JP6463302B2 - High concentration inulin-containing tea beverage - Google Patents
High concentration inulin-containing tea beverage Download PDFInfo
- Publication number
- JP6463302B2 JP6463302B2 JP2016130126A JP2016130126A JP6463302B2 JP 6463302 B2 JP6463302 B2 JP 6463302B2 JP 2016130126 A JP2016130126 A JP 2016130126A JP 2016130126 A JP2016130126 A JP 2016130126A JP 6463302 B2 JP6463302 B2 JP 6463302B2
- Authority
- JP
- Japan
- Prior art keywords
- inulin
- beverage
- tea
- ppm
- content
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
- 229920001202 Inulin Polymers 0.000 title claims description 66
- JYJIGFIDKWBXDU-MNNPPOADSA-N inulin Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)OC[C@]1(OC[C@]2(OC[C@]3(OC[C@]4(OC[C@]5(OC[C@]6(OC[C@]7(OC[C@]8(OC[C@]9(OC[C@]%10(OC[C@]%11(OC[C@]%12(OC[C@]%13(OC[C@]%14(OC[C@]%15(OC[C@]%16(OC[C@]%17(OC[C@]%18(OC[C@]%19(OC[C@]%20(OC[C@]%21(OC[C@]%22(OC[C@]%23(OC[C@]%24(OC[C@]%25(OC[C@]%26(OC[C@]%27(OC[C@]%28(OC[C@]%29(OC[C@]%30(OC[C@]%31(OC[C@]%32(OC[C@]%33(OC[C@]%34(OC[C@]%35(OC[C@]%36(O[C@@H]%37[C@@H]([C@@H](O)[C@H](O)[C@@H](CO)O%37)O)[C@H]([C@H](O)[C@@H](CO)O%36)O)[C@H]([C@H](O)[C@@H](CO)O%35)O)[C@H]([C@H](O)[C@@H](CO)O%34)O)[C@H]([C@H](O)[C@@H](CO)O%33)O)[C@H]([C@H](O)[C@@H](CO)O%32)O)[C@H]([C@H](O)[C@@H](CO)O%31)O)[C@H]([C@H](O)[C@@H](CO)O%30)O)[C@H]([C@H](O)[C@@H](CO)O%29)O)[C@H]([C@H](O)[C@@H](CO)O%28)O)[C@H]([C@H](O)[C@@H](CO)O%27)O)[C@H]([C@H](O)[C@@H](CO)O%26)O)[C@H]([C@H](O)[C@@H](CO)O%25)O)[C@H]([C@H](O)[C@@H](CO)O%24)O)[C@H]([C@H](O)[C@@H](CO)O%23)O)[C@H]([C@H](O)[C@@H](CO)O%22)O)[C@H]([C@H](O)[C@@H](CO)O%21)O)[C@H]([C@H](O)[C@@H](CO)O%20)O)[C@H]([C@H](O)[C@@H](CO)O%19)O)[C@H]([C@H](O)[C@@H](CO)O%18)O)[C@H]([C@H](O)[C@@H](CO)O%17)O)[C@H]([C@H](O)[C@@H](CO)O%16)O)[C@H]([C@H](O)[C@@H](CO)O%15)O)[C@H]([C@H](O)[C@@H](CO)O%14)O)[C@H]([C@H](O)[C@@H](CO)O%13)O)[C@H]([C@H](O)[C@@H](CO)O%12)O)[C@H]([C@H](O)[C@@H](CO)O%11)O)[C@H]([C@H](O)[C@@H](CO)O%10)O)[C@H]([C@H](O)[C@@H](CO)O9)O)[C@H]([C@H](O)[C@@H](CO)O8)O)[C@H]([C@H](O)[C@@H](CO)O7)O)[C@H]([C@H](O)[C@@H](CO)O6)O)[C@H]([C@H](O)[C@@H](CO)O5)O)[C@H]([C@H](O)[C@@H](CO)O4)O)[C@H]([C@H](O)[C@@H](CO)O3)O)[C@H]([C@H](O)[C@@H](CO)O2)O)[C@@H](O)[C@H](O)[C@@H](CO)O1 JYJIGFIDKWBXDU-MNNPPOADSA-N 0.000 title claims description 66
- 229940029339 inulin Drugs 0.000 title claims description 66
- 235000013616 tea Nutrition 0.000 title claims description 56
- CIWBSHSKHKDKBQ-JLAZNSOCSA-N Ascorbic acid Chemical compound OC[C@H](O)[C@H]1OC(=O)C(O)=C1O CIWBSHSKHKDKBQ-JLAZNSOCSA-N 0.000 claims description 59
- 235000013361 beverage Nutrition 0.000 claims description 48
- ADRVNXBAWSRFAJ-UHFFFAOYSA-N catechin Natural products OC1Cc2cc(O)cc(O)c2OC1c3ccc(O)c(O)c3 ADRVNXBAWSRFAJ-UHFFFAOYSA-N 0.000 claims description 42
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- 229960005070 ascorbic acid Drugs 0.000 claims description 30
- 235000010323 ascorbic acid Nutrition 0.000 claims description 29
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- 229920000642 polymer Polymers 0.000 claims description 8
- 239000003205 fragrance Substances 0.000 claims description 6
- 235000011194 food seasoning agent Nutrition 0.000 claims description 4
- 235000003599 food sweetener Nutrition 0.000 claims description 3
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- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 7
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- PFTAWBLQPZVEMU-UHFFFAOYSA-N catechin Chemical compound OC1CC2=C(O)C=C(O)C=C2OC1C1=CC=C(O)C(O)=C1 PFTAWBLQPZVEMU-UHFFFAOYSA-N 0.000 description 3
- 235000013325 dietary fiber Nutrition 0.000 description 3
- XMOCLSLCDHWDHP-IUODEOHRSA-N epi-Gallocatechin Chemical compound C1([C@H]2OC3=CC(O)=CC(O)=C3C[C@H]2O)=CC(O)=C(O)C(O)=C1 XMOCLSLCDHWDHP-IUODEOHRSA-N 0.000 description 3
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- WMBWREPUVVBILR-GHTZIAJQSA-N (+)-gallocatechin gallate Chemical compound O([C@H]1CC2=C(O)C=C(C=C2O[C@@H]1C=1C=C(O)C(O)=C(O)C=1)O)C(=O)C1=CC(O)=C(O)C(O)=C1 WMBWREPUVVBILR-GHTZIAJQSA-N 0.000 description 2
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- LSHVYAFMTMFKBA-TZIWHRDSSA-N (-)-epicatechin-3-O-gallate Chemical compound O([C@@H]1CC2=C(O)C=C(C=C2O[C@@H]1C=1C=C(O)C(O)=CC=1)O)C(=O)C1=CC(O)=C(O)C(O)=C1 LSHVYAFMTMFKBA-TZIWHRDSSA-N 0.000 description 2
- BBMCTIGTTCKYKF-UHFFFAOYSA-N 1-heptanol Chemical compound CCCCCCCO BBMCTIGTTCKYKF-UHFFFAOYSA-N 0.000 description 2
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- XMOCLSLCDHWDHP-UHFFFAOYSA-N L-Epigallocatechin Natural products OC1CC2=C(O)C=C(O)C=C2OC1C1=CC(O)=C(O)C(O)=C1 XMOCLSLCDHWDHP-UHFFFAOYSA-N 0.000 description 2
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Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23F—COFFEE; TEA; THEIR SUBSTITUTES; MANUFACTURE, PREPARATION, OR INFUSION THEREOF
- A23F3/00—Tea; Tea substitutes; Preparations thereof
- A23F3/16—Tea extraction; Tea extracts; Treating tea extract; Making instant tea
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/52—Adding ingredients
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/20—Reducing nutritive value; Dietetic products with reduced nutritive value
- A23L33/21—Addition of substantially indigestible substances, e.g. dietary fibres
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Description
本発明は、高濃度イヌリンを含有する容器詰茶飲料、その製造方法、及び容器詰茶飲料におけるイヌリン特有の雑味を抑制する方法などに関する。 TECHNICAL FIELD The present invention relates to a packaged tea beverage containing a high concentration of inulin, a method for producing the same, a method for suppressing a miscellaneous taste unique to inulin in a packaged tea beverage, and the like.
近年、缶やペット(PET)ボトル等の容器に充填された容器詰飲料が多く開発、市販されている。このうち、容器詰茶飲料は、一般に茶葉を水などの水性溶媒で抽出して茶抽出液を得、この茶抽出液を飲用濃度になるよう濃度調整を行った後、缶、ペットボトルなどの密封容器に封入して販売されている。 In recent years, many container-packed beverages filled in containers such as cans and PET (PET) bottles have been developed and marketed. Of these, container-packed tea beverages are generally obtained by extracting tea leaves with an aqueous solvent such as water to obtain a tea extract, adjusting the concentration of this tea extract to the drinking concentration, It is sold in sealed containers.
イヌリンは水溶性食物繊維の一種であり、整腸作用を有することが知られており、イヌリンを含む飲料に関する報告がある(特許文献1、特許文献2)。 Inulin is a kind of water-soluble dietary fiber and is known to have an intestinal regulating action, and there are reports on beverages containing inulin (Patent Document 1, Patent Document 2).
また、水溶性食物繊維として知られているポリデキストロースには酸味、苦渋みなどの呈味上の問題点があるのに対し、イヌリンには酸味、苦渋みがなく呈味を改良できることが知られている(特許文献3)。 Polydextrose, known as a water-soluble dietary fiber, has taste problems such as acidity and bitterness, whereas inulin is known to improve taste without acidity and bitterness. (Patent Document 3).
上記のとおり、イヌリンはポリデキストロースと比較して、酸味、苦渋みがなく呈味を改良できることが知られている。しかしながら、本発明者らはイヌリンを高濃度で含有する飲料を比較的大量に摂取する際にイヌリン特有の雑味を感じることを見出した。 As described above, it is known that inulin can improve taste without acidity and bitterness compared to polydextrose. However, the present inventors have found that when a relatively large amount of a beverage containing inulin at a high concentration is ingested, a miscellaneous taste peculiar to inulin is felt.
この点、カテキンを配合することでイヌリンの雑味をある程度抑えることができるが、低濃度のカテキンでは十分にイヌリンの雑味を抑えることはできない。一方、カテキンを高濃度で配合すると、カテキンによる渋味が増してしまい、好ましくない。 In this regard, by adding catechin, the miscellaneous taste of inulin can be suppressed to some extent, but the low concentration of catechin cannot sufficiently suppress the miscellaneous taste of inulin. On the other hand, when catechin is blended at a high concentration, the astringency due to catechin increases, which is not preferable.
本発明の目的は、整腸作用を有するイヌリンを高濃度に含み、かつイヌリン特有の雑味が抑制された容器詰茶飲料を提供することにある。 An object of the present invention is to provide a packaged tea beverage containing an inulin having an intestinal regulating action at a high concentration and suppressing the miscellaneous taste unique to inulin.
本発明者らは、上記課題を解決するために、イヌリン高濃度条件においてイヌリンの雑味抑制効果を有する方法を鋭意検討し、非重合体カテキン量が一定の範囲とし、さらにアスコルビン酸を一定量範囲とすることで、イヌリン特有の雑味を抑えることができるとともに、渋みもなく、飲みやすさが増すことを見出し、本発明を完成するに至った。 In order to solve the above problems, the present inventors have intensively studied a method having an inulin miscellaneous taste suppressing effect under high inulin concentration conditions, and the non-polymer catechin amount is within a certain range, and further, ascorbic acid is a certain amount. By setting the range, it was possible to suppress the miscellaneous taste peculiar to inulin, and there was no astringency, and the ease of drinking was found, and the present invention was completed.
すなわち、これに限定されるものではないが、本発明は以下に関する。
1)容器詰茶飲料であって、
イヌリンの含有量が1〜7g/100mlであり、
非重合体カテキンの含有量が1〜800ppmであり、
アスコルビン酸の含有量が100〜800ppmである、
前記飲料。
2)イヌリンの含有量が1.5〜5.0g/100mlである、1)に記載の飲料。
3)イヌリンの含有量が2.0〜4.0g/100mlである、1)に記載の飲料。
4)非重合カテキンの含有量が10〜750ppmである、1)から3)のいずれかに記載の飲料。
5)非重合カテキンの含有量が50〜700ppmである、1)〜3)のいずれかに記載の飲料。
6)アスコルビン酸の含有量が200〜700ppmである、1)〜5)のいずれかに記載の飲料。
7)アスコルビン酸の含有量が300〜600ppmである、1)〜5)のいずれかに記載の飲料。
8)整腸作用を有する、1)〜7)のいずれかに記載の飲料。
9)500ml以上の容器詰茶飲料である、1)〜8)のいずれかに記載の飲料。
10)容器詰茶飲料の製造方法であって、当該飲料中のイヌリンの含有量を1〜7g/100mlに調整する工程、当該飲料中の非重合体カテキンの含有量を1〜800ppmに調整する工程、及び当該飲料中のアスコルビン酸の含有量を100〜800ppmに調整する工程、を含む、前記製造方法。
11)容器詰茶飲料におけるイヌリン特有の雑味を抑制する方法であって、当該飲料中のイヌリンの含有量を1〜7g/100mlとし、当該飲料中の非重合体カテキンの含有量を1〜800ppmとし、さらに当該飲料中のアスコルビン酸の含有量を100〜800ppmとすることによる、前記抑制方法。
That is, although not limited to this, the present invention relates to the following.
1) A packaged tea beverage,
The inulin content is 1-7 g / 100 ml,
The content of non-polymer catechin is 1 to 800 ppm,
The ascorbic acid content is 100-800 ppm,
The beverage.
2) The beverage according to 1), wherein the content of inulin is 1.5 to 5.0 g / 100 ml.
3) The beverage according to 1), wherein the inulin content is 2.0 to 4.0 g / 100 ml.
4) The beverage according to any one of 1) to 3), wherein the content of non-polymerized catechin is 10 to 750 ppm.
5) The beverage according to any one of 1) to 3), wherein the content of non-polymerized catechin is 50 to 700 ppm.
6) The beverage according to any one of 1) to 5), wherein the content of ascorbic acid is 200 to 700 ppm.
7) The beverage according to any one of 1) to 5), wherein the content of ascorbic acid is 300 to 600 ppm.
8) The beverage according to any one of 1) to 7), which has an intestinal regulating action.
9) The beverage according to any one of 1) to 8), which is a 500 ml or more containerized tea beverage.
10) A method for producing a packaged tea beverage, the step of adjusting the content of inulin in the beverage to 1 to 7 g / 100 ml, and the content of non-polymer catechin in the beverage to 1 to 800 ppm The said manufacturing method including the process and the process of adjusting content of ascorbic acid in the said drink to 100-800 ppm.
11) A method for suppressing the miscellaneous taste unique to inulin in a packaged tea beverage, wherein the content of inulin in the beverage is 1 to 7 g / 100 ml, and the content of non-polymer catechin in the beverage is 1 to The said suppression method by setting it as 800 ppm and also making content of ascorbic acid in the said drink into 100-800 ppm.
本発明により、整腸作用を有するイヌリンを高濃度に含み、かつイヌリン特有の雑味が抑制された容器詰茶飲料を提供することができる。 INDUSTRIAL APPLICABILITY According to the present invention, it is possible to provide a packaged tea beverage that contains inulin having an intestinal regulating action at a high concentration and that suppresses the miscellaneous taste unique to inulin.
本発明の容器詰茶飲料(以下、「本発明の茶飲料」とも記載する)、及び関連する方法などについて、以下に説明する。
(茶飲料)
荒茶は、茶樹(学名:Camellia sinensis)から摘採した生葉を原料として製造される加工品である。本発明に用いることのできる生葉は、茶であればその品種、産地、栽培方法、茶期などは限定されない。
The container-packed tea beverage of the present invention (hereinafter also referred to as “the tea beverage of the present invention”) and related methods are described below.
(Tea drink)
Aracha is a processed product made from raw leaves plucked from tea trees (scientific name: Camellia sinensis). The fresh leaf that can be used in the present invention is not limited in its variety, production area, cultivation method, tea season, etc., as long as it is tea.
緑茶飲料の製造に用いられる品種としては、例えば、やぶきた、ゆたかみどり、おくみどり、さやまかおり、かなやみどり、さえみどり、あさつゆ等、産地としては、例えば、静岡、鹿児島、三重、熊本、福岡、京都、宮崎、埼玉等が挙げられ、栽培方法としては露地、かぶせ、玉露等、茶期としては一番茶、二番茶、三番茶、四番茶、冬春秋番茶、刈番等を挙げることができる。 Varieties used in the production of green tea beverages include, for example, Yabukita, Yutaka Midori, Okumidori, Sayaka Kaori, Kanaya Midori, Samidori, Asatsuyu, and other production areas such as Shizuoka, Kagoshima, Mie, and Kumamoto , Fukuoka, Kyoto, Miyazaki, Saitama, etc., cultivation methods include open ground, cover, gyokuro, etc., and tea seasons include first tea, second tea, third tea, fourth tea, winter spring autumn tea, banban, etc. Can do.
仕上茶を加工して茶飲料が得られる。仕上茶から茶飲料を得る工程は一般的には、仕上茶を加温水などで抽出する抽出工程、抽出液から抽出残渣を取り除く粗濾過工程、抽出液を冷却する冷却工程、抽出液から細かな固形分を取り除く濾過工程、抽出液に水や緑茶抽出物、酸化防止剤、pH調整剤などを加えて調合液を得る調合工程、調合液を殺菌する殺菌工程を含む。ただし、前記工程はあくまで一例であり、これに限定するものではなく、例えば、工程の順序を入れ替えたり、別工程を付加したりすることもできる。 Finished tea is processed to obtain a tea beverage. The process of obtaining a tea beverage from finished tea is generally divided into an extraction process for extracting the finished tea with warm water, a coarse filtration process for removing extraction residues from the extract, a cooling process for cooling the extract, and a fine process from the extract. It includes a filtration step for removing solids, a preparation step for adding a water or green tea extract, an antioxidant, a pH adjuster, etc. to the extract to obtain a preparation, and a sterilization step for sterilizing the preparation. However, the said process is an example to the last, and is not limited to this, For example, the order of a process can be replaced or another process can be added.
また、生葉を半発酵させることにより得られる半発酵茶葉を用いることにより烏龍茶飲料を、発酵茶葉を用いることにより紅茶飲料を製造することができる。これらの製造に用いられる品種としては一般的なものを用いることができる。 Moreover, oolong tea drinks can be produced by using semi-fermented tea leaves obtained by semi-fermenting fresh leaves, and black tea drinks can be produced by using fermented tea leaves. A general thing can be used as a kind used for these manufacture.
製造された緑茶、烏龍茶、紅茶は単独で茶飲料とすることもできるが、それぞれを適宜好適な比率で混合することにより混合茶飲料とすることもできる。さらに、これら茶葉抽出液により製造された茶飲料に、さらに穀物類、香草類などの抽出液を添加して茶飲料とすることもできる。 The produced green tea, oolong tea, and black tea can be used alone as a tea beverage, but can also be mixed into a mixed tea beverage by mixing them at an appropriate ratio. Furthermore, it is also possible to add an extract such as cereals and herbs to the tea beverage produced with these tea leaf extracts to make a tea beverage.
(イヌリン)
イヌリンは、種々の植物に含まれる多糖類の一群であり、グルコースにフルクトースが複数個結合した重合体である。水溶性食物繊維の一種であり、腸内において人体に有益な細菌を増やすのに貢献することが知られている(腸内有益菌増殖促進作用)。イヌリンは消化されることなく胃と十二指腸を通過し、腸内の細菌にとって有益な物質となる。
(Inulin)
Inulin is a group of polysaccharides contained in various plants, and is a polymer in which a plurality of fructose bonds to glucose. It is a kind of water-soluble dietary fiber and is known to contribute to increasing bacteria beneficial to the human body in the intestine (intestinal beneficial bacteria growth promoting action). Inulin passes through the stomach and duodenum without being digested and becomes a beneficial substance for bacteria in the intestine.
イヌリンは、整腸作用を有することから、腸や消化管を含むお腹の調子を整える効果を有する。具体的には、腸内機能、腸の状態、大腸環境の改善、改良、向上作用を有する。そして、腸運動を促進し、便秘の軽減や予防に効果がある。 Inulin has the effect of regulating the intestines, and therefore has the effect of adjusting the tone of the stomach including the intestines and digestive tract. Specifically, it has an intestinal function, an intestinal condition, and an improvement, improvement, and improvement of the large intestine environment. It promotes bowel movement and is effective in reducing and preventing constipation.
本発明に係る飲料に使用可能なイヌリンは、フラクトシル単位が主にβ−2,1結合によって結合され、フラクタンの鎖長が2〜100の範囲であり、好ましくは2〜60の範囲である。イヌリン中の結合の少なくとも90%がβ−2,1型である。例えば、チコリ由来のイヌリンとして、Frutafit(商標)またはRaftiline(商標)がある。また、多数の植物種から当業者に周知の方法により得ることができる。 The inulin that can be used in the beverage according to the present invention has fructosyl units bonded mainly by β-2,1 bonds, and the fructan chain length is in the range of 2-100, preferably in the range of 2-60. At least 90% of the binding in inulin is β-2,1 type. For example, chicory-derived inulin includes Frutafit ™ or Raftiline ™. It can also be obtained from a number of plant species by methods well known to those skilled in the art.
本発明の飲料に含有されるイヌリンの含有量は、1〜7g/100ml、好ましくは1.5〜5.0g/100ml、さらに好ましくは2.0〜4.0g/100mlである。 The content of inulin contained in the beverage of the present invention is 1 to 7 g / 100 ml, preferably 1.5 to 5.0 g / 100 ml, more preferably 2.0 to 4.0 g / 100 ml.
イヌリンの含有量は、HPLC法などの公知の方法を用いて定量することができる。例えば、GC−MS、HPLC法などの公知のいずれの方法で測定してもよい。 The inulin content can be quantified using a known method such as an HPLC method. For example, it may be measured by any known method such as GC-MS or HPLC method.
イヌリンの平均重合度の分析は、以下のようにして行うことができる。なお、重合度とは、イヌリン中のサッカライド単位(フルクトース及びグルコース単位)の数であり、平均重合度は、例えば、以下のようにして、HPLC、GC、HPAEC等の通常の分析法によって求めた分析結果のピークのトップを平均重合度とすることができる。カラムとして、例えば、信和化工製のULTRON PS-80N(8×300mm)(溶媒;水、流速;0.5ml/min、温度;50℃)、あるいは、TOSOH製のTSK-GEL G3000PWXL(7.8×300mm)(溶媒;水、流速;0.5ml/min、温度;50℃)を用い、検出器として示差屈折計を使用することによって確認された生成イヌリンの重合度を、標準物質として、例えば、植物由来のイヌリンであるオラフティ社のラフテリンST(平均重合度11)とラフテリンHP(平均重合度22)を用いて作成した検量線により求めることができる。なお、イヌリンの重合度の分析に関しては、Loo等(Critical Reviews in Food Science and Nutrition, 35(6)、525−552(1995)の方法に基づいて実施することができる。
(非重合カテキン)
本発明の茶飲料では、カテキンの含量が茶飲料の容量に対して、1〜800ppm、好ましくは10〜750ppm、さらに好ましくは30〜700ppm、50〜700ppm、より好ましくは200〜500ppmに調整することが重要である。なお、本明細書において、ppmは重量/容量ppmを意味し、これはmg/Lに相当するものである。非重合カテキン含量が800ppmを超えると、カテキン特有の味が強くなり、飲みにくさを感じてしまうことがある。
Analysis of the average degree of polymerization of inulin can be performed as follows. The degree of polymerization is the number of saccharide units (fructose and glucose units) in inulin, and the average degree of polymerization was determined by a usual analysis method such as HPLC, GC, or HPAEC as follows. The top of the peak of the analysis result can be the average degree of polymerization. As the column, for example, ULTRON PS-80N (8 × 300 mm) manufactured by Shinwa Kako (solvent: water, flow rate: 0.5 ml / min, temperature: 50 ° C.) or TSK-GEL G3000PWXL (7.8 manufactured by TOSOH) X300 mm) (solvent; water, flow rate; 0.5 ml / min, temperature; 50 ° C.), and the degree of polymerization of the produced inulin confirmed by using a differential refractometer as a detector, for example, as a standard substance It can be determined by a calibration curve prepared using Olafty's Roughterin ST (average polymerization degree 11) and Roughterin HP (average polymerization degree 22), which are plant-derived inulin. The analysis of the degree of polymerization of inulin can be carried out based on the method of Loo et al. (Critical Reviews in Food Science and Nutrition, 35 (6), 525-552 (1995).
(Non-polymerized catechin)
In the tea beverage of the present invention, the content of catechin is adjusted to 1 to 800 ppm, preferably 10 to 750 ppm, more preferably 30 to 700 ppm, 50 to 700 ppm, more preferably 200 to 500 ppm with respect to the capacity of the tea beverage. is important. In this specification, ppm means weight / volume ppm, which corresponds to mg / L. If the non-polymerized catechin content exceeds 800 ppm, the catechin-specific taste becomes strong, and it may be difficult to drink.
ここで、本明細書における非重合カテキンとは、カテキン、エピカテキン、ガロカテキン、エピガロカテキン、カテキンガレート、エピカテキンガレート、ガロカテキンガレートおよびエピガロカテキンガレートの総称を表す。確認のために記載するが、上記の含量は、これらのカテキン類化合物の総量を意味する。 Here, the non-polymerized catechin in the present specification represents a general term for catechin, epicatechin, gallocatechin, epigallocatechin, catechin gallate, epicatechin gallate, gallocatechin gallate and epigallocatechin gallate. Although described for confirmation, the above content means the total amount of these catechin compounds.
非重合カテキンの組成は特に限定されないが、特に苦味や渋味が大きいとされるガレート型カテキン類(上記カテキン類のうち、カテキンガレート、エピカテキンガレート、ガロカテキンガレート、エピガロカテキンガレートの総称)が好ましく、適度な旨みと渋味のバランスを有する茶飲料とすることができる。したがって、ガレート型カテキン類の比率が大きい茶飲料も、本発明の好ましい態様の一つとして例示できる。具体的には、カテキン中のガレート型カテキン類の割合([ガレート型カテキン類の質量]/[全カテキン類の質量]×100%)が、40〜95%、好ましくは45〜90%、より好ましくは46〜80%程度である。 The composition of the non-polymerized catechin is not particularly limited, but gallate-type catechins that have particularly high bitterness and astringency (among the above catechins, catechin gallate, epicatechin gallate, gallocatechin gallate, epigallocatechin gallate) It is preferable that the tea beverage has a proper balance between umami and astringency. Therefore, a tea beverage having a large ratio of gallate catechins can also be exemplified as one of the preferred embodiments of the present invention. Specifically, the proportion of gallate catechins in catechin ([mass of gallate catechins] / [mass of all catechins] × 100%) is 40 to 95%, preferably 45 to 90%, Preferably it is about 46 to 80%.
ガレート型カテキン量及び遊離型カテキン量(カテキン類のうちガレート基を有しないもの)は、高速液体クロマトグラフィー(HPLC)を用いた方法によって、測定・定量される。 The amount of gallate catechin and the amount of free catechin (of catechins having no gallate group) are measured and quantified by a method using high performance liquid chromatography (HPLC).
非重合カテキン含量の調整は、主成分となる茶葉の抽出液を用いて適宜行うことができる。必要に応じて茶抽出物の濃縮物(例えば、市販の「ポリフェノン」(三井農林)、「テアフラン」(伊藤園)、「サンフェノン」(太陽化学))を配合して行うことができるほか、公知の方法により得られた烏龍茶抽出液濃縮物、紅茶抽出液濃縮物を配合することもできる。ガレート型カテキン類の割合は、その調整のための処理を特に行わずとも、上記の範囲に入ることが多い。
(アスコルビン酸)
本発明の茶飲料では、アスコルビン酸の含量が茶飲料の容量に対して、100〜800ppm、好ましくは200〜700ppm、さらに好ましくは300〜600ppmに調整することが重要である。なお、本明細書において、ppmは重量/容量ppmを意味し、これはmg/Lに相当するものである。アスコルビン酸含量が800ppmを超えると、アスコルビン酸特有の味が強くなり、飲みにくさを感じてしまうことがある。なお,本明細書において単にアスコルビン酸とした場合、その誘導体も含む概念として記載される。
Adjustment of the non-polymerized catechin content can be appropriately performed using an extract of tea leaves as a main component. If necessary, it can be blended with a tea extract concentrate (for example, commercially available “Polyphenone” (Mitsui Norin), “Theafuran” (Itoen), “Sunphenon” (Taiyo Kagaku)) or a known Oolong tea extract concentrate and black tea extract concentrate obtained by the method can also be blended. The ratio of gallate catechins often falls within the above range without special treatment for the adjustment.
(Ascorbic acid)
In the tea beverage of the present invention, it is important that the content of ascorbic acid is adjusted to 100 to 800 ppm, preferably 200 to 700 ppm, more preferably 300 to 600 ppm with respect to the capacity of the tea beverage. In this specification, ppm means weight / volume ppm, which corresponds to mg / L. When the ascorbic acid content exceeds 800 ppm, the taste specific to ascorbic acid becomes strong, and it may be difficult to drink. In the present specification, when only ascorbic acid is used, it is described as a concept including its derivatives.
本発明に使用するアスコルビン酸またはその誘導体としては、食品添加物として用いられるアスコルビン酸またはその誘導体、例えば、アスコルビン酸グリコシド、アスコルビン酸ナトリウム、アスコルビン酸マグネシウムなどが用いられる。抽出工程及び/又は調合工程などの抽出工程以降の工程において、L−アスコルビン酸及び/又はその食品として許容される塩などの酸化防止剤を添加してもよいアスコルビン酸を豊富に含む天然素材(例えば、レモン、オレンジ、アセロラなどの果実由来の天然素材、あるいは、ブロッコリー、メキャベツ、ピーマン、コマツナ、カリフラワーなどの野菜由来の天然素材)も、本発明においてアスコルビン酸として用いることができる。
(他の成分)
本発明の容器詰茶飲料には、酸化防止剤、乳化剤、保存量、pH調整剤、香料、調味料、甘味料、酸味料、品質安定剤等の添加剤を単独、或いは併用して配合してもよい。茶本来の香味を味わうことができるという香味の観点から、香料、調味料、甘味料、酸味料等は添加しないことが好ましく、保存安定性の観点からpHを5.0〜7.0に調整することが好ましい。
As ascorbic acid or a derivative thereof used in the present invention, ascorbic acid or a derivative thereof used as a food additive, for example, ascorbic acid glycoside, sodium ascorbate, magnesium ascorbate or the like is used. A natural material rich in ascorbic acid to which an antioxidant such as L-ascorbic acid and / or a salt acceptable as a food thereof may be added in the steps subsequent to the extraction step such as the extraction step and / or the blending step ( For example, natural materials derived from fruits such as lemon, orange and acerola, or natural materials derived from vegetables such as broccoli, me cabbage, green pepper, komatsuna and cauliflower can also be used as ascorbic acid in the present invention.
(Other ingredients)
In the packaged tea beverage of the present invention, additives such as an antioxidant, an emulsifier, a storage amount, a pH adjuster, a fragrance, a seasoning, a sweetener, a sour agent, and a quality stabilizer are added alone or in combination. May be. It is preferable not to add a fragrance, a seasoning, a sweetener, an acidulant, etc. from the viewpoint of the flavor of the original tea, and the pH is adjusted to 5.0 to 7.0 from the viewpoint of storage stability. It is preferable to do.
本発明における飲料には、他にも、本発明の効果を損なわない限り、飲料に通常配合する添加剤、例えば、香料、ビタミン、色素類、酸化防止剤、保存料、調味料、エキス類、pH調整剤、品質安定剤等を配合することができる。 In the beverage according to the present invention, other additives that are usually blended in the beverage, for example, flavors, vitamins, pigments, antioxidants, preservatives, seasonings, extracts, as long as the effects of the present invention are not impaired. A pH adjuster, a quality stabilizer, etc. can be mix | blended.
本発明の飲料中のアルコール類の含有量は、1重量%未満であり、好ましくは0.3重量%以下、より好ましくは0.1重量%以下、さらに好ましくは0.01重量%以下である。即ち、香料を配合することによりアルコール類が配合されることになるが、本発明の飲料は香料の添加量が少ない方が好ましく、特に好ましくは香料無添加である。なお、ここでいうアルコール類としてはエタノール、1−プロパノール、イソプロパノール、1−ブタノール、イソブタノール、アミルアルコール、イソアミルアルコール、2−ペンタノール、1−ヘキサノール、2−ヘキサノール、3−ヘキサノール、1−ヘプタノール、2−ヘプタノール、3−ヘプタノール、4−ヘプタノール、プロピレングリコール、1,3−ブタンジオール、ネオペンチルグリコール、グリセリンなどが挙げられるが、これらに限定されない。 The alcohol content in the beverage of the present invention is less than 1% by weight, preferably 0.3% by weight or less, more preferably 0.1% by weight or less, and still more preferably 0.01% by weight or less. . That is, although alcohols will be mix | blended by mix | blending a fragrance | flavor, it is preferable that the addition amount of a fragrance | flavor is smaller in the drink of this invention, Especially preferably, there is no fragrance | flavor addition. The alcohols used herein include ethanol, 1-propanol, isopropanol, 1-butanol, isobutanol, amyl alcohol, isoamyl alcohol, 2-pentanol, 1-hexanol, 2-hexanol, 3-hexanol, and 1-heptanol. , 2-heptanol, 3-heptanol, 4-heptanol, propylene glycol, 1,3-butanediol, neopentyl glycol, glycerin, and the like, but are not limited thereto.
(容器詰茶飲料)
本発明の茶飲料は、容器詰の形態で提供される。容器の形態には、缶等の金属容器、ペットボトル、紙パック、瓶、パウチなどが含まれるが、これらに限定されない。例えば、本発明の飲料を容器に充填した後にレトルト殺菌等の加熱殺菌を行う方法や、飲料を殺菌して容器に充填する方法を通じて、殺菌された容器詰製品を製造することができる。
(Packed tea beverage)
The tea beverage of the present invention is provided in the form of a container. Examples of the form of the container include, but are not limited to, a metal container such as a can, a plastic bottle, a paper pack, a bottle, and a pouch. For example, a sterilized container-packed product can be manufactured through a method of performing heat sterilization such as retort sterilization after filling a beverage of the present invention into a container, or a method of sterilizing a beverage and filling the container.
本発明の容器詰飲料は容器から直接飲用するものだけではなく、たとえばバックインボックスなどのバルク容器、あるいはポーション容器などに充填したものを飲用時に別容器に注ぐことによって飲用に供することもできる。また、濃縮液を飲用に供する際に希釈することもできる。その場合、飲用に供する際の各種成分濃度が本発明の濃度範囲にあれば本発明の効果が得られることは言うまでもない。従って、これらの飲料も本発明の態様である。 The container-packed beverage of the present invention is not only drinkable directly from the container, but can also be used for drinking by pouring a bulk container such as a back-in box or a portion filled with a portion container into another container at the time of drinking. Moreover, it can also be diluted when using a concentrate for drinking. In that case, it is needless to say that the effects of the present invention can be obtained if the concentration of various components used for drinking is within the concentration range of the present invention. Therefore, these beverages are also an aspect of the present invention.
容器の容量は、本発明の飲料はイヌリンの雑味が抑制されており、「ごくごく飲める」飲料であるため、容量の大きいものが好ましく、例えば500ml容量以上であり、550mlあるいは600mlであっても良い。 As for the capacity of the container, since the miscellaneous taste of inulin is suppressed and the beverage of the present invention is a “very drinkable” beverage, a large capacity is preferable, for example, 500 ml capacity or more, even if it is 550 ml or 600 ml good.
(茶飲料の製造方法)
本発明は、別の側面では容器詰茶飲料の製造方法である。当該方法は、以下の工程を含む:当該飲料中のイヌリンの含有量を1〜7g/100mlに調整する工程、当該飲料中の非重合カテキンの含有量を1〜800ppmに調整する工程、及び当該飲料中のアスコルビン酸の含有量を100〜800ppmに調整する工程。
(Method for producing tea beverage)
In another aspect, the present invention is a method for producing a containerized tea beverage. The method includes the following steps: a step of adjusting the content of inulin in the beverage to 1 to 7 g / 100 ml, a step of adjusting the content of non-polymerized catechin in the beverage to 1 to 800 ppm, and the step A step of adjusting the content of ascorbic acid in the beverage to 100 to 800 ppm.
ここで、上記各成分の含有量は、イヌリンは1.5〜5.0g/100mlであってもよく、また2.0〜4.0g/100mlであってもよい。カテキンは10〜750ppmであってもよく、また50〜700ppmであってもよい。アスコルビン酸は200〜700ppm、また300〜600ppmであってもよい。 Here, the content of each of the above components may be 1.5 to 5.0 g / 100 ml for inulin, or 2.0 to 4.0 g / 100 ml for inulin. The catechin may be 10 to 750 ppm or 50 to 700 ppm. Ascorbic acid may be 200 to 700 ppm or 300 to 600 ppm.
上記調整工程は、そのタイミングも限定されない。例えば、上記工程を同時に行ってもよいし、別々に行ってもよいし、工程の順番を入れ替えてもよい。最終的に得られた飲料が、上記の条件を満たせばよい。 The timing of the adjustment process is not limited. For example, the above steps may be performed simultaneously, may be performed separately, or the order of the steps may be changed. The drink finally obtained should just satisfy said conditions.
上記の工程の他は、通常の茶飲料の製造方法によって製造することができる。 Other than the above steps, it can be produced by a normal method for producing a tea beverage.
(イヌリン特有の雑味を抑制する方法)
本発明は、別の側面ではイヌリン特有の雑味を抑制する方法である。当該方法は、以下を含む:当該飲料中のイヌリンの含有量を1〜7g/100mlに調整する工程、当該飲料中の非重合カテキンの含有量を1〜800ppmに調整する工程、及び当該飲料中のアスコルビン酸の含有量を100〜800ppmに調整する工程。
(Method to suppress inulin-specific miscellaneous taste)
In another aspect, the present invention is a method for suppressing the miscellaneous taste characteristic of inulin. The method includes: adjusting the content of inulin in the beverage to 1-7 g / 100 ml, adjusting the content of non-polymerized catechin in the beverage to 1-800 ppm, and in the beverage Adjusting the content of ascorbic acid to 100 to 800 ppm.
ここで、上記各成分の含有量は、イヌリンは1.5〜5.0g/100mlであってもよく、また2.0〜4.0g/100mlであってもよい。カテキンは10〜750ppmであってもよく、また50〜700ppmであってもよい。アスコルビン酸は200〜700ppm、また300〜600ppmであってもよい。 Here, the content of each of the above components may be 1.5 to 5.0 g / 100 ml for inulin, or 2.0 to 4.0 g / 100 ml for inulin. The catechin may be 10 to 750 ppm or 50 to 700 ppm. Ascorbic acid may be 200 to 700 ppm or 300 to 600 ppm.
上記調整工程は、そのタイミングも限定されない。例えば、上記工程を同時に行ってもよいし、別々に行ってもよいし、工程の順番を入れ替えてもよい。最終的に得られた飲料が、上記の条件を満たせばよい。 The timing of the adjustment process is not limited. For example, the above steps may be performed simultaneously, may be performed separately, or the order of the steps may be changed. The drink finally obtained should just satisfy said conditions.
(用途)
本発明の茶飲料にはイヌリンが高含有量で含まれることから、整腸作用を有し、腸や消化管を含むお腹の調子を整える飲料が提供される。具体的には、腸内機能、腸の状態、大腸環境の改善、改良、向上作用を有する飲料であり、また腸運動を促進し、便秘の軽減や予防に効果がある飲料でもある。
(Use)
Since the inulin is contained in the tea beverage of the present invention in a high content, a beverage having an intestinal action and adjusting the condition of the stomach including the intestine and digestive tract is provided. Specifically, it is a beverage having an action for improving, improving, and improving the intestinal function, intestinal state, and large intestine environment, and also a beverage that promotes bowel movement and is effective in reducing or preventing constipation.
(数値範囲)
明確化のために記載すると、本明細書において下限値と上限値によって表されている数値範囲、即ち「下限値〜上限値」は、それら下限値及び上限値を含む。例えば、「1〜2」により表される範囲は、1及び2を含む。
(Numeric range)
For the sake of clarity, the numerical range represented by the lower limit value and the upper limit value in the present specification, that is, “lower limit value to upper limit value” includes the lower limit value and the upper limit value. For example, the range represented by “1-2” includes 1 and 2.
以下に実施例に基づいて本発明の説明をするが、本発明はこれらの実施例に限定されるものではない。
<緑茶飲料>
イヌリン及びアスコルビン酸を配合した緑茶飲料を製造し、殺菌処理した後、300ml容器に充填して容器詰緑茶飲料を製造した。製造した容器詰茶飲料のイヌリン、非重合カテキン、アスコルビン酸を測定した結果を表1に示す。ここで、イヌリンとしてはフジ日本精糖株式会社の「フジFF」を1.0〜8.0g/100mlとなるように、アスコルビン酸は殺菌後に10〜900ppmとなるように添加した。
The present invention will be described below based on examples, but the present invention is not limited to these examples.
<Green tea beverage>
A green tea beverage blended with inulin and ascorbic acid was produced, sterilized, and then filled into a 300 ml container to produce a container-packed green tea beverage. Table 1 shows the results of measurement of inulin, non-polymerized catechin, and ascorbic acid in the produced packaged tea beverage. Here, as inulin, ascorbic acid was added so that it might become 10-900 ppm after sterilization so that "Fuji FF" of Fuji Nippon Seika Co., Ltd. might be 1.0-8.0g / 100ml.
訓練されたパネラーにより、得られた緑茶飲料について、イヌリンの雑味の程度、およびカフェインの香味を評点法による官能試験により評価した。専門パネリスト3名が、それらの程度を総合的に判断した:
5:イヌリンの後味の雑味が極めて少なく飲みやすい
4:イヌリンの後味の雑味が少なく飲みやすい
3:イヌリンの後味の雑味がやや少なく、飲みやすい
2:イヌリンの後味の雑味が若干あるが、飲める
1:イヌリンの後味の雑味は少ないが、カテキンやアスコルビン酸特有の味が強く飲みにくい
0:イヌリンの後味の雑味が強く、飲みにくい
得られた飲料のイヌリン、カテキン、及びアスコルビン酸の含有量と、その評価結果は、表1に記載のとおりである。
A trained panelist evaluated the degree of inulin miscellaneous taste and caffeine flavor of the obtained green tea beverage by a sensory test using a scoring method. Three expert panelists comprehensively judged their extent:
5: Very little inulin aftertaste and easy to drink
4: Easy to drink with little inulin aftertaste
3: Slightly less inulin aftertaste and easy to drink
2: There is some inulin aftertaste, but you can drink it
1: There is little aftertaste of inulin, but the taste peculiar to catechin and ascorbic acid is strong and difficult to drink.
0: The aftertaste of inulin is strong and difficult to drink. The contents of inulin, catechin and ascorbic acid in the obtained beverage and the evaluation results are as shown in Table 1.
表1の結果より、イヌリン高濃度条件においても、非重合体カテキン量を一定の範囲とし、さらにアスコルビン酸を一定量範囲とすることで、イヌリン特有の雑味を抑えることができるとともに、渋みもなく、飲みやすさが増すことが分かった。
<烏龍茶飲料>
烏龍茶葉を30倍重量の熱水(95℃)で4分間抽出し、烏龍茶抽出液を得た(非重合カテキン145ppm含有)。別途調整した烏龍茶抽出液濃縮物により非重合カテキン濃度を200ppmに調整し、アスコルビン酸350ppm、イヌリン2.0g/100mlとなるように配合して製造した烏龍茶飲料を殺菌処理した後、300ml容器に充填して容器詰烏龍茶飲料を製造した。官能評価の結果、得られた容器詰烏龍茶飲料はイヌリンの雑味を感じなかった。
From the results shown in Table 1, even in high inulin conditions, by setting the amount of non-polymer catechin to a certain range and further ascorbic acid to a certain amount range, it is possible to suppress the miscellaneous taste peculiar to inulin and to reduce astringency. It turns out that it is easier to drink.
<Oolong tea drink>
Oolong tea leaves were extracted with 30 times the weight of hot water (95 ° C.) for 4 minutes to obtain Oolong tea extract (containing 145 ppm of non-polymerized catechin). A non-polymer catechin concentration adjusted to 200 ppm with a separately prepared Oolong tea extract concentrate, sterilized Oolong tea drink prepared by blending ascorbic acid 350 ppm and inulin 2.0 g / 100 ml, and then filled into a 300 ml container Thus, a container-packed oolong tea drink was produced. As a result of sensory evaluation, the container-packed oolong tea beverage obtained did not feel the inulin miscellaneous taste.
<紅茶飲料>
紅茶葉100gを20倍重量の熱水(95℃)で1時間抽出し、紅茶抽出物を得た。さらに活性炭処理、減圧濃縮を行って得られた紅茶抽出物濃縮液(非重合カテキン200ppm含有)を希釈して非重合カテキンを50ppmに調整し、アスコルビン酸350ppm、イヌリン2.0g/100mlとなるように配合して製造した紅茶飲料を殺菌処理した後、300ml容器に充填して容器詰紅茶飲料を製造した。官能評価の結果、得られた容器詰紅茶飲料はイヌリンの雑味を感じなかった。
<Tea drink>
100 g of tea leaves were extracted with hot water (95 ° C.) of 20 times weight for 1 hour to obtain a black tea extract. Furthermore, a black tea extract concentrate (containing 200 ppm of non-polymerized catechin) obtained by performing activated carbon treatment and vacuum concentration is diluted to adjust the non-polymerized catechin to 50 ppm, so that the concentration of ascorbic acid is 350 ppm and inulin is 2.0 g / 100 ml. After sterilizing the black tea beverage prepared by blending into the above, it was filled into a 300 ml container to produce a bottled black tea beverage. As a result of sensory evaluation, the obtained packaged black tea beverage did not feel the inulin miscellaneous taste.
Claims (2)
イヌリンの含有量が1〜2g/100mlであり、
非重合体カテキンの含有量が50〜600ppmであり、
アスコルビン酸の含有量が100〜700ppmであり、
香料、調味料、甘味料、酸味料を添加していない、
前記飲料。 A packaged tea beverage,
The inulin content is 1-2 g / 100 ml,
The content of non-polymer catechin is 50 to 600 ppm,
The content of ascorbic acid Ri 100~700ppm der,
No fragrances, seasonings, sweeteners, acidulants added ,
The beverage.
The beverage according to claim 1, which is a 500 ml or more container-packed tea beverage.
Priority Applications (3)
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JP2016130126A JP6463302B2 (en) | 2016-06-30 | 2016-06-30 | High concentration inulin-containing tea beverage |
PCT/JP2017/024067 WO2018003956A1 (en) | 2016-06-30 | 2017-06-30 | Tea beverage containing high concentration of inulin |
SG11201810273TA SG11201810273TA (en) | 2016-06-30 | 2017-06-30 | Tea beverage containing high concentration of inulin |
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JP2016130126A JP6463302B2 (en) | 2016-06-30 | 2016-06-30 | High concentration inulin-containing tea beverage |
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JP2018000075A JP2018000075A (en) | 2018-01-11 |
JP2018000075A5 JP2018000075A5 (en) | 2018-04-05 |
JP6463302B2 true JP6463302B2 (en) | 2019-01-30 |
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JP2016130126A Active JP6463302B2 (en) | 2016-06-30 | 2016-06-30 | High concentration inulin-containing tea beverage |
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JP (1) | JP6463302B2 (en) |
SG (1) | SG11201810273TA (en) |
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JP7323276B2 (en) * | 2018-10-19 | 2023-08-08 | サントリーホールディングス株式会社 | packaged beverage |
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JP3660637B2 (en) * | 2002-03-12 | 2005-06-15 | 花王株式会社 | Green tea beverage manufacturing method |
JP2007521010A (en) * | 2003-07-03 | 2007-08-02 | ザ プロクター アンド ギャンブル カンパニー | A composition containing green tea catechins and one or more polyvalent mineral cations |
AU2014227002B2 (en) * | 2013-03-04 | 2016-11-03 | Suntory Holdings Limited | Light-coloured tea beverage |
JP6087769B2 (en) * | 2013-08-30 | 2017-03-01 | サントリー食品インターナショナル株式会社 | Containerized beverage containing oolong tea extract |
JP6241625B2 (en) * | 2014-01-21 | 2017-12-06 | 株式会社東洋新薬 | Container-packed beverage |
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2017
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WO2018003956A1 (en) | 2018-01-04 |
JP2018000075A (en) | 2018-01-11 |
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