JPH0412579B2 - - Google Patents
Info
- Publication number
- JPH0412579B2 JPH0412579B2 JP26005384A JP26005384A JPH0412579B2 JP H0412579 B2 JPH0412579 B2 JP H0412579B2 JP 26005384 A JP26005384 A JP 26005384A JP 26005384 A JP26005384 A JP 26005384A JP H0412579 B2 JPH0412579 B2 JP H0412579B2
- Authority
- JP
- Japan
- Prior art keywords
- glass tube
- protective film
- drying
- suspension
- film
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 239000011521 glass Substances 0.000 claims description 34
- 230000001681 protective effect Effects 0.000 claims description 22
- 239000000725 suspension Substances 0.000 claims description 16
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 15
- 238000000034 method Methods 0.000 claims description 11
- 239000000843 powder Substances 0.000 claims description 8
- 238000004519 manufacturing process Methods 0.000 claims description 6
- 238000009736 wetting Methods 0.000 claims description 3
- 238000001035 drying Methods 0.000 description 20
- 238000004140 cleaning Methods 0.000 description 9
- 239000011248 coating agent Substances 0.000 description 6
- 238000000576 coating method Methods 0.000 description 6
- 239000002245 particle Substances 0.000 description 4
- 238000009826 distribution Methods 0.000 description 3
- QSHDDOUJBYECFT-UHFFFAOYSA-N mercury Chemical compound [Hg] QSHDDOUJBYECFT-UHFFFAOYSA-N 0.000 description 3
- 229910052753 mercury Inorganic materials 0.000 description 3
- 238000005406 washing Methods 0.000 description 3
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 description 2
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 2
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- 238000007664 blowing Methods 0.000 description 1
- 210000000078 claw Anatomy 0.000 description 1
- 238000011109 contamination Methods 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 239000000428 dust Substances 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 239000003595 mist Substances 0.000 description 1
- 239000003973 paint Substances 0.000 description 1
- 238000004904 shortening Methods 0.000 description 1
- 239000000377 silicon dioxide Substances 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
Classifications
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01J—ELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
- H01J9/00—Apparatus or processes specially adapted for the manufacture, installation, removal, maintenance of electric discharge tubes, discharge lamps, or parts thereof; Recovery of material from discharge tubes or lamps
- H01J9/20—Manufacture of screens on or from which an image or pattern is formed, picked up, converted or stored; Applying coatings to the vessel
Landscapes
- Engineering & Computer Science (AREA)
- Manufacturing & Machinery (AREA)
- Formation Of Various Coating Films On Cathode Ray Tubes And Lamps (AREA)
- Vessels And Coating Films For Discharge Lamps (AREA)
Description
〔発明の技術分野〕
本発明は蛍光ランプの製造方法に関し、特にバ
ルブ内面に保護膜を形成する工程の改良に関す
る。
〔発明の技術的背景とその問題点〕
従来、蛍光ランプの製造においては、ガラス管
の内外両面を水で洗浄してごみその他の汚物を除
去し、乾燥したのちガラス管内面に蛍光体けん濁
液を塗布して乾燥し、焼成して蛍光膜を形成して
いた。
近年に到り、ガラス中のアルカリ成分から蛍光
体を保護するため、アルミナやシリカなどの無機
微粉末からなる保護膜をガラス管内面に形成し、
この保護膜上に蛍光膜を形成するようになつた。
この場合、ガラス管の洗浄に当り、保持方法、
洗浄方法および乾燥方法について従来通り何の制
約も設けないで作業した場合、得られた保護膜の
状態が非常に悪く、乾燥むらによる膜厚の不均一
なものがしばしば発生し、このような不良保護膜
のランプは点灯中不均一部分に水銀が付着して細
い帯状の模様が発生し、外観を損うばかりか短寿
命の原因にもなつた。
〔発明の目的〕
本発明は工業的な流れ作業において、均一な保
護膜を形成してその上に蛍光膜を形成し、この結
果水銀による保護膜の汚損や保護膜の厚さ不均一
による短寿命のない蛍光ランプの製造方法を提供
することを目的とする。
〔発明の概要〕
ガラス管を上下方向にして両端で支持し、管の
外面を濡らすことなく内面を水で洗浄し、ついで
内面に無機微粉末のけん濁液を塗布して保護膜を
形成することにより、けん濁液の乾燥を均一にし
て均一な保護膜を得る方法である。
〔発明の実施例〕
本発明者は保護膜が不均一に形成される理由に
ついて調査したところ、乾燥時のガラス管温度の
局部的不均一が理由であり、その原因はチヤツク
への熱伝導とガラス管外面に局部的に残存する洗
浄水の蒸発熱によるものであることを見い出し、
チヤツクの位置および洗浄方法を改善して不良原
因を除くことに成功した。
以下、本発明の詳細を図示の実施例によつて説
明する。本実施例に使用するガラス管は第1図に
示すように直管状をなし、両端縁が焼き丸められ
てわずかに内側にわん曲している。
まず、第1図に示すように、このガラス管1を
上下方向にして上端のわん曲部11を板状の上側
チヤツク2の受け孔21に挿入し、L字形をした
下側チヤツク3をばね31に抗して引下げ、係止
爪32をガラス管1の下端のわん曲部12に係止
する。
つぎに、第2図に示すように、このガラス管1
を両チヤツク2,3に装着したまま洗浄位置に送
り、この送りに連動したソレノイドバルブ41を
開放してガラス管1の上端面に対向したノズル4
2から管1内に洗浄水43を噴射する。このとき
ソレノイドバルブ41の作用によつてガラス管1
がノズル42に正対するまで、水43が噴射され
ることがなく、しかもノズル42の位置および構
造が適正になつているので、洗浄水43はガラス
管1の内面にのみ噴射され、外面に噴射されるこ
とがない。仮に、何んらかの理由によつて、小量
の洗浄水43が霧または滴となつて飛散したとし
ても、上側チヤツク2が板状をなしてガラス管1
の上側わん曲部11の周囲を覆つているので、こ
のチヤツク2に阻止されて霧や水滴がガラス管1
外面に付着することがない。
つぎに、第3図に示すように、このガラス管1
を前述の両チヤツク2,3に装着したまま乾燥位
置に送り、ガラス管1の上端面に対向したノズル
51から乾燥用空気52を管1内に吹込んで管1
内を乾燥させる。この乾燥工程はガラス管1内面
に残存した洗浄水43を減らすためになされるも
ので、後述するように完全乾燥は必ずしも必要な
く、したがつて乾燥用空気52の温度や風量につ
いては自由であり、さらに、乾燥した雰囲気中に
おいてはこの乾燥工程を全く消略してもよい。
つぎに、第4図に示すように、このガラス管1
を前述の両チヤツク2,3に装着したまま塗布位
置に送り、適宜な手段、たとえばガラス管1の上
端面からノズル61によつて無機微粉末のけん濁
液62を管1内面に噴射して均一に塗布する。こ
のけん濁液62はたとえばコロイダルアルミナと
称される粒径5〜30mμのγアルミア微粉末を純
水にけん濁したももので、この塗布により所望厚
さの均一な塗膜63が得られる。しかも、このけ
ん濁液62は溶媒が水であるので、塗布時、ガラ
ス管1内面に全面または局部的に多少の洗浄水4
3が残存していても、たんに回収されたけん濁液
62が薄くなるだけで格別な害はない。
つぎに、第5図に示すように、このガラス管1
を前述の両チヤツク2,3に装着したまま乾燥位
置に送り、ガラス管1の上端面に対向したノズル
71から加熱器72によつて後述する適温に加熱
された乾燥用空気73を管1内に吹込み、けん濁
塗膜63を乾燥させて保護膜8に形成する。この
とき、ガラス管1の外面は完全に乾燥しており、
かつチヤツク2,3が管1直線部にないので、従
来の外面が濡れた状態における乾燥方法と異り、
ガラス管1の局部的温度が均一で、したがつて、
塗膜63の乾燥速度が全面にわたり均一で、得ら
れた保護膜8も膜厚や粒径分布が均一である。
次に、第6図に示すように、この保護膜8上に
通常の方法によつて蛍光膜9を形成し、さらに蛍
光ランプに構成する。
このように、本実施例方法によれば、保護膜8
の膜厚や微粉末の粒径分布が均一であるので、得
られた蛍光ランプは点灯中の水銀付着による外観
不良が発生することなく、また短寿命もない。
また、無機微粉末けん濁液塗膜63の乾燥に際
し、乾燥用空気73の吹込み時間、風速および温
度が保護膜8の状態に大きな影響がある。この関
係の実験値を次表に示す。
[Technical Field of the Invention] The present invention relates to a method for manufacturing a fluorescent lamp, and more particularly to an improvement in the process of forming a protective film on the inner surface of a bulb. [Technical background of the invention and its problems] Conventionally, in the production of fluorescent lamps, both the inside and outside of the glass tube are washed with water to remove dust and other impurities, and after drying, a phosphor suspension is applied to the inside of the glass tube. A fluorescent film was formed by applying a liquid, drying it, and baking it. In recent years, in order to protect the phosphor from the alkaline components in the glass, a protective film made of inorganic fine powder such as alumina or silica has been formed on the inner surface of the glass tube.
A fluorescent film is now formed on this protective film. In this case, when cleaning the glass tube, the holding method,
If the cleaning method and drying method were to be operated without any restrictions as before, the resulting protective film would be in very poor condition, and the film thickness would often be uneven due to uneven drying. When lamps with a protective film are lit, mercury adheres to uneven areas, creating thin band-like patterns, which not only spoils the appearance but also shortens the lamp's lifespan. [Object of the Invention] The present invention forms a uniform protective film and forms a fluorescent film on it in industrial assembly line operations, thereby preventing contamination of the protective film by mercury and shortening due to uneven thickness of the protective film. The purpose of the present invention is to provide a method for manufacturing a fluorescent lamp that has no lifetime. [Summary of the invention] A glass tube is oriented vertically and supported at both ends, the inner surface of the tube is washed with water without wetting the outer surface, and then a suspension of inorganic fine powder is applied to the inner surface to form a protective film. This is a method of uniformly drying the suspension to obtain a uniform protective film. [Embodiments of the Invention] The inventor investigated the reason why the protective film is formed non-uniformly and found that the reason is local non-uniformity in the temperature of the glass tube during drying, and that the cause is heat conduction to the chuck. It was discovered that this was caused by the heat of evaporation of the washing water locally remaining on the outer surface of the glass tube.
We succeeded in eliminating the cause of the defect by improving the chuck position and cleaning method. Hereinafter, details of the present invention will be explained with reference to illustrated embodiments. The glass tube used in this example has a straight tube shape as shown in FIG. 1, and both ends are baked and rounded and curved slightly inward. First, as shown in FIG. 1, the glass tube 1 is turned vertically and the curved part 11 at the upper end is inserted into the receiving hole 21 of the plate-shaped upper chuck 2, and the L-shaped lower chuck 3 is inserted into the spring. 31 to lock the locking claw 32 to the curved portion 12 at the lower end of the glass tube 1. Next, as shown in Fig. 2, this glass tube 1
The solenoid valve 41 linked to this feeding is opened, and the nozzle 4 facing the upper end surface of the glass tube 1 is sent to the cleaning position while being attached to both chucks 2 and 3.
Cleaning water 43 is injected into the pipe 1 from 2. At this time, by the action of the solenoid valve 41, the glass tube 1
Since the water 43 is not sprayed until the glass tube 1 directly faces the nozzle 42, and the position and structure of the nozzle 42 are appropriate, the cleaning water 43 is sprayed only onto the inner surface of the glass tube 1, and is sprayed onto the outer surface. never be done. Even if for some reason a small amount of cleaning water 43 becomes mist or drops and scatters, the upper chuck 2 will form a plate shape and the glass tube 1
Since it covers the upper curved part 11, the chuck 2 prevents fog and water droplets from flowing into the glass tube 1.
Will not adhere to external surfaces. Next, as shown in Fig. 3, this glass tube 1
is sent to the drying position while attached to both chucks 2 and 3, and drying air 52 is blown into the tube 1 from the nozzle 51 facing the upper end surface of the glass tube 1.
Dry inside. This drying process is performed to reduce the cleaning water 43 remaining on the inner surface of the glass tube 1, and as will be described later, complete drying is not necessarily necessary, so the temperature and air volume of the drying air 52 can be freely adjusted. Furthermore, in a dry atmosphere, this drying step may be completely omitted. Next, as shown in FIG.
is attached to both the chucks 2 and 3 mentioned above, and sent to the coating position, and a suspension 62 of inorganic fine powder is injected onto the inner surface of the tube 1 using an appropriate means, for example, a nozzle 61 from the upper end surface of the glass tube 1. Apply evenly. This suspension 62 is, for example, a suspension of fine gamma alumia powder called colloidal alumina with a particle size of 5 to 30 mμ in pure water, and by applying this suspension a uniform coating film 63 of a desired thickness can be obtained. Moreover, since the solvent of this suspension 62 is water, some amount of cleaning water 4 is applied to the inner surface of the glass tube 1 on the entire surface or locally during application.
Even if 3 remains, there is no particular harm as the recovered suspension 62 will simply become diluted. Next, as shown in FIG.
are sent to the drying position while attached to both chucks 2 and 3, and drying air 73 heated to an appropriate temperature (described later) by a heater 72 is introduced into the tube 1 from a nozzle 71 facing the upper end surface of the glass tube 1. The suspended coating film 63 is dried to form the protective film 8. At this time, the outer surface of the glass tube 1 is completely dry.
In addition, since the chucks 2 and 3 are not on the straight part of the tube 1, unlike the conventional drying method in which the outer surface is wet,
The local temperature of the glass tube 1 is uniform and therefore
The drying rate of the coating film 63 is uniform over the entire surface, and the obtained protective film 8 is also uniform in film thickness and particle size distribution. Next, as shown in FIG. 6, a fluorescent film 9 is formed on the protective film 8 by a conventional method, and a fluorescent lamp is further constructed. As described above, according to the method of this embodiment, the protective film 8
Since the film thickness and the particle size distribution of the fine powder are uniform, the obtained fluorescent lamp does not suffer from poor appearance due to mercury adhesion during lighting and does not have a short life. Further, when drying the inorganic fine powder suspension coating film 63, the blowing time, wind speed, and temperature of the drying air 73 have a large effect on the state of the protective film 8. The experimental values for this relationship are shown in the table below.
本発明の蛍光ランプの製造方法はガラス管を上
下方向にして両端で支持し、ガラス管の外面を濡
らすことなく内面を水で洗浄し、ついでガラス管
内面に無機微粉末のけん濁液を塗布し乾燥させて
保護膜を形成し、この保護膜上に蛍光膜を形成し
たので、けん濁液の乾燥に際しガラス管外面が乾
燥状態にあるので従来のような外面乾燥に伴なう
ガラス管の局部的温度不均一がなく、また直線部
にチヤツクが当接していないので伝導による局部
冷却もないので、けん濁液塗膜の乾燥が均一で、
膜厚や粒径分布の不均一がなく、したがつてこれ
に起因する蛍光ランプの外観不良や短寿命がなく
なつた。
The method for manufacturing a fluorescent lamp of the present invention involves supporting a glass tube vertically at both ends, washing the inner surface with water without wetting the outer surface of the glass tube, and then applying a suspension of inorganic fine powder to the inner surface of the glass tube. By drying the suspension, a protective film is formed, and a fluorescent film is formed on this protective film.The outer surface of the glass tube is in a dry state when the suspension is dried. There is no local temperature unevenness, and since the chuck is not in contact with a straight section, there is no local cooling due to conduction, so the suspension coating film dries uniformly.
There is no non-uniformity in film thickness or particle size distribution, and therefore the poor appearance and short life of fluorescent lamps caused by this are eliminated.
第1図ないし第6図は本発明の蛍光ランプの製
造方法の一実施例を工程順に示す説明図である。
1…ガラス管、2,3…チヤツク、43…洗浄
水、52,73…乾燥用空気、62…けん濁液、
63…塗膜、8…保護膜、9…蛍光膜。
1 to 6 are explanatory drawings showing one embodiment of the method for manufacturing a fluorescent lamp of the present invention in the order of steps. 1...Glass tube, 2, 3...Chuck, 43...Washing water, 52,73...Drying air, 62...Suspension liquid,
63... Paint film, 8... Protective film, 9... Fluorescent film.
Claims (1)
で支持し、上記ガラス管の外面を濡らすことなく
内面を水で洗浄し、ついで上記ガラス管内面に無
機微粉末のけん濁液を塗布し乾燥させて保護膜を
形成し、この保護膜上に蛍光膜を形成することを
特徴とする蛍光ランプの製造方法。1. Support a glass tube for a fluorescent lamp vertically at both ends, wash the inner surface of the glass tube with water without wetting the outer surface, and then apply a suspension of inorganic fine powder to the inner surface of the glass tube and dry it. 1. A method for manufacturing a fluorescent lamp, comprising: forming a protective film on the protective film; and forming a fluorescent film on the protective film.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP26005384A JPS61138428A (en) | 1984-12-11 | 1984-12-11 | Manufacture of fluorescent lamp |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP26005384A JPS61138428A (en) | 1984-12-11 | 1984-12-11 | Manufacture of fluorescent lamp |
Publications (2)
Publication Number | Publication Date |
---|---|
JPS61138428A JPS61138428A (en) | 1986-06-25 |
JPH0412579B2 true JPH0412579B2 (en) | 1992-03-05 |
Family
ID=17342647
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP26005384A Granted JPS61138428A (en) | 1984-12-11 | 1984-12-11 | Manufacture of fluorescent lamp |
Country Status (1)
Country | Link |
---|---|
JP (1) | JPS61138428A (en) |
Families Citing this family (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP2702722B2 (en) * | 1987-10-22 | 1998-01-26 | 松下電子工業株式会社 | Manufacturing method of fluorescent lamp |
JP2699556B2 (en) * | 1989-06-19 | 1998-01-19 | 三菱電機株式会社 | Method for forming protective film of discharge lamp |
-
1984
- 1984-12-11 JP JP26005384A patent/JPS61138428A/en active Granted
Also Published As
Publication number | Publication date |
---|---|
JPS61138428A (en) | 1986-06-25 |
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