JP6568819B2 - Method for producing fermented milk - Google Patents

Method for producing fermented milk Download PDF

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JP6568819B2
JP6568819B2 JP2016064303A JP2016064303A JP6568819B2 JP 6568819 B2 JP6568819 B2 JP 6568819B2 JP 2016064303 A JP2016064303 A JP 2016064303A JP 2016064303 A JP2016064303 A JP 2016064303A JP 6568819 B2 JP6568819 B2 JP 6568819B2
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fermented milk
milk
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真理映 谷河
真理映 谷河
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Morinaga Milk Industry Co Ltd
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Description

本発明は、発酵乳の製造方法に関する。本発明は、特に濃縮発酵乳の製造方法に関する。   The present invention relates to a method for producing fermented milk. The present invention particularly relates to a method for producing concentrated fermented milk.

近年、従来の標準的な発酵乳に対して固形分濃度を高めた濃縮発酵乳が、そのクリーミーさ、コク等から、高級感のある製品として人気がある。
濃縮発酵乳の製造方法としては、発酵原料(調乳液)の乳脂肪分や無脂乳固形分を高める方法が知られている。具体的には、全脂乳を膜処理した後、発酵させて発酵乳を製造する方法が知られている(特許文献1)。
また、発酵原料(調乳液)を発酵させて得られた発酵物を膜濃縮することで濃縮発酵乳を製造することも知られている(特許文献2、特許文献3)。
In recent years, concentrated fermented milk having a higher solid content than conventional standard fermented milk has become popular as a product with a high-class feeling due to its creaminess and richness.
As a method for producing concentrated fermented milk, a method for increasing the milk fat content and non-fat milk solid content of a fermentation raw material (milky formula) is known. Specifically, a method of producing fermented milk by subjecting whole fat milk to membrane treatment and then fermenting is known (Patent Document 1).
It is also known that concentrated fermented milk is produced by membrane concentration of a fermented product obtained by fermenting a fermentation raw material (milk preparation liquid) (Patent Documents 2 and 3).

特開平6−14707号公報JP-A-6-14707 特開2014−161237号公報JP 2014-161237 A 特開2005−318855号公報JP 2005-318855 A

従来知られている濃縮発酵乳の製造方法のうち、特許文献1に記載されるような調乳液の固形分濃度を高める方法は、発酵条件などの制約を受けることがあり、良好な風味を達成しにくい。一方、特許文献2、3に記載されるような発酵物を濃縮する方法は酸味が強くなる傾向がある。
濃厚発酵乳は、濃厚でマイルドな味わいが魅力のため、酸味が強くなりすぎることは好ましくない。
Among the conventionally known methods for producing concentrated fermented milk, the method for increasing the solid content concentration of the milk preparation as described in Patent Document 1 may be subject to restrictions such as fermentation conditions, and achieves a good flavor. Hard to do. On the other hand, the method of concentrating a fermented product as described in Patent Documents 2 and 3 tends to be sour.
Concentrated fermented milk has an attractive rich and mild taste, and it is not preferable that the sour taste becomes too strong.

また、人気が高まりつつある濃縮発酵乳の分野において様々な嗜好性を有する製品を開発していく上で、菓子の分野において最もポピュラーな食材の一つである抹茶やチョコレートなどの素材の使用が課題となる。これらの素材は中性付近でおいしく食することができるものであり、濃縮発酵乳の酸味が強い場合には、味の調和が取れずおいしくなくなってしまう。   In addition, the development of products with various tastes in the field of concentrated fermented milk, which is gaining popularity, requires the use of ingredients such as matcha and chocolate, which are one of the most popular ingredients in the confectionery field. It becomes a problem. These materials can be eaten deliciously in the vicinity of neutrality, and if the concentrated fermented milk has a strong sourness, the taste will not be balanced and will not be delicious.

そこで、本発明は、酸度の上昇を抑制しながら、濃縮発酵乳を製造する技術を提供することを課題とする。また、本発明は、非酸性素材を含む濃縮発酵乳を製造する技術を提供することを課題とする。   Then, this invention makes it a subject to provide the technique which manufactures concentrated fermented milk, suppressing the raise of acidity. Moreover, this invention makes it a subject to provide the technique which manufactures the concentrated fermented milk containing a non-acid raw material.

前記課題を解決する本発明は、調乳液を発酵して発酵物を調製する発酵工程と、調製した発酵物を濃縮して濃縮発酵乳を調製する濃縮工程とを含む、濃縮発酵乳の製造方法であって、前記濃縮工程の前に、前記発酵物を希釈液により希釈して希釈発酵物を調製する希釈工程を含むことを特徴とする。
本発明の製造方法によれば、濃縮工程による酸度の上昇を抑制することができ、酸味が抑制された濃縮発酵乳を製造することが可能となる。
The present invention that solves the above-described problems includes a fermentation process in which a fermented milk solution is fermented to prepare a fermented product, and a concentrated fermented milk manufacturing method that includes a concentrated fermented milk product by concentrating the prepared fermented product. And before the said concentration process, the dilution process which dilutes the said fermented material with a dilution liquid and prepares a diluted fermented product is characterized by the above-mentioned.
According to the production method of the present invention, it is possible to suppress an increase in acidity due to the concentration step, and it is possible to produce concentrated fermented milk with reduced acidity.

本発明の好ましい形態では、前記希釈工程中に前記濃縮工程を開始し、該濃縮工程中に前記希釈工程を終了する。
前記希釈工程中に前記濃縮工程を開始することで、酸味が抑制された濃縮発酵乳を効率的に製造することが可能となる。
In a preferred embodiment of the present invention, the concentration step is started during the dilution step, and the dilution step is ended during the concentration step.
By starting the concentration step during the dilution step, it is possible to efficiently produce concentrated fermented milk with reduced acidity.

本発明の好ましい形態では、前記濃縮工程は、前記濃縮発酵乳の質量が、前記発酵物の質量に対して3分の2以下となるように行う。
このような範囲で発酵物を濃縮する場合に、本発明の製造方法の酸度の上昇を抑制する効果が顕著となる。
In the preferable form of this invention, the said concentration process is performed so that the mass of the said concentrated fermented milk may become 2/3 or less with respect to the mass of the said fermented material.
When concentrating a fermented product in such a range, the effect which suppresses the raise of the acidity of the manufacturing method of this invention becomes remarkable.

本発明の好ましい形態では、前記濃縮工程は、前記濃縮発酵乳の無脂乳固形分が10質量%以上となるように行う。
このような範囲で発酵物を濃縮することで、特に、クリーミーさ、コクといった濃厚な風味を有する濃縮発酵乳を製造することが可能となる。
In the preferable form of this invention, the said concentration process is performed so that the non-fat milk solid content of the said concentrated fermented milk may be 10 mass% or more.
By concentrating the fermented product in such a range, it is possible to produce concentrated fermented milk having a rich flavor such as creaminess and richness.

本発明の好ましい形態では、前記希釈工程は、前記希釈発酵物の質量が、前記発酵物の質量に対して1.01〜4倍となるように行う。
このような範囲で希釈することで、発酵物の濃縮による酸度の上昇を効果的に抑制することができ、また、製造効率も良い。
In the preferable form of this invention, the said dilution process is performed so that the mass of the said diluted fermented material may be 1.01-4 times with respect to the mass of the said fermented material.
By diluting in such a range, an increase in acidity due to the concentration of the fermented product can be effectively suppressed, and the production efficiency is also good.

本発明の好ましい形態では、前記希釈工程及び濃縮工程は、前記濃縮発酵乳の乳酸酸度と、前記発酵物の乳酸酸度の差が0.25質量%以下となるように行う。
濃縮工程による乳酸酸度の増加分が前記範囲となるように希釈工程と濃縮工程とを行うことにより、酸度の上昇が抑制され、嗜好性に優れた濃厚発酵乳を製造することが可能となる。
In a preferred embodiment of the present invention, the dilution step and the concentration step are performed such that the difference between the lactic acid acidity of the concentrated fermented milk and the lactic acid acidity of the fermented product is 0.25% by mass or less.
By performing the dilution step and the concentration step so that the increase in the lactic acid acidity due to the concentration step falls within the above range, it is possible to produce concentrated fermented milk excellent in palatability by suppressing an increase in acidity.

本発明の好ましい形態では、前記希釈工程及び濃縮工程は、濃縮発酵乳の乳酸酸度が0.95質量%以下となるように行い、前記濃縮工程後に、濃縮発酵乳に非酸性素材を添加する非酸性素材添加工程を含む。
濃縮発酵乳における乳酸酸度を前記範囲とし、濃縮発酵乳に非酸性素材を添加することで、風味の調和がとれた非酸性素材を含む濃縮発酵乳を製造することが可能となる。
In a preferred embodiment of the present invention, the dilution step and the concentration step are performed such that the lactic acid acidity of the concentrated fermented milk is 0.95% by mass or less, and a non-acidic material is added to the concentrated fermented milk after the concentration step. Includes an acidic material addition step.
By making the lactic acid acidity in concentrated fermented milk within the above range and adding a non-acidic material to the concentrated fermented milk, it becomes possible to produce concentrated fermented milk containing a non-acidic material with a harmonious flavor.

本発明によれば、濃縮発酵乳の製造において、発酵物の濃縮による酸度の上昇を抑制することができる。本発明の好ましい形態によれば、マイルドな風味を有する濃縮発酵乳を製造することができる。さらに、本発明の好ましい形態によれば、滑らかな食感を有する濃縮発酵乳を製造することができる。また、本発明の好ましい形態によれば、風味の調和がとれた非酸性素材を含む濃縮発酵乳を製造することが可能となる。   ADVANTAGE OF THE INVENTION According to this invention, in manufacture of concentrated fermented milk, the raise of the acidity by concentration of fermented material can be suppressed. According to the preferable form of this invention, the concentrated fermented milk which has a mild flavor can be manufactured. Furthermore, according to the preferable form of this invention, the concentrated fermented milk which has smooth texture can be manufactured. Moreover, according to the preferable form of this invention, it becomes possible to manufacture the concentrated fermented milk containing the non-acidic material with which the flavor was harmonized.

実施例及び比較例の製造フローを示す概念図である。It is a conceptual diagram which shows the manufacture flow of an Example and a comparative example. 試験1の各サンプルの粒度分布を示す図である。It is a figure which shows the particle size distribution of each sample of Test 1. 試験2の各サンプルの粒度分布を示す図である。It is a figure which shows the particle size distribution of each sample of Test 2.

以下、本発明を実施するための実施形態について説明する。
本明細書において、乳、乳製品に関する分類は、特に断らない限り、『乳及び乳製品の成分規格等に関する省令』(以下、「乳等省令」という。)に基づくものである。
本明細書において、「%」パーセントについての表示は、特に断らない限り、質量による表示である。
Hereinafter, an embodiment for carrying out the present invention will be described.
In the present specification, the classification of milk and dairy products is based on “Ministerial Ordinance on Component Standards of Milk and Dairy Products” (hereinafter referred to as “Ministerial Ordinance on Milk”) unless otherwise specified.
In the present specification, “%” percent is expressed by mass unless otherwise specified.

本発明の濃縮発酵乳の製造方法は、調乳液を発酵して発酵物を調製する発酵工程と、調製した発酵物を濃縮して濃縮発酵乳を調製する濃縮工程とを含む、濃縮発酵乳の製造方法である。本発明が製造の目的とする濃縮発酵乳は、固形分濃度が、好ましくは10質量%以上、更に好ましくは11質量%以上のものである。   The method for producing concentrated fermented milk according to the present invention includes a fermentation step of fermenting a milk preparation to prepare a fermented product, and a concentration step of concentrating the prepared fermented product to prepare concentrated fermented milk. It is a manufacturing method. The concentrated fermented milk produced by the present invention has a solid concentration of preferably 10% by mass or more, more preferably 11% by mass or more.

本発明の濃縮発酵乳の製造方法は、前記濃縮工程の前に、発酵工程により得られた発酵物を希釈液により希釈して希釈発酵物を調製する希釈工程を含むことを特徴とする。以下、本発明の実施形態について説明する。   The method for producing concentrated fermented milk according to the present invention includes a dilution step of preparing a diluted fermented product by diluting the fermented product obtained by the fermenting step with a diluent before the concentrating step. Hereinafter, embodiments of the present invention will be described.

<1>発酵工程
本発明の実施形態では、調乳液を発酵して発酵物を調製する発酵工程を行う。ここで、「調乳液」とは、発酵乳の製造に用いられる、乳、乳製品などの発酵乳原料を含む種々の原料を調製して得られる原料である。
調乳液の調製には、発酵乳の製造に通常用いられる乳製品及びその他の原料を特に制限なく用いることができる。調乳液に用いる乳製品としては、クリーム、脱脂濃縮乳、脱脂粉乳等が挙げられる。
<1> Fermentation process In embodiment of this invention, the fermentation process which ferments milk solution and prepares a fermented product is performed. Here, the “milk preparation” is a raw material obtained by preparing various raw materials including fermented milk raw materials such as milk and dairy products, which are used in the production of fermented milk.
For the preparation of the milk preparation, dairy products and other raw materials usually used for the production of fermented milk can be used without particular limitation. Examples of the dairy product used in the milk preparation include cream, skim concentrated milk, skim milk powder and the like.

調乳液における無脂乳固形分の含有量は、発酵乳の製造に用いられる通常の範囲で適宜調整することができる。   The content of non-fat milk solids in the formula can be adjusted as appropriate within the normal range used for the production of fermented milk.

調乳液における無脂乳固形分は、好ましくは6〜16質量%であり、更に好ましくは8〜14質量%である。無脂乳固形分の含有量が上記範囲の下限値以上であると濃縮に適した発酵物が得られやすく、上限値以下であると風味の良い濃縮発酵乳が得られやすい。   The non-fat milk solid content in the milk preparation is preferably 6 to 16% by mass, and more preferably 8 to 14% by mass. A fermented product suitable for concentration is easily obtained when the content of the non-fat milk solid content is at least the lower limit of the above range, and concentrated fermented milk having a good flavor is easily obtained when the content is less than the upper limit.

また、調乳液は、乳由来以外の原料を含んでいてもよい。例えば、調乳液にショ糖、果糖等の糖類を含有させることができる。また、調乳液は、好ましくは均質化処理される。   Moreover, the milk preparation liquid may contain raw materials other than milk origin. For example, sugars such as sucrose and fructose can be contained in the milk preparation. Moreover, the milk preparation is preferably homogenized.

このようにして調製された調乳液は、好ましくは加熱処理される。加熱処理工程は、牛乳の殺菌等、乳製品の製造過程において通常用いられる条件を用いることができる。
加熱温度は、85〜95℃とすることが好ましい。また、加熱時間は5〜15分とすることが好ましい。
The milk preparation thus prepared is preferably heat-treated. In the heat treatment step, conditions usually used in the production process of dairy products such as sterilization of milk can be used.
The heating temperature is preferably 85 to 95 ° C. The heating time is preferably 5 to 15 minutes.

調乳液の発酵は、通常の発酵乳の製造に用いられる乳酸菌スターターを特に制限なく用いることができる。乳酸菌スターターとしては、例えば、ラクトバチルス・ブルガリクス(L.bulgaricus)、ラクトコッカス・ラクチス(L.lactis)、ストレプトコッカス・サーモフィラス(S.thermophilus)等の乳酸菌を用いることができる。
また、低酸性乳酸菌スターターを用いることも好ましい。低酸性乳酸菌スターターとは、無脂乳固形分10質量%の還元脱脂乳培地において40℃で発酵を行ったときに、培地のpHが5.0から4.6まで下がるのに要する時間が3時間以上である特徴を有する乳酸菌スターターをいう。
このような低酸性乳酸菌スターターとしては、ストレプトコッカス・サーモフィラス(Streptococcus thermophilus)等の菌種のものが市販されているので、これを用いることが可能である。例えば、クリスチャン・ハンセン社からF−DVS ST−20X、F−DVS ST−BODY−2、F−DVS ST−BODY−3等の商品名で市販されているものを使用することができる。 また、ビフィドバクテリウム属細菌を添加することもできる。
For fermentation of the milk preparation, a lactic acid bacterium starter used for production of ordinary fermented milk can be used without any particular limitation. As the lactic acid bacteria starter, for example, lactic acid bacteria such as Lactobacillus bulgaricus, L. lactis, Streptococcus thermophilus (S. thermophilus) and the like can be used.
It is also preferable to use a low acid lactic acid bacteria starter. The low acid lactic acid bacteria starter is a time required for the pH of the medium to fall from 5.0 to 4.6 when fermented at 40 ° C. in a reduced skim milk medium having a nonfat milk solid content of 10 mass%. It refers to a lactic acid bacteria starter that has the characteristics of being over time.
As such a low-acidic lactic acid bacteria starter, those of bacterial species such as Streptococcus thermophilus are commercially available and can be used. For example, commercially available products such as F-DVS ST-20X, F-DVS ST-BODY-2, and F-DVS ST-BODY-3 from Christian Hansen can be used. Bifidobacterium can also be added.

乳酸菌等の細菌の添加量は、通常の範囲で適宜調節することができる。例えば、調乳液における細菌濃度が、少なくとも1×105CFU/g、好ましくは少なくとも1×106CFU/gとなるような量を添加することが好ましい。
発酵条件も通常の範囲で適宜調節することができる。例えば、35〜43℃の温度で、5〜12時間発酵することにより発酵物を得ることができる。
The addition amount of bacteria such as lactic acid bacteria can be appropriately adjusted within a normal range. For example, it is preferable to add such an amount that the bacterial concentration in the milk preparation is at least 1 × 10 5 CFU / g, preferably at least 1 × 10 6 CFU / g.
Fermentation conditions can also be adjusted as appropriate within a normal range. For example, a fermented material can be obtained by fermenting at a temperature of 35 to 43 ° C. for 5 to 12 hours.

発酵は、通常pHが4〜5、好ましくは4.4〜4.8となった時点で、冷却することにより終了させることができる。
また、得られた発酵物の乳酸酸度は、好ましくは0.55〜0.8質量%、更に好ましくは0.6〜0.7質量%である。
前記範囲のpH、乳酸酸度となるまで発酵させることにより、風味の良い濃縮発酵乳を製造することが可能となる。
得られた発酵物中のカードは破砕し、後述する希釈工程に供する。カードの破砕は、冷却中、冷却後の何れに行ってもよい。
Fermentation can be terminated by cooling when the pH is usually 4 to 5, preferably 4.4 to 4.8.
Moreover, the lactic acid acidity of the obtained fermented material becomes like this. Preferably it is 0.55-0.8 mass%, More preferably, it is 0.6-0.7 mass%.
By fermenting until the pH and lactic acid acidity in the above ranges are satisfied, it is possible to produce a concentrated fermented milk having a good flavor.
The card | curd in the obtained fermented material is crushed and it uses for the dilution process mentioned later. The card may be crushed either during cooling or after cooling.

<2>希釈工程
本発明の実施形態では、続いて、調製された発酵物に希釈液を添加することで、発酵物を希釈して、希釈発酵物を調製する。本発明において、後述する濃縮工程に先立ちこの希釈工程を行うことにより、濃縮工程において発酵物の組織に存在する乳酸を効率よく除去し、濃縮に伴う発酵物の酸度の上昇を抑制することができる。後述する実施例に示すとおり、発酵により調製された発酵物を同じ効率で濃縮する場合であっても、濃縮工程前に希釈工程を行うか否かによって、濃縮発酵乳における酸度に顕著な違いが出る。
<2> Dilution Step In the embodiment of the present invention, subsequently, the diluted fermented product is diluted by adding a diluent to the prepared fermented product to prepare a diluted fermented product. In the present invention, by performing this dilution step prior to the concentration step described later, lactic acid present in the fermented tissue can be efficiently removed in the concentration step, and an increase in the acidity of the fermented product accompanying concentration can be suppressed. . As shown in the examples described later, even if the fermented material prepared by fermentation is concentrated with the same efficiency, there is a significant difference in the acidity in the concentrated fermented milk depending on whether the dilution step is performed before the concentration step. Get out.

ここで、希釈液は、純水であってもよいし、水溶液であってもよい。水溶液としては、例えば、後述する濃縮工程における膜濃縮の副産物である、ホエイタンパク質、ミネラル、乳糖、酸等を含む膜濾過液や、ミネラル、ビタミン、タンパク質、糖類、果汁、香料、増粘安定剤等、各種食品添加物を溶解した水溶液が挙げられる。後述するように、希釈工程中に濃縮工程を開始する形態においては、濃縮工程で得られる副産物である膜濾過液を、希釈液として用いることも可能である。   Here, the dilution liquid may be pure water or an aqueous solution. Examples of the aqueous solution include membrane filtrates containing whey protein, minerals, lactose, acids, etc., which are by-products of membrane concentration in the concentration step described later, minerals, vitamins, proteins, sugars, fruit juices, fragrances, thickening stabilizers. An aqueous solution in which various food additives are dissolved. As will be described later, in a form in which the concentration step is started during the dilution step, a membrane filtrate that is a by-product obtained in the concentration step can be used as the dilution solution.

希釈工程は、希釈発酵物の質量が、前記発酵工程により調製した発酵物の質量に対して、好ましくは1.01倍以上となるように、更に好ましくは1.1倍以上となるように、より好ましくは1.5倍以上となるように行う。
このような範囲で希釈することにより、後述する濃縮工程によって発酵物中の乳酸を効率よく除去することが可能となる。また、希釈発酵物の質量が、前記発酵物の質量に対して、好ましくは1.8倍以上、更に好ましくは2.5倍以上となるように希釈することで、濃縮工程を経て得られる濃縮発酵乳を滑らかな組織とすることができる。より詳細にいうと、希釈工程を行わずに同じ効率で濃縮して得られた濃縮発酵乳に対して、濃縮発酵乳の組織に含まれる粒子を微細化する効果が得られる。
また、製造効率の観点からは、希釈工程は、希釈発酵物の質量が、前記発酵物の質量に対して、好ましくは4倍以下、更に好ましくは3倍以下、より好ましくは2倍以下となるように行う。
In the dilution step, the mass of the diluted fermented product is preferably 1.01 times or more, more preferably 1.1 times or more, with respect to the mass of the fermented product prepared by the fermentation step. More preferably, it is performed so as to be 1.5 times or more.
By diluting in such a range, lactic acid in the fermented product can be efficiently removed by the concentration step described later. Moreover, the concentration obtained through a concentration process by diluting so that the mass of the diluted fermented product is preferably 1.8 times or more, more preferably 2.5 times or more with respect to the mass of the fermented product. Fermented milk can be made into a smooth structure. More specifically, the effect of refining the particles contained in the tissue of the concentrated fermented milk is obtained with respect to the concentrated fermented milk obtained by concentrating at the same efficiency without performing the dilution step.
From the viewpoint of production efficiency, in the dilution step, the mass of the diluted fermented product is preferably 4 times or less, more preferably 3 times or less, more preferably 2 times or less with respect to the mass of the fermented product. Do as follows.

<3>濃縮工程
本発明の実施形態では、希釈工程により調製した希釈発酵物を濃縮して濃縮発酵乳を得る濃縮工程を行う。濃縮工程は、濃縮発酵乳の質量が、前記発酵工程により調製した発酵物の質量に対して好ましくは1以下、更に好ましくは3分の2以下となるように行う。このような効率で濃縮工程を行う場合には、酸度の上昇が特に顕著となる。そのため、前記範囲の効率で濃縮する際に、本発明の製造方法の酸度の上昇を抑制する効果が顕著となる。
<3> Concentration step In the embodiment of the present invention, a concentration step of concentrating the diluted fermented product prepared in the dilution step to obtain concentrated fermented milk is performed. The concentration step is performed so that the mass of the concentrated fermented milk is preferably 1 or less, more preferably 2/3 or less, with respect to the mass of the fermented product prepared by the fermentation step. When the concentration step is performed with such efficiency, the increase in acidity becomes particularly significant. Therefore, when concentrating with the efficiency of the said range, the effect which suppresses the raise of the acidity of the manufacturing method of this invention becomes remarkable.

また、濃縮工程は、濃縮発酵乳の質量が、前記発酵物の質量に対して好ましくは5分の1以上、更に好ましくは3分の1以上となるように行う。このような範囲で濃縮を行うことにより、食感や風味が良好な濃縮発酵乳を得ることができる。   Further, the concentration step is performed so that the mass of the concentrated fermented milk is preferably 1/5 or more, more preferably 1/3 or more of the mass of the fermented product. By concentrating in such a range, concentrated fermented milk having a good texture and flavor can be obtained.

また、濃縮工程は、濃縮発酵乳の無脂乳固形分が、好ましくは10質量%以上、更に好ましくは11質量%以上となるように行う。上限値は、特に制限されないが、好ましくは15質量%以下、更に好ましくは14質量%以下である。
また、濃縮工程は、濃縮発酵乳のタンパク質の含有量が、好ましくは5質量%以上、更に好ましくは6質量%以上となるように行う。上限値は、特に制限されないが、好ましくは11質量%以下、更に好ましくは10質量%以下である。
また、濃縮工程は、濃縮発酵乳の脂肪の含有量が、好ましくは0.2質量%以上、更に好ましくは0.3質量%以上となるように行う。上限値は、特に制限されないが、好ましくは11質量%以下、更に好ましくは10質量%以下である。
このような範囲で濃縮することにより、クリーミーさ、コクといった濃厚な風味を有する濃縮発酵乳を製造することができる。
The concentration step is performed so that the nonfat milk solid content of the concentrated fermented milk is preferably 10% by mass or more, and more preferably 11% by mass or more. The upper limit is not particularly limited, but is preferably 15% by mass or less, and more preferably 14% by mass or less.
The concentration step is performed so that the protein content of the concentrated fermented milk is preferably 5% by mass or more, more preferably 6% by mass or more. The upper limit is not particularly limited, but is preferably 11% by mass or less, and more preferably 10% by mass or less.
The concentration step is performed so that the fat content of the concentrated fermented milk is preferably 0.2% by mass or more, more preferably 0.3% by mass or more. The upper limit is not particularly limited, but is preferably 11% by mass or less, and more preferably 10% by mass or less.
By concentrating in such a range, concentrated fermented milk having a rich flavor such as creaminess and richness can be produced.

また、濃縮工程は、濃縮発酵乳の質量が、希釈発酵物の質量に対して、好ましくは2分の1〜9分の1、更に好ましくは3分の1〜6分の1となるように行う。   In addition, the concentration step is such that the mass of the concentrated fermented milk is preferably 1/2 to 1/9, more preferably 1/3 to 1/6 of the diluted fermented product. Do.

濃縮方法としては、従来、乳製品の成分の濃縮に用いられる方法であれば特に制限なく用いることができ、その方法として、セパレーターによる濃縮や膜濃縮が挙げられる。膜濃縮に用いられる濾過膜としては、精密濾過膜(MF膜)、限外濾過膜(UF膜)、ナノフィルトレーション膜(NF膜)、逆浸透膜(RO膜)等が挙げられる。中でも、限外濾過膜(UF膜)が、良好な風味を実現する観点から好ましく用いられる。濃縮は、従来乳製品の濃縮に用いられている装置を用いて行うことができる。   Any conventional concentration method can be used without limitation as long as it is a method used for concentration of dairy components. Examples of the concentration method include concentration by a separator and membrane concentration. Examples of filtration membranes used for membrane concentration include microfiltration membranes (MF membranes), ultrafiltration membranes (UF membranes), nanofiltration membranes (NF membranes), and reverse osmosis membranes (RO membranes). Among these, an ultrafiltration membrane (UF membrane) is preferably used from the viewpoint of realizing a good flavor. Concentration can be performed using an apparatus conventionally used for concentration of dairy products.

濃縮工程中、希釈発酵物の温度は、好ましくは10〜50℃、更に好ましくは40〜45℃に維持する。濃縮工程が終了した後は、20℃以下に冷却することが好ましい。   During the concentration step, the temperature of the diluted fermented product is preferably maintained at 10 to 50 ° C, more preferably 40 to 45 ° C. After completion of the concentration step, it is preferable to cool to 20 ° C. or lower.

濃縮工程は、前述した希釈工程が終了した後に開始してもよいし、希釈工程中に開始してもよい。特に、希釈工程中に濃縮工程を開始することが、生産効率の観点から好ましい。この場合には、濃縮工程中に希釈工程を終了することで、濃縮発酵乳を得ることができる。このような方法としては、ダイアフィルトレーションが好ましく挙げられる。すなわち、発酵物を収容するタンクに希釈液を供給しながら、発酵物中の水を含む低分子成分を除去することで、発酵物の希釈をした後、これを濃縮することができる。ここで、濃縮工程において得られる副産物である膜濾過液は、希釈液として用いることができる。   The concentration step may be started after the above-described dilution step is completed, or may be started during the dilution step. In particular, it is preferable from the viewpoint of production efficiency to start the concentration step during the dilution step. In this case, concentrated fermented milk can be obtained by terminating the dilution step during the concentration step. As such a method, diafiltration is preferably mentioned. That is, while diluting the fermented product by removing low molecular components including water in the fermented product while supplying the diluent to the tank containing the fermented product, it can be concentrated. Here, the membrane filtrate which is a by-product obtained in the concentration step can be used as a diluent.

前述した希釈工程と濃縮工程は、濃縮発酵乳の乳酸酸度と発酵工程により調製した発酵物の乳酸酸度の差が、好ましくは0.25質量%以内、更に好ましくは0.2質量%以内となるように、行うことが好ましい。後述する実施例に示す通り、希釈倍率を高くするほど、濃縮発酵乳の酸度を低下させることができる。また、濃縮による質量減少が大きい(実施例における濃縮効率が低値である)ほど発酵物の酸度が上昇する。従って、希釈倍率及び濃縮効率を各々調整することによって、濃縮発酵乳の酸度を調整することができる。
濃縮工程による乳酸酸度の増加を前記範囲とすることにより、風味に優れた濃厚発酵乳を製造することが可能となる。
In the dilution step and the concentration step described above, the difference between the lactic acid acidity of the concentrated fermented milk and the lactic acid acidity of the fermented product prepared by the fermentation process is preferably within 0.25% by mass, more preferably within 0.2% by mass. Thus, it is preferable to carry out. As shown in the Example mentioned later, the acidity of concentrated fermented milk can be reduced, so that a dilution rate is made high. Moreover, the acidity of a fermented product rises, so that the mass reduction by concentration is large (concentration efficiency in an Example is a low value). Therefore, the acidity of the concentrated fermented milk can be adjusted by adjusting the dilution ratio and the concentration efficiency, respectively.
By setting the increase in the lactic acid acidity by the concentration step within the above range, it is possible to produce a concentrated fermented milk excellent in flavor.

濃縮工程終了後の発酵物の乳酸酸度は、好ましくは1.1質量%以下、更に好ましくは1質量%以下である。発酵物の乳酸酸度の下限値は特に制限されないが、発酵乳としての風味の観点からは、0.64質量%以上が好ましい。   The lactic acid acidity of the fermented product after the completion of the concentration step is preferably 1.1% by mass or less, more preferably 1% by mass or less. Although the lower limit of the lactic acid acidity of the fermented product is not particularly limited, 0.64% by mass or more is preferable from the viewpoint of flavor as fermented milk.

このようにして得られた濃縮発酵乳は、所望により均質化を行うことができる。また、このようにして得られた濃縮発酵乳は、所望により均質化を行った後、シロップ、果実プレザーブ等の発酵乳以外の素材を添加又は混合する形態とし、これらの素材の風味を生かした製品とすることもできる。このような形態としては、濃縮発酵乳に素材をかける形態、濃縮発酵乳に素材を混合する形態の何れでもよい。
中でも、このような素材として、中性付近で食される非酸性素材を用いることが、本発明の製造方法の酸度上昇を抑制する効果を存分に生かすことができるため好ましい。
The concentrated fermented milk thus obtained can be homogenized as desired. In addition, the concentrated fermented milk thus obtained is homogenized as desired, and then added or mixed with materials other than fermented milk such as syrup and fruit preserves, and the flavors of these materials are utilized. It can also be a product. As such a form, either the form which applies a raw material to concentrated fermented milk, or the form which mixes a raw material with concentrated fermented milk may be sufficient.
Among them, it is preferable to use a non-acidic material eaten near neutral as such a material because the effect of suppressing the increase in acidity of the production method of the present invention can be fully utilized.

非酸性素材が添加される対象である濃縮発酵乳の乳酸酸度は、好ましくは0.6〜0.95質量%、更に好ましくは0.7〜0.8質量%である。
このような範囲とすることで、濃縮発酵乳における非酸性素材との風味の調和が良好となる。
The lactic acid acidity of the concentrated fermented milk to which the non-acidic material is added is preferably 0.6 to 0.95% by mass, more preferably 0.7 to 0.8% by mass.
By setting it as such a range, harmony of the flavor with the non-acidic material in concentrated fermented milk becomes favorable.

本発明において、非酸性素材のpHは5以上、好ましくは5〜7.5である。また、非酸性素材に含有する素材としては、上記pHで素材本来のおいしさを発揮する素材、言い換えれば、酸度が高い食品においては、素材本来の風味が損なわれやすい素材が好ましい。例えば、抹茶、チョコレート、ゴマ、ココア、キャラメル、きな粉、あん、栗、及び芋があげられる。   In the present invention, the non-acidic material has a pH of 5 or more, preferably 5 to 7.5. Moreover, as a raw material contained in a non-acidic raw material, the raw material which demonstrates the original deliciousness of a raw material at the said pH, in other words, in the food with high acidity, the raw material which tends to impair the original flavor of a raw material is preferable. Examples include matcha, chocolate, sesame, cocoa, caramel, kinako, chanterelle, chestnut, and strawberry.

前記非酸性素材は、好ましくは糖を含むものである。糖の種類は特に制限されず、ショ糖、果糖、水飴等が好ましく挙げられる。非酸性素材の糖度は、好ましくは50度以上70度未満である。非酸性素材の糖度をこのような範囲とすることにより、工業的生産において、粘度調整などがしやすい。また、本発明のpH低下が抑制された状態での保存において、微生物汚染を有効に防ぐことができ、良好な風味の保持に有利である。   The non-acidic material preferably contains sugar. The type of sugar is not particularly limited, and sucrose, fructose, starch syrup and the like are preferable. The sugar content of the non-acidic material is preferably 50 degrees or more and less than 70 degrees. By adjusting the sugar content of the non-acidic material to such a range, viscosity adjustment and the like can be easily performed in industrial production. Moreover, in the preservation | save in the state by which pH fall of this invention was suppressed, microbial contamination can be prevented effectively and it is advantageous to maintenance of favorable flavor.

本発明において、糖度はBrix値を意味し、糖度計(Brix計)で測定することができる。
また、非酸性素材としては、シロップ状、ペースト状のものが好ましく用いられる。
In the present invention, the sugar content means a Brix value, and can be measured with a sugar content meter (Brix meter).
In addition, as the non-acidic material, a syrup or paste is preferably used.

前記非酸性素材の粘度は、増粘剤の添加により調整することができる。増粘剤としては、グアガム、キサンタンガム、ペクチン等を用いることができる。   The viscosity of the non-acidic material can be adjusted by adding a thickener. As the thickener, guar gum, xanthan gum, pectin and the like can be used.

非酸性素材の組成として、例えば、以下の処方が好ましく挙げられる。
ショ糖、果糖、水飴から選ばれる糖類:30〜80質量%
水:0〜40質量%
風味づけに用いられる素材(ゴマ、チョコレート、抹茶):4〜40質量%
増粘剤:0〜0.5質量%
As the composition of the non-acidic material, for example, the following prescription is preferably exemplified.
Saccharose selected from sucrose, fructose, and starch syrup: 30-80% by mass
Water: 0 to 40% by mass
Ingredients used for flavoring (sesame, chocolate, matcha): 4-40% by mass
Thickener: 0 to 0.5% by mass

前記非酸性素材の濃縮発酵乳への添加は、発酵物全量に対して、好ましくは5質量%以上30質量%未満、さらに好ましくは10質量%以上25質量%未満の含有量で実施される。このような範囲で非酸性素材を添加することにより、製造される濃縮発酵乳のpHが良好な範囲となる。
また、非酸性素材の発酵物への添加は、非酸性素材を添加した後の濃縮発酵乳のpHが、4.7以上、好ましくはpH4.9〜5.0程度となるように行うことが好ましい。
The addition of the non-acidic material to the concentrated fermented milk is performed with a content of preferably 5% by mass or more and less than 30% by mass, and more preferably 10% by mass or more and less than 25% by mass with respect to the total amount of the fermented product. By adding a non-acidic material in such a range, the pH of the concentrated fermented milk produced becomes a favorable range.
Moreover, the addition of the non-acidic material to the fermented product may be performed so that the pH of the concentrated fermented milk after adding the non-acidic material is 4.7 or more, preferably about pH 4.9 to 5.0. preferable.

また、前記非酸性素材の添加量は、濃縮発酵乳の糖度が15度以上30度未満となるような量を目安とすることもできる。このような範囲で非酸性素材を混合することにより、素材の風味を生かした嗜好性の高い発酵乳を製造できるだけでなく、本発明のpH低下が抑制された状態での保存において、微生物汚染を有効に防ぐことができ、良好な風味の保持に有利である。   Further, the amount of the non-acidic material added may be an amount such that the sugar content of the concentrated fermented milk is 15 degrees or more and less than 30 degrees. By mixing non-acidic materials in such a range, not only can fermented milk with high taste taking advantage of the flavor of the materials be produced, but also in storage in a state where the pH reduction of the present invention is suppressed, microbial contamination is prevented. It can be effectively prevented and is advantageous for maintaining a good flavor.

製造された濃縮発酵乳は、80〜500ml容程度、好ましくは80〜250ml容程度の容器に充填し、密閉する。非酸性素材を添加する形態の濃縮発酵乳については、非酸性素材を濃縮発酵乳とは別にポーション容器等に充填し、喫食する際に非酸性素材を添加するような包装形態としてもよい。
また、容器入りの製品は、通常10℃以下、好ましくは5℃以下で保存する。
容器は、紙製、ガラス製、プラスチック製(例えばポリプロピレン製、ポリエチレンテレフタレート(PET)製、ポリスチレン製、ポリエチレン製)が好ましい。
The produced concentrated fermented milk is filled in a container of about 80 to 500 ml, preferably about 80 to 250 ml, and sealed. About the concentrated fermented milk of the form which adds a non-acidic raw material, it is good also as a packaging form which fills a non-acidic raw material into a portion container etc. separately from concentrated fermented milk, and adds a non-acidic raw material when eating.
The product in a container is usually stored at 10 ° C. or lower, preferably 5 ° C. or lower.
The container is preferably made of paper, glass, or plastic (for example, polypropylene, polyethylene terephthalate (PET), polystyrene, or polyethylene).

[試験1]
本試験は、本発明の方法(濃縮工程前に希釈工程を含む方法)の酸度上昇の抑制効果を測定するために行った。
[Test 1]
This test was performed in order to measure the inhibitory effect on the increase in acidity of the method of the present invention (a method including a dilution step before the concentration step).

<比較例1>
表1に示す処方にて調乳液を調製し、調乳液を均質機で15MPaで均質化し、プレート式加熱機を用いて90℃、10分間加熱処理して発酵乳ベースを調製した。続いて、調製した発酵乳ベースに乳酸菌スターター(クリスチャン・ハンセン社製、YF-L904)を0.001質量%の割合で添加し、pHが4.4になった時点で冷却により発酵を終了し、発酵物中のカードを破砕した。得られた発酵物500gについて、限外濾過膜(UF膜)を用いて質量が2分の1になるまで濃縮を行い、比較例1である250gの濃縮発酵乳を得た。前記発酵物の濃縮の前後における成分組成を表2に示す。
また、図1に比較例1の製造フローの概略、発酵物の質量の増減の概念を示す。
<Comparative Example 1>
A milk preparation was prepared according to the formulation shown in Table 1, the milk preparation was homogenized at 15 MPa with a homogenizer, and heat-treated at 90 ° C. for 10 minutes using a plate heater to prepare a fermented milk base. Subsequently, lactic acid bacteria starter (manufactured by Christian Hansen, YF-L904) was added to the prepared fermented milk base at a rate of 0.001% by mass, and when the pH reached 4.4, the fermentation was terminated by cooling. The curd in the fermented product was crushed. About 500 g of the obtained fermented product, concentration was performed using an ultrafiltration membrane (UF membrane) until the mass became a half, and 250 g of concentrated fermented milk as Comparative Example 1 was obtained. The component composition before and after concentration of the fermented product is shown in Table 2.
Moreover, the outline of the manufacturing flow of the comparative example 1 and the concept of increase / decrease in the mass of fermented material are shown in FIG.

<実施例1>
比較例1と同様の方法にて得られた発酵物500gに対し、500gの純水(希釈液)を混合した後、限外濾過膜(UF膜)を用いて、希釈発酵物の質量が4分の1になるまで濃縮を行い、実施例1である250gの濃縮発酵乳を得た。図1に実施例1の製造フローの概略、発酵物の質量の増減の概念を示す。濃縮発酵乳の無脂乳固形分、脂肪、タンパク質の組成は、比較例1と同じであった。
<Example 1>
After mixing 500 g of pure water (diluted solution) to 500 g of the fermented product obtained by the same method as Comparative Example 1, the mass of the diluted fermented product is 4 using an ultrafiltration membrane (UF membrane). Concentration was performed until it became a fraction, and 250 g of concentrated fermented milk as Example 1 was obtained. The outline of the manufacturing flow of Example 1 and the concept of the increase / decrease in the mass of fermented material are shown in FIG. The composition of the non-fat milk solid content, fat, and protein of the concentrated fermented milk was the same as in Comparative Example 1.

<比較例2>
比較例1と同様に調製した調乳液500gに対し500gの純水(希釈液)を混合した後、pHが4.4になるまで発酵を行った。続いて、限外濾過膜(UF膜)を用いて、発酵物の質量が4分の1になるまで濃縮を行うことにより、比較例2である250gの濃縮発酵乳を得た。図1に比較例2の製造フローの概略、発酵物の質量の増減の概念を示す。濃縮発酵乳の無脂乳固形分、脂肪、タンパク質の組成は、比較例1と同じであった。
<Comparative Example 2>
500 g of pure water (diluent) was mixed with 500 g of the milk preparation prepared in the same manner as in Comparative Example 1, and then fermentation was performed until the pH reached 4.4. Subsequently, 250 g of concentrated fermented milk as Comparative Example 2 was obtained by performing concentration using an ultrafiltration membrane (UF membrane) until the mass of the fermented product became 1/4. The outline of the manufacturing flow of the comparative example 2 and the concept of the increase / decrease in the mass of fermented material are shown in FIG. The composition of the non-fat milk solid content, fat, and protein of the concentrated fermented milk was the same as in Comparative Example 1.

表3に、実施例及び比較例における希釈倍率、濃縮効率、発酵後pH、発酵後酸度、濃縮後酸度、酸度増加分、酸度上昇率、比較例1に対する酸度上昇抑制率を示す。なお、表中、希釈倍率は、希釈発酵物の質量/発酵後の発酵物の質量で表す。また、発酵物に対する濃縮効率は、濃縮発酵乳の質量/発酵後の発酵物の質量で表し、希釈発酵物に対する濃縮効率は、濃縮発酵乳の質量/希釈発酵物の質量で表す。また、酸度は乳酸酸度である。また、酸度上昇率は、(濃縮後酸度−発酵後酸度)/発酵後酸度で表す(いずれも試験2、試験3において同じ)。
また、図2に、得られた濃縮発酵乳の粒度分布をLA−950(HORIBA社製)を用いて測定した結果を示す。
Table 3 shows the dilution rate, concentration efficiency, post-fermentation pH, post-fermentation acidity, post-concentration acidity, acidity increase, acidity increase rate, and acidity increase inhibition rate relative to Comparative Example 1 in Examples and Comparative Examples. In the table, the dilution rate is expressed as the mass of diluted fermented product / the mass of fermented product after fermentation. Moreover, the concentration efficiency with respect to a fermented product is represented by the mass of concentrated fermented milk / the mass of the fermented product after fermentation, and the concentration efficiency with respect to a diluted fermented product is represented by the mass of concentrated fermented milk / the mass of the diluted fermented product. The acidity is lactic acid acidity. The rate of increase in acidity is expressed by (acidity after concentration−acidity after fermentation) / acidity after fermentation (both are the same in Test 2 and Test 3).
Moreover, the result of having measured the particle size distribution of the obtained concentrated fermented milk in FIG. 2 using LA-950 (made by HORIBA) is shown.

表3から分かるように、実施例1の方法で製造した濃縮発酵乳は、比較例1の方法(従来方法)で製造した濃縮発酵乳と比較して、濃縮による酸度上昇を11%抑制することができた。また、図2から分かるように、実施例1の方法で製造した濃縮発酵乳は、比較例1の方法で製造した濃縮発酵乳と近似した粒度分布を有していた。これより、濃縮発酵乳の製造において、発酵工程後、濃縮工程前に希釈工程を行うことで、濃縮発酵乳の食感を維持しながら、酸味を低減した濃縮発酵乳を製造することができることがわかった。   As can be seen from Table 3, the concentrated fermented milk produced by the method of Example 1 suppresses the increase in acidity by 11% compared to the concentrated fermented milk produced by the method of Comparative Example 1 (conventional method). I was able to. Further, as can be seen from FIG. 2, the concentrated fermented milk produced by the method of Example 1 had a particle size distribution that approximated that of the concentrated fermented milk produced by the method of Comparative Example 1. From this, in the production of concentrated fermented milk, it is possible to produce concentrated fermented milk with reduced acidity while maintaining the texture of the concentrated fermented milk by performing a dilution step after the fermentation step and before the concentration step. all right.

一方、比較例2の方法で製造した濃縮発酵乳は、濃縮後に酸度が著しく上昇した。また、比較例1の方法で製造した濃縮発酵乳と比較して、大きい粒子径の粒子の割合が増加し、ぼそぼそとした粗い組織になった。これより、調乳液の調製時に希釈する方法では、酸度を低下させ、風味や食感に優れた濃縮発酵乳を製造することができないことがわかった。   On the other hand, the concentrated fermented milk produced by the method of Comparative Example 2 significantly increased the acidity after concentration. Moreover, compared with the concentrated fermented milk manufactured with the method of the comparative example 1, the ratio of the particle | grains with a large particle diameter increased, and it became a rough and rough structure. From this, it turned out that the method of diluting at the time of preparation of milk preparation liquid cannot manufacture concentrated fermented milk which reduced acidity and was excellent in flavor and texture.

[試験2]
本試験は、希釈倍率を変化させることによる酸度上昇の抑制効果への影響を測定するために行った。
[Test 2]
This test was performed in order to measure the influence on the inhibitory effect of the increase in acidity by changing the dilution factor.

<比較例3>
比較例1と同様の方法により、濃縮発酵乳を製造した。但し、比較例3では、pHが4.8になった時点で冷却により発酵を終了した。
得られた発酵物1000gについて、限外濾過膜(UF膜)を用いて発酵物の質量が2分の1になるまで濃縮を行い、比較例3である500gの濃縮発酵乳を得た。濃縮発酵乳の無脂乳固形分、脂肪、タンパク質の組成は、比較例1と同じであった。
<Comparative Example 3>
Concentrated fermented milk was produced in the same manner as in Comparative Example 1. However, in Comparative Example 3, the fermentation was terminated by cooling when the pH reached 4.8.
About 1000 g of the obtained fermented product, concentration was performed using an ultrafiltration membrane (UF membrane) until the mass of the fermented product was reduced to one half, and 500 g of concentrated fermented milk as Comparative Example 3 was obtained. The composition of the non-fat milk solid content, fat, and protein of the concentrated fermented milk was the same as in Comparative Example 1.

<実施例2、3>
比較例3と同様の方法にて得られた発酵物1000gに対し、500g又は2000gの純水(希釈液)を混合しながら濃縮し、それぞれ実施例2及び実施例3である各500gの濃縮発酵乳を得た。希釈工程及び濃縮工程は、実施例1と同様の方法で行った。何れの実施例で得られた濃縮発酵乳についても、無脂乳固形分、脂肪、タンパク質の組成は、比較例1と同じであった。
<Examples 2 and 3>
Concentrate while mixing 500 g or 2000 g of pure water (diluent) with respect to 1000 g of the fermented product obtained by the same method as in Comparative Example 3, and 500 g of each of concentrated fermentations in Example 2 and Example 3, respectively. I got milk. The dilution step and the concentration step were performed in the same manner as in Example 1. About the concentrated fermented milk obtained in any Example, the composition of non-fat milk solid content, fat, and protein was the same as that of the comparative example 1.

表4に、実施例及び比較例における希釈倍率、濃縮効率、発酵後pH、発酵後酸度、濃縮後酸度、酸度増加分、酸度上昇率、比較例3に対する酸度上昇抑制率を示す。また、図3に各濃縮発酵乳の粒度分布を示す。粒度分布の測定は、試験1と同様に行った。   Table 4 shows the dilution ratio, concentration efficiency, post-fermentation pH, post-fermentation acidity, post-concentration acidity, acidity increase, acidity increase rate, and acidity increase inhibition rate relative to Comparative Example 3 in Examples and Comparative Examples. Moreover, the particle size distribution of each concentrated fermented milk is shown in FIG. The particle size distribution was measured in the same manner as in Test 1.

前述した表3における実施例1(2倍希釈で酸度上昇抑制率11%)と、表4における実施例2(1.5倍希釈で酸度上昇抑制率24%)とを比較すると分かるように、発酵工程後の発酵物の酸度を低く調整することで、希釈工程による酸度上昇抑制効果をより顕著に得ることができることがわかった。また、実施例3の方法では、32%もの酸度上昇抑制率を得ることができた。
また、実施例3の方法で製造した濃縮発酵乳は、比較例3の方法(従来方法)で製造した濃縮発酵乳と比較して、小さい粒子径の粒子の割合が増加し、滑らかな組織となった。これより、希釈発酵物の質量が、発酵により調製した発酵物の3倍以上となるような希釈倍率で希釈することにより、特に滑らかな食感に優れた濃縮発酵乳を製造することができることがわかった。
As can be seen by comparing Example 1 in Table 3 (2% dilution with an acidity increase suppression rate of 11%) and Example 4 in Table 4 (1.5 dilution with an acidity increase suppression rate of 24%), It turned out that the acidity raise inhibitory effect by a dilution process can be acquired more notably by adjusting low the acidity of the fermented material after a fermentation process. Further, in the method of Example 3, an acidity increase suppression rate of 32% could be obtained.
In addition, the concentrated fermented milk produced by the method of Example 3 has an increased proportion of particles with a small particle size compared to the concentrated fermented milk produced by the method of Comparative Example 3 (conventional method), and a smooth tissue. became. From this, it is possible to produce concentrated fermented milk with particularly smooth texture by diluting at a dilution ratio such that the mass of the diluted fermented product is 3 times or more that of the fermented product prepared by fermentation. all right.

[試験3]本試験は、希釈倍率の好ましい範囲を検討する目的で行った。
<比較例4>
比較例1と同様の方法により、濃縮発酵乳を製造した。但し、比較例4では、pHが4.8になった時点で冷却により発酵を終了した。
得られた発酵物1000gについて、限外濾過膜(UF膜)を用いて発酵物の質量が2分の1になるまで濃縮を行い、比較例4である500gの濃縮発酵乳を得た。濃縮発酵乳の無脂乳固形分、脂肪、タンパク質の組成は、比較例1と同じであった。
[Test 3] This test was conducted for the purpose of examining a preferable range of dilution ratio.
<Comparative example 4>
Concentrated fermented milk was produced in the same manner as in Comparative Example 1. However, in Comparative Example 4, the fermentation was terminated by cooling when the pH reached 4.8.
About 1000 g of the obtained fermented product, concentration was performed using an ultrafiltration membrane (UF membrane) until the mass of the fermented product was reduced to one half, and 500 g of concentrated fermented milk as Comparative Example 4 was obtained. The composition of the non-fat milk solid content, fat, and protein of the concentrated fermented milk was the same as in Comparative Example 1.

<実施例4>
比較例4と同様の方法にて得られた発酵物1000gに対し、10gの純水(希釈液)を混合しながら濃縮し、実施例4である500gの濃縮発酵乳を得た。希釈工程及び濃縮工程は、実施例1と同様の方法で行った。濃縮発酵乳の無脂乳固形分、脂肪、タンパク質の組成は、比較例1と同じであった。
<Example 4>
10 g of pure water (diluent) was concentrated while mixing with 1000 g of the fermented product obtained in the same manner as in Comparative Example 4, and 500 g of concentrated fermented milk as Example 4 was obtained. The dilution step and the concentration step were performed in the same manner as in Example 1. The composition of the non-fat milk solid content, fat, and protein of the concentrated fermented milk was the same as in Comparative Example 1.

表5に、実施例4及び比較例4における希釈倍率、濃縮効率、発酵後pH、発酵後酸度、濃縮後酸度、酸度増加分、酸度上昇率、比較例4に対する酸度上昇抑制率を示す。   Table 5 shows the dilution ratio, concentration efficiency, post-fermentation pH, post-fermentation acidity, post-concentration acidity, acidity increase, acidity increase rate, and acidity increase inhibition rate relative to Comparative Example 4 in Example 4 and Comparative Example 4.

表5に示される通り、実施例4では、12%の酸度上昇抑制率を得ることができた。これより、希釈倍率が1.01倍という比較的低い値であっても、本発明の酸度上昇を抑制する効果が得られることがわかった。   As shown in Table 5, in Example 4, an acidity increase suppression rate of 12% could be obtained. From this, it was found that even if the dilution ratio is a relatively low value of 1.01, the effect of suppressing the increase in acidity of the present invention can be obtained.

[試験4]
本試験は、本発明の方法で製造した濃縮発酵乳に非酸性素材を添加した場合の風味について評価するために行った。
官能評価は、訓練された6名のパネリストにより行った。試験2で製造した比較例3、実施例2、3の濃縮発酵乳について、プレーンでの「味のマイルドさ」とチョコレートシロップ(ハーシーチョコレートシロップ、ハーシージャパン株式会社)を適量かけた状態での「チョコレートシロップとの相性」を以下の基準に従い、5段階で評価した。評価結果を、各パネリストが付した評点の平均値として表6に示す。
[Test 4]
This test was conducted to evaluate the flavor when a non-acidic material was added to the concentrated fermented milk produced by the method of the present invention.
Sensory evaluation was performed by six trained panelists. About the concentrated fermented milks of Comparative Example 3 and Examples 2 and 3 produced in Test 2, the “taste mildness” in plain and chocolate syrup (Hershey Chocolate Syrup, Hershey Japan Co., Ltd.) “Compatibility with chocolate syrup” was evaluated according to the following criteria in five stages. The evaluation results are shown in Table 6 as the average value of the scores given by each panelist.

(評価基準)
〔味のマイルドさ〕
1:酸っぱい
2:やや酸っぱい
3:ややマイルド
4:マイルド
5:非常にマイルド
(Evaluation criteria)
[Mild taste]
1: Sour 2: Slightly sour 3: Slightly mild 4: Mild 5: Very mild

〔チョコレートシロップとの相性〕
1:合わない
2:やや合わない
3:やや合う
4:合う
5:非常に合う
[Compatibility with chocolate syrup]
1: Does not fit 2: Does not fit slightly 3: Fits slightly 4: Fits 5: Fits very well

表6に示すように、実施例2、3の方法で製造した濃縮発酵乳が、比較例3(従来方法)より製造した濃縮発酵乳に比較してマイルドであり、チョコレートシロップとの相性も良いという結果となった。特に、濃縮後酸度が0.77質量%である実施例3では、チョコレートシロップとの相性が良いことがわかった。これより、非酸性素材との相性の観点からは、濃縮後酸度は、0.95質量%以下であることが好ましく、0.8質量%以下であることが特に好ましいことがわかった。   As shown in Table 6, the concentrated fermented milk produced by the methods of Examples 2 and 3 is milder than the concentrated fermented milk produced by Comparative Example 3 (conventional method) and has good compatibility with chocolate syrup. It became the result. In particular, in Example 3 where the acidity after concentration was 0.77% by mass, it was found that the compatibility with chocolate syrup was good. From this, it was found that the acidity after concentration is preferably 0.95% by mass or less and particularly preferably 0.8% by mass or less from the viewpoint of compatibility with the non-acidic material.

本発明は、非酸性素材の風味を生かした濃縮発酵乳の製造に利用できる。   INDUSTRIAL APPLICATION This invention can be utilized for manufacture of the concentrated fermented milk using the flavor of a non-acidic material.

Claims (7)

調乳液を発酵して発酵物を調製する発酵工程と、調製した発酵物を濃縮して濃縮発酵乳を調製する濃縮工程とを含む、濃縮発酵乳の製造方法であって、
前記濃縮工程の前に、前記発酵物を希釈液により希釈して希釈発酵物を調製する希釈工程を含むことを特徴とする、濃縮発酵乳の製造方法。
A method for producing concentrated fermented milk, comprising a fermentation step of fermenting a milk preparation to prepare a fermented product and a concentration step of concentrating the prepared fermented product to prepare a concentrated fermented milk,
Before the said concentration process, the manufacturing method of concentrated fermented milk characterized by including the dilution process which dilutes the said fermented material with a diluent, and prepares a diluted fermented material.
前記希釈工程中に前記濃縮工程を開始し、該濃縮工程中に前記希釈工程を終了することを特徴とする、請求項1に記載の濃縮発酵乳の製造方法。   The method for producing concentrated fermented milk according to claim 1, wherein the concentration step is started during the dilution step, and the dilution step is ended during the concentration step. 前記濃縮工程は、前記濃縮発酵乳の質量が、前記発酵物の質量に対して3分の2以下となるように行うことを特徴とする、請求項1又は2に記載の濃縮発酵乳の製造方法。   The said concentration process is performed so that the mass of the said concentrated fermented milk may become 2/3 or less with respect to the mass of the said fermented material, The manufacture of concentrated fermented milk of Claim 1 or 2 characterized by the above-mentioned. Method. 前記濃縮工程は、前記濃縮発酵乳の無脂乳固形分が10質量%以上となるように行うことを特徴とする、請求項1〜3の何れかに記載の濃縮発酵乳の製造方法。   The said concentration process is performed so that the non-fat milk solid content of the said concentrated fermented milk may be 10 mass% or more, The manufacturing method of the concentrated fermented milk in any one of Claims 1-3 characterized by the above-mentioned. 前記希釈工程は、前記希釈発酵物の質量が、前記発酵物の質量に対して1.01〜4倍となるように希釈することを特徴とする、請求項1〜4の何れかに記載の濃縮発酵乳の製造方法。   The said dilution process dilutes so that the mass of the said diluted fermented product may be 1.01-4 times with respect to the mass of the said fermented product, The one in any one of Claims 1-4 characterized by the above-mentioned. A method for producing concentrated fermented milk. 前記希釈工程及び濃縮工程は、前記濃縮発酵乳の乳酸酸度と、前記発酵物の乳酸酸度の差が0.25質量%以下となるように行うことを特徴とする、請求項1〜5の何れかに記載の濃縮発酵乳の製造方法。   The said dilution process and concentration process are performed so that the difference of the lactic acid acidity of the said concentrated fermented milk and the lactic acid acidity of the said fermented product may be 0.25 mass% or less, The any one of Claims 1-5 characterized by the above-mentioned. The manufacturing method of the concentrated fermented milk of crab. 前記希釈工程及び濃縮工程は、濃縮発酵乳における乳酸酸度が0.95質量%以下となるように行い、前記濃縮工程後に、濃縮発酵乳に非酸性素材を添加する非酸性素材添加工程を含むことを特徴とする、請求項1〜6の何れかに記載の濃縮発酵乳の製造方法。   The dilution step and the concentration step include a non-acidic material addition step of adding a non-acidic material to the concentrated fermented milk after the concentration step, so that the lactic acid acidity in the concentrated fermented milk is 0.95% by mass or less. The manufacturing method of the concentrated fermented milk in any one of Claims 1-6 characterized by these.
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JP5940485B2 (en) * 2013-04-18 2016-06-29 森永乳業株式会社 Method for producing fermented milk containing non-acidic material

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