JP6562218B2 - Coke oven coal charging method - Google Patents

Coke oven coal charging method Download PDF

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JP6562218B2
JP6562218B2 JP2016159827A JP2016159827A JP6562218B2 JP 6562218 B2 JP6562218 B2 JP 6562218B2 JP 2016159827 A JP2016159827 A JP 2016159827A JP 2016159827 A JP2016159827 A JP 2016159827A JP 6562218 B2 JP6562218 B2 JP 6562218B2
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光太郎 安村
光太郎 安村
松井 貴
貴 松井
大輔 今西
大輔 今西
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JFE Steel Corp
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本発明は、室炉式コークス炉の炭化室へ装入孔から成型炭を装入するコークス炉の石炭装入方法、特に、原料として成型炭を100%使用する際のコークス炉の石炭装入方法に関する。   The present invention relates to a method for charging coal in a coke oven in which coal is charged from a charging hole into a carbonization chamber of a chamber-type coke oven, and in particular, coal charging in a coke oven when 100% of coal is used as a raw material. Regarding the method.

高炉で使用されるコークスを製造する設備として、室炉式コークス炉(以下、単に「コークス炉」と呼ぶ)が利用されている。コークス炉は、炉幅方向に離間して並列する燃焼室とそれらの燃焼室に挟まれて設けられている炭化室から構成されている。そして、このコークス炉の炭化室の天井には、複数個通常4〜5個の一列に設けられた装入孔が配設されており、原料炭はその装入孔を通じて炭化室内に装入され、前記燃焼室でガスを燃焼して発生する熱を耐火物を介して炭化室に供給することにより、乾留し、コークスを製造している。   As a facility for producing coke used in a blast furnace, a chamber-type coke oven (hereinafter simply referred to as “coke oven”) is used. The coke oven is composed of combustion chambers spaced apart in parallel in the furnace width direction and a carbonization chamber provided between the combustion chambers. A plurality of usually 4 to 5 charging holes are arranged on the ceiling of the carbonizing chamber of the coke oven, and the raw coal is charged into the carbonizing chamber through the charging hole. The coke is produced by dry distillation by supplying heat generated by burning gas in the combustion chamber to the carbonization chamber via a refractory.

高炉で使用されるコークスは、高炉への搬送時の衝撃や、高炉内の高温雰囲気下での流動降下時の摩擦等に耐えるために、冷間強度、熱間強度が高いことが要求される。そのために、原料となる石炭としては、乾留時に溶融、粘結する粘結炭が用いられている。しかし、世界で採掘可能な石炭の内、粘結炭は1割程度であり高価である。そのため、資源の有効利用の観点から、また、コークス製造コストの低減の観点から、原料として粘結性の低い一般炭をコークス炉で使用することが検討されてきた。その一方法として、一般炭を成型した成型炭を作り、これをコークス炉用の原料炭として使用する技術が開発されている。   Coke used in the blast furnace is required to have high cold strength and hot strength in order to withstand impact during transportation to the blast furnace and friction during flow drop in a high-temperature atmosphere in the blast furnace. . Therefore, caking coal that melts and caking during dry distillation is used as the raw material coal. However, caking coal is about 10% of coal that can be mined in the world and is expensive. Therefore, from the viewpoint of effective use of resources and from the viewpoint of reducing coke production costs, it has been studied to use steam coal with low caking property as a raw material in a coke oven. As one of the methods, a technique has been developed in which coking coal obtained by molding steam coal is used as coking coal for coke ovens.

コークス炉の炭化室に上方から成型炭を含む配合炭を装入する成型炭配合法は、1970年代より工業化され、既設コークス製造設備に成型炭製造設備を付設するだけで容易に実施できるプロセスであることから急速に普及し、コークスの品質向上と製造コスト低減に大きな役割を果たしている。一方、成型炭は粉炭をバインダーで結合させて製造されたものであり、衝撃によって容易に粉化するという問題があった。   The coking coal blending method of charging coking coal containing coking coal from above into the carbonization chamber of the coke oven has been industrialized since the 1970s, and is a process that can be easily implemented simply by attaching the coal making facility to existing coke production facilities. As a result, it spreads rapidly and plays a major role in improving coke quality and reducing manufacturing costs. On the other hand, cast charcoal is produced by combining pulverized coal with a binder and has a problem of being easily pulverized by impact.

特に、成型炭をコークス炉の炭化室へ装入するときは、炭化室の炉高分に相当する5〜8m程度落下することで大きな衝撃を受け、粉化することになる。コークス炉内で成型炭が粉化すると、装入された成型炭のかさ密度が部分的に過剰となり、乾留後に得られたコークスのコークス押出時の負荷増大や乾留不良を起こす問題があった。   In particular, when charging the coal into the carbonization chamber of the coke oven, it is impacted and powdered by dropping about 5 to 8 m corresponding to the furnace height of the carbonization chamber. When coking coal is pulverized in a coke oven, the bulk density of the charging coal is partially excessive, and there is a problem in that the coke obtained after dry distillation has increased load during coke extrusion and poor dry distillation.

このような成型炭の粉化を避けるために、特許文献1では、成型炭と粉炭とを使い、最初に粉炭のみを全装炭量の30mass%ないし60mass%入れた後に、残量は粉炭と成型炭の混合物として装入する方法を提案している。   In order to avoid such coal pulverization, Patent Document 1 uses coal coal and pulverized coal, and after only putting pulverized coal at 30 mass% to 60 mass% of the total amount of coal, the remaining amount is pulverized coal. A method of charging as a mixture of coal is proposed.

特開平1−178589号公報JP-A-1-178589

しかしながら、特許文献1の方法は、成型炭と共に配合炭を混合装入する方法であり、高価な配合炭の使用を前提とする方法であって、資源の有効利用の観点から、および、コークス製造コストの低減の観点から、改善が求められていた。   However, the method of Patent Document 1 is a method in which blended coal is mixed and charged with coal, and is a method premised on the use of expensive blended coal, from the viewpoint of effective use of resources, and coke production. Improvement has been demanded from the viewpoint of cost reduction.

そこで本発明の目的は、コークス炉に成型炭のみを装入する場合においても、コークス押出し負荷の増大や乾留不良を招くことなく、しかも、資源の有効利用およびコークス製造コストの低減を達成することができる、新規なコークス炉の石炭装入方法を提案することにある。   Accordingly, an object of the present invention is to achieve effective use of resources and reduction of coke production cost without causing an increase in coke extrusion load and poor carbonization even when only coal is charged into a coke oven. Is to propose a new method for charging coal in a coke oven.

従来技術が抱えている前述した課題について鋭意検討を重ねた結果、発明者らは、コークス炉の炭化室へ装入孔から成型炭を装入する際、成型炭を炭化室の底部に直接落下させる場合と比べ、(1)成型炭の落下によって発生した粉炭がまわり、例えば隣りの装入孔の直下の辺りまで拡散すること、(2)装入する成型炭を炭化室の底部にクッションとなる物体(先行装入した成型炭や粉炭)を介して装入した方が成型炭の粉化が少ないこと、などを突き止めて、本発明を開発した。   As a result of intensive investigations on the above-mentioned problems of the prior art, the inventors dropped the coal directly into the bottom of the carbonization chamber when charging the coal into the carbonization chamber of the coke oven from the charging hole. Compared with the case where (1) the pulverized coal generated by the falling of the charcoal turns, for example, diffuses to just below the adjacent charging hole, and (2) the charging charcoal is placed at the bottom of the carbonization chamber with a cushion. The present invention was developed by ascertaining that there was less pulverization of the charcoal if the charcoal was charged via an object (preceding charcoal or pulverized charcoal).

即ち、本発明は、コークス炉の炭化室へ、この炭化室の天井に設けた複数の装入孔を介して、成型炭のみを装入するコークス炉の石炭装入方法において、まず始めに、1つ置きの装入孔を選んで、成型炭全装入量のうちの一部を装入し、次いて、選択しなかった他の装入孔から、成型炭全装入量のうちのさらに一部を装入し、その後、成型炭全装入量のうちの残部を、全装入孔を使って装入することを特徴とするコークス炉の石炭装入方法にある。   That is, the present invention is a coke oven coal charging method for charging only coking coal into a coking oven carbonization chamber through a plurality of charging holes provided in the ceiling of the carbonization chamber. Select every other charging hole, charge a part of the total charcoal charging amount, and then, from the other charging holes not selected, out of the total charcoal charging amount Further, the present invention lies in a coal charging method for a coke oven, characterized in that a part is charged and then the remaining part of the total charging amount of the coal is charged using all charging holes.

なお、前記のように構成される本発明のコークス炉の石炭装入方法においては、
(1)まず始めに選択した装入孔を通じて装入する成型炭全装入量の一部の装入量が、全装入量の15mass%〜35mass%であり、次いで他の装入孔から装入する成型炭全装入量の一部の装入量が、全装入量の15mass%〜35mass%であり、そしてその後に装入する成型炭は全装入量の残部に当たる量であること、
(2)前記コークス炉が4個の装入孔を備える場合、最初の成型炭の装入をマシンサイドあるいはコークスサイド側から1番目および3番目の装入孔から実施し、次の成型炭の装入を2番目および4番目の装入孔から実施し、また、前記コークス炉が5個の装入孔を備える場合、最初の成型炭の装入をマシンサイドあるいはコークスサイド側から1番目、3番目および5番目とし、そして次の成型炭の装入を2番目および4番目とするかその逆のパターンで装入すること、
(3)前記最初の成型炭の装入、前記2回目の成型炭の装入、および、前記最後の成型炭の装入において、各回で装入すべき量の成型炭を各回で使用する装入孔に等分に分割して装入すること、
がより好ましい解決手段となるものと考えられる。
In addition, in the coal charging method of the coke oven of the present invention configured as described above,
(1) First, a part of the total charging amount of the charcoal charged through the selected charging hole is 15 mass% to 35 mass% of the total charging amount, and then from the other charging holes. A part of the total charging amount of the charcoal to be charged is 15 mass% to 35 mass% of the total charging amount, and the charcoal to be charged thereafter is an amount corresponding to the balance of the total charging amount. about,
(2) When the coke oven has four charging holes, the first charcoal is charged from the first and third charging holes from the machine side or the coke side, When charging is performed from the second and fourth charging holes, and the coke oven has five charging holes, the first charging of charcoal is performed first from the machine side or the coke side, 3rd and 5th, and the next charcoal charge is second and fourth or vice versa,
(3) In the charging of the first charcoal, the charging of the second charcoal, and the charging of the last charcoal, the amount of charcoal to be charged each time is charged each time. Divide into the entrance holes in equal parts,
Is considered to be a more preferable solution.

前述のように構成される本発明によれば、一列に並ぶ複数の装入孔のうち、隣り合わない装入孔例えば1つ置きの装入孔から、成型炭全装入量の一部を装入し、次に先に使用した装入孔とは違う他の装入孔から、残りの成型炭全装入量の一部を装入し、その後、残りの成型炭の全部を全装入孔を使って装入する方法であるから、コークス炉に成型炭のみを装入する場合においても、コークス押出負荷の増大や乾留不良を招くようなことがなくなり、しかも、資源の有効利用およびコークス製造コストの低減を達成することができる。   According to the present invention configured as described above, a part of the total amount of charcoal charging is obtained from the charging holes that are not adjacent to each other among the plurality of charging holes arranged in a row, for example, every other charging hole. First, charge a part of the remaining charcoal charge from another charge hole different from the charge hole used earlier, and then charge all the remaining charcoal. Since it is a method of charging using a hole, even when only coking coal is charged into a coke oven, it does not cause an increase in coke extrusion load or poor dry distillation, and more effective use of resources and A reduction in coke production costs can be achieved.

本発明の前提としてコークス炉への成型炭装入時における成型炭の粉化挙動を調べるために用いた模擬炭化室の一例を示す図である。It is a figure which shows an example of the simulated carbonization chamber used in order to investigate the pulverization behavior of the forming charcoal at the time of the charging of the charcoal to the coke oven as a premise of the present invention. 模擬炭化室内の各部位の粉化率を示す図である。It is a figure which shows the powdering rate of each site | part in a simulation carbonization chamber. 従来例に従って、各装入孔から成型炭を均等に同時に装入した状態を説明するための図である。It is a figure for demonstrating the state which inserted the charcoal equally from each charging hole simultaneously according to the prior art example. 本発明に従って、成型炭のみを各装入孔から適時・適量を1〜3回に分けて装入した状態を説明するための図である。It is a figure for demonstrating the state which injected | thrown-in only the charcoal from each charging hole according to this invention by dividing timely and appropriate quantity into 1 to 3 times.

まず、本発明のコークス炉の石炭装入方法を考える前提として、コークス炉の炭化室への成型炭装入時における成型炭の粉化挙動を調べた。具体的には、コークス炉の炭化室内へ装入孔から成型炭を装入したときの成型炭の粉化挙動を調査した。   First, as a premise for considering the method of charging coal in the coke oven of the present invention, the pulverization behavior of the forming coal at the time of charging the forming coal into the coking chamber of the coke oven was examined. Specifically, the pulverization behavior of the coal was investigated when the coal was charged from the charging hole into the carbonization chamber of the coke oven.

即ち、図1は、コークス炉へ成型炭のみを装入する時における成型炭の粉化挙動を調べるために用いた模擬炭化室の一例を示す図である。図1に示す例において、1は模擬炭化室、2は模擬炭化室1の側面に複数個所(ここでは32か所)に設けたサンプリング口、3は模擬炭化室1の上部に設けた装入孔、4は装入孔3と連通する成型炭ホッパーである。この模擬炭化室1の形状は、高さ(H)が7520mm、長さ(L)が3020mm、幅(W)が430mmである。   That is, FIG. 1 is a diagram showing an example of a simulated carbonization chamber used for investigating the pulverization behavior of coal when only coal is charged into a coke oven. In the example shown in FIG. 1, 1 is a simulated carbonization chamber, 2 is a sampling port provided at a plurality of locations (here 32 locations) on the side of the simulated carbonization chamber 1, and 3 is a charging provided at the top of the simulated carbonization chamber 1 The holes 4 are formed charcoal hoppers that communicate with the charging hole 3. The simulated carbonization chamber 1 has a height (H) of 7520 mm, a length (L) of 3020 mm, and a width (W) of 430 mm.

この模擬炭化室1は、炭化室の実機大を模擬したものであり、一つの装入孔3から成型炭を装入して、成型炭を模擬炭化室1の底部から上部に亘って供給した後に、模擬炭化室1の側面に設けた複数のサンプリング口2から炭化室の各部位に堆積した成型炭をサンプリングすることで、サンプリング口2の存在する各部位における成型炭の粉化率を調査することができる。   This simulated carbonization chamber 1 simulates the actual machine size of the carbonization chamber. Charcoal is charged from one charging hole 3 and fed from the bottom to the top of the simulated carbonization chamber 1. Later, by sampling the coal formed in each part of the carbonization chamber from a plurality of sampling ports 2 provided on the side surface of the simulated carbonization chamber 1, the pulverization rate of the coal in each part where the sampling port 2 exists is investigated. can do.

本発明において用いる成型炭としては、粘結炭、非粘結炭等の炭材原料にバインダーを加えて、成型機にて混練成型し、圧潰強度170kg/個に調整したものを用いた。その成型炭の形状は、44mm×44mm×31mmのマセック型とした。   As the charcoal used in the present invention, a carbonaceous material such as caking coal or non-caking charcoal was added with a binder, kneaded with a molding machine, and adjusted to a crushing strength of 170 kg / piece. The shape of the charcoal was a Macek type of 44 mm × 44 mm × 31 mm.

調査に当たっては、上記成型炭を前記模擬炭化室1の装入孔3から炭化室内へ装入し、各サンプリング口2から取り出した成型炭の粉化率を求め、これを図2に示した。ここで、粉化率とは、各サンプルを15mm角の篩で篩い分けし、篩下の質量のサンプル質量に対する百分率で示した。   In the investigation, the above-mentioned coal was charged into the carbonization chamber from the charging hole 3 of the simulated carbonization chamber 1, and the pulverization rate of the coal was extracted from each sampling port 2, and this is shown in FIG. Here, the pulverization rate was obtained by sieving each sample with a 15 mm square sieve and expressed as a percentage of the mass under the sieve with respect to the sample mass.

図2に示す結果から明らかなように、装入孔3の直下の炭化室炉底部近辺では粉化率が20mass%程度と高いのに比べて、上方に行くに従い粉化率が低下していることが判る。また、装入孔3の直下に隣接するサンプリング口2から採取したサンプルの粉化率は、装入孔3の直下のサンプルと比較して、非常に粉化率が低いことが判る。   As is clear from the results shown in FIG. 2, the powdering rate is lower in the vicinity of the bottom of the carbonization chamber furnace immediately below the charging hole 3 as compared with the high powdering rate of about 20 mass%. I understand that. It can also be seen that the powdering rate of the sample collected from the sampling port 2 adjacent immediately below the charging hole 3 is much lower than that of the sample immediately below the charging hole 3.

粉化率のこのような傾向は、装入孔3の直下の炉底部では、落下する成型炭が硬い炉底耐火物と衝突することでより粉化しやすいためと考えられ、また、既に成型炭が堆積をして炉底耐火物との直接的な衝突が回避できる場合では、堆積した成型炭の山の頂部にある成型炭と落下する成型炭とが衝突することによって粉化が緩和されるためと考えられる。一方、装入孔直下に隣接する領域では、装入された成型炭が両脇へ流れ込むことで堆積することから、衝突の影響が小さいためと考えられる。   Such a tendency of the pulverization rate is thought to be because the falling coal at the bottom of the furnace directly below the charging hole 3 is more likely to be pulverized by colliding with a hard furnace bottom refractory, and has already been formed. In the case where it is possible to avoid a direct collision with the furnace bottom refractory, the pulverization is mitigated by the collision of the coal at the top of the pile of the deposited coal and the falling coal. This is probably because of this. On the other hand, in the region adjacent immediately below the charging hole, the charged coal is deposited by flowing into both sides, so it is considered that the influence of the collision is small.

この結果から考えると、炭化室へ成型炭を装入する際に、従来のように各装入孔から同時装入をすると、図3に示すように、装入初期に各装入孔の直下に装入される成型炭は20mass%程度の粉化を受けることになり、この部分は粉が多いためにかさ密度が上昇し、コークス押出時の負荷を増大する要因となることがわかる。   Considering this result, when charging coal into the carbonization chamber, if simultaneous charging is performed from each charging hole as in the past, as shown in FIG. 3, immediately below each charging hole, as shown in FIG. It can be seen that the cast charcoal to be charged into is subjected to pulverization of about 20 mass%, and this portion has a large amount of powder, so that the bulk density rises and becomes a factor of increasing the load at the time of coke extrusion.

そこで、本発明では、炭化室の天井に複数(例えば4〜5個)の装入孔を配設している場合において、隣り合わない装入孔、つまり1つ置きの装入孔の2個ないし3個から、まず最初に全装炭量のうちの一部、好ましくは15mass%〜35mass%を2分ないし3分して装入した後、次に使用しなかった他の装入孔から、やはり全装炭量の一部、好ましくは15mass%〜35mass%を装入し、最後に、残部の成型炭を全装入孔を使って、できれば均等の量を装入することにした。   Therefore, in the present invention, when a plurality of (for example, 4 to 5) charging holes are provided on the ceiling of the carbonization chamber, two charging holes that are not adjacent to each other, that is, every other charging hole, are provided. From 3 or more, after first charging a portion of the total coal charge, preferably 15 mass% to 35 mass% in 2 to 3 minutes, then from other charging holes not used Also, it was decided that a part of the total coal charge, preferably 15 mass% to 35 mass%, was charged, and finally, the remaining cast charcoal was charged in an equal amount if possible using all the charging holes.

例えば、炭化室の天井に装入孔を4個配設してなる炭化室の場合、図4に示すように、最初に、マシンサイドから#1、#3の1つ置きの装入孔から所定量(一部)の成型炭を装入し、山を形成して隣りの装入孔の直下に粉化率の少ない成型炭を堆積させた後に、他の装入孔から残りの所定量(一部)の成型炭を装入する。そうすることで、他の装入孔から装入した成型炭は硬い炭化室炉底耐火物と衝突をすることなく装入(堆積)することになる。そのため、最初の装入で粉化率が20mass%にも及ぶような従来法と比べると、本発明に従ってまず1つ置きの装入孔から装入し、次いで残りの装入孔から装入する方法では、もっともかさ密度が上昇する部位を従来法の半分とすることができる。   For example, in the case of a carbonization chamber in which four charging holes are arranged on the ceiling of the carbonization chamber, as shown in FIG. 4, first, from every other charging hole # 1, # 3 from the machine side. After charging a predetermined amount (part) of coal, forming a mountain and depositing coal with a low pulverization rate directly under the adjacent charging hole, the remaining amount from other charging holes (Part) of charcoal is charged. By doing so, the charcoal charged from the other charging holes is charged (deposited) without colliding with the hard carburetor bottom refractory. Therefore, as compared with the conventional method in which the powdering rate reaches 20 mass% in the first charging, according to the present invention, the charging is first performed from every other charging hole and then from the remaining charging holes. In the method, the portion where the bulk density increases most can be reduced to half that of the conventional method.

このように、選択的(1つ置き)に使用する1回目の装入孔からの装入、及び他の装入孔からの2回目の装入を終えた後は、炉内に30mass%〜70mass%程度の成型炭が堆積しているため、その後に行う成型炭の装入時の粉化は抑制されるため、全装入孔から残部の成型炭を装入してもよい。もちろん、残部の成型炭を、引き続き最初の装入孔からの装入と次の装入孔からの装入とを交互に繰り返して装入してもよい。ただし、装入完了時には炭化室内の堆積上面の山谷が大きくなりすぎるとレベラーによる堆積上面の均しが難しくなることがあるので、注意する必要がある。   Thus, after finishing the charging from the first charging hole to be used selectively (every other) and the second charging from the other charging holes, 30 mass% in the furnace. Since about 70 mass% of the coal is deposited, pulverization at the time of charging the coal to be performed thereafter is suppressed. Therefore, the remaining coal may be charged from all the charging holes. Of course, the remaining cast charcoal may be continuously charged by alternately repeating the charging from the first charging hole and the charging from the next charging hole. However, it should be noted that when the charging is completed, if the peaks and valleys on the deposition upper surface in the carbonization chamber become too large, it may be difficult to level the deposition upper surface by the leveler.

ここで、最初に装入を行う装入孔からの装炭量は、当該装入孔からの装炭量の15mass%未満であると、隣りの装入孔直下まで成型炭が流れ込む量が少なくなるため、隣りの装入孔から装入される成型炭の粉化を十分に抑制することができない。一方、最初に装入を行う装入孔からの装炭量を35mass%を超えて装入する場合、堆積上面の山谷が大きくなりすぎ、残部の成型炭を装入したときに、レベラーによる堆積上面の均しが難しくなるため、最初の装入と次の装入における装入量は15mass%〜35mass%とすることが好ましい。   Here, if the amount of charcoal from the charging hole to be initially charged is less than 15 mass% of the amount of charging from the charging hole, the amount of coal flowing into the adjacent charging hole is small. Therefore, the pulverization of the charcoal charged from the adjacent charging hole cannot be sufficiently suppressed. On the other hand, when the amount of coal charged from the charging hole to be charged first exceeds 35 mass%, the mountain valley on the top surface of the deposit becomes too large, and the remaining coal coal is charged. Since it becomes difficult to level the upper surface, it is preferable that the charging amount in the first charging and the next charging is 15 mass% to 35 mass%.

なお、図4では、装入孔が4つの場合で説明をしたが、装入孔が奇数の場合、例えば、5つの場合は、最初に#1、#3、#5を使い、次に#2、#4を使う場合の他、まず中央の装入孔(#3)に隣接する二つの装入孔(#2、#4)から最初に装入を行い、その後その二つの装入孔に隣接する装入孔(#1、#3、#5)からの装入を行うことが好ましい。粉化率が大きい装入孔直下炉底部の箇所を少なくできるからである。   In FIG. 4, the case where there are four charging holes has been described. However, when the charging holes are odd numbers, for example, when the number is five, # 1, # 3, and # 5 are used first, and then # In addition to the case of using # 2 and # 4, first, charging is first performed from two charging holes (# 2, # 4) adjacent to the central charging hole (# 3), and then the two charging holes are used. It is preferable to perform charging from the charging holes (# 1, # 3, # 5) adjacent to. This is because it is possible to reduce the number of places at the bottom of the furnace directly below the charging hole with a high powdering rate.

<実施例1>
実際に、炭化室(H:6700mm、L:15000mm、W:430mm)に、全装入量32トンの成型炭を装入し、同じ条件で乾留してコークスを製造した。炭化室として、4つの装入孔(#1〜#4)を有する炭化室を利用した。発明例として、以下の成型炭の装入方法を実施した。即ち、最初に#1と#3の装入孔から、全装入量の一部(10mass%、15mass%、25mass%、35mass%、40mass%)をそれぞれの装入孔に等量ずつ供給して装入した。次いで、#2と#4との装入孔から、残りの一部(25mass%)をそれぞれの装入孔に等量ずつ供給して装入した。次に、残りの全部を#1〜#4の装入孔に等量ずつ供給して装入した。一方、従来例として、同じ全装入量の成型炭を、#1〜#4の装入孔からそれぞれ等量ずつ同時に装入した。
<Example 1>
Actually, the charcoal chamber (H: 6700 mm, L: 15000 mm, W: 430 mm) was charged with 32 tons of total charcoal and carbonized under the same conditions to produce coke. As the carbonization chamber, a carbonization chamber having four charging holes (# 1 to # 4) was used. As an example of the invention, the following method of charging coal was carried out. That is, first, a part (10 mass%, 15 mass%, 25 mass%, 35 mass%, 40 mass%) of the total charging amount is supplied to each charging hole in equal amounts from the charging holes of # 1 and # 3. I was charged. Next, the remaining part (25 mass%) was supplied to each charging hole in an equal amount from the charging holes of # 2 and # 4, and charged. Next, all the remaining parts were supplied to the # 1 to # 4 charging holes by equal amounts and charged. On the other hand, as a conventional example, the same total charging amount of coal char was charged simultaneously in equal amounts from the # 1 to # 4 charging holes.

そして、乾留後に得られたコークス押出時の負荷および乾留不良の有無を測定するとともに、それらの結果から総合判定を行った。ここで、コークス押出時の負荷としては、コークスを押し出す際の押出機の電流値を測定し、押出開始から終了までの平均電流値により評価して、従来例に相当する各装入孔から同時に装入を行ったときの平均電流値を100とし、これに対する比で表記した。また、乾留不良の有無は、良好なものを○、最低限使用可能なものを△、不良のものを×として表記した。さらに、総合判定は、コークス押出時の負荷および乾留不良の有無の結果から、優秀なものを○、最低限使用可能なものを△、不良のものを×として表記した。結果を以下の表1に示す。   And while measuring the load at the time of coke extrusion obtained after dry distillation, and the presence or absence of dry distillation failure, comprehensive judgment was performed from those results. Here, as the load at the time of coke extrusion, the current value of the extruder at the time of extruding coke is measured and evaluated by the average current value from the start to the end of the extrusion, and simultaneously from each charging hole corresponding to the conventional example The average current value at the time of charging was set to 100, and expressed as a ratio to this. Further, the presence or absence of defective carbonization was indicated as “good” as “good”, “minimum usable” as “Δ”, and defective as “poor”. Further, the overall judgment was expressed as “Excellent”, “Minimum usable”, “B”, and “B”, based on the results of coke extrusion load and dry distillation failure. The results are shown in Table 1 below.

Figure 0006562218
Figure 0006562218

表1に示す結果から明らかなように、1回目に全装入量の一部を装入し、2回目に残りの一部を装入し、3回目の残りの全部を装入した発明例は、全装入量の装入を全装入孔から同時に行った従来例と比べて、乾留不良や押出し負荷の増大を招くことなくコークスの製造ができることがわかる。また、発明例の中でも、1回目の装入を15mass%〜35mass%とした例が、それ以外の例と比べて良好な結果を得ることができ、好ましい範囲であることがわかる。   As is apparent from the results shown in Table 1, an example of the invention in which a part of the total charged amount was charged at the first time, the remaining part at the second time was charged, and the remaining at the third time was charged. It can be seen that coke can be produced without causing a dry distillation defect or an increase in extrusion load, as compared with the conventional example in which the entire charging amount is simultaneously charged from all charging holes. In addition, among the examples of the invention, it can be seen that an example in which the first charging is 15 mass% to 35 mass% can obtain better results than the other examples, and is a preferable range.

<実施例2>
実施例1と同様にコークスの製造を行った。その際、発明例として、以下の成型炭の装入方法を実施した。即ち、まず始めに#1と#3の装入孔から、全装入量の一部(25mass%)をそれぞれの装入孔に等量ずつ供給して装入した。次に、#2と#4との装入孔から、残りの一部(10mass%、15mass%、25mass%、35mass%、40mass%)をそれぞれの装入孔に等量ずつ供給して装入した。次に、残りの全部を#1〜#4の装入孔に等量ずつ供給して装入した。一方、従来例として、同じ全装入量の成型炭を、#1〜#4の装入孔からそれぞれ等量ずつ同時に装入した。
<Example 2>
Coke was produced in the same manner as in Example 1. At that time, the following method of charging coal was carried out as an example of the invention. That is, first, a part (25 mass%) of the total charging amount was supplied to each charging hole from the charging holes of # 1 and # 3 and charged. Next, the remaining part (10 mass%, 15 mass%, 25 mass%, 35 mass%, 40 mass%) is supplied to each charging hole by an equal amount from the charging holes of # 2 and # 4. did. Next, all the remaining parts were supplied to the # 1 to # 4 charging holes by equal amounts and charged. On the other hand, as a conventional example, the same total charging amount of coal char was charged simultaneously in equal amounts from the # 1 to # 4 charging holes.

そして、実施例1と同様に、乾留後に得られたコークス押出時の負荷および乾留不良の有無を測定するとともに、それらの結果から総合判定を行った。   And similarly to Example 1, while measuring the load at the time of coke extrusion obtained after dry distillation, and the presence or absence of dry distillation failure, comprehensive judgment was performed from those results.

Figure 0006562218
Figure 0006562218

表2に示す結果から明らかなように、1回目に全装入量の一部を装入し、2回目に残りの一部を装入し、3回目の残りの全部を装入した発明例は、全装入量の装入を全装入孔から同時に行った従来例と比べて、良好な結果を得ることができた。また、発明例の中でも、2回目の装入を15mass%〜35mass%とした例が、それ以外の例と比べて良好な結果を得ることができ、好ましい範囲であることがわかる。   As is apparent from the results shown in Table 2, an example of the invention in which a part of the total charged amount was charged at the first time, the remaining part at the second time was charged, and the remaining at the third time was charged. Compared with the conventional example in which the entire charging amount was charged simultaneously from all the charging holes, good results could be obtained. In addition, among the examples of the invention, it can be seen that an example in which the second charging is 15 mass% to 35 mass% can obtain better results than the other examples, and is a preferable range.

本発明のコークス炉の石炭装入方法によれば、石炭として成型炭を使用する場合であっても、コークス炉の炭化室に成型炭を好適に装入することができ、室炉式コークス炉以外のコークス炉にも適用が可能である。   According to the method for charging coal in a coke oven according to the present invention, even when coal is used as coal, coal can be suitably charged into the carbonization chamber of the coke oven. It can be applied to other coke ovens.

1 模擬炭化室
2 サンプリング口
3 装入孔
4 成型炭ホッパー
1 Simulated carbonization chamber 2 Sampling port 3 Charging hole 4 Cast charcoal hopper

Claims (3)

コークス炉の炭化室へ、この炭化室の天井に設けた複数の装入孔を介して、成型炭のみを装入するコークス炉の石炭装入方法において、まず始めに、1つ置きの装入孔を選んで、成型炭全装入量のうちの15mass%〜35mass%を装入し、次いで、選択しなかった他の装入孔から、成型炭全装入量のうちのさらに15mass%〜35mass%を装入し、その後、成型炭全装入量のうちの残部を、全装入孔を使って装入することを特徴とするコークス炉の石炭装入方法。 In the coke oven coal charging method in which only the coal is charged into the coke oven carbonization chamber through a plurality of charging holes provided in the ceiling of the carbonization chamber, first, every other charge is charged. Select a hole, and charge 15 mass % to 35 mass% of the total charging amount of coal, and then, from other charging holes that were not selected, further 15 mass% of the total charging amount of coal A coal charging method for a coke oven, wherein 35% by mass is charged, and then the remainder of the total amount of the coal is charged using all charging holes. 前記コークス炉が4個の装入孔を備える場合、最初の成型炭の装入をマシンサイドあるいはコークスサイド側から1番目および3番目の装入孔から実施し、次の成型炭の装入を2番目および4番目の装入孔から実施し、また、前記コークス炉が5個の装入孔を備える場合、最初の成型炭の装入をマシンサイドあるいはコークスサイド側から1番目、3番目および5番目とし、そして次の成型炭の装入を2番目および4番目とするかその逆のパターンで装入することを特徴とする請求項1に記載のコークス炉の石炭装入方法。 When the coke oven has four charging holes, the first charcoal is charged from the first and third charging holes from the machine side or the coke side, and the next charcoal is charged. If the coke oven is provided with five charging holes, the first coal charging is performed from the machine side or the coke side side first, third and 5. The method for charging coal in a coke oven according to claim 1, wherein the charging is carried out in a fifth pattern, and the charging of the next coal is second and fourth or vice versa. 前記最初の成型炭の装入、前記2回目の成型炭の装入、および、前記最後の成型炭の装入において、各回で装入すべき量の成型炭を各回で使用する装入孔に等分に分割して装入することを特徴とする請求項1または2に記載のコークス炉の石炭装入方法。
In the first coal charging, the second coal charging, and the final coal charging, the amount of coal to be charged each time is charged in each charging hole. The method for charging coal in a coke oven according to claim 1 or 2 , wherein charging is performed by dividing into equal parts.
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