JPH02501394A - Mechanical pulp manufacturing method - Google Patents

Mechanical pulp manufacturing method

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Publication number
JPH02501394A
JPH02501394A JP50683987A JP50683987A JPH02501394A JP H02501394 A JPH02501394 A JP H02501394A JP 50683987 A JP50683987 A JP 50683987A JP 50683987 A JP50683987 A JP 50683987A JP H02501394 A JPH02501394 A JP H02501394A
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piece
impregnation
liquid
steam
mechanical pulp
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Inventor
ビイーステツド,ホー・エス・インゲマール
セーリン,ヤーン‐ウーウルーウフ・ギユウンナール
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シユンドス・デフイブラトール・アクテイエボラーグ
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Classifications

    • DTEXTILES; PAPER
    • D21PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21BFIBROUS RAW MATERIALS OR THEIR MECHANICAL TREATMENT
    • D21B1/00Fibrous raw materials or their mechanical treatment
    • D21B1/04Fibrous raw materials or their mechanical treatment by dividing raw materials into small particles, e.g. fibres
    • DTEXTILES; PAPER
    • D21PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21BFIBROUS RAW MATERIALS OR THEIR MECHANICAL TREATMENT
    • D21B1/00Fibrous raw materials or their mechanical treatment
    • D21B1/04Fibrous raw materials or their mechanical treatment by dividing raw materials into small particles, e.g. fibres
    • D21B1/12Fibrous raw materials or their mechanical treatment by dividing raw materials into small particles, e.g. fibres by wet methods, by the use of steam
    • D21B1/14Disintegrating in mills

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  • Engineering & Computer Science (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Wood Science & Technology (AREA)
  • Mechanical Engineering (AREA)
  • Paper (AREA)
  • Reinforced Plastic Materials (AREA)
  • Chemical And Physical Treatments For Wood And The Like (AREA)

Abstract

(57)【要約】本公報は電子出願前の出願データであるため要約のデータは記録されません。 (57) [Summary] This bulletin contains application data before electronic filing, so abstract data is not recorded.

Description

【発明の詳細な説明】 本発明は、各種の紙及び厚紙等に使用する目的で、針葉樹。[Detailed description of the invention] The present invention uses coniferous trees for use in various papers, cardboards, etc.

広葉樹又はタケ類のようなリグノセルロース含有材料からなるメ ちニカル、サーモメカニカル及びケミメカニカルバルブを製造する方法に係る。Materials made from lignocellulose-containing materials such as hardwoods or bamboos. The present invention relates to a method for manufacturing mechanical, thermomechanical, and chemimechanical valves.

リファイニング法では、材料をチップに切削し、このチップを通常ディスクリフ ァイナに1〜2回、時には3回通してバルブに精砕する。この方法によって製造 されたバルブは、RMP(リッツイナーメカニカルバルブ)、TMP(サーモメ カニブJルパルブ)、GMP(ケミメカニカルバルブ)及びCTMP(ケミ−サ ーモメカニカルバルブ)に大別される。The refining process involves cutting the material into chips, which are usually disc-refined. It is passed through the finer once or twice, sometimes three times, to be refined into valves. manufactured by this method The valves are RMP (Ritziner Mechanical Valve) and TMP (Thermomechanical Valve). Kanib J Le Parve), GMP (Chemimechanical Valve) and CTMP (Chemisa -Momechanical valves).

RM P:未処理のチップを大気圧下で精砕する。RMP: Untreated chips are refined under atmospheric pressure.

TMP:蒸気処理したチップを過圧下で精砕する。TMP: Refining steam-treated chips under overpressure.

CMP:化学処理したチップを大気圧下で精砕する。CMP: Chemically treated chips are refined under atmospheric pressure.

CTMP:化学処理したチップを過圧トで蒸気中で精砕する。CTMP: Chemically treated chips are refined in steam under overpressure.

バルブは長Ill含有率が高く、優れた強度特性をもつ。しかしながら、エネル ギ消費台は高く、およそ2000KWh/バルブtである。長くかつ堅い繊維を 多く含むために、製紙機に6けるフォーミング(foriing)及び紙の平滑 度や光学特性がときどき不充分となる。The bulb has a high long Ill content and excellent strength properties. However, energy Energy consumption is high, approximately 2000KWh/bulb t. long and stiff fibers 6. Forming and smoothing of paper in paper making machine to increase the content. The power and optical properties are sometimes inadequate.

より旧式の摩砕法では、ブロック、即ち所定長に切断した丸太を水を供給しなが ら回転する砥石に圧着して砕木する。上記したソファイニング法によるバルブに 対応するバルブの種類は次の通りである。In older milling methods, blocks, or logs cut to length, are processed without water. The wood is crushed by pressing it against a rotating whetstone. For valves using the sofaning method described above. The corresponding valve types are as follows.

砕氷パルプ二未加工木材を大気圧下で砕木する。Crushed Ice Pulp 2 Raw wood is crushed under atmospheric pressure.

後者の変形方法として、ストックに薬品を含浸させ、オートクレーブ中で蒸解後 砕木する方法もある( u s p−,2,713,540)。As a variant of the latter method, the stock is impregnated with chemicals and then cooked in an autoclave. There is also a method of crushing wood (Usp-, 2,713,540).

五 砕氷バルブの場合、S繊維の含有率が精砕バルブより低い。Five In the case of ice-breaking valves, the content of S fibers is lower than in refining valves.

このため、強度特性は劣るが、フォーミング、平滑度及び光学特性は精砕バルブ に比べて優れている。エネルギ消!IIはかなり低く、およそ1000kWh/ バルブtである。1つの重大な欠点は、丸太素材を使用しなければならないこと である。For this reason, the strength characteristics are inferior, but the forming, smoothness and optical characteristics of the refined valve are inferior. is better than. Energy disappears! II is quite low, approximately 1000kWh/ This is valve t. One significant drawback is that log material must be used It is.

化学砕氷法によると、すぐれた強度特性をもつバルブが製造される。しかしなが ら、丸太の中心部が含浸されないため該中心部は蒸解しても黒いままであり、バ ルブのISO白色度は低く、バルブの漂白が困難である。従って、この方法は余 り広く使用されていない。The chemical ice crushing process produces valves with excellent strength properties. But long Since the center of the log is not impregnated, the center remains black even after cooking, and the The ISO brightness of the bulb is low, making it difficult to bleach the bulb. Therefore, this method It is not widely used.

本発明の目的は、高エネルギを消費する、強度が劣る、及び砕木時に丸太素材を 使用しなければならないという欠点のない方法を提供することにある。The purpose of the present invention is to eliminate the use of log materials that consume high energy, have poor strength, and The aim is to provide a method that does not have the disadvantages of having to use it.

上記した目的並びにその他の目的は添付した請求の範囲に規定される如き本発明 方法によって達成される。The above objects and other objects are achieved by the present invention as defined in the appended claims. achieved by the method.

添付のブロック図は本発明の1具体例を原理的に示す。The attached block diagram shows in principle one embodiment of the invention.

ジング材(edgiH)又はその他の以下に示す最小寸法をもつ\片である。A piece of edgi material (edgiH) or other material with the minimum dimensions shown below.

2で原料に重水スプレーして原料をきれいに洗滌し、砂及び他の不純物を除去す る。3で、原料を例えば横びき鋸によって、材を開裂して、最大50#R1好ま しくは最大25gの!線方向を横切る最小寸法をもつスティックにする。従って 、スティックはその幅が原料の横断方向寸法と同じようなリプの形態であり得る が、しかしその厚さは上記した寸法を超えない。開裂(cleaving)は各 種タイプの開裂HN、好ましくはm維を可能な限り完全のまま残すべくそのm線 構造に沿って木材を開裂する装置によって行われる。開裂の目的は後続の含浸作 業を容易にするためである。原料が例えば薄い背板又はエツジング材から構成さ れるときには、もちろん開裂工程を省略することができる。In Step 2, spray the raw material with heavy water to clean the raw material and remove sand and other impurities. Ru. In Step 3, the raw material is split into pieces, for example with a crosscut saw, and the material is cut into pieces with a maximum of 50 #R1 Or up to 25g! Make a stick with the smallest dimension across the line direction. Therefore , the stick can be in the form of a lip whose width is similar to the transverse dimension of the raw material However, its thickness does not exceed the dimensions mentioned above. Cleaving is for each Seed-type cleaved HN, preferably the m-fiber to leave it as intact as possible It is carried out by a device that splits the wood along the structure. The purpose of cleavage is the subsequent impregnation process. This is to make the work easier. If the raw material consists of e.g. a thin backing or an edging material, Of course, the cleavage step can be omitted when the cleavage process is carried out.

5で、スティックを大気圧もしくは低圧蒸気で加熱し、含浸を妨げる空気を除く 。6で、スティックに液を含浸させる。この液は水でも、薬品を含む水であって もよい。液は高油圧ポンプを用いて繊維材料にJf入される。Step 5: Heat the stick with atmospheric pressure or low-pressure steam to remove air that interferes with impregnation. . Step 6: Impregnate the stick with the liquid. This liquid may be water or water containing chemicals. Good too. The liquid is pumped into the textile material using a high hydraulic pump.

薬品は苛性ソーダのような塩基、亜硫酸ナトリウム、亜硫酸水素ナトリウムのよ うなアルカリ金属塩、又は過酸化物のような退化合物であり得る。例えば苛性ソ ーダと亜硫酸ナトリウム又は過酸化物との混合物を使用してもよい。含浸は異な る薬品を用いて2回以上行ってもよく、この場合余分の薬品を工程の間で除去す る。Chemicals include bases such as caustic soda, sodium sulfite, and sodium bisulfite. It can be an alkali metal salt, such as an alkali metal salt, or a decomposed compound, such as a peroxide. For example, caustic Mixtures of powder and sodium sulfite or peroxide may also be used. Impregnation is different The process may be carried out more than once using different chemicals, in which case the excess chemicals are removed between steps. Ru.

液体含浸すると、残留空気は木材から除去され、液に一換される。IlFは膨張 し、離解時のスラッシングを容易にするため度の優れたバルブが得られる。液等 の組成に従って強度隻変更させ得る。最も温和な効果は水だけを用いて得られ、 アルカリを用いると木材の半セルロースがよりf!張する。亜硫II塩又は次亜 硫酸塩を用いると、部分的にスルホン化し、リグニンが脱離する。アルカリによ る黄着色は過酸化物の作用を妨害し得る。During liquid impregnation, residual air is removed from the wood and replaced with liquid. IIF expands This allows for easy thrashing during disintegration, resulting in a valve with excellent strength. liquid etc. The strength can be varied according to the composition. The mildest effect is obtained using only water; When alkali is used, the semi-cellulose of wood becomes more f! Expand. sulfite II salt or hypochlorite When sulfate is used, partial sulfonation occurs and lignin is eliminated. Alkaline The yellow coloration can interfere with the action of peroxides.

薬品がより多く遊離すると、バルブ収量が低下し、光学特性は劣化し、薬品消費 量は多くなり、重大な環境問題をひきおこす。As more chemicals are liberated, bulb yields decrease, optical properties deteriorate, and chemical consumption increases. The amount is large and causes serious environmental problems.

従って薬品は注意深く計量する必要がある。Therefore, chemicals need to be measured carefully.

7で、含浸させたスティックを一定v1問、一定温度で薬品と反応させる。反応 は大気圧もしくは過圧下で液相又は蒸気相中で行われる。反応完了後、余分の液 を排出させる。8で、スティックを、水を供給しながら繊維を一定方向に配向さ せた状態で回転離解装置の表面に圧着するようにして離解する。従って、□、シ ゛7”L/”28盲t”こ°二゛ン08、□、6.。。In step 7, the impregnated stick is reacted with a chemical at a constant temperature for a constant v1 period. reaction is carried out in the liquid or vapor phase at atmospheric pressure or overpressure. After the reaction is complete, remove the excess liquid. to be discharged. At step 8, the stick is oriented in a certain direction while supplying water. The material is defibrated by pressing it against the surface of the rotary disintegrator while the product is being held in place. Therefore, □, ゛7"L/"28blindt"This second 08, □, 6...

運動方向はtian方向に垂直である、通常の例えば酸化アルミニウム又は炭化 けい素からなる鋭い固い粒子をセラミック結合剤で保持して形成された砥石を含 む砕氷機(可能ならば加圧された)が用いられ得る。砕氷機とその送り装置はブ ロックの代りにスティックの処理に適していなければならない。既存のブレス装 置、チェーン、スクリュー等は余り適切でない。圧力板によって木材を砕氷面に 押圧するポケット型装置は好ましい。The direction of motion is perpendicular to the tian direction, for example aluminum oxide or carbide Contains a grinding wheel made of sharp, hard particles made of silicon held together by a ceramic bond. An ice crusher (preferably pressurized) may be used. The ice crusher and its feeder are Must be suitable for handling sticks instead of locks. Existing bracelet Places, chains, screws, etc. are not very suitable. Pressure plate turns wood into ice crushing surface Pocket-type devices that press are preferred.

9で、離解後のバルブを取り出し、後続の処理、例えばスクリーニング、洗滌、 8j!白等の処理に付される。At step 9, the bulb after disintegration is taken out and subjected to subsequent processing, such as screening, washing, 8j! Subjected to white and other treatments.

勿論・その他の具体例を本発明の思想の範囲内で創案することができる。各工程 で、さまざまな連続及び不連続装置が使用され得る。3における横断裁を離解装 置に適した最終長さの2倍又は数倍長い木材が得られるように実施してもよく、 仕上りの横断裁を離解前に行ってもよい。Of course, other embodiments can be devised within the spirit of the invention. Each process A variety of continuous and discontinuous devices may be used. Disassembling the cross cutting in 3 It may be carried out to obtain wood that is twice or several times longer than the final length suitable for installation. A final crosscut may be performed before disaggregation.

5の蒸気加熱工程を省略するか又は例えば真空蒸発に変えてもよい、7における 反応を省略することもできる。その他の形式の難解装置を用い章±ることもでき る。例えば離解ディスクの平表面に対して1解を行うことができる。離解表面を 他の材料例えば鋼及び結合(cesented)炭化物で構成することもで、き イ メカニカルパルブ:所要により蒸気加熱し、水に含浸し、大気圧下で!!lji する。The steam heating step in step 5 may be omitted or replaced with e.g. vacuum evaporation, in step 7. The reaction can also be omitted. It is also possible to use other types of esoteric devices. Ru. For example, one solution can be performed on the flat surface of a disintegrating disk. Disintegration surface It may also be constructed of other materials such as steel and cemented carbides. stomach Mechanical valve: Steam heated as required, impregnated with water, and under atmospheric pressure! ! lji do.

サーモメカニカルバルブ二所要により蒸気加熱し、薬品に含浸し、所要により蒸 解し、蒸気肚下で 離解する。Two thermomechanical valves are heated with steam as required, impregnated with chemicals, and steamed as required. Under the steam disintegrate.

ケミメカニカルパルプ二W&気加熱し、薬品に含浸し、所要により蒸解し、大気 圧下で離解する。Chemi-mechanical pulp is heated twice, impregnated with chemicals, digested if necessary, and released into the atmosphere. Disintegrates under pressure.

ケミ−サーモメカニカルバルブ:蒸気処理し、薬品に含浸し、所要により蒸解し 、蒸気圧下で離解 その他の変更例も本発明の思想の範囲内で思案することができる。Chemi-thermomechanical valve: Steam treated, impregnated with chemicals, and if necessary cooked. , disintegrated under steam pressure Other modifications may also be envisaged within the spirit of the invention.

! 補 正 請 求 の 範 1.繊維を接線プレス表面と同じ平面に配向させかつ表面を好ましくは繊維方向 に垂直に動かしながら材料を回転離解部材に対して押圧して離解させることから なる少なくとも200a+の繊維方向長さをもつ断片状のリグノセルロース含有 材料からなるメカニカルパルプを製造する方法であって、まず材料の繊維構造に 沿って開裂させることにより材料片の厚さを最大50awの繊2、材料片を含浸 の直前に蒸気処理することを特徴とする請求の範囲1に記載の方法。! Scope of request for correction 1. The fibers are oriented in the same plane as the tangential press surface and the surface is preferably in the fiber direction. The material is pressed against a rotating disintegrating member while moving perpendicularly to the disintegrating member. containing fragmented lignocellulose having a length in the fiber direction of at least 200a+ A method for producing mechanical pulp made of materials, in which the fiber structure of the material is first The thickness of the material piece can be increased up to 50 aw by splitting it along the fibers2, impregnating the material piece. 2. A method according to claim 1, characterized in that the method is steam-treated immediately before.

3、含浸が数回の工程で異なる含浸液を用いて実施されることを特徴とする請求 の範囲1又は2に記載の方法。3. A claim characterized in that the impregnation is carried out in several steps using different impregnating liquids. The method according to scope 1 or 2.

4、含浸と離解との間に材料片を蒸気相又は油相中過圧下で蒸解させることを特 徴とする請求の範囲1〜3のいずれかに記載の方法。4. Between impregnation and disintegration, the material pieces are cooked under superpressure in a vapor phase or an oil phase. The method according to any one of claims 1 to 3, characterized in that:

国際調査報告 or〒zcrQ7/nnaqainternational search report or〒zcrQ7/nnaqa

Claims (5)

【特許請求の範囲】[Claims] 1.液体を供給しながら材料を回転離解部材に対して押圧して離解させることか らなる少なくとも200mmの繊維方向長さをもつ断片状のリグノセルロース含 有材料からなるメカニカルパルプを製造する方法であって、ます材料片の厚さを 最大50mmの繊維方向を横切る最小寸法に減少させ、材料片に液体を含浸させ その後離解を行うことを特徴とする方法。1. Pressing the material against a rotating disintegrating member while supplying liquid to disintegrate it fragmented lignocellulose-containing material having a length in the fiber direction of at least 200 mm. A method for producing mechanical pulp made of organic material, in which the thickness of a piece of material is Reduced to a minimum dimension transverse to the fiber direction of up to 50 mm and impregnated the piece of material with liquid. A method characterized by subsequently performing disaggregation. 2.材料片の厚さを材料の繊維構造に沿って開裂させることによって減らすこと を特徴とする請求の範囲1に記載の方法。2. reducing the thickness of a piece of material by cleaving it along the fibrous structure of the material The method according to claim 1, characterized in that: 3.材料片を含浸の直前に蒸気処理することを特徴とする請求の範囲1又は2に 記載の方法。3. According to claim 1 or 2, characterized in that the piece of material is steam-treated immediately before impregnation. Method described. 4.含浸が数回の工程で異なる含浸液を用いて実施されることを特徴とする請求 の範囲1〜3のいずれかに記載の方法。 ヰ4. Claim characterized in that the impregnation is carried out in several steps with different impregnating liquids The method according to any one of ranges 1 to 3. ヰ 5.含浸と離解との間に材料片を蒸気相又は液相中過圧下で蒸解させることを特 徴とする請求の範囲1〜4のいずれかに記載の方法。5. During impregnation and disintegration, the material pieces are cooked under superpressure in the vapor phase or in the liquid phase. 5. The method according to any one of claims 1 to 4, characterized in that:
JP50683987A 1986-11-06 1987-10-27 Mechanical pulp manufacturing method Pending JPH02501394A (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
SE8604769-3 1986-11-06
SE8604769A SE458690B (en) 1986-11-06 1986-11-06 MAKE MANUFACTURING MECHANICAL MASS FROM LIGNOCELLULOSALLY MATERIAL IN PIECE FORM WITH A LENGTH IN THE FIBER DIRECTION OF AT LEAST 200 MM

Publications (1)

Publication Number Publication Date
JPH02501394A true JPH02501394A (en) 1990-05-17

Family

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Family Applications (1)

Application Number Title Priority Date Filing Date
JP50683987A Pending JPH02501394A (en) 1986-11-06 1987-10-27 Mechanical pulp manufacturing method

Country Status (7)

Country Link
EP (1) EP0329694A1 (en)
JP (1) JPH02501394A (en)
AU (1) AU8233887A (en)
FI (1) FI892152A0 (en)
NZ (1) NZ222448A (en)
SE (1) SE458690B (en)
WO (1) WO1988003581A1 (en)

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FI126694B (en) * 2005-12-02 2017-04-13 Metsä Board Oyj Chemical-mechanical pulp and process for producing chemical-mechanical pulp

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DE3676490D1 (en) * 1985-09-20 1991-02-07 Scott Paper Co PULP PRE-TREATMENT PROCESS WITH STABILIZING AGENTS AND PEROXIDE BEFORE MECHANICAL REFINING.

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FI892152A (en) 1989-05-04
EP0329694A1 (en) 1989-08-30
FI892152A0 (en) 1989-05-04
AU8233887A (en) 1988-06-01
SE8604769L (en) 1988-05-07
WO1988003581A1 (en) 1988-05-19
SE458690B (en) 1989-04-24
SE8604769D0 (en) 1986-11-06
NZ222448A (en) 1989-02-24

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