JPH0327902A - Manufacture of composite timber using water vapor explosion - Google Patents
Manufacture of composite timber using water vapor explosionInfo
- Publication number
- JPH0327902A JPH0327902A JP16478989A JP16478989A JPH0327902A JP H0327902 A JPH0327902 A JP H0327902A JP 16478989 A JP16478989 A JP 16478989A JP 16478989 A JP16478989 A JP 16478989A JP H0327902 A JPH0327902 A JP H0327902A
- Authority
- JP
- Japan
- Prior art keywords
- wood
- pressure
- timber
- steam
- water vapor
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 title claims abstract description 35
- 238000004880 explosion Methods 0.000 title claims abstract description 21
- 239000002131 composite material Substances 0.000 title claims abstract description 10
- 238000004519 manufacturing process Methods 0.000 title claims description 4
- 238000002347 injection Methods 0.000 claims abstract description 16
- 239000007924 injection Substances 0.000 claims abstract description 16
- 239000000126 substance Substances 0.000 claims abstract description 15
- 238000000034 method Methods 0.000 claims abstract description 14
- 229920006395 saturated elastomer Polymers 0.000 claims abstract description 14
- 239000011347 resin Substances 0.000 claims abstract description 7
- 229920005989 resin Polymers 0.000 claims abstract description 7
- 239000002023 wood Substances 0.000 claims description 67
- 238000001256 steam distillation Methods 0.000 claims description 6
- 238000010438 heat treatment Methods 0.000 abstract description 3
- 238000004821 distillation Methods 0.000 abstract 1
- 238000011282 treatment Methods 0.000 description 5
- 239000011148 porous material Substances 0.000 description 4
- 238000001035 drying Methods 0.000 description 3
- 230000006378 damage Effects 0.000 description 2
- 206010011732 Cyst Diseases 0.000 description 1
- 235000008708 Morus alba Nutrition 0.000 description 1
- 240000000249 Morus alba Species 0.000 description 1
- 238000013019 agitation Methods 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000000903 blocking effect Effects 0.000 description 1
- 239000013043 chemical agent Substances 0.000 description 1
- 238000005336 cracking Methods 0.000 description 1
- 208000031513 cyst Diseases 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- 238000005238 degreasing Methods 0.000 description 1
- 230000002542 deteriorative effect Effects 0.000 description 1
- 238000000635 electron micrograph Methods 0.000 description 1
- 239000003517 fume Substances 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 238000002844 melting Methods 0.000 description 1
- 230000008018 melting Effects 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 239000004071 soot Substances 0.000 description 1
- 241000894007 species Species 0.000 description 1
- 230000000638 stimulation Effects 0.000 description 1
- 239000010875 treated wood Substances 0.000 description 1
Landscapes
- Chemical And Physical Treatments For Wood And The Like (AREA)
Abstract
Description
【発明の詳細な説明】
本頴は、化学桑品の注入I!Ifiであった木材に、水
ぶ気蒸留と水蒸気爆発を用いて作られた新しい注入ルー
トを作くり、化学薬品の冫1人を容功にさせて、化学薬
品と木材との複合木+4の製iΔを容易にさせることに
関するものである.
始めに、本願は、特j’F 9 2 5 ] 5 2
1 IV.F木4イの割れ防止法」、持詐1 0 6
5 3 8 6 ’木材の1色法」、特i129778
4 r木材乾燥法」、特371315521}1jfl
生$4 ノjb liE及び1u11法J特詐1380
370 I木材の水蒸気蒸留による脱脂処理法」、特許
1 3 9 1 4 6 1 ’加圧瓜動滅圧乾燥機と
その方法」より発展した扶術開発であることを、明記し
ておく.
従来からI》る・木材注入法では、木材に化?条品を1
1人しようとしても、木材の辺周部を除いて、z1一人
できる注入法はない.その理山は、木tイ内に樹脂と言
う障゛,9物が7f在していること、樹木が成長してい
くにつれて、樹木の辺周を陥けば.細胞腔の出口に島た
る紋孔や毛細管が小さくなってゆくこと、細胞腔が袋状
になっていること等によりて、lL人が困難になってい
る.このために、大然の状Bでなく、木材の強度を劣化
させることなくして、注入を容易にならしめるための、
新しい注入ルートを人工的に作る必要がある.
注入や木材の内部温度の均一にすることを、困難にして
いる樹脂の除去については、通常の飽和蒸気処理と減圧
を用いる方法や薬品処理ではできないことは、前記の特
許に明記されており、木材の全体から,その障害となっ
ている樹脂の除去法について、水蒸気蒸留の必要なこと
は、上記の特許に記載されている.そして、注入を困難
にしているW1繍な毛細管や、細胞腔の出口にあたる紋
孔を拡大させる工法も、上記の特許に記叙されている.
しかし、これだけでは、注入しラる化学薬品の[111
は限定され、とても、化学薬品と木材との複合木材を作
ることはできない.
それを打開するために、微細な毛細管や細胞腔壁を,木
材の強度低下させない小規模の破壊をさせる必要がある
.この破壊を発生させるために、外部からの圧力を利用
することでは,それ等を圧縮するだけで、破壊すること
はできない.それ等を破壊するためには、その内部の圧
力を急上昇させることによって蛤めて可能となる.
大正年間に会津磐梯山が爆発したのや、ソ連の原始力発
電所が煤発したのも、水蒸気爆発によるものである.こ
の水蒸気爆発を、木材内で制御しうる状態にして起こさ
せることができれば、化学薬品の木材内への均一な注入
ルートが新しく作られ、化学薬品と木材との複合木材の
生産方法の道が+mかれる.
木材内の温度を均一にlOO度以上に加熱する工法は、
上記の特許に明記されている.木材内には、始めから水
を含右しているため,圧力容器内で、圧力を上昇させて
から、木材の温度を100度以上のなるべく高い64に
加熱してから、その圧力を急速に低下させると、木材内
にあった含有水は急激に沸騰し、水蒸気となり木材の内
部は、使用に耐えない程の水蒸気爆発がおきる.水蒸気
爆発がおきる現象において、水蒸気爆発が起きない状態
と,大水蒸気爆発の間に,0の次は無限と言う数字の配
列はないのと同様に、小規模の水蒸気煽発と言うものが
存在しなくてはならない.その小規模の水蒸気爆発が可
能にする方法を次に示すことにする.
住力容器内の圧力変化を少なくすれば、水蒸気爆発の規
模が小さくなるのは明らかであるが、木材内に部分的に
、樹脂が存在していたり、毛細管に極めて小さいものが
あったり、細胞腔の出口の紋孔が極めて小さいければ、
その部分のみに水蒸気爆発が大となり、他の部分に水蒸
気爆発が起こらないので、木材に化学薬品を注入すれば
、その薬^ムが注入している所と、注入していない所が
生じて、均一な複合木材とはならない.そのため,木材
全体に均一に小規模の水蒸気爆発をおこさせる様に,あ
らかじめ不均−な水蒸気爆発が起きる原因を餘去してお
かないと、均一な複合木材は作ることはできない.
ルカ容器に木材を入れ扉を閉じてがら、ボイラーよりの
高圧蒸気を容器内に注入し,約0 5〜0.7kgGの
範囲の変動圧力を加えて、木材の湿度を高温にならし、
次いで約1.0〜0.7kgGの範囲を変動する圧力を
加えると、木材表面に発生する結露水が、圧力上昇中に
木材の中心に肉かって押し込まれ、当初から木材内にあ
った含イf水は,圧力が減少して行く時、木材の表面に
向かって押し出す現象が生じる.これ等の新旧の水の移
動により、木材内でk4流が起きることが無いために、
新旧の水の混合が起きなかったのが、新旧の水の混合が
可能となり,木材内の水の温度の均一となって、木材の
軍さの如何にかかわらず,木材内の温度は均一となる.
そして,加圧された蒸気で処理されているため、圧力容
器内の木材の位lに関係無く、木材の厚さに比例した飽
和蒸気の変動加圧処理時間で、全木材内の温度は均一と
なる.その処理時間が過ぎれば,圧力容器内の飽和蒸気
を放出し、容器を密1利し、真空ポンプを用いて.’#
器内の圧力を大気圧以下に減圧する.この様にすれば,
木材内の全含イf水は均一に沸胱して、含ノ1水の移動
を妨げていた全Ill脂I』水蒸気蒸留により化学分解
して餘去される.そして,加圧していた飽和蒸気の放出
スピードの変化で,木材内の水の移動を困難にしていた
、極めて細い毛細管や紋孔の拡大現象も生じさせうる.
これ等の事IQは上記の特許に配載されている.
この一連の処理で、全細胞腔の水の全量を水蒸気に転換
させうるエネルギーを与えることはできないことは、処
理後の木材を零下20度以下で、全含イ1水を結氷させ
てから、試験片を作り、電子顕微鏡にてM胞腔を撮影す
ると、水が無くなっている所は、思<写り、水が残って
いる所は白く写る.この電子顕wi鏡写真で、全細胞腔
に均一に水が残っていることが確認できる.この全細胞
腔に均一に残っている水をエネルギーに替える方法が見
付かれば、注入を困難にしている繍胞腔や微細な毛細管
の、それぞれの壁面に対して、水蒸気煽発による迅裂が
つけられ、新しい注入ルートが現出することとなる.
次に、この細胞腔に均一に残された水を、エネルギーに
替える方法を記載する.変動する飽和蒸気圧を用いた加
圧加熱してから、大気圧以下の減圧処理した木材を、圧
力容器に入れたまま、容器内に高圧蒸気を噴射して、大
気圧以上の約1.0kgGの所定の圧力まで圧力を上昇
させてから、木材内の温度が均一になるまでの、木材の
11さに比例した時間のjL飽和蒸気の圧力を約1.0
〜0.7kgGの間を頻繁に変動させる.そのt1vA
Nにより、飽和蒸気圧を更に高めて圧力を変動させて、
木材内の温度を高める方が良い場合もあり,又、変動し
ている圧力をそのまま維持して、加圧加熟している飽和
蒸気を加熱蒸気に変えて、木材内の温度を高めて行く方
が良い結果が択られる場合もある.この温度上昇と、そ
れ等の温度−L昇後の均一温度にする時間は、樹種によ
り異なるも,VA脂が餘去されていることや、極めて細
い毛細管や紋孔が拡大されていることとにより、前述の
6Pに記載している木材内部温度を均一にする時間より
も甚しく短い.そして、上昇させる木材内の均一温度は
、1.0kgGの蒸気温度に比例した温度より、約lO
度以上の温度にする方が、より有益な結果がえられ易い
.
この木材内部のより高い温度にしてから、飽和蒸気又は
加熱蒸気の注入を停止し、圧力容器の下についているバ
ルブより、圧力容器内の蒸気及びドレン水を放出して、
最高時の圧力より、圧力を0.4〜0.7kgGの範囲
の急速な圧力低下させると,残留していた各細胞腔内の
含有水は急激にf#騰して水蒸気に替り,木材内の繕胞
腔や極めて細い毛細管のある所のみで水蒸気爆発が起き
るが、この範囲での水蒸気煽発ては、木材が使用に耐え
ない程の爆発とならず,注入を困難にしていた細l1腔
や毛細管の壁面の亀裂だけで済む水蒸気爆発゛となり、
新しい注入ルートが人工的に作りうる様になった.
かくして、水蒸気蒸留で処理した木材内で、小規模の水
蒸気燻発を無数に発生させうることの発見により、人工
的に作られた注入ルートで化学薬品の注入が容易になっ
て、無数に考えられる、化学薬品と木材との複合木材の
開発しうる道が開がれることとなった.そして、この工
法を利用することにより、この処理後の木材乾燥のスピ
ードが甚しく速くなることは言うまでもない.泉
兵 五[Detailed Description of the Invention] This product is a chemical mulberry injection I! A new injection route was created using hydrodistillation and steam explosion in the wood that was Ifi, and one of the chemical agents was made to have good luck, and a composite tree of chemicals and wood + 4 was created. This is related to facilitating the production of iΔ. At the outset, this application specifies that
1 IV. ``How to prevent cracking of F wood 4 I'', Possessor fraud 1 0 6
5 3 8 6 'One color method for wood', special i129778
4r wood drying method”, special 371315521}1jfl
Raw $4 Nojb liE and 1u11 law J special fraud 1380
It should be clearly stated that this is a Fujutsu development developed from ``370 I Method for Degreasing Wood by Steam Distillation'' and Patent 1 39 1 4 6 1 ``Pressure Melting Pressure Drying Machine and Its Method.'' Does the conventional wood injection method convert it into wood? 1 item
Even if one person tries it, there is no injection method that can be done by one person except for the edges of the wood. The reason for this is that there are 9 obstacles called resin inside the tree, and as the tree grows, it will cause damage to the surrounding area of the tree. It is difficult to carry out LL due to the fact that the pores and capillaries that are islands at the exit of the cell cavity become smaller and the cell cavity becomes bag-shaped. For this reason, instead of the natural condition B, in order to make the injection easier without deteriorating the strength of the wood,
It is necessary to artificially create a new injection route. The above-mentioned patent clearly states that the removal of the resin, which makes it difficult to inject and equalize the internal temperature of the wood, cannot be done by ordinary methods using saturated steam treatment and reduced pressure, or by chemical treatment. The above-mentioned patent describes the necessity of steam distillation as a method for removing the resin that is an obstacle from the whole wood. The above-mentioned patent also describes a method of enlarging the W1-shaped capillaries that make injection difficult and the pores that serve as the exits of cell cavities.
However, this alone is insufficient for the [111
However, it is not possible to create a composite wood using chemicals and wood. To overcome this problem, it is necessary to destroy the microscopic capillaries and cell cavity walls on a small scale without reducing the strength of the wood. Using external pressure to cause this destruction only compresses them, but does not destroy them. In order to destroy them, it is possible to rapidly increase the pressure inside them. The explosion of Mt. Aizu Bandai in the Taisho era and the soot emitted from the Soviet Union's primitive power plants were also caused by steam explosions. If this steam explosion can be caused within the wood in a controllable manner, a new route for uniformly injecting chemicals into the wood will be created, paving the way for the production of composite wood with chemicals and wood. +m is lost. The method of uniformly heating the inside of wood to over 100 degrees is
This is clearly stated in the above patent. Since the wood contains water from the beginning, the pressure is increased in the pressure vessel, the temperature of the wood is heated to 100 degrees or higher, as high as possible, and then the pressure is rapidly reduced. When the temperature is lowered, the water contained within the wood rapidly boils and turns into water vapor, causing a steam explosion inside the wood that is unusable. In the phenomenon of phreatic explosions, just as there is no sequence of numbers that are infinite after 0 between the state where phreatic explosions do not occur and the large phreatic explosions, there is something called small-scale phreatic instigation. I have to. The method by which this small-scale steam explosion is possible will be shown below. It is obvious that the scale of the steam explosion will be reduced by reducing the pressure change inside the vessel, but if resin is partially present in the wood, there are extremely small capillaries, or cells are If the foramen at the exit of the cavity is extremely small,
The steam explosion will be large only in that area and not in other parts, so if you inject a chemical into the wood, there will be areas where the chemical is injected and areas where it is not. , it does not result in a uniform composite wood. Therefore, uniform composite wood cannot be produced unless the causes of uneven steam explosions are eliminated in advance so that small-scale steam explosions occur uniformly throughout the wood. Place the wood in a container and close the door, then inject high-pressure steam from the boiler into the container and apply a fluctuating pressure in the range of about 0.5 to 0.7 kgG to normalize the humidity of the wood to a high temperature.
Next, when a pressure varying in the range of approximately 1.0 to 0.7 kgG is applied, the condensed water that forms on the wood surface is forced into the center of the wood while the pressure increases, removing the impurities that were present in the wood from the beginning. f When the pressure decreases, a phenomenon occurs in which water is pushed toward the surface of the wood. Because this movement of water between old and new water does not cause K4 flow within the wood,
Previously, mixing of old and new water did not occur, but now it is possible to mix old and new water, and the temperature of the water inside the wood becomes uniform, so regardless of the strength of the wood, the temperature inside the wood is uniform. Become.
Since it is treated with pressurized steam, the temperature inside all the wood is uniform regardless of the position of the wood in the pressure vessel, and the pressure treatment time of the saturated steam fluctuates in proportion to the thickness of the wood. becomes. After the processing time has elapsed, the saturated steam inside the pressure vessel is released, the vessel is sealed tightly, and a vacuum pump is used to release the saturated steam inside the pressure vessel. '#
Reduce the pressure inside the vessel to below atmospheric pressure. If you do it like this,
All of the water contained in the wood boils uniformly, and all of the fat that was blocking the movement of water is chemically decomposed and removed by steam distillation. Additionally, changes in the release speed of pressurized saturated steam can cause the extremely thin capillaries and pores that make it difficult for water to move through the wood to expand.
These matters IQ are published in the above patent. The fact that this series of treatments cannot provide enough energy to convert the entire amount of water in all cell cavities into water vapor is that the treated wood is frozen at -20 degrees Celsius or below to freeze the entire water content. When a test piece is made and the M cell cavity is photographed using an electron microscope, the areas where water has disappeared will be visible, and the areas where water remains will appear white. This electron micrograph shows that water remains uniformly in all cell cavities. If we could find a way to convert the water that remains uniformly in all cell cavities into energy, we would be able to generate rapid rupture by steam stimulation on the walls of the cyst cavities and minute capillaries, which make injection difficult. is added, and a new injection route appears. Next, we will describe a method to convert the water uniformly left in the cell cavity into energy. After pressurizing and heating the wood using fluctuating saturated steam pressure, the wood is depressurized below atmospheric pressure, and while it is placed in a pressure vessel, high pressure steam is injected into the vessel to produce approximately 1.0 kg of pressure above atmospheric pressure. After increasing the pressure to a predetermined pressure of , until the temperature inside the wood becomes uniform, the pressure of jL saturated steam is approximately 1.0.
Frequently fluctuate between ~0.7 kgG. That t1vA
By using N, the saturated vapor pressure is further increased and the pressure is varied,
In some cases, it is better to raise the temperature inside the wood.Also, it is better to maintain the fluctuating pressure as it is and convert the pressurized and ripened saturated steam into heated steam to increase the temperature inside the wood. In some cases, the best result is selected. This temperature rise and the time it takes to reach a uniform temperature after the temperature -L rises vary depending on the wood species, but it is important to note that the VA fat is removed and the extremely thin capillaries and pores are enlarged. Therefore, the time required to equalize the internal temperature of the wood is much shorter than the time described in 6P above. The uniform temperature within the wood to be raised is approximately 1O
It is easier to obtain more beneficial results if the temperature is higher than 30°F. After the temperature inside the wood reaches a higher temperature, the injection of saturated steam or heated steam is stopped, and the steam and drain water inside the pressure vessel are released from the valve attached to the bottom of the pressure vessel.
When the pressure is rapidly reduced in the range of 0.4 to 0.7 kgG from the maximum pressure, the remaining water contained in each cell cavity rapidly rises to f# and turns into water vapor, causing the water inside the wood to rise. Steam explosions occur only in the stamen cavities and extremely thin capillaries, but steam agitation in these areas does not cause explosions that make the wood unusable; This results in a steam explosion that only causes cracks in the walls of cavities and capillaries.
New injection routes can now be created artificially. Thus, the discovery that numerous small-scale steam fumes can be generated in wood treated with steam distillation has facilitated the injection of chemicals through artificially created injection routes, leading to countless ideas. This paved the way for the development of composite wood made of chemicals and wood. It goes without saying that by using this method, the speed of wood drying after this treatment is greatly increased. fountain
Soldier 5
Claims (1)
せる飽和蒸気による加熱を行なつた後該容器内を減圧し
て該木材内の樹脂を水蒸気蒸留して除去すると同時に該
木材内の紋腔及び極めて細い毛細管を拡大させる現象を
起させた後、該木材を加熱蒸気又は高圧飽和蒸気による
加圧加熱を加えた後該圧力容器内の圧力を急激に低下さ
せて該木材の細胞腔内に残留している水を急激に水蒸気
に転換させて水蒸気爆発を起し、細胞腔及び極めて細い
毛細管を小規模に破壊して該木材に化学薬品の注入ルー
トを新しく作るための、水蒸気蒸留と水蒸気爆発を併用
して用いることを特徴とする化学薬品と木材との複合木
材の製造法。The wood contained in the pressure vessel is heated with saturated steam that varies the pressurization pressure, and then the pressure inside the vessel is reduced to remove the resin in the wood by steam distillation. After causing the phenomenon of enlarging the crest cavity and extremely thin capillaries, the wood is heated under pressure using heated steam or high-pressure saturated steam, and then the pressure in the pressure vessel is rapidly reduced to expand the cell cavities of the wood. Steam distillation is a process that rapidly converts the water remaining in the wood into steam, causing a steam explosion, destroying cell cavities and extremely thin capillaries on a small scale, and creating a new injection route for chemicals into the wood. A method for producing composite wood of chemicals and wood, characterized by using a combination of water vapor explosion and steam explosion.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP1164789A JP2518694B2 (en) | 1989-06-27 | 1989-06-27 | Production method of composite wood using steam explosion |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP1164789A JP2518694B2 (en) | 1989-06-27 | 1989-06-27 | Production method of composite wood using steam explosion |
Publications (2)
Publication Number | Publication Date |
---|---|
JPH0327902A true JPH0327902A (en) | 1991-02-06 |
JP2518694B2 JP2518694B2 (en) | 1996-07-24 |
Family
ID=15799972
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP1164789A Expired - Lifetime JP2518694B2 (en) | 1989-06-27 | 1989-06-27 | Production method of composite wood using steam explosion |
Country Status (1)
Country | Link |
---|---|
JP (1) | JP2518694B2 (en) |
Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS574706A (en) * | 1980-06-12 | 1982-01-11 | Hiyougo Izumi | Wood in which defect do not generate and its manufacture |
JPS57165206A (en) * | 1981-04-04 | 1982-10-12 | Hiyougo Izumi | Method of removing resin in resin bag |
-
1989
- 1989-06-27 JP JP1164789A patent/JP2518694B2/en not_active Expired - Lifetime
Patent Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS574706A (en) * | 1980-06-12 | 1982-01-11 | Hiyougo Izumi | Wood in which defect do not generate and its manufacture |
JPS57165206A (en) * | 1981-04-04 | 1982-10-12 | Hiyougo Izumi | Method of removing resin in resin bag |
Also Published As
Publication number | Publication date |
---|---|
JP2518694B2 (en) | 1996-07-24 |
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