JP5145131B2 - Manufacturing method of polishing head - Google Patents

Manufacturing method of polishing head Download PDF

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JP5145131B2
JP5145131B2 JP2008164723A JP2008164723A JP5145131B2 JP 5145131 B2 JP5145131 B2 JP 5145131B2 JP 2008164723 A JP2008164723 A JP 2008164723A JP 2008164723 A JP2008164723 A JP 2008164723A JP 5145131 B2 JP5145131 B2 JP 5145131B2
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polishing
rubber film
workpiece
rigid ring
polishing head
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JP2010010213A (en
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寿 桝村
浩昌 橋本
幸治 森田
敬実 岸田
悟 荒川
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FUJIKOSHI MACHINE INDUSTRY CO.,LTD.
Shin Etsu Handotai Co Ltd
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FUJIKOSHI MACHINE INDUSTRY CO.,LTD.
Shin Etsu Handotai Co Ltd
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Priority to JP2008164723A priority Critical patent/JP5145131B2/en
Priority to US12/992,782 priority patent/US20110070813A1/en
Priority to PCT/JP2009/002450 priority patent/WO2009157137A1/en
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B24GRINDING; POLISHING
    • B24BMACHINES, DEVICES, OR PROCESSES FOR GRINDING OR POLISHING; DRESSING OR CONDITIONING OF ABRADING SURFACES; FEEDING OF GRINDING, POLISHING, OR LAPPING AGENTS
    • B24B37/00Lapping machines or devices; Accessories
    • B24B37/27Work carriers
    • B24B37/30Work carriers for single side lapping of plane surfaces
    • B24B37/32Retaining rings
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B24GRINDING; POLISHING
    • B24BMACHINES, DEVICES, OR PROCESSES FOR GRINDING OR POLISHING; DRESSING OR CONDITIONING OF ABRADING SURFACES; FEEDING OF GRINDING, POLISHING, OR LAPPING AGENTS
    • B24B37/00Lapping machines or devices; Accessories
    • B24B37/04Lapping machines or devices; Accessories designed for working plane surfaces
    • B24B37/042Lapping machines or devices; Accessories designed for working plane surfaces operating processes therefor
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B24GRINDING; POLISHING
    • B24BMACHINES, DEVICES, OR PROCESSES FOR GRINDING OR POLISHING; DRESSING OR CONDITIONING OF ABRADING SURFACES; FEEDING OF GRINDING, POLISHING, OR LAPPING AGENTS
    • B24B37/00Lapping machines or devices; Accessories
    • B24B37/11Lapping tools
    • B24B37/20Lapping pads for working plane surfaces
    • B24B37/24Lapping pads for working plane surfaces characterised by the composition or properties of the pad materials

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  • Engineering & Computer Science (AREA)
  • Mechanical Engineering (AREA)
  • Finish Polishing, Edge Sharpening, And Grinding By Specific Grinding Devices (AREA)
  • Mechanical Treatment Of Semiconductor (AREA)

Description

本発明は、ワークの表面を研磨する際にワークを保持するための研磨ヘッドを製造する方法、及びその方法で製造された研磨ヘッドを備えた研磨装置に関し、特には、ラバー膜でワークを保持する研磨ヘッドの製造方法及びその製造された研磨ヘッドを備えた研磨装置に関する。   The present invention relates to a method for manufacturing a polishing head for holding a workpiece when polishing the surface of the workpiece, and a polishing apparatus having a polishing head manufactured by the method, and in particular, holding a workpiece with a rubber film. The present invention relates to a polishing head manufacturing method and a polishing apparatus including the manufactured polishing head.

シリコンウェーハ等のワークの表面を研磨する装置として、ワークを片面ずつ研磨する片面研磨装置と、両面を同時に研磨する両面研磨装置とがある。
一般的な片面研磨装置は、例えば図9に示したように研磨布89が貼り付けられた定盤88と、研磨剤供給機構90と、研磨ヘッド82等から構成されている。このような研磨装置81では、研磨ヘッド82でワークWを保持し、研磨剤供給機構90から研磨布89上に研磨剤を供給するとともに、定盤88と研磨ヘッド82をそれぞれ回転させてワークWの表面を研磨布89に摺接させることにより研磨を行う。
As a device for polishing the surface of a workpiece such as a silicon wafer, there are a single-side polishing device for polishing a workpiece one side at a time and a double-side polishing device for polishing both surfaces simultaneously.
A typical single-side polishing apparatus includes, for example, a surface plate 88 to which a polishing cloth 89 is attached, an abrasive supply mechanism 90, a polishing head 82, and the like as shown in FIG. In such a polishing apparatus 81, the workpiece W is held by the polishing head 82, the polishing agent is supplied from the polishing agent supply mechanism 90 onto the polishing cloth 89, and the surface plate 88 and the polishing head 82 are rotated to rotate the workpiece W. Polishing is performed by bringing the surface of the substrate into sliding contact with the polishing cloth 89.

ワークを研磨ヘッドに保持する方法としては、平坦な円盤状のプレートにワックス等の接着剤を介してワークを貼り付ける方法等がある。その他、特にワークの外周部における跳ね上げやダレを抑制し、ワーク全体の平坦性を向上させるための保持方法として、ワーク保持部をラバー膜とし、該ラバー膜の背面に空気等の加圧流体を流し込み、均一の圧力でラバー膜を膨らませて研磨布にワークを押圧する、いわゆるラバーチャック方式がある(例えば特許文献1参照)。   As a method of holding the work on the polishing head, there is a method of attaching the work to a flat disk-shaped plate via an adhesive such as wax. In addition, as a holding method for improving the flatness of the entire workpiece by suppressing the jumping and sagging especially at the outer periphery of the workpiece, the workpiece holding portion is made of a rubber film, and a pressurized fluid such as air is provided on the back surface of the rubber film. There is a so-called rubber chuck system in which a rubber film is inflated with a uniform pressure and a workpiece is pressed against a polishing cloth (see, for example, Patent Document 1).

従来のラバーチャック方式の研磨ヘッドの構成の一例を模式的に図8に示す。この研磨ヘッド102の要部は、環状のSUS製などの剛性リング104と、剛性リング104に接着されたラバー膜103と、剛性リング104に結合された中板105とからなる。剛性リング104と、ラバー膜103と、中板105とによって、密閉された空間106が画成される。また、ラバー膜103の下面部の周辺部には、剛性リング104と同心に、環状のテンプレート114が具備される。また、中板105の中央には圧力調整機構107により加圧流体を供給するなどして空間の圧力を調節する。また、中板105を研磨布109方向に押圧する図示しない押圧手段を有している。   An example of the configuration of a conventional rubber chuck type polishing head is schematically shown in FIG. The main part of the polishing head 102 includes an annular rigid ring 104 made of SUS, a rubber film 103 bonded to the rigid ring 104, and an intermediate plate 105 coupled to the rigid ring 104. A sealed space 106 is defined by the rigid ring 104, the rubber film 103, and the intermediate plate 105. Further, an annular template 114 is provided concentrically with the rigid ring 104 around the lower surface of the rubber film 103. Further, the pressure of the space is adjusted by supplying a pressurized fluid to the center of the intermediate plate 105 by a pressure adjusting mechanism 107. Further, a pressing means (not shown) for pressing the intermediate plate 105 in the direction of the polishing pad 109 is provided.

ラバー膜103の材質としては、特許文献2にゴム硬度10〜100、引っ張り強度3〜20MPa、引っ張り伸度50〜1000%の範囲にあるフッ素系ゴム、ウレタンゴム、シリコンゴムやエチレンプロピレンゴム等の様々なゴム材料が提案されている。
このように構成された研磨ヘッド102を用いて、ラバー膜103の下面部でバッキングパッド113を介してワークWを保持するとともに、テンプレート114でワークWのエッジ部を保持し、中板105を押圧して定盤108の上面に貼り付けられた研磨布109にワークWを摺接させて研磨する。
As a material of the rubber film 103 , Patent Document 2 discloses a rubber hardness of 10 to 100, a tensile strength of 3 to 20 MPa, a tensile elongation of 50 to 1000%, such as fluorine-based rubber, urethane rubber, silicon rubber, and ethylene propylene rubber. Various rubber materials have been proposed.
Using the thus configured polishing head 102, the work W is held on the lower surface portion of the rubber film 103 via the backing pad 113, the edge portion of the work W is held by the template 114, and the intermediate plate 105 is pressed. Then, the work W is brought into sliding contact with the polishing cloth 109 attached to the upper surface of the surface plate 108 and polished.

特開平5−69310号公報Japanese Patent Laid-Open No. 5-69310 特開2005-7521号公報JP 2005-7521 A

このような、ラバー膜103にワークWを保持する研磨ヘッド102を用いてワークWの研磨を行う事により、ワークW全体の平坦性及び研磨代均一性が向上する場合もあったが、ラバー膜103の材質や、同じ材質でも製造ロットが異なった場合に平坦性及び研磨代均一性が低下し、安定したワークWの平坦度が得られないという問題があった。   By polishing the workpiece W using such a polishing head 102 that holds the workpiece W on the rubber film 103, the flatness and polishing margin uniformity of the entire workpiece W may be improved. When the production lot is different even with the material 103 or the same material, there is a problem that the flatness and the polishing margin uniformity are lowered, and a stable flatness of the workpiece W cannot be obtained.

本発明は前述のような問題に鑑みてなされたもので、ワークWの研磨において、安定して一定の平坦性が得られる研磨ヘッドの製造方法及び研磨装置を提供する事を目的とする。   The present invention has been made in view of the above-described problems, and an object of the present invention is to provide a polishing head manufacturing method and a polishing apparatus that can stably obtain a certain flatness in polishing a workpiece W.

上記目的を達成するために、本発明によれば、少なくとも、環状の剛性リングと、該剛性リングに均一の張力で接着されたラバー膜と、前記剛性リングに結合され、前記ラバー膜と前記剛性リングとともに空間部を形成する中板と、前記空間部の圧力を変化させる圧力調整機構とを具備し、前記ラバー膜の下面部にワークの裏面を保持し、該ワークの表面を定盤上に貼り付けた研磨布に摺接させて研磨する研磨ヘッドの製造方法であって、少なくとも、前記ラバー膜を剛性リングに接着する前に、該ラバー膜のJIS K6251に準拠した引張試験を行い、歪が5%以内の応力―歪曲線を線形近似して得られる傾きの値が10MPa以下となるものを選別する工程を含み、該選別された前記傾きの値が10Mpa以下となるラバー膜を用いて前記剛性リングに接着して研磨ヘッドを製造することを特徴とする研磨ヘッドの製造方法を提供する(請求項1)。   In order to achieve the above object, according to the present invention, at least an annular rigid ring, a rubber film bonded to the rigid ring with a uniform tension, and a rubber film coupled to the rigid ring, the rubber film and the rigid An intermediate plate that forms a space together with the ring, and a pressure adjusting mechanism that changes the pressure of the space, holds the back surface of the work on the bottom surface of the rubber film, and places the surface of the work on a surface plate A method of manufacturing a polishing head that is polished by being brought into sliding contact with an attached polishing cloth, and at least before the rubber film is bonded to a rigid ring, a tensile test based on JIS K6251 is performed on the rubber film to obtain a strain. Using a rubber film including a step of selecting a slope value obtained by linearly approximating a stress-strain curve within 5% and having a slope value of 10 MPa or less, wherein the selected slope value is 10 MPa or less. To provide a method of manufacturing a polishing head, characterized in that to produce a polishing head and adhered to the rigid ring (claim 1).

このように、少なくとも、前記ラバー膜を剛性リングに接着する前に、該ラバー膜のJIS K6251に準拠した引張試験を行い、歪が5%以内の応力―歪曲線を最小二乗法による線形近似して得られる傾きの値が10MPa以下となるものを選別する工程を含み、該選別された前記傾きの値が10Mpa以下となるラバー膜を用いて前記剛性リングに接着して研磨ヘッドを製造すれば、ワークを研磨する際に、ラバー膜の材質の種類や、ラバー膜の材料のロット間で発生する研磨代均一性のばらつきを抑制することができ、安定して良好な平坦性を確保できる研磨ヘッドを製造することができる。   In this way, at least before the rubber film is bonded to the rigid ring, a tensile test based on JIS K6251 of the rubber film is performed, and a stress-strain curve within 5% of the strain is linearly approximated by the least square method. And manufacturing a polishing head by bonding to the rigid ring using a rubber film having the selected inclination value of 10 Mpa or less. When polishing a workpiece, it is possible to suppress variations in the type of rubber film and the variation in polishing stock uniformity that occurs between lots of rubber film material, and to ensure stable and good flatness A head can be manufactured.

このとき、前記保持するワークは、直径が300mm以上のシリコン単結晶ウェーハであることができる(請求項2)。
このように、前記保持するワークが、直径が300mm以上のような大直径のシリコン単結晶ウェーハであっても、本発明によりワークの全面にわたってより均一の押圧力で研磨することができ、良好な平坦性を確保することができる。
At this time, the workpiece to be held may be a silicon single crystal wafer having a diameter of 300 mm or more.
Thus, even if the workpiece to be held is a silicon single crystal wafer having a large diameter such as 300 mm or more, the present invention can be polished with a more uniform pressing force over the entire surface of the workpiece. Flatness can be ensured.

また、本発明は、少なくとも、定盤上に貼り付けられた研磨布と、該研磨布上に研磨剤を供給するための研磨剤供給機構と、ワークを保持するための研磨ヘッドを具備し、前記研磨ヘッドでワークの裏面を保持して前記ワークの表面を研磨する研磨装置であって、前記研磨ヘッドは、少なくとも、環状の剛性リングと、該剛性リングに均一の張力で接着されたラバー膜と、前記剛性リングに結合され、前記ラバー膜と前記剛性リングとともに空間部を形成する中板と、前記空間部の圧力を変化させる圧力調整機構とを具備し、前記ラバー膜は、該ラバー膜のJIS K6251に準拠した引張試験で得られる歪が5%以内の応力―歪曲線を線形近似して得られる傾きの値が10MPa以下となるゴム材料で形成され、前記研磨布のヤング率は3.5MPa以下であり、前記圧力調整機構で前記空間部の圧力を制御しつつ、前記ワークの表面を前記定盤上に貼り付けた前記研磨布に摺接させて研磨するものであることを特徴とする研磨装置を提供する。 Further, the present invention comprises at least an abrasive cloth affixed on a surface plate, an abrasive supply mechanism for supplying an abrasive onto the abrasive cloth, and an abrasive head for holding a workpiece, A polishing apparatus for holding a back surface of a work by the polishing head and polishing the surface of the work, wherein the polishing head includes at least an annular rigid ring and a rubber film bonded to the rigid ring with a uniform tension. And an intermediate plate coupled to the rigid ring and forming a space portion together with the rubber film and the rigid ring, and a pressure adjusting mechanism for changing the pressure of the space portion, the rubber film comprising the rubber film The strain obtained by a tensile test in accordance with JIS K6251 is a rubber material having a slope of 10 MPa or less obtained by linear approximation of a stress-strain curve having a strain of 5% or less. The Young's modulus of the abrasive cloth is 3 The surface of the workpiece is slidably contacted with the polishing cloth affixed on the surface plate and polished while the pressure of the space is controlled by the pressure adjusting mechanism. that provides a polishing apparatus for a.

このように、前記研磨ヘッドは、少なくとも、環状の剛性リングと、該剛性リングに均一の張力で接着されたラバー膜と、前記剛性リングに結合され、前記ラバー膜と前記剛性リングとともに空間部を形成する中板と、前記空間部の圧力を変化させる圧力調整機構とを具備し、前記ラバー膜は、該ラバー膜のJIS K6251に準拠した引張試験で得られる歪が5%以内の応力―歪曲線を線形近似して得られる傾きの値が10MPa以下となるゴム材料で形成され、前記研磨布のヤング率は3.5MPa以下であり、前記圧力調整機構で前記空間部の圧力を制御しながら、前記ワークの表面を前記定盤上に貼り付けた前記研磨布に摺接させて研磨するものであれば、ラバー膜の材質の種類や、ラバー膜の材料のロット間で発生する研磨代均一性のばらつきを抑制でき、安定して良好な平坦性を確保してワークを研磨することができる。   As described above, the polishing head includes at least an annular rigid ring, a rubber film bonded to the rigid ring with a uniform tension, and the rigid ring, and a space portion is formed together with the rubber film and the rigid ring. An inner plate to be formed; and a pressure adjusting mechanism for changing the pressure in the space. The rubber film has a stress-strain of 5% or less in a strain obtained by a tensile test according to JIS K6251 of the rubber film. It is formed of a rubber material having an inclination value obtained by linearly approximating a line of 10 MPa or less, and the Young's modulus of the polishing cloth is 3.5 MPa or less, while controlling the pressure of the space portion with the pressure adjusting mechanism. If the surface of the workpiece is polished by being brought into sliding contact with the polishing cloth affixed on the surface plate, the kind of rubber film material or the polishing average generated between lots of rubber film material Can suppress the variation in sex, it is possible to polish the workpiece stably by ensuring good flatness.

このとき、前記研磨するワークは、直径が300mm以上のシリコン単結晶ウェーハであることができる。
このように、前記研磨するワークが、直径が300mm以上のような大直径のシリコン単結晶ウェーハであっても、本発明の前記研磨ヘッドで保持して研磨することによって、ワークの全面にわたってより均一の押圧力で研磨することができ、良好な平坦性を確保することができる。
At this time, the work of the polishing, Ru can diameter of more silicon single crystal wafers 300 mm.
Thus, even if the workpiece to be polished is a silicon single crystal wafer having a large diameter such as 300 mm or more, it is more uniform over the entire surface of the workpiece by holding and polishing with the polishing head of the present invention. It is possible to polish with a pressing force of 2 to ensure good flatness.

本発明では、少なくとも、ラバー膜を剛性リングに接着する前に、該ラバー膜のJIS K6251に準拠した引張試験を行い、歪が5%以内の応力―歪曲線を線形近似して得られる傾きの値が10MPa以下となるものを選別する工程を含み、該選別された前記傾きの値が10MPa以下となるラバー膜を用いて剛性リングに接着して研磨ヘッドを製造するので、ワークを研磨する際に、ラバー膜の材質の種類や、ラバー膜の材料のロット間で発生する研磨代均一性のばらつきを抑制することができ、安定して良好な平坦性を確保できる研磨ヘッドを製造することができる。   In the present invention, at least before the rubber film is bonded to the rigid ring, a tensile test in accordance with JIS K6251 of the rubber film is performed, and a stress-strain curve having a strain within 5% is linearly approximated. Including a step of selecting one having a value of 10 MPa or less, and a polishing head is manufactured by adhering to a rigid ring using a rubber film having the selected inclination value of 10 MPa or less. In addition, it is possible to manufacture a polishing head that can suppress variations in polishing material uniformity between types of rubber films and lots of rubber film materials, and can stably ensure good flatness. it can.

また、本発明に係る研磨装置は、少なくとも、定盤上に貼り付けられた研磨布と、該研磨布上に研磨剤を供給するための研磨剤供給機構と、上述した本発明に係る製造方法で製造した研磨ヘッドを具備し、前記研磨布のヤング率は3.5MPa以下であり、ワークの表面を前記定盤上に貼り付けた前記研磨布に摺接させて研磨するものなので、ラバー膜の材質の種類や、ラバー膜の材料のロット間で発生する研磨代均一性のばらつきを抑制でき、安定して良好な平坦性を確保してワークを研磨することができる。   The polishing apparatus according to the present invention includes at least an abrasive cloth affixed on a surface plate, an abrasive supply mechanism for supplying an abrasive onto the abrasive cloth, and the manufacturing method according to the present invention described above. The polishing cloth has a Young's modulus of 3.5 MPa or less, and the surface of the workpiece is polished by being brought into sliding contact with the polishing cloth affixed on the surface plate. The variation in the polishing allowance uniformity generated between the types of the materials and the lots of the rubber film material can be suppressed, and the workpiece can be polished stably while securing good flatness.

以下、本発明について実施の形態を説明するが、本発明はこれに限定されるものではない。
従来の研磨ヘッドを用い、ラバー膜にワークを保持してワークの研磨を行った際、該研磨ヘッドのラバー膜の材料であるゴムの種類の違いや、同じ種類のゴムでもロットが異なることで、研磨特性にばらつきが生じて良好な平坦性が得られないという問題があった。
しかも、このような研磨特性のばらつきは、ラバー膜の材料であるゴムの原料ロットの硬度や引張り強度等の物性値等から予測する事は困難であった。
Hereinafter, although an embodiment is described about the present invention, the present invention is not limited to this.
When using a conventional polishing head to hold the workpiece on the rubber film and polishing the workpiece, the difference in the type of rubber that is the material of the rubber film of the polishing head, As a result, there is a problem in that the polishing characteristics vary and good flatness cannot be obtained.
Moreover, it has been difficult to predict such variations in polishing characteristics from physical properties such as hardness and tensile strength of rubber raw material lots that are rubber film materials.

そこで、本発明者らは、このような問題が生じる原因について鋭意実験及び検討を行った。
その結果、本発明者らは、以下のことを見出した。
すなわち、ラバー膜の材料として使用するゴムの種類、硬度、及び引張り強度とは関係なく、歪が5%以下の微小な変形に対する応力が小さいゴム材料を用いることで、良好な研磨代均一性が得られることが分かった。すなわち、研磨ヘッドのラバー膜として、微小変形時の応力が小さいラバー膜を用いてワークを研磨することで、ワークの全面にわたって均一の押圧力によって研磨することができることが分かった。さらに、テンプレートを有する研磨ヘッドを用いてワークを研磨する際、テンプレートの下端面の高さとワークの下端面の高さの僅かな差によって生じるワーク外周部の圧力分布が緩和され、その結果として研磨代均一性が良好となることを見出した。
Accordingly, the present inventors have conducted intensive experiments and studies on the cause of such problems.
As a result, the present inventors have found the following.
In other words, regardless of the type, hardness, and tensile strength of the rubber used as the material for the rubber film, the use of a rubber material having a small stress with respect to a minute deformation having a strain of 5% or less provides good polishing margin uniformity. It turns out that it is obtained. That is, it has been found that polishing can be performed with uniform pressing force over the entire surface of the work by polishing the work using a rubber film having a small stress at the time of minute deformation as the rubber film of the polishing head. Furthermore, when polishing a workpiece using a polishing head having a template, the pressure distribution on the outer periphery of the workpiece caused by a slight difference between the height of the lower end surface of the template and the height of the lower end surface of the workpiece is alleviated, resulting in polishing. It has been found that the stock uniformity is good.

そこで、本発明者らは、更に鋭意実験及び検討を行い、ラバー膜として使用されるゴム材料の微小変形時の応力の数値化を行い、それらのゴム材料における研磨特性を調査し、最適化を行い、本発明を完成させた。   Therefore, the present inventors conducted further diligent experiments and studies, quantified the stress at the time of minute deformation of rubber materials used as rubber films, investigated the polishing characteristics of those rubber materials, and optimized them. The present invention was completed.

図1に、本発明に係る研磨ヘッドおよび研磨装置の一例を示す。
図1に示すように、研磨装置1は研磨ヘッド2、定盤8を有している。定盤8は円盤形状であり、上面にワークWを研磨する研磨布9が貼付されている。そして、定盤8の下部には駆動軸11が垂直に連結され、その駆動軸11の下部に連結された定盤回転モータ(不図示)によって回転するようになっている。
FIG. 1 shows an example of a polishing head and a polishing apparatus according to the present invention.
As shown in FIG. 1, the polishing apparatus 1 has a polishing head 2 and a surface plate 8. The surface plate 8 has a disk shape, and a polishing cloth 9 for polishing the workpiece W is attached to the upper surface. A drive shaft 11 is vertically connected to the lower portion of the surface plate 8 and is rotated by a surface plate rotation motor (not shown) connected to the lower portion of the drive shaft 11.

この定盤8の上方に、研磨ヘッド2が設置されている。研磨ヘッド2は、環状の剛性リング4と剛性リング4に均一の張力で接着され、下面が平坦であるラバー膜3と剛性リング4に、例えばボルト等で連結された中板5とを備える。この剛性リング4と、ラバー膜3と、中板5とによって、密閉された空間部6が形成されている。   The polishing head 2 is installed above the surface plate 8. The polishing head 2 includes an annular rigid ring 4 and a rubber film 3 that is bonded to the rigid ring 4 with a uniform tension and has a flat bottom surface and an intermediate plate 5 that is connected to the rigid ring 4 with, for example, a bolt or the like. A sealed space 6 is formed by the rigid ring 4, the rubber film 3, and the intermediate plate 5.

また、研磨ヘッド2は、その軸周りに回転可能となっている。
ここで、剛性リング4の材質は、特に限定されることはないが、例えばSUS(ステンレス)等の剛性材料とすることができる。また、中板の材質、形状等は特に限定されず、空間部6が形成できるものであれば良い。
またここで、ラバー膜3の厚さは、特に限定されることはないが、例えば1mm程度とすることができる。
Further, the polishing head 2 is rotatable around its axis.
Here, the material of the rigid ring 4 is not particularly limited, but may be a rigid material such as SUS (stainless steel). The material, shape, etc. of the intermediate plate are not particularly limited as long as the space 6 can be formed.
Here, the thickness of the rubber film 3 is not particularly limited, but can be, for example, about 1 mm.

ここで、本発明に係る研磨装置の研磨ヘッドに用いられるラバー膜は、以下に記述するような特性を持つものが用いられる。
図2(A)にJIS K6251に準拠した引張試験で得られたラバー膜の応力―歪曲線の一例を示す。図2(B)は、図2(A)の応力―歪曲線の歪が5%以内の部分を拡大したものである。ここで、図2(B)のような、歪が5%以内の応力―歪曲線を最小二乗法による線形近似して得られた直線は、応力=a×歪+bで表わされる。
本発明では、この直線の傾きaが10MPa以下となるようなラバー膜が用いられる。
Here, the rubber film used in the polishing head of the polishing apparatus according to the present invention has a characteristic as described below.
FIG. 2A shows an example of a stress-strain curve of a rubber film obtained by a tensile test based on JIS K6251. FIG. 2B is an enlarged view of a portion where the strain of the stress-strain curve of FIG. Here, a straight line obtained by linearly approximating a stress-strain curve with a strain of 5% or less as shown in FIG. 2B by the least square method is expressed as stress = a × strain + b.
In the present invention, a rubber film is used in which the straight line inclination a is 10 MPa or less.

また、図1に示すように、定盤8の上方に研磨用のスラリーを供給するための研磨スラリー供給手段10を具備する。
またこのとき、ラバー膜3の下面部の周辺部には、研磨中にワークWが外れないようにワークWのエッジ部を保持するための環状のテンプレート14を配設することができる。この場合、テンプレート14は、剛性リング4と同心となるようにし、ラバー膜3の下面部の外周部に沿って、下方に突出するように配設することができる。
Moreover, as shown in FIG. 1, the polishing slurry supply means 10 for supplying the slurry for polishing above the surface plate 8 is provided.
At this time, an annular template 14 for holding the edge portion of the workpiece W can be disposed around the lower surface portion of the rubber film 3 so that the workpiece W is not detached during polishing. In this case, the template 14 can be arranged so as to be concentric with the rigid ring 4 and protrude downward along the outer peripheral portion of the lower surface portion of the rubber film 3.

ここで、テンプレート14の下端面の高さは、保持されたワークWの下端面の高さと同じか、あるいはワークWの下端面の高さよりも、例えば10μm程度僅かに下方に突出しているようにすることができる。
このように、テンプレート14を配設すれば、ワーク外周部の圧力分布を緩和することができ、ワーク外周部の過研磨が防止され、ワークの研磨代均一性を向上することができる。
Here, the height of the lower end surface of the template 14 is the same as the height of the lower end surface of the workpiece W held, or is slightly lower than the height of the lower end surface of the workpiece W, for example by about 10 μm. can do.
Thus, if the template 14 is provided, the pressure distribution on the outer periphery of the workpiece can be relaxed, overpolishing of the outer periphery of the workpiece can be prevented, and the polishing allowance uniformity of the workpiece can be improved.

また、テンプレート14は、その外径が少なくとも剛性リング4の内径よりも大きいもので、かつ、その内径が剛性リング4の内径よりも小さいものとすることができる。
このようにすれば、ワーク全面にかかる押圧力をより均一にして研磨することができる。
またここで、テンプレート14の材質は、ワークWを汚染せず、かつ、キズや圧痕をつけないために、ワークWよりも柔らかく、研磨中に研磨布9と摺接されても磨耗しにくい、耐磨耗性の高い材質であることが好ましい。
Further, the template 14 can have an outer diameter that is at least larger than the inner diameter of the rigid ring 4 and an inner diameter that is smaller than the inner diameter of the rigid ring 4.
In this way, the pressing force applied to the entire surface of the work can be made more uniform and polished.
Here, the material of the template 14 does not contaminate the workpiece W and does not cause scratches or indentations, so it is softer than the workpiece W and is not easily worn even if it is in sliding contact with the polishing pad 9 during polishing. A material with high wear resistance is preferred.

また、図1に示すように、研磨装置1は、研磨ヘッド2の空間部6の圧力を変化させる圧力調整機構7を具備している。
そして、中板5の中央には圧力調整機構7に連通する圧力調整用の貫通孔12が設けられており、圧力調整機構7により加圧流体を供給するなどして空間部6の圧力を調整することができるようになっている。
また、中板5を研磨布9に押圧する手段を有している(不図示)。
As shown in FIG. 1, the polishing apparatus 1 includes a pressure adjusting mechanism 7 that changes the pressure in the space 6 of the polishing head 2.
A pressure adjusting through hole 12 communicating with the pressure adjusting mechanism 7 is provided at the center of the intermediate plate 5, and the pressure of the space portion 6 is adjusted by supplying pressurized fluid by the pressure adjusting mechanism 7. Can be done.
In addition, it has means for pressing the intermediate plate 5 against the polishing pad 9 (not shown).

またこのとき、ラバー膜3の下面にバッキングパッド13を貼設することができる。バッキングパッド13は、水を含ませてワークWを貼りつけ、ラバー膜3のワーク保持面にワークWを保持するものである。ここで、バッキングパッド13は、例えば発泡ポリウレタン製とすることができる。このようなバッキングパッド13を設けて水を含ませる事で、バッキングパッド13に含まれる水の表面張力によりワークWを確実に保持することができる。   At this time, the backing pad 13 can be attached to the lower surface of the rubber film 3. The backing pad 13 attaches the work W with water and holds the work W on the work holding surface of the rubber film 3. Here, the backing pad 13 can be made of foamed polyurethane, for example. By providing such a backing pad 13 and containing water, the workpiece W can be reliably held by the surface tension of the water contained in the backing pad 13.

また、定盤8の上面に貼付されている研磨布9は、ヤング率が3.5MPa以下の軟質なものが使用される。本発明に係る研磨ヘッド2とヤング率が3.5MPa以下の軟質な研磨布9を組み合わせて使用することで、ワークWと研磨布9間の接触圧力分布をより確実に緩和させることができ、ワークWの研磨代均一性をより確実に向上することができる。
なお、図1ではテンプレート14が直接ラバー膜3に接着される態様を示したが、本発明は、テンプレート14がラバー膜3にバッキングパッド13等を介して接着される場合を排除するものではない。
As the polishing cloth 9 attached to the upper surface of the surface plate 8, a soft cloth having a Young's modulus of 3.5 MPa or less is used. By using the polishing head 2 according to the present invention in combination with a soft polishing cloth 9 having a Young's modulus of 3.5 MPa or less, the contact pressure distribution between the workpiece W and the polishing cloth 9 can be more reliably relaxed, The polishing margin uniformity of the workpiece W can be improved more reliably.
Although FIG. 1 shows a mode in which the template 14 is directly bonded to the rubber film 3, the present invention does not exclude the case where the template 14 is bonded to the rubber film 3 via the backing pad 13 or the like. .

このように構成された研磨装置1を用いて、図示しない中板押圧手段により中板5を定盤8上に貼り付けられた研磨布9の方向に押圧し、研磨剤供給機構10を介して研磨剤を供給しながら、ワークWを研磨布9に摺接してワークWの表面を研磨するものとなっている。ここで、中板押圧手段は、例えば、エアシリンダーなど用いて中板5を全面にわたって均一の圧力で押圧できるものが好ましい。   Using the polishing apparatus 1 configured in this way, the intermediate plate 5 is pressed in the direction of the polishing cloth 9 affixed on the surface plate 8 by an intermediate plate pressing means (not shown), and the abrasive supply mechanism 10 is used. While supplying the abrasive, the work W is brought into sliding contact with the polishing cloth 9 to polish the surface of the work W. Here, it is preferable that the intermediate plate pressing means can press the intermediate plate 5 with a uniform pressure over the entire surface using, for example, an air cylinder.

このように、本発明に係る研磨装置1を用いてワークWを研磨すれば、ラバー膜3の材質の種類や、ラバー膜3の材料のロット間で発生する研磨代均一性のばらつきを抑制することができ、安定して良好な平坦性を確保してワークWを研磨することができる。
また、テンプレート14の下端面の高さとワークWの下端面の高さの僅かな差によって生じるワークWの外周部の圧力分布を緩和することができる。従って、ワークWの厚さやテンプレート14の厚さがある程度ばらついている場合であっても、ワークWに加わる押圧力を全面にわたって均一に保って研磨を行うことができる。その結果、ワークWの研磨代均一性が良好な研磨を行うことができる。
Thus, if the workpiece | work W is grind | polished using the grinding | polishing apparatus 1 which concerns on this invention, the kind of material of the rubber film 3 and the dispersion | variation in the grinding | polishing allowance uniformity which generate | occur | produce between lots of the material of the rubber film 3 will be suppressed. Therefore, the workpiece W can be polished with stable and good flatness.
Further, the pressure distribution in the outer peripheral portion of the workpiece W caused by a slight difference between the height of the lower end surface of the template 14 and the height of the lower end surface of the workpiece W can be relaxed. Therefore, even when the thickness of the workpiece W or the thickness of the template 14 varies to some extent, polishing can be performed while the pressing force applied to the workpiece W is kept uniform over the entire surface. As a result, it is possible to perform polishing with a good polishing margin uniformity of the workpiece W.

このとき、研磨するワークは、直径が300mm以上のシリコン単結晶ウェーハであることができる。
このように、研磨するワークが、直径が300mm以上のような大直径のシリコン単結晶ウェーハであっても、本発明の研磨ヘッドで保持して研磨することによって、ワークの全面にわたってより均一の押圧力で研磨することができ、良好な平坦性を確保することができる。
At this time, the workpiece to be polished can be a silicon single crystal wafer having a diameter of 300 mm or more.
As described above, even if the workpiece to be polished is a silicon single crystal wafer having a large diameter such as 300 mm or more, by holding and polishing with the polishing head of the present invention, more uniform pressing can be performed over the entire surface of the workpiece. Polishing can be performed with pressure, and good flatness can be ensured.

次に、本発明に係る研磨ヘッドの製造方法について説明する。
本発明に係る製造方法で製造する研磨ヘッドは、例えば図1に示すように、少なくとも、環状の剛性リング4と、該剛性リング4に均一の張力で接着されたラバー膜3と、剛性リング4に結合され、ラバー膜3と剛性リング4とともに空間部6を形成する中板5と、空間部6の圧力を変化させる圧力調整機構7とを具備する構成となっている。
Next, a method for manufacturing a polishing head according to the present invention will be described.
As shown in FIG. 1, for example, the polishing head manufactured by the manufacturing method according to the present invention includes at least an annular rigid ring 4, a rubber film 3 bonded to the rigid ring 4 with a uniform tension, and a rigid ring 4. The middle plate 5 that forms the space 6 together with the rubber film 3 and the rigid ring 4, and the pressure adjustment mechanism 7 that changes the pressure in the space 6 are provided.

本発明に係る研磨ヘッドの製造方法は、以下に示すような、少なくとも、ラバー膜3を選別する工程を含んでいる。
まず、ラバー膜3に対して、JIS K6251に準拠した引張試験を行い、図2(A)に示すような応力―歪曲線を得る。そして、この応力―歪曲線から、図2(B)に示すような、歪が5%以内の応力―歪曲線を抽出し、抽出した曲線を最小二乗法による線形近似して直線を得る。この直線は、応力=a×歪+bで表わされる。
The method for producing a polishing head according to the present invention includes at least a step of selecting the rubber film 3 as described below.
First, the rubber film 3 is subjected to a tensile test based on JIS K6251 to obtain a stress-strain curve as shown in FIG. Then, from this stress-strain curve, a stress-strain curve having a strain of 5% or less as shown in FIG. 2B is extracted, and the extracted curve is linearly approximated by the least square method to obtain a straight line. This straight line is expressed as stress = a × strain + b.

そして、この直線の傾きaの値が10MPa以下となるようなラバー膜3を選別する。
このようにして選別したラバー膜3を用いて、剛性リング4に均一の張力で接着する。
ここで、ラバー膜3の選別は、ラバー膜3だけを形成する前のゴム材料の段階で行うこともでき、とにかく、ラバー膜3を剛性リング4に接着する前に行えば良い。
Then, the rubber film 3 is selected so that the value of the straight line inclination a is 10 MPa or less.
The rubber film 3 thus selected is used to adhere to the rigid ring 4 with a uniform tension.
Here, the selection of the rubber film 3 can be performed at the stage of the rubber material before forming the rubber film 3 alone, and anyway, it may be performed before the rubber film 3 is bonded to the rigid ring 4.

このように、少なくとも、ラバー膜3を剛性リング4に接着する前に、該ラバー膜3のJIS K6251に準拠した引張試験を行い、歪が5%以内の応力―歪曲線を線形近似して得られる傾きの値が10MPa以下となるものを選別する工程を含み、該選別された前記傾きの値が10MPa以下となるラバー膜3を用いて剛性リング4に接着して研磨ヘッド2を製造すれば、ワークWを研磨する際に、ラバー膜3の材質の種類や、ラバー膜3の材料のロット間で発生する研磨代均一性のばらつきを抑制することができ、安定して良好な平坦性を確保できる研磨ヘッド2を製造することができる。   Thus, at least before the rubber film 3 is bonded to the rigid ring 4, a tensile test based on JIS K6251 of the rubber film 3 is performed, and a stress-strain curve with a strain within 5% is obtained by linear approximation. Including a step of selecting a slope having a slope value of 10 MPa or less, and manufacturing the polishing head 2 by adhering to the rigid ring 4 using the rubber film 3 having the selected slope value of 10 MPa or less. When polishing the workpiece W, it is possible to suppress variations in the type of the rubber film 3 and the variation in polishing margin uniformity that occurs between lots of the material of the rubber film 3, and stable and good flatness. A polishing head 2 that can be secured can be manufactured.

次に、剛性リング4と中板5とを結合し、該剛性リング4と、中板5と、剛性リング4に接着されたラバー膜3とで空間部6を形成する。そして、圧力調整機構7を中板5の上方に配設する。これらの工程は、従来と同様の方法で行うことができる。   Next, the rigid ring 4 and the intermediate plate 5 are joined together, and the space 6 is formed by the rigid ring 4, the intermediate plate 5, and the rubber film 3 bonded to the rigid ring 4. Then, the pressure adjustment mechanism 7 is disposed above the intermediate plate 5. These steps can be performed by a method similar to the conventional method.

このとき、ラバー膜3の下面部の周辺部には、研磨中にワークWが外れないようにワークWのエッジ部を保持するための環状のテンプレート14を配設することができる。この場合、テンプレート14は、剛性リング4と同心となるようにし、ラバー膜3の下面部の外周部に沿って、下方に突出するように配設することができる。   At this time, an annular template 14 for holding the edge portion of the workpiece W can be disposed around the lower surface portion of the rubber film 3 so that the workpiece W is not detached during polishing. In this case, the template 14 can be arranged so as to be concentric with the rigid ring 4 and protrude downward along the outer peripheral portion of the lower surface portion of the rubber film 3.

ここで、テンプレート14の下端面の高さは、保持された時のワークWの下端面の高さと同じか、あるいはワークWの下端面の高さよりも、例えば10μm程度僅かに下方に突出しているようにすることができる。
このように、テンプレート14を配設すれば、ワーク外周部にかかる過剰な圧力分布を緩和することができ、ワークの研磨代均一性を向上することができる研磨ヘッドとすることができる。
Here, the height of the lower end surface of the template 14 is the same as the height of the lower end surface of the workpiece W when it is held, or slightly protrudes downward by, for example, about 10 μm from the height of the lower end surface of the workpiece W. Can be.
Thus, if the template 14 is disposed, an excessive pressure distribution applied to the outer periphery of the workpiece can be relaxed, and a polishing head capable of improving the workpiece polishing uniformity can be obtained.

またここで、テンプレート14は、その外径が少なくとも剛性リング4の内径よりも大きいもので、かつ、その内径が剛性リング4の内径よりも小さいものとすることができる。
このようにすれば、ワーク全面にかかる押圧力をより均一にして研磨することができる研磨ヘッドとすることができる。
Here, the template 14 may have an outer diameter that is at least larger than an inner diameter of the rigid ring 4 and an inner diameter that is smaller than the inner diameter of the rigid ring 4.
In this way, it is possible to obtain a polishing head capable of polishing with a more uniform pressing force applied to the entire surface of the workpiece.

またここで、テンプレート14の材質は、ワークWを汚染せず、かつ、キズや圧痕をつけないために、ワークWよりも柔らかく、研磨中に研磨布9と摺接されても磨耗しにくい、耐磨耗性の高い材質のものを用いるのが好ましい。   Here, the material of the template 14 does not contaminate the workpiece W and does not cause scratches or indentations, so it is softer than the workpiece W and is not easily worn even if it is in sliding contact with the polishing pad 9 during polishing. It is preferable to use a material with high wear resistance.

このとき、ラバー膜3の下面に、例えば発泡ポリウレタン製のバッキングパッド13を貼設することができる。このようなバッキングパッド13を設けて水を含ませる事で、バッキングパッド13に含まれる水の表面張力によりワークWを確実に保持することができる研磨ヘッドとすることができる。   At this time, a backing pad 13 made of, for example, polyurethane foam can be attached to the lower surface of the rubber film 3. By providing such a backing pad 13 and including water, a polishing head that can reliably hold the workpiece W by the surface tension of the water contained in the backing pad 13 can be obtained.

またこのとき、保持するワークは、直径が300mm以上のシリコン単結晶ウェーハであることができる。
このように、保持するワークが、直径が300mm以上のような大直径のシリコン単結晶ウェーハであっても、本発明によりワークの全面にわたってより均一の押圧力で研磨することができ、良好な平坦性を確保することができる。
At this time, the work to be held can be a silicon single crystal wafer having a diameter of 300 mm or more.
Thus, even if the workpiece to be held is a silicon single crystal wafer having a large diameter such as a diameter of 300 mm or more, the present invention can be polished with a more uniform pressing force over the entire surface of the workpiece. Sex can be secured.

以下、本発明の実施例を示して本発明をより具体的に説明するが、本発明はこれらに限定されるものではない。   EXAMPLES Hereinafter, the present invention will be described more specifically with reference to examples of the present invention, but the present invention is not limited thereto.

(実施例1)
図1に示すような研磨ヘッドを本発明に係る製造方法で製造し、その研磨ヘッドを具備した研磨装置でシリコン単結晶ウェーハを研磨し、研磨したワークの研磨代均一性を評価した。
Example 1
A polishing head as shown in FIG. 1 was manufactured by the manufacturing method according to the present invention, a silicon single crystal wafer was polished by a polishing apparatus equipped with the polishing head, and polishing stock removal uniformity of the polished workpiece was evaluated.

まず、ラバー膜の選別を行うために、ラバー膜用のゴム材料として、JIS K6253に準拠したゴム硬度で硬度規格80°のエチレンプロピレンジエンゴム(EPDM)の2種類のロットA及びBと(以降、EPDM80°A及びEPDM80°Bと略す)、シリコーンゴムで硬度規格70、80、90°の3種類(以降、シリコーン70°、シリコーン80°、シリコーン90°と略す)を準備した。そして、これら5種類のゴム材料について、JIS K6251引張り試験を行い、応力−歪曲線の測定を実施した。   First, in order to select a rubber film, as rubber materials for rubber film, two types of lots A and B of ethylene propylene diene rubber (EPDM) having a rubber hardness conforming to JIS K6253 and a hardness standard of 80 ° (hereinafter referred to as “rubber film material”) , EPDM 80 ° A and EPDM 80 ° B), and silicone rubber, hardness standards 70, 80 and 90 ° (hereinafter, silicone 70 °, silicone 80 ° and silicone 90 °) were prepared. And about these 5 types of rubber materials, the JIS K6251 tensile test was done and the measurement of the stress-strain curve was implemented.

表1にその結果を示す。また、得られた応力−歪曲線の結果を図3(A)に示す。そして、図3(B)に示すような、図3(A)の5%歪までの応力―歪曲線を用いて、応力=a×歪+bにて線形近似を行い、傾きaの値を求めた。
その結果を図4に示す。図4に示すように、同一の種類のゴム材料を用いてもロットの違いにより、傾きaの値が異なっていることが分かる。そして、EPDM80°B、シリコーン70°、シリコーン80°のゴム材料は、傾きaの値が10MPa以下であることが分かる。
Table 1 shows the results. Moreover, the result of the obtained stress-strain curve is shown in FIG. Then, using the stress-strain curve up to 5% strain shown in FIG. 3A as shown in FIG. 3B, linear approximation is performed with stress = a × strain + b to obtain the value of the slope a. It was.
The result is shown in FIG. As shown in FIG. 4, it can be seen that even if the same type of rubber material is used, the value of the slope a varies depending on the lot. It can be seen that the rubber material of EPDM 80 ° B, silicone 70 °, and silicone 80 ° has a slope a value of 10 MPa or less.

このようにして、ラバー膜のゴム材料を選別し、傾きaの値が10MPa以下である、EPDM80°B、シリコーン70°、シリコーン80°を用いて3つの研磨ヘッドを以下のようにして製造した。   In this way, the rubber material of the rubber film was selected, and three polishing heads were manufactured as follows using EPDM 80 ° B, silicone 70 °, and silicone 80 ° with a slope a value of 10 MPa or less. .

まず、上部を中板に閉塞されたSUS製の外径が360mmの環状の剛性リングの外周に、傾きaの値が10MPa以下の3種類のゴム材料(EPDM80°B、シリコーン70°、シリコーン80°)にて厚さ1mmのラバー膜を均一の張力で貼り付けた。   First, three kinds of rubber materials (EPDM 80 ° B, silicone 70 °, silicone 80) having an inclination a of 10 MPa or less are formed on the outer periphery of an annular rigid ring made of SUS having an outer diameter of 360 mm and closed at the top by an intermediate plate. At 1 °, a rubber film having a thickness of 1 mm was attached with a uniform tension.

また、それぞれの研磨ヘッドのラバー膜のワーク保持面に、バッキングパッドを貼設し、該バッキングパッドの表面に外径355mm、内径302mmのガラスエポキシ積層板のテンプレートを貼り付けた市販のテンプレートアセンブリを両面テープにて貼りつけた。また、シリコーンゴムで成型したラバー膜の表面は、両面テープとの接着性を向上する目的で数μm程度の薄いポリウレタン膜のコーティング処理を施した。また、テンプレートは、テンプレートの下面位置が、ワークの下面位置よりも僅かに突出するように、厚み787μmの市販のテンプレートアセンブリを用いた。   In addition, a commercially available template assembly in which a backing pad is attached to the work holding surface of the rubber film of each polishing head, and a glass epoxy laminate template having an outer diameter of 355 mm and an inner diameter of 302 mm is attached to the surface of the backing pad. Affixed with double-sided tape. Further, the surface of the rubber film molded with silicone rubber was subjected to a coating process of a thin polyurethane film of about several μm for the purpose of improving the adhesion to the double-sided tape. Further, as the template, a commercially available template assembly having a thickness of 787 μm was used so that the lower surface position of the template slightly protruded from the lower surface position of the workpiece.

このような本発明に係る研磨ヘッドの製造方法で製造した研磨ヘッドを備えた、図1に示すような研磨装置を用いて、ワークWとして直径300mm、厚さ775μmのシリコン単結晶ウェーハの研磨を行った。なお、使用したシリコン単結晶ウェーハは、その両面には予め一次研磨を施し、エッジ部にも研磨を施したものである。また、定盤には直径800mmのものを使用し、研磨布には不織布にウレタンを含浸させたタイプを用い、ヤング率が3.5MPa以下である2.2MPaのものを用いた。   Using a polishing apparatus as shown in FIG. 1 equipped with a polishing head manufactured by such a manufacturing method of a polishing head according to the present invention, a silicon single crystal wafer having a diameter of 300 mm and a thickness of 775 μm is polished as a workpiece W. went. Note that the silicon single crystal wafer used was subjected to primary polishing on both surfaces in advance, and the edge portion was also polished. Further, a surface plate having a diameter of 800 mm was used, and a polishing cloth using a non-woven fabric impregnated with urethane and a Young's modulus of 2.2 MPa having a pressure of 3.5 MPa or less were used.

そして、研磨の際には、研磨剤としてコロイダルシリカを含有するアルカリ溶液を使用し、研磨ヘッドと定盤はそれぞれ31、29rpmで回転させた。ワークWの研磨荷重(押圧力)は15KPaとした。研磨時間を3分とした。   In polishing, an alkaline solution containing colloidal silica was used as an abrasive, and the polishing head and the surface plate were rotated at 31 and 29 rpm, respectively. The polishing load (pressing force) of the workpiece W was 15 KPa. The polishing time was 3 minutes.

このようにして研磨を行ったワークについて研磨代均一性及び研磨時の研磨圧力分布について評価した。なお研磨代均一性は、平坦度測定器で研磨前後のワークの厚さをウェーハの直径方向について、平坦度保証エリアとして最外周部2mm幅を除外した領域について測定し、厚みの差分をとることで求められ、研磨代均一性(%)=(直径方向の最大研磨代−直径方向の最小研磨代)/直径方向の平均研磨代の式で表される。   The workpieces polished in this way were evaluated for polishing margin uniformity and polishing pressure distribution during polishing. The polishing margin uniformity is obtained by measuring the thickness of the workpiece before and after polishing in the diameter direction of the wafer with a flatness measuring device in the area excluding the outermost 2 mm width as the flatness guarantee area. The polishing allowance uniformity (%) = (maximum polishing allowance in the diameter direction−minimum polishing allowance in the diameter direction) / average polishing allowance in the diameter direction.

図5に、ラバー膜のゴム材料としてEPDM80°Bを用いた研磨ヘッドで研磨されたウェーハの半径方向で中心から120〜148mmの範囲の研磨圧力分布を示す。圧力分布は、各位置での研磨代を、各位置での研磨代/平均研磨代×研磨荷重(15MPa)で換算して求めた。
図5に示すように、傾きaの値が10MPaより大きい、後述する比較例のゴム材料のラバー膜を用いた研磨ヘッドに比べ、ワークWの外周部分の圧力低下が抑制され、研磨圧力分布の均一性が良好であることが分かる。
FIG. 5 shows a polishing pressure distribution in the range of 120 to 148 mm from the center in the radial direction of a wafer polished by a polishing head using EPDM 80 ° B as the rubber material of the rubber film. The pressure distribution was determined by converting the polishing allowance at each position by polishing allowance at each position / average polishing allowance × polishing load (15 MPa).
As shown in FIG. 5, the pressure drop in the outer peripheral portion of the workpiece W is suppressed compared to a polishing head using a rubber film of a rubber material of a comparative example, which will be described later, having a slope a value larger than 10 MPa, and the polishing pressure distribution It can be seen that the uniformity is good.

また、図6に、研磨代均一性の結果を示す。
図6に示すように、EPDM80°B、シリコーン70°、シリコーン80°を材料としたラバー膜を用いた研磨ヘッドを具備した研磨装置で研磨することで、後述の比較例の結果に比べて研磨代均一性が改善され、10%以下と良好な結果となることが分かった。
このことにより、本発明に係る製造方法で製造した研磨ヘッドを具備した、本発明の研磨装置を用いれば、ワークを研磨する際に、ラバー膜の材質の種類や、ラバー膜の材料のロット間で発生する研磨代均一性のばらつきを抑制することができ、安定して良好な平坦性を確保できることが確認できた。
Further, FIG. 6 shows the result of the polishing allowance uniformity.
As shown in FIG. 6, by polishing with a polishing apparatus equipped with a polishing head using a rubber film made of EPDM 80 ° B, silicone 70 °, and silicone 80 °, polishing is performed in comparison with the results of comparative examples described later. It was found that the non-uniformity was improved and a good result of 10% or less was obtained.
Accordingly, when the polishing apparatus of the present invention including the polishing head manufactured by the manufacturing method according to the present invention is used, the type of the rubber film and the lot of the rubber film material between the lots of the material of the rubber film are polished. It was confirmed that the variation in the polishing allowance uniformity generated in step 1 can be suppressed, and good flatness can be secured stably.

(実施例2)
研磨布として、ヤング率が3.2MPaのものを用いた以外、実施例1と同様な方法で、EPDM80°Bをラバー膜の材料として使用したものを用いた研磨ヘッドのみを製造し、その研磨ヘッドを具備した研磨装置でシリコン単結晶ウェーハを研磨し、研磨代均一性を評価した。
その結果を図7に示す。図7に示すように、後述の比較例の結果に比べて研磨代均一性が改善され、10%以下と良好な結果となることが分かった。
そして、図7に示すように、研磨布のヤング率が3.5MPa以下の場合において、研磨代均一性が10%以下と良好な結果となっていることが分かった。
(Example 2)
As the polishing cloth, except that the one having a Young's modulus of 3.2 MPa was used, only a polishing head using EPDM 80 ° B as a rubber film material was manufactured in the same manner as in Example 1, and the polishing was performed. A silicon single crystal wafer was polished by a polishing apparatus equipped with a head, and polishing stock removal uniformity was evaluated.
The result is shown in FIG. As shown in FIG. 7, it was found that the polishing allowance uniformity was improved as compared with the results of the comparative example described later, and a favorable result of 10% or less was obtained.
As shown in FIG. 7, it was found that when the Young's modulus of the polishing pad was 3.5 MPa or less, the polishing margin uniformity was 10% or less, which was a good result.

(比較例)
実施例1において、5%歪までの応力―歪曲線を応力=a×歪+bにて線形近似を行い求めた傾きaの値が10MPaより大きいゴム材料、すなわち、EPDM80°A及びシリコーン90°をラバー膜の材料として使用して研磨ヘッドを製造した以外、実施例1と同様な条件でシリコン単結晶ウェーハを研磨し、研磨後のウェーハの研磨代均一性及び研磨時の研磨圧力分布を評価した。
(Comparative example)
In Example 1, a rubber material having a slope a value greater than 10 MPa obtained by linear approximation of a stress-strain curve up to 5% strain with stress = a × strain + b, that is, EPDM 80 ° A and silicone 90 °. A silicon single crystal wafer was polished under the same conditions as in Example 1 except that the polishing head was manufactured by using it as a rubber film material, and the polishing margin uniformity of the wafer after polishing and the polishing pressure distribution during polishing were evaluated. .

図5に研磨圧力分布の結果を示す。図5に示すように、傾きaの値が10MPa以下となるラバー膜を選別した実施例1の結果と比較すると、ワークの外周部分の圧力低下がより顕著になり、研磨圧力分布の均一性が低下していることが分かる。
図6に研磨代均一性の結果を示す。図6に示すように、実施例1の結果と比較して研磨代均一性が悪化していることが分かる。
FIG. 5 shows the result of the polishing pressure distribution. As shown in FIG. 5, when compared with the results of Example 1 in which a rubber film having a slope a value of 10 MPa or less was selected, the pressure drop in the outer peripheral portion of the workpiece became more remarkable, and the uniformity of the polishing pressure distribution was It turns out that it has fallen.
FIG. 6 shows the result of the polishing allowance uniformity. As shown in FIG. 6, it can be seen that the polishing margin uniformity is worse than the result of Example 1.

このことにより、従来の研磨装置を用いてワークを研磨する際、ラバー膜の材質や、同じ材質でも製造ロットが異なった場合に、研磨代均一性にバラツキが発生し、安定したワークの平坦度が得られないことが確認できた。
次に、研磨布として、ヤング率が4.5MPaのものを使用した以外、実施例2と同様な条件でシリコン単結晶ウェーハを研磨し、研磨後のウェーハの研磨代均一性を評価した。
その結果を図7に示す。図7に示すように、研磨代均一性は実施例2の結果と比較して悪化しているのが分かる。すなわち、ラバー膜として、歪が5%以内の応力―歪曲線を線形近似して得られる傾きの値が10MPa以下となるものを選別した本発明の研磨ヘッドで、研磨代均一性を改善できるが、これを研磨装置に配置して研磨する場合、定盤に貼付される研磨布はヤング率が3.5MPa以下である必要がある。
As a result, when polishing a workpiece using a conventional polishing device, even if the material of the rubber film and the same material are different from each other in the production lot, there will be variations in the polishing stock uniformity and stable workpiece flatness. It was confirmed that cannot be obtained.
Next, a silicon single crystal wafer was polished under the same conditions as in Example 2 except that a polishing cloth having a Young's modulus of 4.5 MPa was used, and the polishing margin uniformity of the polished wafer was evaluated.
The result is shown in FIG. As shown in FIG. 7, it can be seen that the polishing allowance uniformity is worse than the result of Example 2. That is, with the polishing head of the present invention selected as a rubber film that has a slope value of 10 MPa or less obtained by linear approximation of a stress-strain curve with a strain within 5%, the polishing margin uniformity can be improved. When this is placed in a polishing apparatus for polishing, the polishing cloth adhered to the surface plate needs to have a Young's modulus of 3.5 MPa or less.

Figure 0005145131
Figure 0005145131

なお、本発明は、上記実施形態に限定されるものではない。上記実施形態は例示であり、本発明の特許請求の範囲に記載された技術的思想と実質的に同一な構成を有し、同様な作用効果を奏するものは、いかなるものであっても本発明の技術的範囲に包含される。
例えば、本発明に係る製造方法で製造する研磨ヘッドは、図1に示した態様に限定されず、例えば中板の形状等は適宜設計すればよい。
また、研磨装置の構成も図1に示したものに限定されず、例えば、本発明に係る製造方法で製造した研磨ヘッドを複数備えた研磨装置とすることもできる。
The present invention is not limited to the above embodiment. The above-described embodiment is an exemplification, and the present invention has any configuration that has substantially the same configuration as the technical idea described in the claims of the present invention and that exhibits the same effects. Are included in the technical scope.
For example, the polishing head manufactured by the manufacturing method according to the present invention is not limited to the embodiment shown in FIG. 1. For example, the shape of the intermediate plate may be appropriately designed.
Further, the configuration of the polishing apparatus is not limited to that shown in FIG. 1. For example, a polishing apparatus including a plurality of polishing heads manufactured by the manufacturing method according to the present invention may be used.

本発明に係る研磨装置の一例を示した概略図である。It is the schematic which showed an example of the grinding | polishing apparatus which concerns on this invention. 本発明に係る研磨ヘッドの製造方法において得られる応力―歪曲線の一例を示したグラフである。(A)全ての応力―歪曲線。(B)歪が5%以内の応力―歪曲線。5 is a graph showing an example of a stress-strain curve obtained in the method for manufacturing a polishing head according to the present invention. (A) All stress-strain curves. (B) Stress-strain curve with a strain within 5%. 実施例1のラバー膜の選別工程における、応力―歪曲線を示すグラフである。(A)全ての応力―歪曲線。(B)歪5%以内の応力―歪曲線。3 is a graph showing a stress-strain curve in the rubber film selection process of Example 1. FIG. (A) All stress-strain curves. (B) Stress-strain curve within 5% strain. 実施例1のラバー膜の選別工程における、歪が5%以内の応力―歪曲線を線形近似し得られた傾きの値の結果を示す図である。It is a figure which shows the result of the value of the inclination obtained by carrying out the linear approximation of the stress-strain curve in which the distortion | strain is less than 5% in the selection process of the rubber film of Example 1. 実施例1、比較例における、研磨圧力分布の結果を示す図である。It is a figure which shows the result of polishing pressure distribution in Example 1 and a comparative example. 実施例1、比較例における、研磨代均一性の結果を示す図である。It is a figure which shows the result of the grinding | polishing allowance uniformity in Example 1 and a comparative example. 実施例2、比較例における、研磨代均一性の結果を示す図である。It is a figure which shows the result of grinding | polishing allowance uniformity in Example 2 and a comparative example. 従来の研磨ヘッドの一例を示す概略図である。It is the schematic which shows an example of the conventional grinding | polishing head. 従来の片面研磨装置の一例を示す概略図である。It is the schematic which shows an example of the conventional single-side polish apparatus.

符号の説明Explanation of symbols

1…研磨装置、2…研磨ヘッド、3…ラバー膜、
4…剛性リング、5…中板、6…空間部、
7…圧力調整機構、8…定盤、9…研磨布、10…研磨剤供給機構、
11…駆動軸、12…貫通孔、13…バッキングパッド、
14…テンプレート。
DESCRIPTION OF SYMBOLS 1 ... Polishing apparatus, 2 ... Polishing head, 3 ... Rubber film,
4 ... Rigid ring, 5 ... Middle plate, 6 ... Space part,
7 ... Pressure adjusting mechanism, 8 ... Surface plate, 9 ... Polishing cloth, 10 ... Abrasive supply mechanism,
DESCRIPTION OF SYMBOLS 11 ... Drive shaft, 12 ... Through-hole, 13 ... Backing pad,
14 ... Template.

Claims (2)

少なくとも、環状の剛性リングと、該剛性リングに均一の張力で接着されたラバー膜と、前記剛性リングに結合され、前記ラバー膜と前記剛性リングとともに空間部を形成する中板と、前記空間部の圧力を変化させる圧力調整機構とを具備し、前記ラバー膜の下面部にワークの裏面を保持し、該ワークの表面を定盤上に貼り付けた研磨布に摺接させて研磨する研磨ヘッドの製造方法であって、少なくとも、
前記ラバー膜を剛性リングに接着する前に、該ラバー膜のJIS K6251に準拠した引張試験を行い、歪が5%以内の応力―歪曲線を線形近似して得られる傾きの値が10MPa以下となるものを選別する工程を含み、該選別された前記傾きの値が10MPa以下となるラバー膜を用いて前記剛性リングに接着して研磨ヘッドを製造することを特徴とする研磨ヘッドの製造方法。
At least an annular rigid ring, a rubber film bonded to the rigid ring with a uniform tension, an intermediate plate coupled to the rigid ring and forming a space with the rubber film and the rigid ring, and the space And a pressure adjusting mechanism for changing the pressure of the rubber film. The polishing head holds the back surface of the work on the lower surface of the rubber film and polishes the work surface by sliding the surface of the work on a polishing cloth affixed on a surface plate. A manufacturing method of at least
Before adhering the rubber film to the rigid ring, a tensile test based on JIS K6251 of the rubber film is performed, and a slope value obtained by linearly approximating a stress-strain curve with a strain within 5% is 10 MPa or less. A method of manufacturing a polishing head, comprising: a step of selecting a target, and a polishing head is manufactured by adhering to the rigid ring using a rubber film having the selected inclination value of 10 MPa or less.
前記保持するワークは、直径が300mm以上のシリコン単結晶ウェーハであることを特徴とする請求項1に記載の研磨ヘッドの製造方法。   The method of manufacturing a polishing head according to claim 1, wherein the workpiece to be held is a silicon single crystal wafer having a diameter of 300 mm or more.
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JP5392483B2 (en) * 2009-08-31 2014-01-22 不二越機械工業株式会社 Polishing equipment
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JP5677004B2 (en) * 2010-09-30 2015-02-25 株式会社荏原製作所 Polishing apparatus and method
KR20140048894A (en) * 2011-06-29 2014-04-24 신에쯔 한도타이 가부시키가이샤 Polishing head and polishing apparatus
JP5878733B2 (en) * 2011-11-02 2016-03-08 株式会社東京精密 Template pressing wafer polishing system
JP6360586B1 (en) * 2017-04-13 2018-07-18 三菱電線工業株式会社 Elastic film for wafer holding of CMP apparatus
JP7125839B2 (en) * 2017-12-28 2022-08-25 株式会社東京精密 CMP equipment

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JP2001113457A (en) * 1999-10-18 2001-04-24 Hitachi Ltd Chemical mechanical polishing method and manufacturing method of semiconductor integrated circuit device
JP2002264005A (en) * 2001-03-09 2002-09-18 Toshiba Ceramics Co Ltd Polishing method for semiconductor wafer and polishing device therefor
JP2004296591A (en) * 2003-03-26 2004-10-21 Fujitsu Ltd Method for producing semiconductor device
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