JPH04254440A - Method and apparatus for producing optical fiber - Google Patents
Method and apparatus for producing optical fiberInfo
- Publication number
- JPH04254440A JPH04254440A JP3031342A JP3134291A JPH04254440A JP H04254440 A JPH04254440 A JP H04254440A JP 3031342 A JP3031342 A JP 3031342A JP 3134291 A JP3134291 A JP 3134291A JP H04254440 A JPH04254440 A JP H04254440A
- Authority
- JP
- Japan
- Prior art keywords
- cylindrical body
- optical fiber
- light
- resin
- coating
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 239000013307 optical fiber Substances 0.000 title claims abstract description 47
- 238000000034 method Methods 0.000 title claims abstract description 8
- 239000011347 resin Substances 0.000 claims abstract description 40
- 229920005989 resin Polymers 0.000 claims abstract description 40
- 239000011248 coating agent Substances 0.000 claims abstract description 15
- 238000000576 coating method Methods 0.000 claims abstract description 15
- 239000011261 inert gas Substances 0.000 claims abstract description 6
- 238000004519 manufacturing process Methods 0.000 claims description 17
- 230000031700 light absorption Effects 0.000 abstract description 2
- 230000001678 irradiating effect Effects 0.000 abstract 2
- 239000003595 mist Substances 0.000 description 8
- 239000007789 gas Substances 0.000 description 7
- 239000010453 quartz Substances 0.000 description 7
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N silicon dioxide Inorganic materials O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 7
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 5
- 239000010410 layer Substances 0.000 description 5
- 239000000463 material Substances 0.000 description 5
- 239000004925 Acrylic resin Substances 0.000 description 4
- 238000010586 diagram Methods 0.000 description 4
- UHESRSKEBRADOO-UHFFFAOYSA-N ethyl carbamate;prop-2-enoic acid Chemical compound OC(=O)C=C.CCOC(N)=O UHESRSKEBRADOO-UHFFFAOYSA-N 0.000 description 4
- 239000000835 fiber Substances 0.000 description 4
- 238000010926 purge Methods 0.000 description 4
- NIXOWILDQLNWCW-UHFFFAOYSA-M Acrylate Chemical compound [O-]C(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-M 0.000 description 3
- 229910001873 dinitrogen Inorganic materials 0.000 description 3
- XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 description 2
- 230000002238 attenuated effect Effects 0.000 description 2
- 239000011247 coating layer Substances 0.000 description 2
- 230000000052 comparative effect Effects 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 238000012423 maintenance Methods 0.000 description 2
- 239000004593 Epoxy Substances 0.000 description 1
- JOYRKODLDBILNP-UHFFFAOYSA-N Ethyl urethane Chemical compound CCOC(N)=O JOYRKODLDBILNP-UHFFFAOYSA-N 0.000 description 1
- 238000009825 accumulation Methods 0.000 description 1
- 229910052786 argon Inorganic materials 0.000 description 1
- 230000005540 biological transmission Effects 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 238000004891 communication Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 150000002148 esters Chemical class 0.000 description 1
- 238000007380 fibre production Methods 0.000 description 1
- 230000007774 longterm Effects 0.000 description 1
- QSHDDOUJBYECFT-UHFFFAOYSA-N mercury Chemical compound [Hg] QSHDDOUJBYECFT-UHFFFAOYSA-N 0.000 description 1
- 229910052753 mercury Inorganic materials 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 230000003287 optical effect Effects 0.000 description 1
- 239000002356 single layer Substances 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 239000012780 transparent material Substances 0.000 description 1
Landscapes
- Optical Fibers, Optical Fiber Cores, And Optical Fiber Bundles (AREA)
- Surface Treatment Of Glass Fibres Or Filaments (AREA)
Abstract
Description
【0001】0001
【産業上の利用分野】本発明は、光通信用として用いる
光ファイバの製造装置及びそれを用いた光ファイバの製
造方法、特に光ファイバ被覆用光硬化型樹脂を硬化する
ための光照射装置の改良に関する。[Industrial Application Field] The present invention relates to an apparatus for manufacturing optical fibers used for optical communication and a method for manufacturing optical fibers using the same, and particularly to a light irradiation apparatus for curing photocurable resin for coating optical fibers. Regarding improvements.
【0002】光ファイバは、機械的な保護の目的で各種
樹脂で被覆されて用いられているが、生産性の観点から
光硬化型樹脂が一般に用いられる。図2は、従来の光フ
ァイバの製造装置及びそれを用いた光ファイバの製造方
法を示す概念図である。[0002] Optical fibers are used coated with various resins for the purpose of mechanical protection, and photocurable resins are generally used from the viewpoint of productivity. FIG. 2 is a conceptual diagram showing a conventional optical fiber manufacturing apparatus and an optical fiber manufacturing method using the same.
【0003】ここで、線引された光ファイバ3は、樹脂
塗布装置4により光硬化型樹脂が塗布され、光照射装置
11内の筒状体6を通過する時に光照射ランプ5から発
光する光により硬化し、単層又は複層の樹脂被覆層を形
成して巻取機8に巻き取られ、樹脂被覆層光ファイバ7
が製造される。Here, the drawn optical fiber 3 is coated with a photocurable resin by a resin coating device 4, and when it passes through a cylindrical body 6 in a light irradiation device 11, light emitted from a light irradiation lamp 5 is applied. is cured to form a single or multi-layer resin coating layer, which is wound up by a winder 8 to form a resin coating layer optical fiber 7.
is manufactured.
【0004】この場合に、樹脂を硬化させる光としては
、通常紫外線が、また、この紫外線の発光源としては主
として水銀ランプが、さらに筒状体としては紫外線の透
過性の点で石英管が一般に用いられている。In this case, the light for curing the resin is usually ultraviolet rays, the source of this ultraviolet light is mainly a mercury lamp, and the cylindrical body is generally a quartz tube due to its transparency to ultraviolet rays. It is used.
【0005】[0005]
【発明が解決しようとする課題】従来のこの種の装置で
は、筒状体6の中で光ファイバに塗布された樹脂が光照
射を受けて硬化する時に、照射光中の熱線成分を樹脂が
吸収したり、硬化時の反応熱により発熱し、ミストや揮
発成分を発生し、それが筒状体の内面に付着し易いため
に、光照射ランプからの光が、筒状体6内面の付着物に
より吸収を受けて減衰し、硬化する能力が低下する。従
って、光ファイバ製造時の線速を高める上で、あるいは
長時間にわたり連続して運転する上で問題があった。[Problems to be Solved by the Invention] In conventional devices of this kind, when the resin coated on the optical fiber in the cylindrical body 6 is cured by being irradiated with light, the resin absorbs the heat ray component in the irradiated light. The light from the light irradiation lamp does not cause any damage to the inner surface of the cylindrical body 6 because it absorbs heat and generates heat due to reaction heat during curing, generating mist and volatile components, which tend to adhere to the inner surface of the cylindrical body 6. It is absorbed and attenuated by the kimono, reducing its ability to harden. Therefore, there are problems in increasing the linear speed during optical fiber production or in continuous operation over a long period of time.
【0006】また、上記の問題点の解決法として、ファ
イバ温度を下げるために、光照射ランプからの照射光の
うち、熱線成分をガスなどを流すなどにより遮断する方
法が提案されているが、装置のメンテナンスに手間がか
かったり、高価であると言う問題があった(特開平1−
148733号公報)。[0006] Furthermore, as a solution to the above problem, a method has been proposed in which the hot ray component of the irradiated light from the light irradiation lamp is blocked by flowing gas or the like in order to lower the fiber temperature. There was a problem that the maintenance of the equipment was time-consuming and expensive (Japanese Patent Application Laid-Open No. 1999-1-
148733).
【0007】[0007]
【課題を解決するための手段】本発明者らは、従来の種
々の課題を解決すべく、検討した結果、光ファイバを製
造する装置において、光照射装置11中の光透過性筒状
体6の内径を細くし、かつ不活性ガスの流量を増大させ
る方法を見出し、本発明を完成するに至った。[Means for Solving the Problems] As a result of studies in order to solve various conventional problems, the present inventors have developed a light-transmitting cylindrical body 6 in a light irradiation device 11 in an apparatus for manufacturing optical fibers. The present invention was completed by discovering a method for reducing the inner diameter and increasing the flow rate of inert gas.
【0008】すなわち、本発明は;■ 光ファイバに
光硬化型樹脂を塗布した後、光透過性筒状体の中を通過
させ、該筒状体の外周より光を照射して該光硬化型樹脂
を硬化させて被覆を形成する光ファイバの製造方法にお
いて、光透過性筒状体6の内径を10mm以下にし、か
つ光透過性筒状体6の中に流す不活性ガスの流量を10
L/分以上にしたことを特徴とする光ファイバの製造方
法に関するし、また■ 光ファイバに光硬化型樹脂を
塗布した後、光透過性筒状体の中を通過させ、該筒状体
の外周より光を照射して該光硬化型樹脂を硬化させて被
覆を形成する光照射装置において、光透過性筒状体の内
径を10mm以下と細径にしたことを特徴とする、光照
射装置を提供する。That is, the present invention provides: (1) After applying a photocurable resin to an optical fiber, the optical fiber is passed through a light-transmitting cylindrical body, and light is irradiated from the outer periphery of the cylindrical body to form the photocurable resin. In an optical fiber manufacturing method in which a coating is formed by curing a resin, the inner diameter of the light-transmitting cylindrical body 6 is set to 10 mm or less, and the flow rate of the inert gas flowing into the light-transmitting cylindrical body 6 is set to 10 mm or less.
This invention relates to a method for manufacturing an optical fiber, characterized in that the optical fiber is coated with a photocurable resin, and then passed through a light-transmitting cylindrical body, and the cylindrical body is A light irradiation device that irradiates light from the outer periphery to cure the photocurable resin to form a coating, characterized in that the light-transmitting cylindrical body has a small inner diameter of 10 mm or less. I will provide a.
【0009】以下、本発明を図面に基づいて詳細に説明
する。図1は光ファイバ3に被覆された光硬化型樹脂を
光照射装置、とくに紫外線照射装置11に通して硬化す
る際に、該紫外線照射装置11内の筒状体6として内径
が10mm以下の細径のものを使用した状態を示す模式
図である。The present invention will be explained in detail below based on the drawings. FIG. 1 shows that when the photocurable resin coated on the optical fiber 3 is passed through a light irradiation device, particularly an ultraviolet irradiation device 11, to be cured, a thin tube with an inner diameter of 10 mm or less is used as a cylindrical body 6 in the ultraviolet irradiation device 11. FIG.
【0010】本発明において、光照射装置11内に設置
する筒状体6の内径を10mm以下のきわめて小さくす
ることが重要である。筒状体の内径が10mmを超える
と、予定する流速を得るのが難しい。このように、筒状
体6が細径としたので、この中を流入する不活性ガスの
流速が増大し、発生するミストや揮発成分が、筒状体6
表面上で滞留することがなく、容易に外部に排出される
。そのためには、この流速が10L/分以上であること
が必要であって、これ以下では所期の効果が得られない
。In the present invention, it is important that the inner diameter of the cylindrical body 6 installed in the light irradiation device 11 is extremely small, 10 mm or less. When the inner diameter of the cylindrical body exceeds 10 mm, it is difficult to obtain the expected flow rate. In this way, since the cylindrical body 6 has a small diameter, the flow rate of the inert gas flowing through the cylindrical body 6 increases, and the generated mist and volatile components are transferred to the cylindrical body 6.
It does not accumulate on the surface and is easily discharged to the outside. For this purpose, it is necessary that the flow rate is 10 L/min or more, and if it is less than this, the desired effect cannot be obtained.
【0011】該筒状体6を構成する素材としては、紫外
線などの照射光の透過に支障のない透明な素材、例えば
石英などが好ましく使用される。光ファイバ3を被覆す
るのに用いる光硬化型樹脂としては特に制限されないが
、紫外線などの光で容易に硬化する、例えばウレタン(
メタ)アクリレート、エポキシ(メタ)アクリレート、
エステル(メタ)アクリレートなどを挙げることができ
る。光ファイバ上に被覆される光硬化性樹脂は単層でも
複層でも良い。[0011] As the material constituting the cylindrical body 6, a transparent material such as quartz, which does not impair the transmission of irradiation light such as ultraviolet light, is preferably used. The photocurable resin used to coat the optical fiber 3 is not particularly limited, but it can be easily cured by light such as ultraviolet rays, such as urethane (
meth)acrylate, epoxy(meth)acrylate,
Examples include ester (meth)acrylate. The photocurable resin coated on the optical fiber may be a single layer or a multilayer.
【0012】0012
【作用】光ファイバに塗布された樹脂材から発生するミ
ストや揮発成分が筒状体に付着するメカニズムについて
は明確になっていないが、窒素等のパージガス中のミス
トや揮発成分が石英などの材料からなる筒状体表面で冷
却され、その結果固体として筒状体表面に付着すると推
定される。[Operation] The mechanism by which the mist and volatile components generated from the resin material coated on the optical fiber adhere to the cylindrical body is not clear, but the mist and volatile components in the purge gas such as nitrogen are attached to the material such as quartz. It is presumed that the material is cooled on the surface of the cylindrical body, and as a result, it adheres to the surface of the cylindrical body as a solid.
【0013】本発明によれば、ファイバ周辺付近のパー
ジガスは、筒状体6の径がきわめて小さいために流速が
速く、パージガス中のミストや揮発成分は筒状体6内表
面で冷却され付着する以前に、パージガスと一緒に光照
射装置11外に排出される。According to the present invention, the purge gas near the fiber periphery has a high flow rate because the diameter of the cylindrical body 6 is extremely small, and the mist and volatile components in the purge gas are cooled and attached to the inner surface of the cylindrical body 6. Previously, it is discharged to the outside of the light irradiation device 11 together with the purge gas.
【0014】従って、本発明の細径の筒状体6を用いた
装置によると、光照射ランプ5からの光が筒状体6内表
面の付着物により吸収を受けて減衰することはなく、ま
た硬化能力も低下せず、線速を高める上で、あるいは長
時間にわたり連続して運転する上での問題はない。しか
も、本発明を実施するための装置は、簡便で、且つメン
テナンスも殆ど不要である。Therefore, according to the device using the small-diameter cylindrical body 6 of the present invention, the light from the light irradiation lamp 5 is not attenuated by being absorbed by the deposits on the inner surface of the cylindrical body 6. Further, the curing ability does not decrease, and there are no problems in increasing the linear speed or in continuous operation over a long period of time. Furthermore, the apparatus for carrying out the present invention is simple and requires almost no maintenance.
【0015】[0015]
【実施例】本発明を下記の実施例で具体的に説明するが
、これらは本発明の範囲を制限するものではない。EXAMPLES The present invention will be specifically explained with the following examples, but these are not intended to limit the scope of the invention.
【実施例1】図1に示すような光ファイバ製造装置にお
いて、外径13mm、内径10mmの石英管からなる筒
状体6内壁に窒素ガスを流量10L/分で流入させた。Example 1 In an optical fiber manufacturing apparatus as shown in FIG. 1, nitrogen gas was flowed into the inner wall of a cylindrical body 6 made of a quartz tube with an outer diameter of 13 mm and an inner diameter of 10 mm at a flow rate of 10 L/min.
【0016】これにより、ウレタンアクリレート系樹脂
を順次2層塗布し、硬化しながら線速200m/分で1
0時間連続で線引した。線引後に光照射装置11の筒状
体6の内面を調べたが、樹脂から発生するミストや揮発
成分の付着は殆どなかった。また、線引して得られたフ
ァイバの被覆樹脂の硬化度を調べたところ、全長にわた
って完全硬化していることが判った。[0016] As a result, two layers of urethane acrylate resin were applied in sequence, and while curing, the resin was applied at a linear speed of 200 m/min.
The line was drawn continuously for 0 hours. After drawing, the inner surface of the cylindrical body 6 of the light irradiation device 11 was examined, and there was almost no mist generated from the resin or attachment of volatile components. Furthermore, when the degree of curing of the coating resin of the fiber obtained by drawing was examined, it was found that the entire length was completely cured.
【0017】[0017]
【実施例2】図1に示すような光ファイバ製造装置にお
いて、実施例1と同じ径の石英管を用いてアルゴンガス
を流量10L/分で流入させた。これにより、ウレタン
アクリレート系樹脂を順次2層塗布し、硬化しながら線
速200m/分で10時間連続で線引した。実施例1と
同様に筒状体6内面に樹脂の付着はなく、ファイバ被覆
も全長にわたり完全硬化していることが判った。Example 2 In an optical fiber manufacturing apparatus as shown in FIG. 1, a quartz tube having the same diameter as in Example 1 was used, and argon gas was introduced at a flow rate of 10 L/min. Thereby, two layers of urethane acrylate resin were sequentially applied, and while curing the resin was drawn continuously at a drawing speed of 200 m/min for 10 hours. As in Example 1, there was no resin adhesion to the inner surface of the cylindrical body 6, and it was found that the fiber coating was completely cured over the entire length.
【0018】[0018]
【比較例1】図1に示すような光ファイバ製造装置にお
いて、実施例1と同じ径の石英管を用いて窒素ガスを流
量5L/分で流入させた。これにより、ウレタンアクリ
レート系樹脂を順次2層塗布し、硬化しながら線速20
0m/分で10時間連続で線引した。線引後に筒状体6
内面を調べたところ、樹脂成分が付着し、紫外線は透過
しにくくなっていることが判った。また、得られた光フ
ァイバのうち後半の約1/3は被覆が完全硬化していな
いことが判った。[Comparative Example 1] In an optical fiber manufacturing apparatus as shown in FIG. 1, a quartz tube having the same diameter as in Example 1 was used, and nitrogen gas was introduced at a flow rate of 5 L/min. As a result, two layers of urethane acrylate resin are sequentially applied, and while curing, the line speed is 20.
The wire was drawn continuously for 10 hours at 0 m/min. Cylindrical body 6 after drawing
When we examined the inner surface, we found that a resin component had adhered to it, making it difficult for ultraviolet rays to pass through. Furthermore, it was found that the coating of about 1/3 of the obtained optical fiber was not completely cured.
【0019】[0019]
【比較例2】図1に示すような光ファイバ製造装置にお
いて、内径20mm、外径23mmの石英管を用いて窒
素ガスを流量10L/分で流入させた。これにより、ウ
レタンアクリレート系樹脂を順次2層塗布し、硬化しな
がら線速200m/分で10時間連続で線引した。線引
後に筒状体内面を調べたところ、樹脂成分が付着し、紫
外線は透過しにくくなっていることが判った。また得ら
れた光ファイバのうち後半の約1/2は被覆が完全硬化
していないことが判った。[Comparative Example 2] In an optical fiber manufacturing apparatus as shown in FIG. 1, nitrogen gas was introduced at a flow rate of 10 L/min using a quartz tube having an inner diameter of 20 mm and an outer diameter of 23 mm. Thereby, two layers of urethane acrylate resin were sequentially applied, and while curing the resin was drawn continuously at a drawing speed of 200 m/min for 10 hours. When the inner surface of the cylindrical body was examined after drawing, it was found that resin components had adhered to it, making it difficult for ultraviolet rays to pass through. It was also found that the coating of about 1/2 of the obtained optical fibers was not completely cured.
【0020】[0020]
【発明の効果】本発明の光ファイバ製造装置およびそれ
を用いた光ファイバの製造方法によると、筒状体6の内
面の付着ミストや揮発物あるいは筒状体6内部の滞留ミ
ストの発生がなくて、これによる光吸収が起こりにくく
、光強度を高くしかも長時間に維持することが出来る。
従って、硬化速度が上がり、線速度を向上させることが
出来、また長時間の運転を行う上で支障もない。[Effects of the Invention] According to the optical fiber manufacturing apparatus and optical fiber manufacturing method using the same of the present invention, there is no generation of adhering mist or volatile matter on the inner surface of the cylindrical body 6 or accumulation of mist inside the cylindrical body 6. Therefore, light absorption due to this is difficult to occur, and the light intensity can be maintained high and for a long time. Therefore, the curing speed increases, the linear speed can be improved, and there is no problem in long-term operation.
【図1】光ファイバ3に被覆された光硬化型樹脂を紫外
線照射装置11に通して硬化する際に、該紫外線照射装
置11内の筒状体6の内径を10mm以下にした状態を
示す模式図である。FIG. 1 is a schematic diagram showing a state in which the inner diameter of the cylindrical body 6 in the ultraviolet irradiation device 11 is set to 10 mm or less when the photocurable resin coated on the optical fiber 3 is cured by passing it through the ultraviolet irradiation device 11. It is a diagram.
【図2】従来の光ファイバの製造装置及びそれを用いた
光ファイバの製造方法を示す模式図である。FIG. 2 is a schematic diagram showing a conventional optical fiber manufacturing apparatus and an optical fiber manufacturing method using the same.
1 光ファイバ母材 2 線引炉 3 光ファイバ 4 樹脂塗布装置 5 光照射ランプ 6 筒状体 7 樹脂被覆光ファイバ 8 巻取機 9 ガス供給管 10 反射鏡 11 光照射装置 12 内径10mm以下の筒状体 1 Optical fiber base material 2 Drawing furnace 3 Optical fiber 4 Resin coating equipment 5 Light irradiation lamp 6 Cylindrical body 7 Resin coated optical fiber 8 Winder 9 Gas supply pipe 10 Reflector 11. Light irradiation device 12 Cylindrical body with an inner diameter of 10 mm or less
Claims (2)
後、光透過性筒状体の中を通過させ、該筒状体の外周よ
り光を照射して該光硬化型樹脂を硬化させて被覆を形成
する光ファイバの製造方法において、光透過性筒状体の
内径を10mm以下にした光照射装置を用い、かつ光透
過性筒状体の中に流す不活性ガスの流量を10L/分以
上にしたことを特徴とする、光ファイバの製造方法。Claim 1: After coating an optical fiber with a photocurable resin, the optical fiber is passed through a light-transmitting cylindrical body, and light is irradiated from the outer periphery of the cylindrical body to cure the photocurable resin. In the method of manufacturing an optical fiber forming a coating, a light irradiation device is used in which the inner diameter of the light-transmitting cylindrical body is 10 mm or less, and the flow rate of the inert gas flowing into the light-transmitting cylindrical body is 10 L/min. A method for manufacturing an optical fiber, characterized by the above.
後、光透過性筒状体の中を通過させ、該筒状体の外周よ
り光を照射して該光硬化型樹脂を硬化させて被覆を形成
する光照射装置において、光透過性筒状体の内径を10
mm以下と細径にしたことを特徴とする、光照射装置。2. After coating an optical fiber with a photocurable resin, the optical fiber is passed through a light-transmitting cylindrical body, and light is irradiated from the outer periphery of the cylindrical body to cure the photocurable resin. In the light irradiation device that forms the coating, the inner diameter of the light-transmitting cylindrical body is set to 10
A light irradiation device characterized by having a small diameter of less than mm.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP3031342A JPH04254440A (en) | 1991-02-01 | 1991-02-01 | Method and apparatus for producing optical fiber |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP3031342A JPH04254440A (en) | 1991-02-01 | 1991-02-01 | Method and apparatus for producing optical fiber |
Publications (1)
Publication Number | Publication Date |
---|---|
JPH04254440A true JPH04254440A (en) | 1992-09-09 |
Family
ID=12328561
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP3031342A Pending JPH04254440A (en) | 1991-02-01 | 1991-02-01 | Method and apparatus for producing optical fiber |
Country Status (1)
Country | Link |
---|---|
JP (1) | JPH04254440A (en) |
-
1991
- 1991-02-01 JP JP3031342A patent/JPH04254440A/en active Pending
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