JPH04328200A - Transparent soap - Google Patents
Transparent soapInfo
- Publication number
- JPH04328200A JPH04328200A JP9853291A JP9853291A JPH04328200A JP H04328200 A JPH04328200 A JP H04328200A JP 9853291 A JP9853291 A JP 9853291A JP 9853291 A JP9853291 A JP 9853291A JP H04328200 A JPH04328200 A JP H04328200A
- Authority
- JP
- Japan
- Prior art keywords
- soap
- weight
- transparent soap
- transparent
- amount
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 239000000344 soap Substances 0.000 title claims abstract description 30
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims abstract description 9
- RUTSRVMUIGMTHJ-UHFFFAOYSA-M sodium;tetradec-1-ene-1-sulfonate Chemical compound [Na+].CCCCCCCCCCCCC=CS([O-])(=O)=O RUTSRVMUIGMTHJ-UHFFFAOYSA-M 0.000 claims abstract description 9
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 6
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 claims abstract 6
- 235000011187 glycerol Nutrition 0.000 claims description 3
- 238000001035 drying Methods 0.000 abstract description 9
- 230000032683 aging Effects 0.000 abstract description 7
- 238000007517 polishing process Methods 0.000 abstract description 6
- 238000004519 manufacturing process Methods 0.000 abstract description 3
- 239000002994 raw material Substances 0.000 abstract description 3
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 6
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 description 6
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 6
- 239000008395 clarifying agent Substances 0.000 description 4
- 239000000654 additive Substances 0.000 description 3
- 238000005187 foaming Methods 0.000 description 3
- 238000000034 method Methods 0.000 description 3
- 239000002904 solvent Substances 0.000 description 3
- CZMRCDWAGMRECN-UGDNZRGBSA-N Sucrose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 CZMRCDWAGMRECN-UGDNZRGBSA-N 0.000 description 2
- 229930006000 Sucrose Natural products 0.000 description 2
- GSEJCLTVZPLZKY-UHFFFAOYSA-N Triethanolamine Chemical compound OCCN(CCO)CCO GSEJCLTVZPLZKY-UHFFFAOYSA-N 0.000 description 2
- 235000015278 beef Nutrition 0.000 description 2
- 239000004359 castor oil Substances 0.000 description 2
- 235000019438 castor oil Nutrition 0.000 description 2
- 239000003795 chemical substances by application Substances 0.000 description 2
- 239000003240 coconut oil Substances 0.000 description 2
- 235000019864 coconut oil Nutrition 0.000 description 2
- 239000003086 colorant Substances 0.000 description 2
- 230000000052 comparative effect Effects 0.000 description 2
- 238000007796 conventional method Methods 0.000 description 2
- 235000014113 dietary fatty acids Nutrition 0.000 description 2
- 239000003814 drug Substances 0.000 description 2
- 229940079593 drug Drugs 0.000 description 2
- 239000003925 fat Substances 0.000 description 2
- 235000019197 fats Nutrition 0.000 description 2
- 239000000194 fatty acid Substances 0.000 description 2
- 229930195729 fatty acid Natural products 0.000 description 2
- 150000004665 fatty acids Chemical class 0.000 description 2
- 239000003205 fragrance Substances 0.000 description 2
- ZEMPKEQAKRGZGQ-XOQCFJPHSA-N glycerol triricinoleate Natural products CCCCCC[C@@H](O)CC=CCCCCCCCC(=O)OC[C@@H](COC(=O)CCCCCCCC=CC[C@@H](O)CCCCCC)OC(=O)CCCCCCCC=CC[C@H](O)CCCCCC ZEMPKEQAKRGZGQ-XOQCFJPHSA-N 0.000 description 2
- 238000002844 melting Methods 0.000 description 2
- 230000008018 melting Effects 0.000 description 2
- 239000003921 oil Substances 0.000 description 2
- 235000019198 oils Nutrition 0.000 description 2
- 238000005498 polishing Methods 0.000 description 2
- 235000011118 potassium hydroxide Nutrition 0.000 description 2
- 235000011121 sodium hydroxide Nutrition 0.000 description 2
- 239000005720 sucrose Substances 0.000 description 2
- 239000003760 tallow Substances 0.000 description 2
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 1
- 239000002738 chelating agent Substances 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 238000005336 cracking Methods 0.000 description 1
- 238000005520 cutting process Methods 0.000 description 1
- 230000006866 deterioration Effects 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 229920005862 polyol Polymers 0.000 description 1
- 150000003077 polyols Chemical class 0.000 description 1
- 238000013441 quality evaluation Methods 0.000 description 1
- 230000005070 ripening Effects 0.000 description 1
- 238000007127 saponification reaction Methods 0.000 description 1
- 238000004904 shortening Methods 0.000 description 1
- 229910052708 sodium Inorganic materials 0.000 description 1
- 239000011734 sodium Substances 0.000 description 1
- BDHFUVZGWQCTTF-UHFFFAOYSA-M sulfonate Chemical compound [O-]S(=O)=O BDHFUVZGWQCTTF-UHFFFAOYSA-M 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D17/00—Detergent materials or soaps characterised by their shape or physical properties
- C11D17/0095—Solid transparent soaps or detergents
Abstract
Description
【０００１】0001
【産業上の利用分野】本発明は透明石けん、更に詳細に
は透明化のための乾燥・熟成工程並びに表面みがき工程
を必要としない枠練り透明石けんに関する。BACKGROUND OF THE INVENTION 1. Field of the Invention The present invention relates to a transparent soap, and more particularly to a frame-kneaded transparent soap that does not require a drying/aging process or a surface polishing process for transparency.
【０００２】0002
【従来の技術】一般に透明石けんの組成としては、牛脂
、ヤシ油、ヒマシ油、脂肪酸類等の油脂を苛性ソーダ、
苛性カリ、トリエタノールアミン等のアルカリ剤でけん
化して得た石けん素地；グリセリン、蔗糖等の透明化剤
；エタノール、水等の溶剤；その他キレート剤、薬剤、
色剤、香料等の添加剤が配合されており、その製造に当
っては、これらの温溶液を固化、切断、乾燥・熟成した
後、型打ち、みがき等の工程を経て製品とされていた。[Prior Art] Generally, the composition of transparent soap is to mix fats and oils such as beef tallow, coconut oil, castor oil, and fatty acids with caustic soda,
Soap base obtained by saponification with alkaline agents such as caustic potash and triethanolamine; Clarifying agents such as glycerin and sucrose; Solvents such as ethanol and water; Other chelating agents, drugs,
Additives such as coloring agents and fragrances are mixed in, and in manufacturing, these hot solutions are solidified, cut, dried and aged, and then processed through processes such as stamping and polishing to become products. .
【０００３】0003
【発明が解決しようとする課題】然しながら、斯かる従
来法による透明石けんは、エタノールや水を３０〜５０
重量％と多量に配合使用するものであったため、乾燥・
熟成工程に５０〜７０日間と云う長期間を必要とする欠
点があった。[Problems to be Solved by the Invention] However, transparent soap made by the conventional method is made by adding 30 to 50% ethanol or water.
Since it was used in a large amount by weight, drying and
There was a drawback that the aging process required a long period of 50 to 70 days.
【０００４】而して、従来より乾燥・熟成工程の短縮化
や省略化を目的として種々の改善方法が試みられている
ものの、今度は使用中に起泡力の低下や亀裂の発生、更
には溶け崩れや透明度の低下と云う品質劣化の問題が派
生し、何れも未だ、十分満足のいくものが得られていな
かったのが実状であった。[0004] Although various improvement methods have been attempted in the past with the aim of shortening or omitting the drying and ripening process, there are problems such as a decrease in foaming power, the occurrence of cracks, and even cracking during use. This led to quality deterioration problems such as melting and loss of transparency, and the reality was that a fully satisfactory product had not yet been obtained.
【０００５】また、従来法によるときは、何れもみがき
作業による表面仕上げ工程が避けられず、多くの人手を
要すると云う難点を免れなかった。[0005] Furthermore, in all conventional methods, a surface finishing step by polishing is inevitable, and a large amount of manpower is required.
【０００６】そこで、本発明者は斯かる実状に於て、透
明化のための乾燥・熟成工程並びに表面みがき工程を必
要としない高品質の透明石けんを提供すべく種々研究を
重ねた結果、テトラデセンスルホン酸ナトリウムを特定
量配合せしめれば、極めて良い結果が得られることを見
い出し、本発明を完成した。[0006] Under these circumstances, the inventor of the present invention has conducted various studies in order to provide a high-quality transparent soap that does not require a drying/aging process or a surface polishing process for transparency, and has developed Tetra. They discovered that extremely good results could be obtained by incorporating a specific amount of sodium desene sulfonate, and completed the present invention.
【０００７】[0007]
【課題を解決するための手段】すなわち、本発明はテト
ラデセンスルホン酸ナトリウムを１６〜２５重量％含有
することを特徴とする透明石けんである。[Means for Solving the Problems] That is, the present invention is a transparent soap characterized by containing 16 to 25% by weight of sodium tetradecene sulfonate.
【０００８】本発明透明石けんは、石けん素地、テトラ
デセンスルホン酸ナトリウム、透明化剤、水及びその他
の添加剤から構成される。The transparent soap of the present invention is composed of a soap base, sodium tetradecene sulfonate, a clarifying agent, water and other additives.
【０００９】ここに石けん素地とは、牛脂、ヤシ油、ヒ
マシ油、脂肪酸類等の油脂を苛性ソーダ、苛性カリ、ト
リエタノールアミン等のアルカリ剤でけん化したものを
いい、例えば表１の組成より成るものが好ましいものと
して挙げられる。[0009] The soap base herein refers to a product obtained by saponifying fats and oils such as beef tallow, coconut oil, castor oil, and fatty acids with an alkaline agent such as caustic soda, caustic potash, and triethanolamine. For example, soap base has the composition shown in Table 1. are listed as preferred.
【００１０】0010
【表１】[Table 1]
【００１１】透明化剤としては例えばグリセリン、蔗糖
、ポリオール類が挙げられるが、溶剤としてはエタノー
ルを用いることなく水を用いる。尚、その他の添加剤と
しては薬剤、色剤、香料等が挙げられる。Examples of the clarifying agent include glycerin, sucrose, and polyols, but as the solvent, water is used instead of ethanol. Note that other additives include drugs, coloring agents, fragrances, and the like.
【００１２】本発明に於て、テトラデセンスルホン酸ナ
トリウムは、透明石けん全量中に１６〜２５重量％含有
せられるが、更にこの範囲内で石けん素地量の６５〜１
００重量％相当量とするのが特に有利である。テトラデ
センスルホン酸ナトリウムの含有量が１６重量％より少
ない場合には乾燥工程を経ない限り不透明となり、他方
２５重量％より多過ぎる場合には不透明となり本発明の
目的を達し得ない。[0012] In the present invention, sodium tetradecene sulfonate is contained in the total amount of transparent soap in an amount of 16 to 25% by weight, and within this range, it is contained in an amount of 65 to 1% by weight based on the amount of the soap base.
Particularly advantageous is an amount corresponding to 0.00% by weight. If the content of sodium tetradecene sulfonate is less than 16% by weight, it will become opaque unless a drying step is performed, while if it is more than 25% by weight, it will become opaque and the object of the present invention cannot be achieved.
【００１３】また、本発明に於ける他の成分の含有量と
しては、石けん素地２５〜３０重量％、透明化剤３０〜
４３重量％、溶剤７〜２０重量％が好ましく、具体的に
は表２記載の配合組成の透明石けんが特に優れた結果を
与える。[0013] In addition, the content of other components in the present invention is 25 to 30% by weight of the soap base, 30 to 30% by weight of the clarifying agent.
43% by weight and 7 to 20% by weight of the solvent. Specifically, transparent soaps having the composition shown in Table 2 give particularly excellent results.
【００１４】[0014]
【表２】[Table 2]
【００１５】本発明透明石けんは、上記原料より成る温
溶液を所定の枠に流し込んで冷却固化し、次いで切断、
型打ちして製品とされ、乾燥・熟成工程及びみがき工程
を必要としない。[0015] The transparent soap of the present invention is produced by pouring a hot solution made of the above raw materials into a predetermined frame, cooling and solidifying it, and then cutting it.
It is molded into a product and does not require drying, aging or polishing processes.
【００１６】[0016]
【実施例】以下実施例を挙げて本発明を更に説明する。[Examples] The present invention will be further explained with reference to Examples below.
【００１７】実施例１〜３
表３記載の原料を混合溶解せしめて得た各温溶液を所定
の枠に流し込んで冷却固化し、次いで切断、型打ちした
後、包装して透明石けんを得た。得られた石けんは、乾
燥・熟成工程並びに表面みがき工程が存在しないにも拘
わらず、透明性に優れ、また起泡力が低下することなく
、溶け崩れも生じることがなかった。尚、比較例１〜３
として、テトラデセンスルホン酸ナトリウムの含有量を
表３記載の通りに代えた以外は実施例１と同様にして石
けんを得た。これら実施例及び比較例で得られた石けん
につき、品質評価を行なった結果は表５の通りであった
。Examples 1 to 3 Each hot solution obtained by mixing and dissolving the raw materials listed in Table 3 was poured into a predetermined frame, cooled and solidified, then cut, stamped, and packaged to obtain transparent soap. . The obtained soap had excellent transparency, did not have a decrease in foaming power, and did not melt or crumble, even though there was no drying/aging process or surface polishing process. In addition, Comparative Examples 1 to 3
A soap was obtained in the same manner as in Example 1 except that the content of sodium tetradecene sulfonate was changed as shown in Table 3. Table 5 shows the results of quality evaluation of the soaps obtained in these Examples and Comparative Examples.
【００１８】[0018]
【表３】[Table 3]
【００１９】＊ 表３中、石けん素地は下記表４処方の
ものを用いた。* In Table 3, the soap bases used were those prescribed in Table 4 below.
【００２０】[0020]
【表４】[Table 4]
【００２１】[0021]
【表５】[Table 5]
【００２２】[0022]
【発明の効果】本発明透明石けんは、その製造の際、乾
燥・熟成工程並びに表面みがき工程が不要であると共に
、起泡力の低下や溶け崩れが生じることがなく、優れた
品質を保持する。[Effect of the invention] The transparent soap of the present invention does not require a drying/aging process or a surface polishing process during its production, and maintains excellent quality without a decrease in foaming power or melting. .
Claims (2)
１６〜２５重量％含有することを特徴とする透明石けん
。1. A transparent soap containing 16 to 25% by weight of sodium tetradecene sulfonate.
デセンスルホン酸ナトリウム１６〜２５重量％、プロピ
レングリコール２０〜２８重量％、グリセリン１０〜１
５重量％及び水７〜２０重量％を含有することを特徴と
する透明石けん。Claim 2: 25-30% by weight of soap base, 16-25% by weight of sodium tetradecene sulfonate, 20-28% by weight of propylene glycol, 10-1% by weight of glycerin.
A transparent soap containing 5% by weight and 7 to 20% by weight of water.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP9853291A JPH04328200A (en) | 1991-04-30 | 1991-04-30 | Transparent soap |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP9853291A JPH04328200A (en) | 1991-04-30 | 1991-04-30 | Transparent soap |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| JPH04328200A true JPH04328200A (en) | 1992-11-17 |
Family
ID=14222290
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP9853291A Pending JPH04328200A (en) | 1991-04-30 | 1991-04-30 | Transparent soap |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPH04328200A (en) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO1996004360A1 (en) * | 1994-08-03 | 1996-02-15 | The Procter & Gamble Company | Transparent personal cleansing bar |
| WO1996004361A1 (en) * | 1994-08-03 | 1996-02-15 | The Procter & Gamble Company | Process for making a transparent personal cleansing bar |
| US5786311A (en) * | 1994-08-03 | 1998-07-28 | The Procter & Gamble Company | Monohydric alcohol-free process for making a transparent pour molded personal cleansing bar |
| US6730643B2 (en) | 2001-07-23 | 2004-05-04 | Unilever Home & Personal Care Usa Division Of Conopco, Inc. | Detergent bar and a process for manufacture |
-
1991
- 1991-04-30 JP JP9853291A patent/JPH04328200A/en active Pending
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO1996004360A1 (en) * | 1994-08-03 | 1996-02-15 | The Procter & Gamble Company | Transparent personal cleansing bar |
| WO1996004361A1 (en) * | 1994-08-03 | 1996-02-15 | The Procter & Gamble Company | Process for making a transparent personal cleansing bar |
| US5703025A (en) * | 1994-08-03 | 1997-12-30 | The Procter & Gamble Company | Monohydric alcohol-free process for making a transparent pour molded personal cleansing bar |
| US5786311A (en) * | 1994-08-03 | 1998-07-28 | The Procter & Gamble Company | Monohydric alcohol-free process for making a transparent pour molded personal cleansing bar |
| US6730643B2 (en) | 2001-07-23 | 2004-05-04 | Unilever Home & Personal Care Usa Division Of Conopco, Inc. | Detergent bar and a process for manufacture |
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