JP7380255B2 - analytical balance - Google Patents

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JP7380255B2
JP7380255B2 JP2020011292A JP2020011292A JP7380255B2 JP 7380255 B2 JP7380255 B2 JP 7380255B2 JP 2020011292 A JP2020011292 A JP 2020011292A JP 2020011292 A JP2020011292 A JP 2020011292A JP 7380255 B2 JP7380255 B2 JP 7380255B2
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windshield
case
top surface
windshield case
analytical balance
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JP2021117129A (en
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淳史 飯塚
正幸 河合
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Shimadzu Corp
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本発明は、風防ケースを備える分析天びんに関する。 The present invention relates to an analytical balance equipped with a windshield case.

高精度、高分解能の分析天びんでは、外部の気流が計量精度に大きく影響するため、外部気流の影響を受けないように、風防ケースにより計量皿の周囲を包囲して、ひょう量室を設けることが一般に行われている。 For high-precision, high-resolution analytical balances, external airflow has a large effect on measurement accuracy, so a weighing chamber must be provided with a windshield case surrounding the weighing pan to prevent it from being affected by external airflow. is commonly practiced.

すなわち、従来の分析天びんは図4に示すように構成され、分析天びん51の風防ケース52は下面が開口した直方体の箱状を有し、試料重量を計測する電気回路や計量値を表示する表示部53などを収容した本体ケース54の上面に風防ケース52が配置され、本体ケース54の上面に設けられた計量皿55の周囲が風防ケース52により包囲されて、風防ケース52内に外部気流の影響を受けないひょう量室56が形成される。このひょう量室56を外部から透視できるように、風防ケース52の天面57および4つの側面58が、例えば透明ガラスによって構成される(例えば、特許文献1参照)。 That is, the conventional analytical balance is constructed as shown in FIG. 4, and the windshield case 52 of the analytical balance 51 has a rectangular parallelepiped box shape with an open bottom, and is equipped with an electric circuit for measuring the weight of the sample and a display for displaying the weight value. A windshield case 52 is disposed on the upper surface of the main body case 54 that houses the parts 53 and the like, and the measuring pan 55 provided on the upper surface of the main body case 54 is surrounded by the windshield case 52 to prevent external airflow from flowing inside the windshield case 52. An unaffected weighing chamber 56 is formed. A top surface 57 and four side surfaces 58 of the windshield case 52 are made of, for example, transparent glass so that the weighing chamber 56 can be viewed from the outside (see, for example, Patent Document 1).

このとき、風防ケース52の天面57および左右の側面58は開閉可能に形成され、被ひょう量物の出し入れを行う際に、天面57または左右の側面58のいずれか出し入れし易い面を開放できる構成が採用される。このような風防ケースを備えた分析天びんは、通常、外部の気流や温度が安定した所定の測定室などの測定環境のもとに設置される。 At this time, the top surface 57 and left and right side surfaces 58 of the windshield case 52 are formed to be openable and closable, and when taking out and taking out the weighed object, either the top surface 57 or the left and right side surfaces 58, whichever is easier to take in and out, is opened. A possible configuration will be adopted. An analytical balance equipped with such a windshield case is usually installed in a measurement environment such as a predetermined measurement room with stable external airflow and temperature.

特開2011-257305号公報(段落0002~0003および図7)JP2011-257305A (Paragraphs 0002-0003 and Figure 7)

ところで、分析天びん51が設置される測定環境はその温度を一定に保持するために、通常、空調設備が設置されるが、特許文献1に記載のような従来の風防ケース52の場合、空調の影響を受けないと考えられてきた。ところが本願発明者が鋭意研究した結果、特許文献1に記載のような従来の風防ケース52を備える分析天びんであっても、風防ケース52内に対流が発生することを発見した。この原因として、風防ケース52の天面57に冷風や温風が当たって風防ケース52の天面57に温度変化が生じ、天面57とひょう量室56の下方の計量皿55周辺に温度差をさらに生じさせ、温度変化が風防ケース52内の対流を発生させるということを特定した。 Incidentally, the measurement environment in which the analytical balance 51 is installed is usually equipped with air conditioning equipment in order to maintain its temperature constant, but in the case of the conventional windshield case 52 as described in Patent Document 1, air conditioning equipment is installed in order to maintain the temperature constant. It was thought that it would not be affected. However, as a result of intensive research, the inventor of the present application discovered that even in an analytical balance equipped with a conventional windshield case 52 as described in Patent Document 1, convection occurs within the windshield case 52. The cause of this is that cold air or hot air hits the top surface 57 of the windshield case 52, causing a temperature change on the top surface 57 of the windshield case 52, and a temperature difference between the top surface 57 and the area around the weighing pan 55 below the weighing chamber 56. It was also determined that the temperature change caused convection within the windshield case 52.

このように、例えば冷房環境では風防ケース52の天面57の温度が下がると、これに起因してひょう量室56の上部の空気の温度が下部よりも低下するため、ひょう量室56の下部の空気の上昇と上部の空気の下降が促されてひょう量室56内に空気の対流が発生し、その結果、計量の安定性の低下や再現性能の劣化を招くおそれがある。 In this way, for example, in an air-conditioned environment, when the temperature of the top surface 57 of the windshield case 52 drops, the temperature of the air in the upper part of the weighing chamber 56 becomes lower than that in the lower part. The upward movement of the air and the downward movement of the upper air are promoted, and air convection occurs within the weighing chamber 56, which may result in a decrease in the stability of measurement and a deterioration in reproducibility.

本発明は、上記した課題に鑑みてなされたものであり、風防ケース内のひょう量室における空気の対流の発生を防止して、計量の安定性の低下や再現性能の劣化を防止できるようにすることを目的とする。 The present invention has been made in view of the above-mentioned problems, and it is possible to prevent the occurrence of air convection in the weighing chamber in the windshield case, thereby preventing a decrease in weighing stability and deterioration in reproducibility performance. The purpose is to

上記した目的を達成するために、本発明の分析天びんは、風防ケースを備える分析天びんにおいて、前記風防ケースの少なくとも天面が、前記風防ケース内への外部の熱の影響を遮断する熱遮断構造を有することを特徴としている。 In order to achieve the above object, the analytical balance of the present invention is an analytical balance equipped with a windshield case, in which at least the top surface of the windshield case has a heat insulation structure that blocks the influence of external heat into the inside of the windshield case. It is characterized by having the following.

また、少なくとも2枚の板材がそれらの間に断熱層を介在して配設されて前記天面が形成され、前記熱遮断構造が構成されていてもよく、前記天面が該天面を除く前記風防ケースの他の面よりも熱伝導率の低い材質の板材により形成され、前記熱遮断構造が構成されていてもよい。 Further, the top surface may be formed by disposing at least two plates with a heat insulating layer interposed between them, and the heat insulation structure may be configured, and the top surface may be configured such that the top surface excludes the top surface. The heat shielding structure may be formed of a plate material having a lower thermal conductivity than other surfaces of the windshield case.

また、風防ケースを備える分析天びんにおいて、 前記風防ケースの天面に設けられて前記天面を加熱する加熱手段を備えていてもよい。 Moreover, in the analytical balance equipped with a windshield case, a heating means may be provided on the top surface of the windshield case to heat the top surface.

本発明によれば、分析天びんの測定環境における空調によって風防ケースの天面の温度が低下したとしても、従来のように風防ケースの天面内部の温度が変化することを防止できるため、風防ケース内温度の変化に起因した風防ケース内の空気の対流の発生を未然に防止することができ、計量の安定性の低下や再現性能の劣化を防止することができ、計量精度の優れた分析天びんを提供することが可能になる。 According to the present invention, even if the temperature of the top surface of the windshield case decreases due to air conditioning in the measurement environment of the analytical balance, it is possible to prevent the temperature inside the top surface of the windshield case from changing as in the past. An analytical balance with excellent weighing accuracy that can prevent air convection inside the windshield case caused by changes in internal temperature, preventing a decline in weighing stability and reproducibility. It becomes possible to provide

本発明の第1実施形態に係る分析天びんの斜視図である。FIG. 1 is a perspective view of an analytical balance according to a first embodiment of the present invention. 図1における風防ケースの天面の分解斜視図である。FIG. 2 is an exploded perspective view of the top surface of the windshield case in FIG. 1. FIG. 本発明の第2実施形態に係る分析天びんの一部の平面図である。FIG. 3 is a plan view of a portion of an analytical balance according to a second embodiment of the present invention. 従来の分析天びんの斜視図である。FIG. 1 is a perspective view of a conventional analytical balance.

<第1実施形態>
本発明に係る分析天びんの第1実施形態について、図1および図2を参照して説明する。なお、図1は全体の斜視図、図2は風防ケースの天面の分解斜視図である。
<First embodiment>
A first embodiment of an analytical balance according to the present invention will be described with reference to FIGS. 1 and 2. Note that FIG. 1 is an overall perspective view, and FIG. 2 is an exploded perspective view of the top surface of the windshield case.

図1に示すように、本実施形態における分析天びん1は、試料重量を計測する電気回路を内蔵した本体ケース2と、本体ケース2の前上面に配設されて計量値を表示する表示部3と、本体ケース2の上面に配設された計量皿4と、下面が開口し本体ケース2に上面側から被せられて計量皿4の周囲を包囲する直方体の箱状の風防ケース5とを備え、外部気流の影響を受けないひょう量室6が風防ケース5の内部に形成される。 As shown in FIG. 1, an analytical balance 1 according to the present embodiment includes a main body case 2 that has a built-in electric circuit for measuring the weight of a sample, and a display section 3 that is disposed on the front upper surface of the main body case 2 and that displays weighed values. , a weighing pan 4 disposed on the top surface of the main body case 2, and a rectangular box-shaped windshield case 5 having an open bottom surface and covering the main body case 2 from the top side to surround the measuring pan 4. A weighing chamber 6 that is not affected by external airflow is formed inside the windshield case 5.

風防ケース5は、天面を構成する天面風防ガラス7と、左側面および右側面それぞれを構成する左側面風防ガラス8aおよび右側面風防ガラス8bと、前面および後面それぞれを構成する前面風防ガラス8cおよび後面風防ガラス8dとを備えており、天面風防ガラス7および左、右側面風防ガラス8a,8bには把手9が取り付けられ、把手9を把持してこれらの風防ガラス7,8a,8bを開閉できるように各風防ガラス7,8a,8bが設けられている。 The windshield case 5 includes a top windshield 7 that constitutes the top, a left windshield 8a and a right windshield 8b that constitute the left and right sides, respectively, and a front windshield 8c that constitutes the front and rear sides, respectively. and a rear windshield 8d, and handles 9 are attached to the top windshield 7 and the left and right side windshields 8a, 8b, and the handles 9 are gripped to open these windshields 7, 8a, 8b. Each windshield glass 7, 8a, 8b is provided so that it can be opened and closed.

ところで、天面風防ガラス7は、図2に示すように、いわゆるぺアガラスにより形成され、2枚の矩形ガラス板7a,7bの周縁が、これらガラス板7a,7bとほぼ同じ外寸を有する矩形枠状のスペーサ7cの上下に貼り合わされて形成されている。ここで、2枚のガラス板7a,7b間には断熱層が形成され、ペアガラスによる熱遮断構造の採用により、風防ケース5内のひょう量室6への外部の熱の影響が遮断される。 By the way, as shown in FIG. 2, the top windshield 7 is formed of so-called double glass, and the peripheries of the two rectangular glass plates 7a, 7b are rectangular having approximately the same outer dimensions as these glass plates 7a, 7b. It is formed by being bonded to the top and bottom of a frame-shaped spacer 7c. Here, a heat insulating layer is formed between the two glass plates 7a and 7b, and by adopting a heat shielding structure using double glass, the influence of external heat on the weighing chamber 6 inside the windshield case 5 is blocked. .

なお、2枚のガラス板7a,7b間の断熱層は、乾燥空気のほか窒素ガス、アルゴンガスなどのガラスよりも熱伝導率の低い気体を充填して形成したものや、熱伝導率がガラスよりも低い透明な樹脂を充填したり、透明な樹脂板を介挿したりして形成したものであってもよい。ここで、透明な樹脂として、例えばアクリル樹脂、ポリカーボネート樹脂、ポリ塩化ビニル樹脂、ポリエチレンテレフタレート樹脂などを使用するとよい。 The heat insulating layer between the two glass plates 7a and 7b may be formed by filling a gas with a lower thermal conductivity than glass, such as nitrogen gas or argon gas, in addition to dry air, or a layer with a thermal conductivity of glass. It may also be formed by filling a transparent resin with a lower temperature than 100 ml or by inserting a transparent resin plate. Here, as the transparent resin, for example, acrylic resin, polycarbonate resin, polyvinyl chloride resin, polyethylene terephthalate resin, etc. may be used.

そして、風防ケース5の天面にペアガラスによる熱遮断構造を採用したことにより、風防ケース5の天面風防ガラス7に測定環境における空調の風が当たっても、ひょう量室6の上部の空気の温度が変化するのを防止できるため、ひょう量室6の上部の空気と下部の空気の温度差が小さく抑えられるため、ひょう量室6における空気の対流の発生が抑制される。 By adopting a heat-insulating structure with double glass on the top surface of the windshield case 5, even if the top windshield glass 7 of the windshield case 5 is hit by air conditioning wind in the measurement environment, the air in the upper part of the weighing chamber 6 Since the temperature difference between the air in the upper part of the weighing chamber 6 and the air in the lower part of the weighing chamber 6 can be prevented from changing, the generation of air convection in the weighing chamber 6 can be suppressed.

したがって、従来の風防ケースを備えた分析天びんであれば風防ケース外部の対流しか抑制することができなかったが、上記した実施形態によれば、測定環境の空調の冷却風によって風防ケース5の天面風防ガラス7の温度が低下してひょう量室6の上部の温度が下部よりも下がるのを防止することができ、従来のように風防ケースの天面の温度が低下することに起因した風防ケース内の空気の対流の発生を未然に防止することができ、計量の安定性の低下や再現性能の劣化を防止することができ、計量精度の優れた分析天びんを提供することができる。 Therefore, with conventional analytical balances equipped with a windshield case, convection could only be suppressed outside the windshield case, but according to the above-described embodiment, the cooling air of the air conditioner in the measurement environment It is possible to prevent the temperature of the upper part of the weighing chamber 6 from lowering than the lower part due to the temperature of the front windshield glass 7 decreasing, and it is possible to prevent the temperature of the upper part of the weighing chamber 6 from becoming lower than that of the lower part. It is possible to prevent the occurrence of air convection within the case, thereby preventing deterioration in weighing stability and reproducibility, and providing an analytical balance with excellent weighing accuracy.

このとき、風防ケース5の天面風防ガラス7をペアガラスにより形成することにより、風防ケース5の天面の透明性を維持できて外部からひょう量室6を視認することができ、ひょう量室6の様子を確認しつつ計測作業を行うことができる。 At this time, by forming the top windshield glass 7 of the windshield case 5 with double glass, the transparency of the top surface of the windshield case 5 can be maintained and the weighing chamber 6 can be visually recognized from the outside. Measurement work can be carried out while checking the situation in step 6.

<第2実施形態>
本発明に係る分析天びんの第2実施形態について、図3を参照して説明する。
<Second embodiment>
A second embodiment of the analytical balance according to the present invention will be described with reference to FIG.

本実施形態において、上記した第1の実施形態と異なるのは、図3に示すように、例えば風防ケース5の天面風防ガラス7の表面周縁部に加熱手段としての熱線抵抗11を配置し、ITO(Indium Tin Oxide/酸化インジウム錫)の成膜技術により熱線抵抗11を天面風防ガラス7の表面に貼りつけ、図外の電源により熱線抵抗11に通電して天面風防ガラス7を加熱するようにした点である。このとき、ひょう量室6に空気の対流が生じないよう、ひょう量室6の上部の空気を加熱でき計測に支障が生じない程度に加熱するように、熱線抵抗11の発熱量を設定しておくのが望ましい。 This embodiment is different from the above-described first embodiment in that, as shown in FIG. A hot wire resistor 11 is pasted on the surface of the top windshield 7 using ITO (Indium Tin Oxide) film formation technology, and the top windshield 7 is heated by energizing the hot wire resistor 11 with a power supply not shown. This is what we did. At this time, in order to prevent air convection from occurring in the weighing chamber 6, the heat generation amount of the hot wire resistor 11 is set so that the air above the weighing chamber 6 can be heated to an extent that does not interfere with measurement. It is preferable to leave it there.

そして、加熱手段である熱線抵抗11に、図示しない電源装置により例えば常時通電しておくことによって、分析天びん1の測定環境における空調の冷却風が風防ケース5の天面風防ガラス7に当たっても、天面風防ガラス7が加熱されることから、ひょう量室6の上部の空気の温度が下部よりも低下することが未然に防止される。 By constantly energizing the hot wire resistor 11, which is the heating means, from a power supply device (not shown), even if the cooling air from the air conditioner in the measurement environment of the analytical balance 1 hits the top windshield 7 of the windshield case 5, the Since the surface windshield 7 is heated, the temperature of the air in the upper part of the weighing chamber 6 is prevented from becoming lower than that in the lower part.

したがって、第2実施形態によれば、上記した第1実施形態と同様、従来のように風防ケース5の天面風防ガラス7の温度が低下することに起因したひょう量室6における空気の対流の発生を未然に防止することができ、計量の安定性の低下や再現性能の劣化のない計量精度の優れた分析天びんを提供することができる。 Therefore, according to the second embodiment, similar to the first embodiment described above, the convection of air in the weighing chamber 6 due to a decrease in the temperature of the top windshield glass 7 of the windshield case 5 as in the conventional case. It is possible to provide an analytical balance that can prevent such occurrence and has excellent weighing accuracy without deteriorating weighing stability or reproducibility.

なお、本発明は上記した各実施形態に限定されるものではなく、その趣旨を逸脱しない限りにおいて、上記したもの以外に種々の変更を行なうことが可能である。例えば、上記した第1実施形態では、風防ケース5の天面をペアガラスから成る天面風防ガラス7とした例について説明したが、天面風防ガラス7に代えて、単にガラスよりも熱伝導率の低い透明樹脂の板材により天面を構成してもよい。 Note that the present invention is not limited to the embodiments described above, and various changes other than those described above can be made without departing from the spirit thereof. For example, in the first embodiment described above, an example has been described in which the top surface of the windshield case 5 is made of the top windshield glass 7 made of double glass. The top surface may be made of a transparent resin plate material with a low resistance.

また、上記した第1実施形態では、ペアガラスによる熱遮断構造を風防ケース5の天面にのみ採用した例について説明したが、風防ケース5の前後左右のすべての側面もペアガラスによる熱遮断構造を採用してもよい。 In addition, in the first embodiment described above, an example was explained in which the heat isolation structure using double glass was adopted only on the top surface of the windshield case 5, but all sides of the windshield case 5 on the front, back, left and right also have a heat isolation structure using double glass. may be adopted.

また、上記した第2実施形態では、加熱手段である熱線抵抗11を天面風防ガラス7の表面周縁部に配置した場合について説明したが、熱線抵抗11は周縁部に配置される場合に限定されるものではなく、加熱手段も熱線抵抗11に限るものではない。 Further, in the second embodiment described above, a case has been described in which the hot wire resistor 11 serving as a heating means is arranged at the peripheral edge of the surface of the top windshield 7, but the hot wire resistor 11 is limited to the case where it is arranged at the peripheral edge. The heating means is not limited to the hot wire resistor 11 either.

また、上記した第2実施形態では、熱線抵抗11により風防ケース5の天面を常時加熱するとしたが、ひょう量室6の上部および下部の空気の温度それぞれをセンサにより検出し、風防ケース5の上部の温度が下部よりも低下してひょう量室6で空気の対流が発生しそうなときに、加熱手段に通電して天面を加熱する制御を行うようにしてもよい。 Further, in the second embodiment described above, the top surface of the windshield case 5 is constantly heated by the hot wire resistance 11, but the temperature of the air in the upper and lower parts of the weighing chamber 6 is detected by the sensor, and the temperature of the air in the upper and lower parts of the weighing chamber 6 is detected. When the temperature of the upper part is lower than that of the lower part and air convection is likely to occur in the weighing chamber 6, the heating means may be energized to heat the top surface.

また、上記した第2実施形態において、電源装置は測定環境における室内灯の光で発電する太陽電池を使用すればよく、さらに太陽電池により発電した電気エネルギーを蓄電地に溜めて加熱手段に給電するようにしてもよい。 Further, in the second embodiment described above, the power supply device may use a solar cell that generates power using the light of an indoor light in the measurement environment, and further stores the electric energy generated by the solar cell in a power storage area to supply power to the heating means. You can do it like this.

また、本発明は、風防ケースを備える分析天びんに適用することができる。 Further, the present invention can be applied to an analytical balance equipped with a windshield case.

1 …分析天びん
5 …風防ケース
7 …天面風防ガラス(天面)
11 …熱線抵抗(加熱手段)
1...Analytical balance 5...Windshield case 7...Top windshield glass (top)
11...Hot wire resistance (heating means)

Claims (2)

風防ケースを備える分析天びんにおいて、
前記風防ケースの少なくとも天面が前記風防ケース内に対する前記風防ケース外部の熱の影響を遮断することにより、前記風防ケース内の対流を抑制する熱遮断構造を有し、
前記天面が該天面を除く前記風防ケースの他の面よりも熱伝導率の低い材質の板材により形成され、前記熱遮断構造が構成されていることを特徴とする分析天びん
For analytical balances equipped with a windshield case,
At least a top surface of the windshield case has a heat isolation structure that suppresses convection within the windshield case by blocking the influence of heat outside the windshield case on the inside of the windshield case;
An analytical balance characterized in that the top surface is formed of a plate made of a material having a lower thermal conductivity than other surfaces of the windshield case other than the top surface, and the heat isolation structure is configured.
少なくとも2枚の板材がそれらの間に断熱層を介在して配設されて前記天面が形成され、前記熱遮断構造が構成されていることを特徴とする請求項1に記載の分析天びん。 2. The analytical balance according to claim 1, wherein the top surface is formed by disposing at least two plates with a heat insulating layer interposed therebetween, and the heat shielding structure is configured.
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Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2004264283A (en) 2002-09-06 2004-09-24 Mettler Toledo Gmbh Balance with heat radiator
JP2010217176A (en) 2009-03-16 2010-09-30 Mettler-Toledo Ag Balance
CN102778278A (en) 2012-08-03 2012-11-14 昆山旭虹精密零组件有限公司 Electronic balance capable of preventing air convection
JP2019113349A (en) 2017-12-21 2019-07-11 株式会社島津製作所 electronic balance

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2004264283A (en) 2002-09-06 2004-09-24 Mettler Toledo Gmbh Balance with heat radiator
JP2010217176A (en) 2009-03-16 2010-09-30 Mettler-Toledo Ag Balance
CN102778278A (en) 2012-08-03 2012-11-14 昆山旭虹精密零组件有限公司 Electronic balance capable of preventing air convection
JP2019113349A (en) 2017-12-21 2019-07-11 株式会社島津製作所 electronic balance

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