値は、各センサー7,8によって
検出され、油中ガス濃度に換算されて、各指示計11,
12に表示される。この測定が完了したら、電磁弁4の
吸気口、排気口を開放してから、エアーポンプ5を駆動
して、抽出された油中ガスを系外に排出する。これによ
って系内が清浄され、各センサーの指示値が初期値に戻
る。このあと次の試料油の測定に移る。
The equilibrium value is detected by each of the sensors 7 and 8 and converted into the gas concentration in oil to obtain each indicator 11,
12 is displayed. When this measurement is completed, the intake port and the exhaust port of the solenoid valve 4 are opened, and then the air pump 5 is driven to discharge the extracted gas in oil to the outside of the system. As a result, the inside of the system is cleaned and the indicated value of each sensor returns to the initial value. After this, the measurement of the next sample oil is started.

【0011】図3に本発明の他の実施例を示す。ここで
はガスセル18の一部に水素ガスセンサー7を設置した
構成であり、これによって両センサーチャンバーを一体
とする。このような構成によれば、全体構成を小型化す
ることができて都合がよい。
FIG. 3 shows another embodiment of the present invention. Here, the hydrogen gas sensor 7 is installed in a part of the gas cell 18, so that both sensor chambers are integrated. With such a configuration, the entire configuration can be downsized, which is convenient.

【0012】次に本発明者が行った実験について説明す
る。試料油量を90ml、系内全体積を180ml、エ
アーポンプによる流量を11/分、気泡発生部の直径2
mmとし、前記した各センサーを用いて測定を行ったと
ころ、約2分で気液の濃度が平衡値に達した。この構成
による濃度測定範囲は、水素ガスで10〜2000pp
m、アセチレンガスで2〜100ppmであった。
Next, the experiment conducted by the present inventor will be described. 90 ml sample oil, 180 ml total volume in the system, 11 / min flow rate by air pump, diameter of bubble generating part 2
When the measurement was performed using each sensor described above, the concentration of gas-liquid reached the equilibrium value in about 2 minutes. With this configuration, the concentration measurement range is 10 to 2000 pp with hydrogen gas.
m and acetylene gas were 2 to 100 ppm.

【0013】[0013]

【発明の効果】以上詳述したように本発明によれば、油
中溶存ガスの濃度測定にあたり、水素ガス濃度と、アセ
チレンガス濃度の両方を計測するセンサーを設置するよ
うにしたので、1回の測定操作で、同時に水素ガスと、
アセチレンガスの濃度を計測することができるようにな
り、したがって電気機器の局部過熱、放電現象の両方を
同時に診断することができるようになるといった効果を
奏する。
As described above in detail, according to the present invention, when measuring the concentration of dissolved gas in oil, a sensor for measuring both the hydrogen gas concentration and the acetylene gas concentration is installed. With the measurement operation of, at the same time with hydrogen gas,
As a result, it becomes possible to measure the concentration of acetylene gas, and therefore it is possible to simultaneously diagnose both local overheating and electric discharge phenomenon of electric equipment.

【図面の簡単な説明】[Brief description of drawings]

【図1】本発明の実施例を示す配置図である。FIG. 1 is a layout view showing an embodiment of the present invention.

【図2】図1の部分詳細配置図である。FIG. 2 is a partial detailed layout diagram of FIG.

【図3】図2の変形例を示す配置図である。FIG. 3 is an arrangement diagram showing a modification example of FIG.

【符号の説明】[Explanation of symbols]

1 ガス抽出容器 2 試料油 3 気泡発生部 5 エアーポンプ 6 センサーチャンバー 7 水素ガスセンサー 8 アセチレンガスセンサー 1 Gas extraction container 2 Sample oil 3 Air bubble generation part 5 Air pump 6 Sensor chamber 7 Hydrogen gas sensor 8 Acetylene gas sensor

Claims (1)

【特許請求の範囲】[Claims] 【請求項1】 循環バブリングによる油中溶存ガス手段
を用いた油中溶存ガス測定装置において、バブリングの
循環経路中に、水素ガスセンサーと、アセチレンガスセ
ンサーの両方を設置し、前記両センサーによって前記循
環バブリングの過程で水素ガスの濃度と、アセチレンガ
スの濃度の両方を同時に検出するようにしてなる油中溶
存ガス測定装置。
1. An apparatus for measuring dissolved gas in oil using means for dissolved gas in oil by circulating bubbling, wherein both a hydrogen gas sensor and an acetylene gas sensor are installed in the bubbling circulation path, and the both sensors are used to perform the An apparatus for measuring dissolved gas in oil, which detects both the concentration of hydrogen gas and the concentration of acetylene gas at the same time during the circulation bubbling.
JP3296724A 1991-08-26 1991-08-26 Oil dissolved gas measuring device Expired - Lifetime JP2748751B2 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP3296724A JP2748751B2 (en) 1991-08-26 1991-08-26 Oil dissolved gas measuring device

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP3296724A JP2748751B2 (en) 1991-08-26 1991-08-26 Oil dissolved gas measuring device

Publications (2)

Publication Number Publication Date
JPH0552787A true JPH0552787A (en) 1993-03-02
JP2748751B2 JP2748751B2 (en) 1998-05-13

Family

ID=17837274

Family Applications (1)

Application Number Title Priority Date Filing Date
JP3296724A Expired - Lifetime JP2748751B2 (en) 1991-08-26 1991-08-26 Oil dissolved gas measuring device

Country Status (1)

Country Link
JP (1) JP2748751B2 (en)

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2006284184A (en) * 2005-03-31 2006-10-19 Ishikawajima Inspection & Instrumentation Co Measuring method of concentration of dissolved combustible gas and measuring instrument therefor
JP2014527838A (en) * 2011-04-08 2014-10-23 センティーレ メディカル システムズ エルエルシーSentire Medical Systems Llc Intestinal perforation detection method and apparatus
JP5705388B1 (en) * 2014-08-27 2015-04-22 三菱電機株式会社 Diagnostic method for oil-filled electrical equipment
JP2015081799A (en) * 2013-10-21 2015-04-27 東西化学産業株式会社 Measuring apparatus and measuring method of dissolved hydrogen concentration
RU2569765C2 (en) * 2013-02-28 2015-11-27 Общество с ограниченной ответственностью "Северо-Западный Центр Сертификации" Method of assessment of dispersing and solubilising properties of fuels and oils and device for its implementation
US9266067B2 (en) 2011-11-28 2016-02-23 Korea Institute Of Science And Technology Composite separation membrane structure for gas sensor, gas sensor apparatus comprising the same, and method and apparatus for measuring gas concentration using the same

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH01227045A (en) * 1988-03-07 1989-09-11 Hitachi Ltd Detecting apparatus of gas for oil-immersed apparatus, collecting apparatus of gas in oil and detecting method of gas

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH01227045A (en) * 1988-03-07 1989-09-11 Hitachi Ltd Detecting apparatus of gas for oil-immersed apparatus, collecting apparatus of gas in oil and detecting method of gas

Cited By (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2006284184A (en) * 2005-03-31 2006-10-19 Ishikawajima Inspection & Instrumentation Co Measuring method of concentration of dissolved combustible gas and measuring instrument therefor
JP2014527838A (en) * 2011-04-08 2014-10-23 センティーレ メディカル システムズ エルエルシーSentire Medical Systems Llc Intestinal perforation detection method and apparatus
JP2017164529A (en) * 2011-04-08 2017-09-21 センティーレ メディカル システムズ エルエルシーSentire Medical Systems Llc Devices for detecting bowel perforation
US9266067B2 (en) 2011-11-28 2016-02-23 Korea Institute Of Science And Technology Composite separation membrane structure for gas sensor, gas sensor apparatus comprising the same, and method and apparatus for measuring gas concentration using the same
RU2569765C2 (en) * 2013-02-28 2015-11-27 Общество с ограниченной ответственностью "Северо-Западный Центр Сертификации" Method of assessment of dispersing and solubilising properties of fuels and oils and device for its implementation
JP2015081799A (en) * 2013-10-21 2015-04-27 東西化学産業株式会社 Measuring apparatus and measuring method of dissolved hydrogen concentration
JP5705388B1 (en) * 2014-08-27 2015-04-22 三菱電機株式会社 Diagnostic method for oil-filled electrical equipment
WO2016030984A1 (en) * 2014-08-27 2016-03-03 三菱電機株式会社 Method for inspecting oil-filled electrical apparatus
US10302618B2 (en) 2014-08-27 2019-05-28 Mitsubishi Electric Corporation Method for diagnosing oil-filled electrical apparatus

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Publication number Publication date
JP2748751B2 (en) 1998-05-13

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