JPH04168180A - Production of cooked paste - Google Patents
Production of cooked pasteInfo
- Publication number
- JPH04168180A JPH04168180A JP29209090A JP29209090A JPH04168180A JP H04168180 A JPH04168180 A JP H04168180A JP 29209090 A JP29209090 A JP 29209090A JP 29209090 A JP29209090 A JP 29209090A JP H04168180 A JPH04168180 A JP H04168180A
- Authority
- JP
- Japan
- Prior art keywords
- paste
- starch
- glue
- anhydrous silica
- takinori
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 238000004519 manufacturing process Methods 0.000 title claims description 8
- 229920002472 Starch Polymers 0.000 claims abstract description 28
- 235000019698 starch Nutrition 0.000 claims abstract description 23
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims abstract description 20
- 238000000034 method Methods 0.000 claims abstract description 19
- 239000008107 starch Substances 0.000 claims abstract description 17
- 239000000377 silicon dioxide Substances 0.000 claims abstract description 9
- 239000000203 mixture Substances 0.000 claims description 5
- 229910052784 alkaline earth metal Inorganic materials 0.000 claims description 4
- -1 alkaline earth metal salts Chemical class 0.000 claims description 4
- 238000004026 adhesive bonding Methods 0.000 claims description 3
- 230000008014 freezing Effects 0.000 abstract description 5
- 238000007710 freezing Methods 0.000 abstract description 5
- 238000010257 thawing Methods 0.000 abstract description 5
- 239000011369 resultant mixture Substances 0.000 abstract 2
- 239000003513 alkali Substances 0.000 abstract 1
- 150000003839 salts Chemical class 0.000 abstract 1
- 239000003292 glue Substances 0.000 description 13
- 230000000052 comparative effect Effects 0.000 description 5
- 238000011156 evaluation Methods 0.000 description 5
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 5
- VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 description 4
- 230000032683 aging Effects 0.000 description 4
- 229940100445 wheat starch Drugs 0.000 description 4
- 239000004831 Hot glue Substances 0.000 description 3
- GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 description 3
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 3
- 230000000694 effects Effects 0.000 description 3
- 229910017604 nitric acid Inorganic materials 0.000 description 3
- 238000003756 stirring Methods 0.000 description 3
- 229910002012 Aerosil® Inorganic materials 0.000 description 2
- 240000003183 Manihot esculenta Species 0.000 description 2
- 235000016735 Manihot esculenta subsp esculenta Nutrition 0.000 description 2
- 230000003115 biocidal effect Effects 0.000 description 2
- 239000003139 biocide Substances 0.000 description 2
- 229910000019 calcium carbonate Inorganic materials 0.000 description 2
- 239000002245 particle Substances 0.000 description 2
- 239000003755 preservative agent Substances 0.000 description 2
- 230000002335 preservative effect Effects 0.000 description 2
- 239000002002 slurry Substances 0.000 description 2
- 241001474374 Blennius Species 0.000 description 1
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 1
- 229910052791 calcium Inorganic materials 0.000 description 1
- 239000011575 calcium Substances 0.000 description 1
- 230000032050 esterification Effects 0.000 description 1
- 238000005886 esterification reaction Methods 0.000 description 1
- 238000006266 etherification reaction Methods 0.000 description 1
- 239000010419 fine particle Substances 0.000 description 1
- ZLNQQNXFFQJAID-UHFFFAOYSA-L magnesium carbonate Chemical compound [Mg+2].[O-]C([O-])=O ZLNQQNXFFQJAID-UHFFFAOYSA-L 0.000 description 1
- 239000001095 magnesium carbonate Substances 0.000 description 1
- 229910000021 magnesium carbonate Inorganic materials 0.000 description 1
- 238000006386 neutralization reaction Methods 0.000 description 1
- 229920001592 potato starch Polymers 0.000 description 1
Landscapes
- Adhesives Or Adhesive Processes (AREA)
- Chemical Or Physical Treatment Of Fibers (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
Abstract
Description
【発明の詳細な説明】
（産業上の利用分野）
本発明は、洗濯糊、壁紙糊などの種々の用途に用いる「
たきのり」の製造法に関するものであり、詳しくはコシ
が強くて凍結、解凍時の老化の少ない「たきのり」の製
造法に関するものである。Detailed Description of the Invention (Field of Industrial Application) The present invention is applicable to various applications such as laundry paste, wallpaper paste, etc.
This article relates to a method for producing ``Takinori,'' and more specifically, to a method for producing ``Takinori,'' which is firm and does not deteriorate easily when frozen and thawed.
（従来の技術）
従来の「たきのり」は、主に小麦澱粉が用いられ、この
澱粉から温糊法、冷糊法（アルカリ糊化法、アパラチン
法）などの方法により製造されている。(Prior Art) Conventional "Takinori" mainly uses wheat starch, and is produced from this starch by methods such as hot glue method and cold glue method (alkaline gelatinization method, Apalachin method).
（発明が解決しようとする課題）
上記の「たきのり」は、その製造の過程や製品の処理な
どについて種々の研究がなされているが、未だ十分な品
質のものは見あたらず、品質の安定性にばらつきが大き
い。特に品質特性のうち糊のコシが製品によってばらつ
きが大きく、使用工種々の問題がある。(Problem to be solved by the invention) Various studies have been conducted on the manufacturing process and product processing of the above-mentioned "Takinori", but there is still no product of sufficient quality, and the stability of quality is still unknown. There is a large variation in In particular, among the quality characteristics, the stiffness of the glue varies greatly depending on the product, and there are various problems with the use of the glue.
また、 「たきのり」はその製品の保存のために凍結す
るが、使用の際に解凍するので一般にその凍結−解凍時
などに老化する傾向にある。そこで上記の欠点を解消す
るためや、凍結−解凍時などの糊の耐老化性を改良する
ために、一部エーテル化澱粉を使用しているが、この改
良法では原料澱粉のコスト上昇の要因となるので好まし
い方法ではない・ 本発明は、上記の問題に鑑みてな
されたものであり、その目的は比較的廉価な方法で、出
来上がった糊のコシが強く、かつ凍結−解凍時の老化を
少なくする効果を発揮する「たきのり」の製造法を提供
することである。Furthermore, ``Takinori'' is frozen to preserve the product, but it is thawed before use, so it generally tends to age during the freezing and thawing process. Therefore, in order to eliminate the above disadvantages and improve the aging resistance of the glue during freezing and thawing, some etherified starch is used, but this improved method increases the cost of raw starch. Therefore, it is not a preferred method. The present invention was made in view of the above problems, and its purpose is to provide a relatively inexpensive method that gives the finished glue a strong stiffness and prevents aging during freezing and thawing. The purpose of the present invention is to provide a method for producing "Takinori" that exhibits the effect of reducing the amount of seaweed.
（課題を解決するための手段および作用）本発明者らは
、上記の問題点を克服せんとして種々検討した結果、無
水シリカの微粒子や炭酸カルシウム、炭酸マグネシウム
などのアルカリ土類金属塩を単独または併用して混合し
た澱粉から糊を作ると、出来上がった糊のコシが強くな
り、耐老化性も大幅に改良されることを見いだした。(Means and effects for solving the problem) As a result of various studies in an attempt to overcome the above-mentioned problems, the present inventors have found that fine particles of anhydrous silica and alkaline earth metal salts such as calcium carbonate and magnesium carbonate are used alone or in It has been found that when starch is used in combination to make a glue, the resulting glue becomes stronger and its aging resistance is greatly improved.
すなわち本発明の要旨は、 「澱粉に微粉末状の無水シ
リカ、アルカリ土類金属塩のうち少なくとも１種以上を
添加して混合し、この混合物を用いて温糊法または冷糊
法のいずれかの方法で製糊することを特徴とする「たき
のり」の製造法」である。That is, the gist of the present invention is as follows: ``At least one of finely powdered anhydrous silica and alkaline earth metal salts is added to starch and mixed, and this mixture is used to apply either the hot gluing method or the cold gluing method. This is a method for producing ``takinori'' which is characterized by making starch using the following method.
本発明に使用する無水シリカは平均粒径１〜１１００ｎ
のものが好ましく、アルカリ土類金属塩は０．１〜１０
μの平均粒径のものがよい。The anhydrous silica used in the present invention has an average particle size of 1 to 1100n.
The alkaline earth metal salt is preferably 0.1 to 10
The average particle size of μ is preferable.
また使用される澱粉は小麦澱粉、タピオカ澱粉、馬鈴薯
澱粉などの未処理の澱粉およびエステル化、エーテル化
などの加工澱粉など「たきのり」用として使用されてい
るすべての澱粉が挙げられる。The starches used include all starches used for ``Takinori'' such as unprocessed starches such as wheat starch, tapioca starch, and potato starch, and processed starches such as esterification and etherification.
そしてこれらの澱粉に無水シリカ等を添加、混合する方
法としては、あらかじめ澱粉に吸着させる、あらかじめ
澱粉と混合しておく、「たきのり」の製造時に添加する
などの方法が挙げられる。また、無水シリカ等の添加量
は澱粉に対して０．０１〜１０％の範囲が好ましい。Methods for adding and mixing anhydrous silica and the like to these starches include methods such as adsorbing it to the starch in advance, mixing it with the starch in advance, and adding it during the production of "Takinori". Further, the amount of anhydrous silica etc. added is preferably in the range of 0.01 to 10% based on the starch.
以下実施例について説明する。Examples will be described below.
（実施例等）
実施例１．小麦澱粉１００部に無水シリカ（アエロジル
Ｒ−８１２、日本アエロジル工業）０゜１部、炭酸カル
シウム（コロカルソーＷＳ１ 白石カルシウム）０．２
部を添加し、家庭用の混練機（ナショナルタックマスタ
ー）で十分混合したちの。(Examples, etc.) Example 1. 100 parts of wheat starch, 0.1 part of anhydrous silica (Aerosil R-812, Nippon Aerosil Kogyo), and 0.2 parts of calcium carbonate (Colocalso WS1 Shiraishi Calcium)
of water and mix well with a household kneader (National Tack Master).
比較例１．アセチル化小麦澱粉（輸入品）。Comparative example 1. Acetylated wheat starch (imported).
比較例２．比較例１の澱粉９０部とエーテル化タピオカ
澱粉１０部を混合したもの。Comparative example 2. A mixture of 90 parts of the starch of Comparative Example 1 and 10 parts of etherified tapioca starch.
実施例２．加熱製糊の場合（温糊法）について説明する
。実施例１および比較例１，２の澱粉をそれぞれ３２０
ｇとり、これに水１６８ｃｃを加えてスラリーとして、
これを２段スクリューペラで撹拌しながら加熱し、内温
７５０℃で２０分間クツキングする。この後急冷し、重
量補正後、防腐剤（ビオサイド）を４ｇ加え、再度１５
分間攪拌して混練して仕上がりとする。ここでえられた
糊の評価を第１表に示す。Example 2. The case of hot glue making (hot glue method) will be explained. 320% of the starch of Example 1 and Comparative Examples 1 and 2, respectively.
g, add 168cc of water to it to make a slurry,
This was heated while being stirred with a two-stage screw propeller, and was cooked for 20 minutes at an internal temperature of 750°C. After that, it was rapidly cooled, and after weight correction, 4g of preservative (biocide) was added, and again
Mix and knead for a minute to finish. Table 1 shows the evaluation of the glue obtained here.
実施例３．アルカリ製糊（アパラチン法）の場合につい
て説明する。実施例１および比較例１゜２の澱粉をそれ
ぞれ４６７ｇとり、水を１１３３ｃ ｃ加えてスラリー
とする。これを卓上型ニーダ−（ダブルＺタイプ）に入
れ撹拌しながら水酸化ナトリウム３２ｇ＋水７０２ｃｃ
の溶液をゆっくり添加し２０分間室温２Ｓ±３℃で撹拌
する。その後、硝酸８０ｇ＋水１８Ｂｃｃの溶液を滴下
して中和する（ＰＨ７±０．２）。硝酸が大部分滴下し
たところで、防腐剤（ビオサイド）５ｇを加え、さらに
硝酸を加えて中和する。中和後さらに１５分間攪拌して
仕上がりとする。ここでえられた糊の評価を第２表に示
す。Example 3. The case of alkaline glue (Apalatin method) will be explained. Take 467 g of each of the starches of Example 1 and Comparative Example 1.2 and add 1133 cc of water to make a slurry. Place this in a tabletop kneader (double Z type) and add 32g of sodium hydroxide + 702cc of water while stirring.
Slowly add the solution and stir for 20 minutes at room temperature 2S±3°C. Thereafter, a solution of 80 g of nitric acid + 18 Bcc of water was added dropwise to neutralize (PH7±0.2). When most of the nitric acid has been dropped, 5 g of a preservative (biocide) is added, and further nitric acid is added to neutralize. After neutralization, stir for another 15 minutes to finish. Table 2 shows the evaluation of the glue obtained here.
第１表 糊の評価
第２表 糊の評価
（注）第１，２表の評価は良◎←０４−△←×不良で表
示
（発明の効果）
本発明によって製造される「たきのり」は、糊のコシが
強く、かつ凍結−解凍時の老化を少なくする効果を発揮
する、そして比較的廉価な方法でたきのりをつくること
が出来るのでその実用上の価値は大なるものがある。Table 1 Glue Evaluation Table 2 Glue Evaluation (Note) The evaluations in Tables 1 and 2 are expressed as Good ◎←04-△←×Poor (Effects of the Invention) “Takinori” produced by the present invention is It has great practical value because it has a strong glue and is effective in reducing aging during freezing and thawing, and it can be made using a relatively inexpensive method.
特 許 出 願 人 敷島スターチ株式会社手続補正書 平成３年２月２１日Patent applicant: Shikishima Starch Co., Ltd. Procedural amendment February 21, 1991
Claims (1)
ち少なくとも１種以上を添加して混合し、この混合物を
用いて温糊法または冷糊法のいずれかの方法で製糊する
ことを特徴とする「たきのり」の製造法。At least one of finely powdered anhydrous silica and alkaline earth metal salts is added to starch and mixed, and the mixture is used to make starch using either a hot or cold gluing method. The manufacturing method of ``takinori'' is a feature.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP29209090A JPH04168180A (en) | 1990-10-31 | 1990-10-31 | Production of cooked paste |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP29209090A JPH04168180A (en) | 1990-10-31 | 1990-10-31 | Production of cooked paste |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| JPH04168180A true JPH04168180A (en) | 1992-06-16 |
Family
ID=17777425
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP29209090A Pending JPH04168180A (en) | 1990-10-31 | 1990-10-31 | Production of cooked paste |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPH04168180A (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0972812A1 (en) * | 1998-07-13 | 2000-01-19 | Korea Research Institute Of Chemical Technology | Adhesive for a multi-ply sheet and a method for manufacturing the multi-ply sheet using the same |
| CN107099263A (en) * | 2017-05-08 | 2017-08-29 | 武汉理工大学 | A kind of Nano-meter SiO_22The preparation method of/starch base composite adhesive |
-
1990
- 1990-10-31 JP JP29209090A patent/JPH04168180A/en active Pending
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0972812A1 (en) * | 1998-07-13 | 2000-01-19 | Korea Research Institute Of Chemical Technology | Adhesive for a multi-ply sheet and a method for manufacturing the multi-ply sheet using the same |
| CN107099263A (en) * | 2017-05-08 | 2017-08-29 | 武汉理工大学 | A kind of Nano-meter SiO_22The preparation method of/starch base composite adhesive |
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