JP6328383B2 - Method for producing effervescent beverage containing cereal decomposition product in container - Google Patents

Method for producing effervescent beverage containing cereal decomposition product in container

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JP6328383B2
JP6328383B2 JP2013129954A JP2013129954A JP6328383B2 JP 6328383 B2 JP6328383 B2 JP 6328383B2 JP 2013129954 A JP2013129954 A JP 2013129954A JP 2013129954 A JP2013129954 A JP 2013129954A JP 6328383 B2 JP6328383 B2 JP 6328383B2
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foam
layer
decomposition product
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司 均 庄
司 均 庄
石 和 弘 平
石 和 弘 平
原 健 司 小
原 健 司 小
野 忍 上
野 忍 上
伸 吉 久保寺
伸 吉 久保寺
下 悟 木
下 悟 木
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Kirin Co Ltd
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Description

本発明は、容器入り穀類分解物含有発泡性飲料の製造方法に関する。より詳細には、本発明は、飲料の液面下に微細泡含有層を発生させた容器入り穀類分解物含有発泡性飲料の製造方法に関する。   The present invention relates to a method for producing an effervescent beverage containing a containerized cereal decomposition product. In more detail, this invention relates to the manufacturing method of the cereal decomposition product containing effervescent drink containing a container which generated the fine foam content layer under the liquid level of the drink.

ビール、ノンアルコールビール、発泡酒をはじめとする穀類分解物含有発泡性飲料の泡は、炭酸ガスの逃げを防止するとともに、香味の維持し、美観を付与するなどの重要な機能を有している。近年、発泡性飲料の研究分野において、泡質の向上を目的とした様々な手段が報告されている。   Foam of cereal decomposition product-containing sparkling beverages such as beer, non-alcoholic beer, and sparkling liquor has important functions such as preventing escape of carbon dioxide gas, maintaining flavor, and imparting aesthetics. Yes. In recent years, various means for improving foam quality have been reported in the research field of sparkling beverages.

例えば、特許文献1には、泡持ちを簡易かつ効果的に向上させるため、穀類分解物含有発泡性飲料をその凍結温度よりも高い温度で外気ガス成分を用いて予め発泡させて得られた発泡体を、別の穀類分解物含有発泡性飲料に混合することを特徴とする飲料ディスペンサーを用いることが報告されている。   For example, Patent Document 1 discloses foaming obtained by foaming a cereal decomposition product-containing sparkling beverage in advance using an outside gas component at a temperature higher than its freezing temperature in order to improve foam retention easily and effectively. It has been reported to use a beverage dispenser characterized by mixing the body with another cereal breakdown product-containing sparkling beverage.

また、特許文献2には、密度の高いクリーミー感のあるビール泡を形成することができる、陽圧解放手段とトリガーとを有することを特徴とする容器が報告されている。   Further, Patent Document 2 reports a container characterized by having a positive pressure releasing means and a trigger capable of forming a beer foam having a high density and creamy feeling.

また、特許文献3には、容器に注がれたそのままの状態またはそれにできるだけ近い状態で、起泡性飲料の泡粒の粒径を精度良く測定することを目的とした、撮影デバイス付き実体顕微鏡を用いた泡の泡質を評価する方法が報告されている。   Patent Document 3 discloses a stereomicroscope with an imaging device for accurately measuring the particle size of foam particles of a foamable beverage in a state as poured into a container or in a state as close as possible. There has been reported a method for evaluating the foam quality of a foam using the above.

また、特許文献4には、飲料の有する視覚的効果を勘案して、複数の泡状の液体層を容器中に分配する方法が報告されている。   Patent Document 4 reports a method of distributing a plurality of foam-like liquid layers into a container in consideration of the visual effect of a beverage.

一方、穀物含有発泡性飲料を容器に注出する際に、泡と飲料との境界液面下に発生する霧状の肌理細かい微細泡含有層が生じる場合のあることが知られている。特に、この微細泡含有層は「スモーキーバブルス」または「フロスティミスト」と称され、飲料をおいしく見せる視覚的効果がある。しかしながら、この微細泡含有層は通常薄く、比較的短期間で消失してしまう。また、微細泡含有層の発生メカニズムの詳細およびその視覚的効果の向上方法は何ら報告されていない。   On the other hand, it is known that when a cereal-containing sparkling beverage is poured into a container, a mist-like fine foam-containing layer generated below the boundary liquid surface between the foam and the beverage may occur. In particular, this fine foam-containing layer is referred to as “smoky bubbles” or “frosty mist” and has a visual effect that makes the beverage look delicious. However, this fine bubble-containing layer is usually thin and disappears in a relatively short period of time. Further, details of the generation mechanism of the fine bubble-containing layer and a method for improving the visual effect are not reported at all.

特開2012−254801号公報JP2012-254801A 特開2010−143625号公報JP 2010-143625 A 特開2010−223701号公報JP 2010-223701 A 特許第4875985号公報Japanese Patent No. 4875985

本発明は、容器入り穀類分解物含有発泡性飲料において、微細泡含有層の厚さおよび持続時間を向上させることをその目的としている。   The object of the present invention is to improve the thickness and duration of a fine foam-containing layer in a sparkling beverage containing a cereal decomposition product in a container.

本発明者らは、今般、穀類分解物含有発泡性飲料に添加する発泡体の泡の粒径の範囲を予め調節すると、穀類分解物含有発泡性飲料の液面下に発生する微細泡含有層の厚さおよび/または持続時間を効果的に調節しうることを見出した。さらに、本発明者らは、今般、特定の泡の粒径の範囲を有する発泡体を穀類分解物含有発泡性飲料上に添加すると、微細泡含有層の厚さおよび/または持続時間が顕著に向上することを見出した。本発明は、かかる知見に基づくものである。   The inventors of the present invention have recently adjusted the particle size range of the foam foam added to the cereal decomposition product-containing sparkling beverage in advance, and the fine foam-containing layer generated below the liquid level of the cereal decomposition product-containing sparkling beverage It has been found that the thickness and / or duration of can be effectively adjusted. Furthermore, the inventors have now noticed that when a foam having a specific foam particle size range is added onto a cereal breakdown product-containing sparkling beverage, the thickness and / or duration of the fine foam-containing layer is significantly increased. I found it to improve. The present invention is based on such knowledge.

本発明によれば以下の発明が提供される。
(1)発泡体層と、微細泡含有層と、穀類分解物含有発泡性飲料層とを含んでなる容器入り穀類分解物含有発泡性飲料の製造方法であって、
上記微細泡含有層を発生させる有効範囲に泡の粒径を調整してなる穀類分解物含有発泡性飲料の発泡体を、
予め容器に注出された穀類分解物含有発泡性飲料上に添加して、発泡体層と、穀類分解物含有発泡性飲料層との境界液面下に微細泡含有層を発生させること
を含んでなる、方法。
(2)上記泡の粒径の有効範囲が、微細泡含有層の厚さおよび/または持続時間の閾値を参照して予め設定される、(1)に記載の方法。
(3)上記発泡体における泡の平均粒径が47μm以下、標準偏差40以下である、(1)または(2)に記載の方法。
(4)上記泡の粒径の調整が大気下で行われる、(1)〜(3)のいずれか一項に記載の方法。
(5)上記泡の粒径の調整が、攪拌、振動、減圧、および気体注出からなる群から選択される方法によって行われる、(1)〜(3)のいずれか一項に記載の方法。
(6)上記微細泡含有層の持続時間が上記発泡体の添加後3分間以上である、(1)〜(5)のいずれか一項に記載の方法。
(7)上記微細泡含有層の厚さが10mm以上である、(1)〜(6)のいずれか一項に記載の方法。
(8)上記微細泡含有層に任意の色相の可視光を照射して、光散乱を生じさせることをさらに含んでなる、(1)〜(7)のいずれか一項に記載の方法。
(9)上記穀類分解物含有発泡性飲料がビール系飲料である、(1)〜(8)のいずれか一項に記載の製造方法。
(10)(1)〜(9)のいずれか一項に記載の方法により得られる、容器入り穀類分解物含有発泡性飲料。
(11)発泡体層と、微細泡含有層と、穀類分解物含有発泡性飲料層とを含んでなる容器入り穀類分解物含有発泡性飲料のディスペンス方法であって、
上記微細泡含有層を発生させる有効範囲に泡の粒径を調整してなる穀類分解物含有発泡性飲料の発泡体を、
予め容器に注出された穀類分解物含有発泡性飲料上に添加して、発泡体層と、穀類分解物含有発泡性飲料層との境界液面下に微細泡含有層を発生させること
を含んでなる、方法。
(12)穀類分解物含有発泡性飲料の発泡体の製造方法であって、
微細泡含有層を発生させる有効範囲に発泡体中の泡の粒径を調整することを含んでなり、
ここで、上記微細泡含有層は、上記発泡体を予め容器に注出された穀類分解物含有発泡性飲料上に添加する場合、発泡体層と、穀類分解物含有発泡性飲料層との境界液面下に発生するものである、方法。
(13)上記泡の粒径の調整が、攪拌、振動、減圧、および気体注出からなる群から選択される方法によって行われる、(12)に記載の方法。
(14)泡の平均粒径が47μm以下、標準偏差40以下である穀類分解物含有発泡性飲料の発泡体からなる、穀類分解物含有発泡性飲料における微細泡含有層発生剤。
According to the present invention, the following inventions are provided.
(1) A method for producing a cereal decomposed product-containing sparkling beverage in a container comprising a foam layer, a fine foam-containing layer, and a cereal decomposed product-containing sparkling beverage layer,
A foam of a cereal decomposition product-containing sparkling beverage obtained by adjusting the particle size of the foam within an effective range for generating the fine foam-containing layer,
Adding to the cereal decomposition product-containing sparkling beverage previously poured into the container, and generating a fine foam-containing layer below the boundary liquid surface between the foam layer and the cereal decomposition product-containing sparkling beverage layer A method that consists of
(2) The method according to (1), wherein an effective range of the particle size of the foam is preset with reference to a thickness and / or duration threshold of the fine foam-containing layer.
(3) The method according to (1) or (2), wherein the foam has an average particle diameter of 47 μm or less and a standard deviation of 40 or less.
(4) The method according to any one of (1) to (3), wherein the adjustment of the particle size of the bubbles is performed in the atmosphere.
(5) The method according to any one of (1) to (3), wherein the adjustment of the particle size of the foam is performed by a method selected from the group consisting of stirring, vibration, decompression, and gas extraction. .
(6) The method according to any one of (1) to (5), wherein the duration of the fine foam-containing layer is 3 minutes or more after the addition of the foam.
(7) The method according to any one of (1) to (6), wherein the thickness of the fine bubble-containing layer is 10 mm or more.
(8) The method according to any one of (1) to (7), further comprising irradiating the fine bubble-containing layer with visible light having an arbitrary hue to cause light scattering.
(9) The production method according to any one of (1) to (8), wherein the cereal decomposition product-containing sparkling beverage is a beer-based beverage.
(10) A sparkling beverage containing a cereal decomposition product in a container, obtained by the method according to any one of (1) to (9).
(11) A dispensing method for a containerized cereal decomposition product-containing effervescent beverage comprising a foam layer, a fine foam-containing layer, and a cereal decomposition product-containing effervescent beverage layer,
A foam of a cereal decomposition product-containing sparkling beverage obtained by adjusting the particle size of the foam within an effective range for generating the fine foam-containing layer,
Adding to the cereal decomposition product-containing sparkling beverage previously poured into the container, and generating a fine foam-containing layer below the boundary liquid surface between the foam layer and the cereal decomposition product-containing sparkling beverage layer A method that consists of
(12) A method for producing a foam of a cereal decomposition product-containing sparkling beverage,
Adjusting the particle size of the foam in the foam to an effective range for generating a fine foam-containing layer,
Here, the fine foam-containing layer is a boundary between the foam layer and the cereal decomposition product-containing effervescent beverage layer when the foam is added onto the cereal decomposition product-containing effervescent beverage previously poured into the container. A method that occurs below the surface of the liquid.
(13) The method according to (12), wherein the adjustment of the particle size of the bubbles is performed by a method selected from the group consisting of stirring, vibration, decompression, and gas extraction.
(14) A fine foam-containing layer generator in a cereal decomposition product-containing effervescent beverage, comprising a foam of a cereal decomposition product-containing effervescent beverage having an average foam particle size of 47 μm or less and a standard deviation of 40 or less.

本発明によれば、微細泡含有層の厚さおよび/または持続時間を所望の範囲に調節しまたは顕著に向上させることができる。また、本発明によれば、微細泡含有層に対して継続的に光照射を行い、光散乱を長期間生じさせることができる。したがって、本発明は、穀類分解物含有発泡性飲料に視覚的効果を付与する上で有利である。   According to the present invention, the thickness and / or duration of the fine bubble-containing layer can be adjusted to a desired range or significantly improved. Moreover, according to this invention, light irradiation can be continuously performed to a fine bubble content layer, and light scattering can be produced for a long period of time. Therefore, this invention is advantageous when providing a visual effect to a cereal decomposition product containing sparkling beverage.

攪拌時間5秒で得られた穀類分解物含有発泡性飲料の発泡体の泡粒の平均粒径(μm)および単位面積あたりの泡の数(個/3mm)と、攪拌速度との関係を示すグラフである。The relationship between the average particle size (μm) and the number of bubbles per unit area (pieces / 3 mm 2 ) and the stirring speed of the foamed product of the cereal decomposition product-containing sparkling beverage obtained with a stirring time of 5 seconds It is a graph to show. 攪拌時間10秒で得られた穀類分解物含有発泡性飲料の発泡体の泡粒の平均粒径(μm)および単位面積あたりの泡の数(個/3mm)と、攪拌速度との関係を示すグラフである。The relationship between the average particle size (μm) and the number of bubbles per unit area (pieces / 3 mm 2 ) and the stirring speed of the foamed product of the cereal decomposition product-containing sparkling beverage obtained with a stirring time of 10 seconds It is a graph to show. 攪拌時間30秒で得られた穀類分解物含有発泡性飲料の発泡体の泡粒の平均粒径(μm)および単位面積あたりの泡の数(個/3mm)と、攪拌速度との関係を示すグラフである。The relationship between the average particle size (μm) and the number of bubbles per unit area (pieces / 3 mm 2 ) and the stirring speed of the foamed product of the cereal decomposition product-containing sparkling beverage obtained with a stirring time of 30 seconds It is a graph to show. 攪拌時間5秒で得られた穀類分解物含有発泡性飲料の発泡体の泡の平均粒径(μm)およびその標準偏差と、攪拌速度との関係を示すグラフである。It is a graph which shows the relationship between the average particle diameter (micrometer) of the foam of the cereal decomposition product containing sparkling beverage obtained by stirring time 5 second, its standard deviation, and stirring speed. 攪拌時間10秒で得られた穀類分解物含有発泡性飲料の発泡体の泡の平均粒径(μm)およびその標準偏差と、攪拌速度との関係を示すグラフである。It is a graph which shows the relationship between the average particle diameter (micrometer) of the foam of the cereal decomposition product containing sparkling drink obtained by stirring time 10 second, its standard deviation, and stirring speed. 攪拌時間30秒で得られた穀類分解物含有発泡性飲料の発泡体の泡の平均粒径(μm)およびその標準偏差と、攪拌速度との関係を示すグラフである。It is a graph which shows the relationship between the average particle diameter (micrometer) of the foam of the cereal decomposition product containing sparkling beverage obtained by stirring time 30 second, its standard deviation, and stirring speed. 穀類分解物含有発泡性飲料の発泡体を予め容器に注出した穀類分解物含有発泡性飲料上に添加した3分間経過後、微細泡含有層の厚さを測定している写真である。It is the photograph which is measuring the thickness of a fine foam content layer after progress for 3 minutes which added the foam of the cereal decomposition product containing effervescent drink on the cereal decomposition product containing effervescent drink poured out into the container beforehand. 攪拌時間10秒、攪拌速度8,000rpmで得られた穀類分解物含有発泡性飲料の発泡体の泡の画像である。It is an image of the foam of the foam of the cereal decomposition product containing sparkling beverage obtained by stirring time 10 second and stirring speed 8,000 rpm. 攪拌時間10秒、攪拌速度10,000rpmで得られた穀類分解物含有発泡性飲料の発泡体の泡の画像である。It is the image of the foam of the foam of the cereal decomposition product containing sparkling drink obtained by stirring time 10 seconds and stirring speed 10,000rpm. 攪拌時間10秒、攪拌速度13,000rpmで得られた穀類分解物含有発泡性飲料の発泡体の泡の画像である。It is an image of the foam of the foam of the cereal decomposition product containing sparkling beverage obtained by stirring time 10 second and stirring speed 13,000 rpm. 攪拌時間10秒、攪拌速度18,000rpmで得られた穀類分解物含有発泡性飲料の発泡体の泡の画像である。It is an image of the foam of the foam of the cereal decomposition product containing sparkling drink obtained by stirring time 10 second and stirring speed 18,000 rpm.

発明の具体的説明Detailed description of the invention

本発明の容器入り穀類分解物含有発泡性飲料の製造方法は、微細泡含有層を発生させる有効範囲に泡の粒径を調整してなる穀類分解物含有発泡性飲料の発泡体を、予め容器に注出された穀類分解物含有発泡性飲料上に添加して、発泡体層と、穀類分解物含有発泡性飲料層との境界液面下に微細泡含有層を発生させることを特徴としている。   The method for producing an effervescent beverage containing a cereal decomposed product in a container according to the present invention is a method for preparing a foam of an effervescent beverage containing a cereal decomposed product by adjusting the particle size of foam within an effective range for generating a fine foam-containing layer. It is added to the cereal decomposition product-containing effervescent beverage poured out in the above, and a fine foam-containing layer is generated below the boundary liquid surface between the foam layer and the cereal decomposition product-containing effervescent beverage layer. .

本発明における「微細泡含有層」について、以下説明する。
ビール等の穀類分解物含有発泡性飲料を容器中に注出する場合、穀類分解物含有発泡性飲料により形成される泡層と、穀類分解物含有発泡性飲料層とが発生する。ここで、上記穀類分解物含有発泡性飲料層のうち、泡層との境界液面下に、泡層中の気泡よりも平均粒径の小さい微細気泡を含有する層状の領域が発生する場合がある。この微細気泡を含有する層状の領域を「微細泡含有層」という。本発明における微細泡含有層は、後述する試験例1Bに記載の方法により、光散乱が確認される範囲を基準に特定することができる。
The “fine bubble-containing layer” in the present invention will be described below.
When a cereal decomposition product-containing sparkling beverage such as beer is poured into a container, a foam layer formed by the cereal decomposition product-containing sparkling beverage and a cereal decomposition product-containing sparkling beverage layer are generated. Here, in the cereal decomposition product-containing foamable beverage layer, a layered region containing fine bubbles having an average particle size smaller than the bubbles in the foam layer may be generated below the boundary liquid surface with the foam layer. is there. This layered region containing fine bubbles is referred to as a “fine bubble-containing layer”. The fine bubble-containing layer in the present invention can be specified on the basis of a range in which light scattering is confirmed by the method described in Test Example 1B described later.

発泡体の調整
本発明の容器入り穀類分解物含有発泡性飲料の製造方法では、まず、穀類分解物含有発泡性飲料を発泡させて得られる発泡体中の泡の粒径を、微細泡含有層を発生させる有効範囲に調整する。
Preparation of Foam In the method for producing an effervescent beverage containing a cereal decomposed product in a container according to the present invention, first, the particle size of the foam in the foam obtained by foaming the effervescent beverage containing the cereal decomposed product is determined using a fine foam-containing layer Adjust the effective range to generate

本発明において、微細泡含有層を発生させる泡の粒径の有効範囲は、微細泡含有層の所望の厚さの閾値および/または持続時間の閾値に応じて適宜決定することができる。したがって、本発明の好ましい態様によれば、泡の粒径の有効範囲は、微細泡含有層の厚さの閾値および/または持続時間の閾値を参照して予め設定される。ここで、微細泡含有層の厚さの「閾値」および/または持続時間の「閾値」とは、飲料に付与する視覚的効果およびその持続性を勘案して当業者が適宜決定してよく、例えば、後述する試験例1および2において示される通り、微細泡含有層の厚さの閾値を10mm、持続時間の閾値を3分間と設定することができる。   In the present invention, the effective range of the particle size of the bubbles for generating the fine bubble-containing layer can be appropriately determined according to the desired thickness threshold and / or the duration threshold of the fine bubble-containing layer. Therefore, according to a preferred embodiment of the present invention, the effective range of the bubble particle size is preset with reference to the thickness threshold and / or duration threshold of the fine bubble-containing layer. Here, the “threshold value” of the thickness of the fine foam-containing layer and / or the “threshold value” of the duration may be appropriately determined by those skilled in the art in consideration of the visual effect imparted to the beverage and its persistence, For example, as shown in Test Examples 1 and 2 to be described later, the threshold value of the thickness of the fine bubble-containing layer can be set to 10 mm, and the threshold value of the duration can be set to 3 minutes.

また、本発明において、泡の平均粒径および標準偏差は、容器に注がれた発泡体を、撮影デバイス付きデジタルカメラによって撮影して、発泡体中の泡粒の画像を得、得られた泡粒の画像を解析して、画像中にある円形の像を泡粒の輪郭として認識させ、その認識された輪郭に基づいて泡粒の粒径および泡の数を求め、この泡粒の粒径および泡の数に基づき、算出することができる。具体的には、泡の平均粒径および標準偏差の決定は、特開2010−223701号公報に記載の方法に準じ、本発明の実施例に記載の方法に基づき決定することができる。   In the present invention, the average particle size and standard deviation of the foam were obtained by photographing the foam poured into the container with a digital camera with a photographing device to obtain an image of the foam particles in the foam. Analyzing the image of the bubble particle, the circular image in the image is recognized as the outline of the bubble particle, the particle size of the bubble particle and the number of bubbles are obtained based on the recognized contour, and the bubble particle It can be calculated based on the diameter and the number of bubbles. Specifically, the average particle diameter and standard deviation of the foam can be determined based on the method described in Examples of the present invention in accordance with the method described in JP 2010-223701 A.

本発明の発泡体において、泡の平均粒径の範囲は、所望の微細泡含有層の厚さおよび/または持続時間を考慮して適宜決定することができるが、微細泡含有層の厚さおよび/または持続時間の向上ためには、上限は、好ましくは47μmであり、より好ましくは40μmであり、さらに好ましくは35μmである。   In the foam of the present invention, the range of the average particle diameter of the foam can be appropriately determined in consideration of the desired thickness and / or duration of the fine foam-containing layer. In order to improve the duration, the upper limit is preferably 47 μm, more preferably 40 μm, and even more preferably 35 μm.

また、本発明の発泡体において、泡の平均粒径の標準偏差は、所望の微細泡含有層の厚さおよび/または持続時間を考慮して適宜決定することができるが、泡の均質性の保持を勘案すれば小さいことが好ましい。泡の平均粒径の標準偏差の上限は、好ましくは40であり、より好ましくは35であり、さらに好ましくは25であり、さらに好ましくは20である。   In the foam of the present invention, the standard deviation of the average particle diameter of the foam can be appropriately determined in consideration of the desired thickness and / or duration of the fine foam-containing layer. In view of holding, it is preferable to be small. The upper limit of the standard deviation of the average particle diameter of the foam is preferably 40, more preferably 35, still more preferably 25, and still more preferably 20.

また、本発明の発泡体において、単位面積あたりの泡の数は、所望の微細泡含有層の厚さおよび/または持続時間を考慮して適宜決定することができるが、好ましくは600個以上(個/3mm)であり、より好ましくは1000個以上(個/3mm)であり、さらに好ましくは1300個(個/3mm)である。 In the foam of the present invention, the number of bubbles per unit area can be appropriately determined in consideration of the desired thickness and / or duration of the fine bubble-containing layer, but preferably 600 or more ( Pieces / 3 mm 2 ), more preferably 1000 pieces or more (pieces / 3 mm 2 ), and even more preferably 1300 pieces (pieces / 3 mm 2 ).

また、本発明において、発泡体における泡の粒径の調整工程は、所望の微細泡含有層の厚さおよび/または持続時間を達成しうる限り特に限定されず、攪拌、振動、減圧または気体注出により処理する方法で行ってよいが、好ましくは撹拌処理である。かかる調整の具体的手法はいずれも、公知装置を用いて実施することができる。   Further, in the present invention, the step of adjusting the particle size of the foam in the foam is not particularly limited as long as the desired thickness and / or duration of the fine foam-containing layer can be achieved, and stirring, vibration, decompression, or gas injection is performed. Although it may be carried out by a method of treating by taking out, stirring treatment is preferred. Any specific method of such adjustment can be carried out using a known apparatus.

また、本発明の好ましい態様によれば、上記泡の粒径の調整工程は、穀類分解物含有発泡性飲料に対して攪拌、振動、減圧または気体注出処理を行う場合、攪拌速度、振動レベル、加圧レベルまたは気体注出速度を調整し、発泡体における泡の粒径を、微細泡含有層を発生させる有効範囲とする工程をさらに含んでなる。また、別の態様によれば、上記調整工程は、泡の粒径の調整中または調整後に、泡の粒径および/または標準偏差を測定する工程を含んでなる。かかる測定工程を実施する具体的手法は、特に限定されず、例えば、攪拌速度、振動レベル、加圧レベルまたは気体注出速度の測定による間接的方法であってもよく、後述する実施例記載の方法に従った泡の粒径および標準偏差の直接的測定方法であってもよい。   Moreover, according to the preferable aspect of this invention, when the adjustment process of the said particle size of foam performs stirring, vibration, pressure reduction, or gas extraction processing with respect to a cereal decomposition product containing sparkling beverage, stirring speed, a vibration level The method further comprises the step of adjusting the pressure level or the gas pouring speed and setting the particle size of the foam in the foam to an effective range for generating the fine foam-containing layer. Moreover, according to another aspect, the said adjustment process comprises the process of measuring the particle size and / or standard deviation of a bubble during adjustment after adjustment of the particle size of a bubble. The specific method for carrying out such a measurement step is not particularly limited, and may be, for example, an indirect method by measurement of a stirring speed, a vibration level, a pressurization level, or a gas extraction speed, which will be described in Examples described later. It may be a direct measurement method of the bubble particle size and standard deviation according to the method.

泡の粒径の調整を撹拌により行う場合、撹拌速度は、泡の粒径が上記範囲となる限り特に限定されないが、例えば、7,000〜18,000rpmであり、好ましくは8000〜18,000rpmである。   When the foam particle size is adjusted by stirring, the stirring speed is not particularly limited as long as the foam particle size falls within the above range, but is, for example, 7,000 to 18,000 rpm, preferably 8000 to 18,000 rpm. It is.

穀類分解物含有発泡性飲料の撹拌時間は、特に限定されないが、好ましくは5秒以上であり、より好ましくは5〜30秒である。   The stirring time of the cereal decomposition product-containing sparkling beverage is not particularly limited, but is preferably 5 seconds or more, and more preferably 5 to 30 seconds.

本発明において、発泡体の泡の粒径の調整は、大気下またはそれに近い組成のガス雰囲気下で好適に行われる。より具体的には、発泡体の泡の粒径の調整は、例えば、大気と同一組成(窒素が約78%、酸素が約21%、その他アルゴン、二酸化炭素など)、または、窒素含有割合が1〜100%の気体、好ましくは70〜100%の気体中で行われることが好ましい。   In the present invention, the particle size of the foam foam is suitably adjusted in the atmosphere or in a gas atmosphere having a composition close thereto. More specifically, the adjustment of the particle size of the foam foam is, for example, the same composition as the atmosphere (about 78% nitrogen, about 21% oxygen, other argon, carbon dioxide, etc.) It is preferable to be carried out in a gas of 1 to 100%, preferably 70 to 100%.

また、本発明において、発泡体の泡の粒径の調整は、本発明の効果を妨げない限り特に限定されないが、大気圧下で行われることが好ましい。   In the present invention, the adjustment of the particle size of the foam foam is not particularly limited as long as the effect of the present invention is not hindered, but it is preferably performed under atmospheric pressure.

また、本発明において、発泡体を形成する穀類分解物含有発泡性飲料の温度は、特に限定されないが、好ましくは0〜20℃であり、より好ましくは0〜10℃である。   Moreover, in this invention, although the temperature of the cereal decomposition product containing sparkling beverage which forms a foam is not specifically limited, Preferably it is 0-20 degreeC, More preferably, it is 0-10 degreeC.

本発明によれば、上述のように調整された発泡体を用いて、微細泡含有層を効果的に発生させることができる。したがって、本発明の好ましい態様によれば、本発明の発泡体は、穀類分解物含有発泡性飲料における微細泡含有層発生剤として用いられる。また、本発明の好ましい態様によれば、微細泡含有層発生剤における泡の平均粒径は47μm以下、標準偏差40以下である。   According to the present invention, the fine foam-containing layer can be effectively generated using the foam adjusted as described above. Therefore, according to a preferred embodiment of the present invention, the foam of the present invention is used as a fine foam-containing layer generator in a cereal decomposition product-containing sparkling beverage. Moreover, according to the preferable aspect of this invention, the average particle diameter of the foam in a fine bubble content layer generating agent is 47 micrometers or less, and the standard deviation is 40 or less.

微細泡含有層の発生
本発明によれば、上述の穀類分解物含有発泡性飲料の発泡体を、予め容器に注出された穀類分解物含有発泡性飲料上に添加して、発泡体と、穀類分解物含有発泡性飲料の境界液面下に微細泡含有層を発生させることができる。
Generation of the fine foam-containing layer According to the present invention, the foam of the above-described cereal decomposition product-containing sparkling beverage is added onto the cereal decomposition product-containing sparkling beverage previously poured into a container, and the foam, A fine foam-containing layer can be generated below the boundary liquid surface of the cereal decomposition product-containing sparkling beverage.

穀類分解物含有発泡性飲料を予め容器へ注出する手法は、微細泡含有層の発生が妨げられない限り特に限定されず、公知手法により行うことができる。本発明においては、上述の発泡体を添加することから、穀類分解物含有発泡性飲料は泡立たないように予め容器中に注出することが好ましい。したがって、本発明においては、例えば、ビールサーバーにおいて行われるような、細かい泡を容器中のビールに後注ぎする工程は行わなくてもよい。   The method of pouring the cereal decomposition product-containing sparkling beverage into the container in advance is not particularly limited as long as the generation of the fine foam-containing layer is not hindered, and can be performed by a known method. In the present invention, since the above-mentioned foam is added, it is preferable to pour the cereal decomposition product-containing sparkling beverage into the container in advance so as not to foam. Therefore, in the present invention, for example, a step of pouring fine bubbles into the beer in the container as in a beer server may not be performed.

本発明において、発泡体の添加は、微細泡含有層の発生を妨げない限り特に限定されないが、泡の平均粒径の保持を勘案すれば、好ましくは発泡体の製造後20秒以内、より好ましくは10秒以内、さらに好ましくは製造後直ちに行うことが好ましい。   In the present invention, the addition of the foam is not particularly limited as long as it does not interfere with the generation of the fine foam-containing layer, but it is preferably within 20 seconds after the production of the foam, more preferably considering the maintenance of the average particle diameter of the foam. Is preferably performed within 10 seconds, more preferably immediately after production.

また、発泡体の添加方法は、微細泡含有層の発生を妨げない限り特に限定されないが、好ましくは、容器中の穀類分解物含有発泡性飲料の液面上方から、発泡体を容器中に注出することにより行われる。発泡体を添加する位置は、微細泡含有層の発生を妨げない限り特に限定されないが、好ましくは、穀類分解物含有発泡性飲料の液面から高さ50mm以上、より好ましくは70mm以上、さらに好ましくは100mm以上の地点である。かかる高さは、穀類分解物含有発泡性飲料内に乱流を発生させ、微細泡含有層を濃厚にする上で好ましい。   The method for adding the foam is not particularly limited as long as it does not prevent the generation of the fine foam-containing layer, but preferably the foam is poured into the container from above the liquid level of the cereal decomposition product-containing sparkling beverage in the container. It is done by putting out. The position at which the foam is added is not particularly limited as long as it does not prevent the generation of the fine foam-containing layer, but is preferably 50 mm or more in height from the liquid level of the cereal decomposition product-containing sparkling beverage, more preferably 70 mm or more, and even more preferably. Is a point of 100 mm or more. Such height is preferable for generating turbulent flow in the cereal decomposition product-containing sparkling beverage and thickening the fine foam-containing layer.

予め容器に注出された穀物含有発泡性飲料の温度は、微細泡含有層の発生を妨げない限り特に限定されないが、好ましくは5〜20℃であり、より好ましくは5〜10℃である。   The temperature of the cereal-containing sparkling beverage previously poured into the container is not particularly limited as long as it does not hinder the generation of the fine foam-containing layer, but is preferably 5 to 20 ° C, more preferably 5 to 10 ° C.

微細泡含有層における微細気泡のサイズは、上述の穀物含有発泡性飲料の発泡体の泡サイズおよび添加方法に応じて適宜調節することができるが、微細気泡の平均粒径は、穀物含有発泡性飲料により通常形成される泡または本発明の発泡体よりも小さくてもよい。したがって、微細気泡の平均粒径は、例えば後述する試験例1Cを考慮すれば、66μm以下とすることができる。また、微細泡含有層における微細気泡の密度は、例えば、穀類分解物含有発泡性飲料の液面から垂直下方向に向かってが徐々に小さくなるように変化してもよい。   The size of the fine bubbles in the fine foam-containing layer can be adjusted as appropriate according to the foam size and the addition method of the foam of the above-mentioned grain-containing sparkling beverage. It may be smaller than the foam normally formed by the beverage or the foam of the present invention. Therefore, the average particle diameter of the fine bubbles can be set to 66 μm or less in consideration of Test Example 1C described later, for example. Moreover, the density of the fine bubbles in the fine foam-containing layer may change, for example, so as to gradually decrease from the liquid level of the cereal decomposition product-containing sparkling beverage toward the vertically downward direction.

本発明によれば、微細泡含有層の厚さおよび保持時間は、発泡体の泡サイズに応じて適宜調節してよいが、視覚的効果を勘案すれば、厚く、長期間となるように調整することが好ましい。
微細泡含有層の保持時間は、特に限定されないが、好ましくは1分間以上であり、より好ましくは2分間以上であり、より好ましくは3分間以上であり、さらに好ましくは3〜5分間以上である。
According to the present invention, the thickness and holding time of the fine foam-containing layer may be adjusted as appropriate according to the foam size of the foam, but if the visual effect is taken into account, it is adjusted to be thick and long. It is preferable to do.
The retention time of the fine bubble-containing layer is not particularly limited, but is preferably 1 minute or more, more preferably 2 minutes or more, more preferably 3 minutes or more, and further preferably 3 to 5 minutes or more. .

微細泡含有層の厚さは、特に限定されないが、穀物含有発泡性飲料層の液面を基準として、好ましくは10mm以上であり、より好ましくは10〜20mmである。   Although the thickness of a fine foam content layer is not specifically limited, Preferably it is 10 mm or more on the basis of the liquid level of a grain containing sparkling beverage layer, More preferably, it is 10-20 mm.

本発明の微細泡含有層の厚さおよび範囲は、後述する試験例1に記載の方法に準じて、穀物含有発泡性飲料の入った透明容器の真下に位置する光照射装置から照射し、光散乱の生じる範囲を基準として決定することができる。   The thickness and range of the fine foam-containing layer of the present invention are irradiated from a light irradiation device located directly below a transparent container containing a cereal-containing sparkling beverage according to the method described in Test Example 1 described later. The range in which scattering occurs can be determined as a reference.

容器入り穀類分解物含有発泡性飲料/光照射
本発明において、容器入り穀類分解物含有発泡性飲料は、上述の方法により製造することができる。
Containerized cereal decomposition product-containing sparkling beverage / light irradiation In the present invention, the containered cereal decomposition product-containing sparkling beverage can be produced by the method described above.

本発明の穀類分解物含有発泡性飲料は、穀類の分解物を含む炭酸飲料であればどのような態様の飲料であっても含まれるが、麦芽の分解物を含む飲料であることが好ましい。本発明において、穀類とは、本発明の効果を奏する穀物であれば特に限定されないが、大麦、小麦、大豆、エンドウ豆またはトウモロコシであることが好ましく、より好ましくは大麦である。穀類の分解物の具体的な態様としては、特に限定されないが、大麦、小麦、大豆、エンドウ豆またはトウモロコシの分解物であり、例えば大豆タンパク、エンドウタンパク、コーンタンパク分解物が挙げられる。   The cereal decomposition product-containing sparkling beverage of the present invention is included in any form of beverage as long as it is a carbonated beverage containing a cereal decomposition product, but is preferably a beverage containing a malt decomposition product. In the present invention, cereals are not particularly limited as long as they have the effects of the present invention, but are preferably barley, wheat, soybeans, peas, or corn, and more preferably barley. Although it does not specifically limit as a concrete aspect of the decomposition product of cereals, it is a decomposition product of barley, wheat, soybean, pea, or corn, for example, soybean protein, pea protein, corn protein decomposition product is mentioned.

本発明の穀類分解物含有発泡性飲料は、好ましくは麦芽分解物含有炭酸飲料であり、より好ましくはビール系飲料である。ビール系飲料とは、通常にビールを製造した場合、すなわち、酵母等による発酵に基づいてビールを製造した場合に得られるビール特有の味わい、香りを有する飲料をいい、例えば、ビール、発泡酒、リキュール等の発酵麦芽飲料や、その他の醸造酒、もしくは完全無アルコール麦芽飲料等の非発酵麦芽飲料が挙げられる。また、ビール系飲料である限り、麦芽飲料に限定されるものではなく、麦や麦芽を使用しない非麦飲料の形態であってもよい。本発明において「非麦飲料」は炭酸ガス等により清涼感が付与された清涼飲料も含まれるものとする。非麦飲料としては、アルコール含量が0重量% である完全無アルコール飲料のような非発酵飲料や、アルコールを含有するアルコール含有飲料が挙げられるが、アルコールを含む態様が好ましい。このアルコール含有非麦飲料としては、発酵して得られた発酵飲料とアルコールが添加された飲料が挙げられる。非麦飲料としては、また、発酵して得られた発酵飲料からアルコール、その他の低沸点成分や低分子成分を除去して得られた非アルコール発酵飲料が挙げられる。ビール系飲料の好ましい態様としては、ビール、発泡酒、完全無アルコール麦芽飲料、非麦飲料が挙げられ、中でもビールが特に好ましい。本発明の穀類分解物含有発泡性飲料は市販の飲料を用いてもよい。   The cereal decomposition product-containing sparkling beverage of the present invention is preferably a malt decomposition product-containing carbonated beverage, and more preferably a beer-based beverage. A beer-based beverage refers to a beverage having a taste and aroma peculiar to beer obtained when beer is usually produced, that is, when beer is produced based on fermentation by yeast or the like. For example, beer, sparkling liquor, Non-fermented malt beverages such as fermented malt beverages such as liqueurs, other brewed liquors, or completely alcohol-free malt beverages. Moreover, as long as it is a beer-type drink, it is not limited to a malt drink, The form of the non-wheat drink which does not use wheat and malt may be sufficient. In the present invention, the “non-wheat beverage” includes a soft drink imparted with a refreshing feeling by carbon dioxide gas or the like. Examples of non-wheat beverages include non-fermented beverages such as completely alcohol-free beverages having an alcohol content of 0% by weight, and alcohol-containing beverages containing alcohol, but embodiments containing alcohol are preferred. Examples of the alcohol-containing non-wheat beverage include fermented beverages obtained by fermentation and beverages to which alcohol is added. Examples of non-wheat beverages include non-alcoholic fermented beverages obtained by removing alcohol, other low-boiling components and low-molecular components from fermented beverages obtained by fermentation. Preferred embodiments of the beer beverage include beer, sparkling liquor, completely alcohol-free malt beverage, and non-wheat beverage, and beer is particularly preferred among them. Commercially available beverages may be used for the cereal decomposition product-containing sparkling beverage of the present invention.

本発明の容器は、特に限定されないが、微細泡含有層の視覚的効果を勘案すれば、透明容器が好ましい。かかる容器としては、特に限定されないが、ガラス製グラスまたはジョッキ等が挙げられる。   Although the container of this invention is not specifically limited, If the visual effect of a fine bubble content layer is considered, a transparent container is preferable. Such a container is not particularly limited, and examples thereof include glass glass or a mug.

また、本発明の容器入り穀類分解物含有発泡性飲料の視覚的効果の向上を勘案すれば、微細泡含有層に、任意の色相の可視光を照射して、光散乱を生じさせることが好ましい。したがって、本発明の容器は、好ましくは、微細泡含有層に任意の色相の可視光を照射しうる光照射装置と着脱可能にまたは一体的に構成されている。かかる光照射装置としては、特に限定されないが、例えば、本発明の容器の基底部と着脱可能であり、容器の真下または斜め下方向から微細泡含有層に光照射しうる蛍光ランプが挙げられる。   Further, considering the improvement of visual effects of the containerized cereal decomposition product-containing sparkling beverage of the present invention, it is preferable to irradiate the fine foam-containing layer with visible light of an arbitrary hue to cause light scattering. . Therefore, the container of the present invention is preferably configured to be detachable or integral with a light irradiation device that can irradiate visible light of an arbitrary hue onto the fine bubble-containing layer. Such a light irradiation device is not particularly limited, and examples thereof include a fluorescent lamp that is detachable from the base of the container of the present invention and can irradiate the fine bubble-containing layer with light from directly below or obliquely below the container.

また、本発明の別の態様によれば、発泡体層と、微細泡含有層と、穀類分解物含有発泡性飲料層とを含んでなる容器入り穀類分解物含有発泡性飲料のディスペンス方法であって、微細泡含有層を発生させる有効範囲に泡の粒径を調整してなる穀類分解物含有発泡性飲料の発泡体を、予め容器に注出された穀類分解物含有発泡性飲料上に添加して、発泡体層と、穀類分解物含有発泡性飲料層との境界液面下に微細泡含有層を発生させることを含んでなる方法が提供される。   According to another aspect of the present invention, there is provided a dispensing method for a cereal decomposed product-containing effervescent beverage in a container comprising a foam layer, a fine foam-containing layer, and a cereal decomposed product-containing effervescent beverage layer. In addition, the foam of the cereal decomposition product-containing effervescent beverage obtained by adjusting the particle size of the foam within the effective range for generating the fine foam-containing layer is added onto the cereal decomposition product-containing effervescent beverage that has been poured into the container in advance. Then, a method comprising generating a fine foam-containing layer below the boundary liquid surface between the foam layer and the cereal decomposition product-containing sparkling beverage layer is provided.

また、本発明のさらに別の態様によれば、穀類分解物含有発泡性飲料の発泡体の製造方法であって、微細泡含有層を発生させる有効範囲に発泡体中の泡の粒径を調整することを含んでなり、ここで、微細泡含有層は、前記発泡体を予め容器に注出された穀類分解物含有発泡性飲料上に添加する場合、発泡体層と、穀類分解物含有発泡性飲料層との境界液面下に発生するものである方法が提供される。   According to still another aspect of the present invention, there is provided a method for producing a foam of a cereal decomposition product-containing sparkling beverage, wherein the foam particle size is adjusted to an effective range for generating a fine foam-containing layer. Here, the fine foam-containing layer, when the foam is added onto the cereal decomposed product-containing effervescent beverage previously poured into the container, the foam layer and the cereal decomposed product-containing foam A method is provided that occurs below the boundary liquid level with the sexual beverage layer.

本発明のディスペンス方法および発泡体の製造方法は、上述の本発明の容器入り穀類分解物含有発泡性飲料の製造方法と同様の手法により行うことができる。   The dispensing method and the foam production method of the present invention can be performed by the same method as the method for producing the above-described containerized cereal decomposition product-containing sparkling beverage.

本発明を以下の例によって詳細に説明するが、本発明はこれらに限定されるものではない。   The present invention will be described in detail by the following examples, but the present invention is not limited thereto.

材料および方法
(1)使用した透明ガラス容器
発泡体の泡の粒径およびその標準偏差を測定する際に発泡体を収容する容器として、直径5cm、高さ10cmの円筒を縦に2分割した、半円筒形の透明ガラス容器を作成した。この容器では、2分割した円筒軸に平行な平面(垂直面)にもガラスが付けられており、容器は円筒軸が鉛直方向となるように立てて使用した。
Materials and methods :
(1) Used transparent glass container A semi-cylindrical shape in which a cylinder having a diameter of 5 cm and a height of 10 cm is divided into two vertically as a container for containing a foam when measuring the particle size of foam and the standard deviation thereof. A transparent glass container was prepared. In this container, glass was also attached to a plane (vertical surface) parallel to the cylindrical axis divided into two, and the container was used upright so that the cylindrical axis was in the vertical direction.

(2)試料およびその状態
試料としては、市販ビール(麒麟麦酒株式会社、一番搾り)を用意して使用した。試料は、飲用する際の温度を勘案して、予め0〜5℃に調整しておいた。
(2) Sample and its state As a sample, commercial beer (Soba Wine Co., Ltd., Ichiban Shibori) was prepared and used. The sample was previously adjusted to 0 to 5 ° C. in consideration of the temperature at the time of drinking.

(3)発泡体の調整
発泡体の泡の粒径の調整は、25℃に調整した室内で大気圧下、後述する通り攪拌処理により行った。
(3) Adjustment of foam The adjustment of the particle size of the foam foam was performed by a stirring process as described later in a room adjusted to 25 ° C under atmospheric pressure.

(4)撮影装置
撮影装置してはデジタルカメラ(東芝製IK−HR2Dを使用し、ここに、対物レンズ(モリテックス製MP−ZE25−200)を、装着したものを使用した。
(4) Shooting device A digital camera (IK-HR2D manufactured by Toshiba) was used as the shooting device, and an objective lens (MP-ZE25-200 manufactured by Moritex Corp.) was attached thereto.

(5)撮影の状態
上記(3)において調整された発泡体が入った透明ガラス容器をテーブルに置き、容器の垂直面側から、光源として、LEDライト(モリテックス製)を用いて、光を当てた。このとき容器に照射される光量を、ライトコントローラで画像を見ながら適宜調整した。
容器の表側、即ち円筒軸に平行な平面側を、上記(4)の装置の撮像デバイス方向に向け、該平面越しに泡層を撮影した。撮影は縦撮影した。またこのときカメラ倍率の倍率は、200倍であった。
なお、撮影に際しては、画像解析ソフトのキャリブレーション(1画素当りの実際の長さ、単位設定)を予め行い、また、予備試料を用いて光量や液量等の各種の撮影条件を予め適宜調整しておいた。
(5) Shooting state Place the transparent glass container containing the foam adjusted in (3) above on a table, and apply light from the vertical surface side of the container using an LED light (Mortex) as a light source. It was. At this time, the amount of light applied to the container was appropriately adjusted while viewing the image with a light controller.
The front side of the container, that is, the plane side parallel to the cylindrical axis was directed toward the imaging device of the apparatus (4), and the foam layer was photographed through the plane. The photo was taken vertically. At this time, the camera magnification was 200 times.
When photographing, calibration of image analysis software (actual length per pixel, unit setting) is performed in advance, and various photographing conditions such as light quantity and liquid amount are appropriately adjusted in advance using a preliminary sample. I kept it.

(6)画像解析ソフトウエア
撮影された泡粒の画像について、画像中にある円形の像を泡粒の輪郭として認識させ、認識された輪郭に基づいて泡粒の直径を算出した。このとき使用した画像解析ソフトウエアとしては、Win ROOF(ウインルーフ) ver. 8.0(三谷商事株式会社製)を使用した。
(6) Image analysis software About the image | photographed bubble particle | grain image, the circular image in an image was made to recognize as a bubble particle | grain outline, and the diameter of the bubble particle | grain was computed based on the recognized outline. As the image analysis software used at this time, Win ROOF ver. 8.0 (manufactured by Mitani Corporation) was used.

試験例1
A:発泡体の調整
ビール100mLを攪拌機(商品名マジックブレッド、会社名ショップジャパン)を用いて、大気圧下、大気中で、攪拌速度5,000〜18,000rpm(5,000rpm、6,000rpm、7,000rpm、8,000rpm、10,000rpm、13,000rpmまたは18,000rpm)で、5、10または30秒間攪拌し、ビールの発泡体を得た。
Test example 1
A: Preparation of foamed beer 100 mL of stirrer 5,000 to 18,000 rpm (5,000 rpm, 6,000 rpm) in the atmosphere under atmospheric pressure using a stirrer (trade name : Magicbread, company name: Shop Japan) , 7,000 rpm, 8,000 rpm, 10,000 rpm, 13,000 rpm or 18,000 rpm) for 5 to 10 or 30 seconds to obtain a foam of beer.

各条件下で得られた発泡体を、上述したように専用の透明ガラス容器に注いだ後、直ちに、画像を撮影した。
次に、撮影された画像を、上記画像解析ソフトウエアを使用して解析し、泡径(泡粒の直径)を計測した。同じ試料を用いて3回繰り返し測定を行った。得られた泡径の結果と測定された泡粒の個数のデータから、各時点での、泡粒の平均粒径(mm)、および単位面積あたりの泡の数およびその標準偏差を求めた。
Images were taken immediately after pouring the foam obtained under each condition into a dedicated transparent glass container as described above.
Next, the photographed image was analyzed using the image analysis software, and the bubble diameter (the diameter of the foam particles) was measured. Measurements were repeated three times using the same sample. From the result of the obtained bubble diameter and the data of the number of foam particles measured, the average particle diameter (mm) of the foam particles, the number of bubbles per unit area and the standard deviation thereof were obtained at each time point.

次に、攪拌時間5、1または30秒で得られた発泡体における泡の平均粒径(mm)および単位面積あたりの泡の数(個/3mm)と攪拌速度(rpm)との関係を解析した。その結果は、図1A〜1Cに示される通りであった。
なお、図1A〜1Cにおいて、泡粒の平均粒径は四角で示され、泡の数(個/3mm)は菱形で示されている。また、点線は、後述する試験例2のように、微細泡含有層の持続時間が3分間以上であり、微細泡含有層の厚さ10mm以上であることを微細泡含有層の閾値として設定した場合、この閾値を満たす発泡体の境界線は示している。
Next, the relationship between the average particle diameter (mm) and the number of bubbles per unit area (number / 3 mm 2 ) and the stirring speed (rpm) in the foam obtained with stirring time of 5, 1 or 30 seconds is shown below. Analyzed. The results were as shown in FIGS.
In FIGS. 1A to 1C, the average particle diameter of the foam particles is indicated by a square, and the number of bubbles (number / 3 mm 2 ) is indicated by a rhombus. Moreover, the dotted line set as the threshold value of the fine bubble content layer that the duration of the fine foam content layer is 3 minutes or more and the thickness of the fine foam content layer is 10 mm or more as in Test Example 2 described later. In the case, the boundary line of the foam satisfying this threshold is shown.

また、攪拌時間5、1または30秒で得られた発泡体における泡の平均粒径(mm)およびその標準偏差と攪拌速度を解析した。その結果、図2A〜2Cに示される通りであった。
なお、図2A〜2Cにおいて、泡粒の平均粒径は四角で示され、その標準偏差(泡径のばらつき)は菱形で示されている。また、点線は、後述する試験例2のように、微細泡含有層の持続時間が3分間以上であり、微細泡含有層の厚さ10mm以上であることを微細泡含有層の閾値として設定した場合、この閾値を満たす発泡体の境界線は示している。
Moreover, the average particle diameter (mm) of the foam in the foam obtained by stirring time 5, 1 or 30 second, its standard deviation, and stirring speed were analyzed. As a result, it was as shown in FIGS.
2A to 2C, the average particle diameter of the foam particles is indicated by a square, and the standard deviation (variation of the bubble diameter) is indicated by a rhombus. Moreover, the dotted line set as the threshold value of the fine bubble content layer that the duration of the fine foam content layer is 3 minutes or more and the thickness of the fine foam content layer is 10 mm or more as in Test Example 2 described later. In the case, the boundary line of the foam satisfying this threshold is shown.

B:微細泡含有層を発生させたビールの製造
ビール(305ml)を予め注いだ435mlの透明ガラス製グラス(高さ19cm、ビール305mlを注いだ際の液面面積48cm)を用意した。ここで、透明ガラス製グラスは、厚さ5mmの透明プラスチック板上に置き、グラス底面の真下から白熱電球(100V用、40W形、E26口金)により光照射を行った。
B: Production of beer in which a fine foam-containing layer was generated A 435 ml transparent glass glass (height 19 cm, liquid surface area 48 cm 2 when pouring beer 305 ml) pre-poured with beer (305 ml) was prepared. Here, the glass made of transparent glass was placed on a transparent plastic plate having a thickness of 5 mm, and was irradiated with an incandescent bulb (for 100 V, 40 W type, E26 base) from directly below the bottom of the glass.

次に、ビール液面より垂直上方100mmの高さから、Aにおいて得られた各発泡体をそれぞれビール液面に添加した。その結果、発泡体とビールとの境界に位置する液面下に微細泡含有層が発生したことが確認された。ここで、微細泡含有層の確認は、視力1.0の健常なパネラー3名が、境界液面の水平横方向であり、かつグラス壁面から15cm離れた地点から、目視により行った。また、パネラーにより、泡による光散乱が確認された範囲を微細泡含有層と認定した。   Next, each foam obtained in A was added to the beer liquid surface from a height of 100 mm vertically above the beer liquid surface. As a result, it was confirmed that a fine foam-containing layer was generated below the liquid level located at the boundary between the foam and the beer. Here, three fine panelists with a visual acuity of 1.0 confirmed the fine bubble-containing layer visually from a point in the horizontal horizontal direction of the boundary liquid surface and 15 cm away from the glass wall surface. Moreover, the range in which the light scattering by a bubble was confirmed by the panel was recognized as a fine bubble content layer.

次に、発泡体を添加して3分間経過後、各試料において、微細泡含有層の厚さが10mm以上であるか否かを確認した。ここで、図3に示される通り、微細泡含有層の厚さは、発泡体とビール液面との境界液面から垂直下方向の微細泡含有層の末端までの長さを定規により確認した。   Next, after 3 minutes have passed since the foam was added, it was confirmed in each sample whether the thickness of the fine foam-containing layer was 10 mm or more. Here, as shown in FIG. 3, the thickness of the fine foam-containing layer was confirmed by a ruler from the boundary liquid surface between the foam and the beer liquid surface to the end of the vertical fine foam-containing layer in the vertical downward direction. .

その結果、攪拌速度5,000rpmでは、攪拌時間5、10または30秒のいずれの発泡体であっても、微細泡含有層の厚さは10mm未満であった。
また、攪拌速度7,000rpmでは、攪拌時間5または10秒では、微細泡含有層の厚さは10mm未満であった。一方、攪拌時間30秒では、微細泡含有層の厚さは10mm以上であった。
また、攪拌速度8,000、10,000、13,000および18,000rpmでは、攪拌時間5、10秒または30秒のいずれの発泡体であっても、微細泡含有層の厚さは10mm以上であった。なお、攪拌時間10秒でありかつ攪拌速度8,000、10,000、13,000および18,000rpmの発泡体の泡の画像は、図4A〜Dに示される通りであった。
As a result, at a stirring speed of 5,000 rpm, the thickness of the fine foam-containing layer was less than 10 mm regardless of the foam with a stirring time of 5, 10 or 30 seconds.
At a stirring speed of 7,000 rpm, the thickness of the fine bubble-containing layer was less than 10 mm when the stirring time was 5 or 10 seconds. On the other hand, when the stirring time was 30 seconds, the thickness of the fine bubble-containing layer was 10 mm or more.
In addition, at a stirring speed of 8,000, 10,000, 13,000, and 18,000 rpm, the thickness of the fine foam-containing layer is 10 mm or more regardless of whether the foam has a stirring time of 5, 10 seconds, or 30 seconds. Met. In addition, the image of the foam of the foam whose stirring time is 10 seconds and whose stirring speed is 8,000, 10,000, 13,000, and 18,000 rpm was as being shown by FIG.

C:微細泡含有層の発生と、発泡体の泡粒径との関係の解析
図1A〜1Cおよび図2A〜2Cにおいて、発泡体を添加して3分間経過後に微細泡含有層の厚さが10mm以上であった場合の泡の粒径、単位面積当たりの泡の数、および泡の標準偏差を確認した。
その結果、発泡体を添加して3分間経過後に微細泡含有層の厚さが10mm以上であったのは、泡の平均粒径47μm以下、その標準偏差40以下、単位面積当たりの泡の数600(個/3mm)以上の場合であることが確認された。
C: Analysis of relationship between generation of fine bubble-containing layer and foam particle size of foam In FIGS. 1A to 1C and FIGS. 2A to 2C, the thickness of the fine foam-containing layer is 3 minutes after the addition of the foam. When the diameter was 10 mm or more, the particle diameter of the foam, the number of foam per unit area, and the standard deviation of the foam were confirmed.
As a result, the thickness of the fine foam-containing layer was 10 mm or more after the addition of the foam for 3 minutes. The average particle diameter of the foam was 47 μm or less, its standard deviation was 40 or less, and the number of bubbles per unit area. It was confirmed that this was the case of 600 (pieces / 3 mm 2 ) or more.

表1は、発泡体を添加して3分間経過後に微細泡含有層の厚さが10mm以上となることが確認された試料の発泡体の泡の平均粒径(μm)、その標準偏差、および単位面積当たりの泡の個数(個/3mm)を示す。
なお、以下の表1における通常泡(コントロール)とは、生ビールサーバーから泡のみを透明ガラス容器に直接注ぎ出して形成された泡を意味する。
Table 1 shows the average particle diameter (μm) of the foam foam of the sample in which the thickness of the fine foam-containing layer was confirmed to be 10 mm or more after 3 minutes from the addition of the foam, its standard deviation, and The number of bubbles per unit area (pieces / 3 mm 2 ) is shown.
In addition, the normal foam (control) in the following Table 1 means a foam formed by pouring only foam from a draft beer server directly into a transparent glass container.

試験例2
試験例1と同様の手法により、泡の平均粒径47μm、標準偏差40、単位面積当たりの泡の数600個以上(個/3mm)の発泡体を得た。
次に、試験例1と同様の手法により、ビール液面より垂直上方30mm、50mmまたは100mmの高さから、発泡体をビール液面に添加した。その結果、いずれの高さから発泡体を添加した場合でもビールとの境界液面下に微細泡含有層が発生し、3分間後も微細泡含有層が存在することが確認された。
Test example 2
By the same method as in Test Example 1, a foam having an average particle diameter of bubbles of 47 μm, a standard deviation of 40, and the number of bubbles per unit area of 600 or more (pieces / 3 mm 2 ) was obtained.
Next, the foam was added to the beer liquid level from a height of 30 mm, 50 mm, or 100 mm vertically above the beer liquid level by the same method as in Test Example 1. As a result, it was confirmed that even when the foam was added from any height, a fine foam-containing layer was generated below the boundary liquid surface with beer, and the fine foam-containing layer was still present after 3 minutes.

なお、ビール液面より垂直上方100mmの高さから、発泡体を添加した場合は、高さ30mmおよび50mmの場合よりも、微細泡含有層の厚さが大きかった。特に、100mmの場合には、発泡体の添加3分間後も10mmを超える厚さの微細泡含有層が確認された。   When the foam was added from a height of 100 mm vertically above the beer liquid level, the thickness of the fine foam-containing layer was larger than when the height was 30 mm and 50 mm. In particular, in the case of 100 mm, a fine foam-containing layer having a thickness exceeding 10 mm was confirmed even after 3 minutes from the addition of the foam.

Claims (12)

発泡体層と、微細泡含有層と、穀類分解物含有発泡性飲料層とを含んでなる容器入り穀類分解物含有発泡性飲料の製造方法であって、
前記微細泡含有層を発生させる有効範囲に泡の粒径を調整してなる穀類分解物含有発泡性飲料の発泡体を、
予め容器に注出された穀類分解物含有発泡性飲料上に添加して、発泡体層と、穀類分解物含有発泡性飲料層との境界液面下に微細泡含有層を発生させること
を含んでなり、
前記泡の粒径の調整が大気またはそれに近い組成のガス雰囲気下で行われ、
前記大気またはそれに近い組成のガスの窒素含有割合が70〜100%であり、
前記発泡体における泡の平均粒径が47μm以下、標準偏差40以下であり、
前記発泡体における単位面積あたりの泡の数が、600個以上(個/3mm )であり、
前記穀類分解物含有発泡性飲料がビール系飲料である、方法。
A method for producing a cereal decomposition product-containing effervescent beverage in a container comprising a foam layer, a fine foam-containing layer, and a cereal decomposition product-containing effervescent beverage layer,
A foam of a cereal decomposition product-containing sparkling beverage obtained by adjusting the particle size of foam within an effective range for generating the fine foam-containing layer,
Adding to the cereal decomposition product-containing sparkling beverage previously poured into the container, and generating a fine foam-containing layer below the boundary liquid surface between the foam layer and the cereal decomposition product-containing sparkling beverage layer And
Adjustment of the particle size of the bubbles is performed in a gas atmosphere having a composition close to the atmosphere,
The nitrogen content of the gas having the composition close to the atmosphere or 70 to 100%,
The average particle size of the foam in the foam is 47 μm or less, the standard deviation is 40 or less,
The number of bubbles per unit area in the foam is 600 or more (pieces / 3 mm 2 ),
The method according to which the cereal decomposition product-containing sparkling beverage is a beer-based beverage.
前記泡の粒径の有効範囲が、微細泡含有層の厚さの閾値および/または持続時間の閾値を参照して予め設定される、請求項1に記載の方法。   The method according to claim 1, wherein the effective range of the bubble particle size is preset with reference to a thickness threshold and / or a duration threshold of the fine bubble-containing layer. 前記泡の粒径の調整が、攪拌、振動、減圧、および気体注出からなる群から選択される方法によって行われる、請求項1または2に記載の方法。 The method according to claim 1 or 2 , wherein the adjustment of the particle size of the bubbles is performed by a method selected from the group consisting of stirring, vibration, decompression, and gas extraction. 前記微細泡含有層の持続時間が前記発泡体の添加後3分間以上である、請求項1〜のいずれか一項に記載の方法。 The method according to any one of claims 1 to 3 , wherein a duration of the fine foam-containing layer is 3 minutes or more after the addition of the foam. 前記微細泡含有層の厚さが10mm以上である、請求項1〜のいずれか一項に記載の方法。 The method as described in any one of Claims 1-4 whose thickness of the said fine bubble content layer is 10 mm or more. 前記微細泡含有層に任意の色相の可視光を照射して、光散乱を生じさせることをさらに含んでなる、請求項1〜のいずれか一項に記載の方法。 Said irradiated with visible light of any color in the microfoam containing layer, further comprising a to cause light scattering method according to any one of claims 1-5. 前記穀類分解物含有発泡性飲料がビールである、請求項1〜のいずれか一項に記載の製造方法。 The cereal hydrolyzate is comprising effervescent beverage beer, the production method according to any one of claims 1-6. 発泡体層と、微細泡含有層と、穀類分解物含有発泡性飲料層とを含んでなる容器入り穀類分解物含有発泡性飲料であって、
前記発泡体が、大気またはそれに近い組成のガスと穀類分解物含有発泡性飲料とを用いて形成された発泡体であり、
前記大気またはそれに近い組成のガスの窒素含有割合が70〜100%であり、
前記発泡体における泡の平均粒径が47μm以下、標準偏差40以下であり、
前記発泡体における単位面積あたりの泡の数が、600個以上(個/3mm )であり、
前記微細泡含有層が、発泡体層と、穀類分解物含有発泡性飲料層との境界液面下にあり、
前記微細泡含有層の厚さが10mm以上であり、
前記微細泡含有層を3分間以上持続して保持することが可能であり、
前記穀類分解物含有発泡性飲料がビール系飲料である、容器入り穀類分解物含有発泡性飲料。
A cereal decomposition product-containing effervescent beverage in a container comprising a foam layer, a fine foam-containing layer, and a cereal decomposition product-containing effervescent beverage layer,
The foam is a foam formed by using a gas having a composition close to the atmosphere or a cereal decomposition product-containing sparkling beverage,
The nitrogen content of the gas having the composition close to the atmosphere or 70 to 100%,
The average particle size of the foam in the foam is 47 μm or less, the standard deviation is 40 or less,
The number of bubbles per unit area in the foam is 600 or more (pieces / 3 mm 2 ),
The fine foam-containing layer is below the boundary liquid surface between the foam layer and the cereal decomposition product-containing foamable beverage layer,
The thickness of the fine bubble-containing layer is 10 mm or more,
It is possible to hold the fine foam-containing layer continuously for 3 minutes or more,
A cereal decomposition product-containing effervescent beverage in a container, wherein the cereal decomposition product-containing effervescent beverage is a beer-based beverage.
発泡体層と、微細泡含有層と、穀類分解物含有発泡性飲料層とを含んでなる容器入り穀類分解物含有発泡性飲料のディスペンス方法であって、
前記微細泡含有層を発生させる有効範囲に泡の粒径を調整してなる穀類分解物含有発泡性飲料の発泡体を、
予め容器に注出された穀類分解物含有発泡性飲料上に添加して、発泡体層と、穀類分解物含有発泡性飲料層との境界液面下に微細泡含有層を発生させること
を含んでなり、
前記泡の粒径の調整が大気またはそれに近い組成のガス雰囲気下で行われ、
前記大気またはそれに近い組成のガスの窒素含有割合が70〜100%であり、
前記発泡体における泡の平均粒径が47μm以下、標準偏差40以下であり、
前記発泡体における単位面積あたりの泡の数が、600個以上(個/3mm )であり、
前記穀類分解物含有発泡性飲料がビール系飲料である、方法。
A method for dispensing a cereal decomposed product-containing sparkling beverage in a container comprising a foam layer, a fine foam-containing layer, and a cereal decomposed product-containing sparkling beverage layer,
A foam of a cereal decomposition product-containing sparkling beverage obtained by adjusting the particle size of foam within an effective range for generating the fine foam-containing layer,
Adding to the cereal decomposition product-containing sparkling beverage previously poured into the container, and generating a fine foam-containing layer below the boundary liquid surface between the foam layer and the cereal decomposition product-containing sparkling beverage layer And
Adjustment of the particle size of the bubbles is performed in a gas atmosphere having a composition close to the atmosphere,
The nitrogen content of the gas having the composition close to the atmosphere or 70 to 100%,
The average particle size of the foam in the foam is 47 μm or less, the standard deviation is 40 or less,
The number of bubbles per unit area in the foam is 600 or more (pieces / 3 mm 2 ),
The method according to which the cereal decomposition product-containing sparkling beverage is a beer-based beverage.
穀類分解物含有発泡性飲料の発泡体の製造方法であって、
微細泡含有層を発生させる有効範囲に発泡体中の泡の粒径を調整することを含んでなり、
ここで、前記微細泡含有層は、前記発泡体を予め容器に注出された穀類分解物含有発泡性飲料上に添加する場合、発泡体層と、穀類分解物含有発泡性飲料層との境界液面下に発生するものでなり、
前記泡の粒径の調整が大気またはそれに近い組成のガス雰囲気下で行われ、
前記大気またはそれに近い組成のガスの窒素含有割合が70〜100%であり、
前記発泡体における泡の平均粒径が47μm以下、標準偏差40以下であり、
前記発泡体における単位面積あたりの泡の数が、600個以上(個/3mm )であり、
前記穀類分解物含有発泡性飲料がビール系飲料である、方法。
A method for producing a foam of a cereal decomposition product-containing sparkling beverage,
Adjusting the particle size of the foam in the foam to an effective range for generating a fine foam-containing layer,
Here, the fine foam-containing layer is a boundary between the foam layer and the cereal decomposition product-containing effervescent beverage layer when the foam is added onto the cereal decomposition product-containing effervescent beverage previously poured into the container. It occurs under the liquid level,
Adjustment of the particle size of the bubbles is performed in a gas atmosphere having a composition close to the atmosphere,
The nitrogen content of the gas having the composition close to the atmosphere or 70 to 100%,
The average particle size of the foam in the foam is 47 μm or less, the standard deviation is 40 or less,
The number of bubbles per unit area in the foam is 600 or more (pieces / 3 mm 2 ),
The method according to which the cereal decomposition product-containing sparkling beverage is a beer-based beverage.
前記泡の粒径の調整が、攪拌、振動、減圧、および気体注出からなる群から選択される方法によって行われる、請求項10に記載の方法。   The method according to claim 10, wherein the adjustment of the bubble particle size is performed by a method selected from the group consisting of stirring, vibration, decompression, and gas extraction. 泡の平均粒径が47μm以下、標準偏差40以下であり、単位面積あたりの泡の数が、600個以上(個/3mm )である、大気またはそれに近い組成のガスと穀類分解物含有発泡性飲料とを用いて形成された発泡体からなる、穀類分解物含有発泡性飲料における微細泡含有層発生剤であって、
前記大気またはそれに近い組成のガスの窒素含有割合が70〜100%であり、
前記穀類分解物含有発泡性飲料がビール系飲料であり、
前記微細泡含有層が、容器入り穀類分解物含有発泡性飲料における発泡体層と、穀類分解物含有発泡性飲料層との境界液面下に発生する、微細泡含有層発生剤。
A foam having an average particle size of 47 μm or less, a standard deviation of 40 or less, and a number of bubbles per unit area of 600 or more (pieces / 3 mm 2 ), and a gas having a composition close to the atmosphere and a cereal decomposition product It is a fine foam-containing layer generator in a cereal decomposition product-containing sparkling beverage, comprising a foam formed using a functional beverage,
The nitrogen content of the gas having the composition close to the atmosphere or 70 to 100%,
The cereal decomposition product-containing sparkling beverage is a beer-based beverage,
A fine foam-containing layer generator, wherein the fine foam-containing layer is generated below a boundary liquid surface between a foam layer in a cereal decomposed product-containing sparkling beverage in a container and a cereal decomposed product-containing sparkling beverage layer.
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