JP4618547B2 - Film for sealing, and method for manufacturing honeycomb filter using the same - Google Patents

Film for sealing, and method for manufacturing honeycomb filter using the same Download PDF

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JP4618547B2
JP4618547B2 JP2005046559A JP2005046559A JP4618547B2 JP 4618547 B2 JP4618547 B2 JP 4618547B2 JP 2005046559 A JP2005046559 A JP 2005046559A JP 2005046559 A JP2005046559 A JP 2005046559A JP 4618547 B2 JP4618547 B2 JP 4618547B2
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flow path
honeycomb structure
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outer peripheral
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JP2005270967A (en
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慎弥 徳丸
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Hitachi Metals Ltd
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本発明は、ハニカム構造体の流路端部を封止するための封止用フィルム、およびこれを用いたハニカムフィルタの製造方法に関する。   The present invention relates to a sealing film for sealing a channel end of a honeycomb structure and a method for manufacturing a honeycomb filter using the same.

図6は、自動車の排気ガス中のパティキュレートを捕集するハニカムフィルタの一例の模式図を示し、(a)は正面図、(b)は収納容器を含む断面図である。図6(a)(b)で、ハニカムフィルタ60は、多孔質セラミックからなり、外周壁61aと、この外周壁61aの内側に各々直交するセル壁61bで形成された複数の流路61cを有するハニカム構造体61と、このハニカム構造体61の流入側の流路端部61dと、流出側の流路端部61eとを交互に封止材62d、62eで封止している。また、ハニカム構造体61の外周壁61aを、金属メッシュあるいはセラミックス製のマットなどで形成した把持部材63a〜63cで使用中に動かないように把持し、金属製の収納容器64に配置している。   FIG. 6 is a schematic view of an example of a honeycomb filter that collects particulates in the exhaust gas of an automobile, where (a) is a front view and (b) is a cross-sectional view including a storage container. 6 (a) and 6 (b), the honeycomb filter 60 is made of porous ceramic, and has a plurality of flow paths 61c formed by an outer peripheral wall 61a and cell walls 61b orthogonal to each other inside the outer peripheral wall 61a. The honeycomb structure 61, the inflow side channel end 61d of the honeycomb structure 61, and the outflow side channel end 61e are alternately sealed with the sealing materials 62d and 62e. Further, the outer peripheral wall 61a of the honeycomb structure 61 is gripped so as not to move during use by gripping members 63a to 63c formed of a metal mesh or a ceramic mat, and is disposed in the metal storage container 64. .

図6のハニカムフィルタ60で、排気ガスの浄化は以下の通り行われる。排気ガス65aは、流入側の流路端部61dに開口している流路61cから流入する。そして、排気ガス65aに含まれるパティキュレートは、セル壁61bを通過(65b)する際に捕捉され、浄化された排気ガス65cは、流出側の流路端部61eの開口している流路61cから流出、大気中に放出される。一方、セル壁61bに捕捉されたパティキュレートが一定量以上になると、ハニカムフィルタ60に目詰まりが発生するので、バーナーや電気ヒーターによりこれを燃焼させ、ハニカムフィルタ60の再生が行われる。   In the honeycomb filter 60 of FIG. 6, purification of exhaust gas is performed as follows. The exhaust gas 65a flows in from the flow path 61c opened to the flow path end 61d on the inflow side. Particulates contained in the exhaust gas 65a are captured when passing through the cell wall 61b (65b), and the purified exhaust gas 65c flows into the flow path 61c opened in the flow path end 61e on the outflow side. Spilled from the atmosphere and released into the atmosphere. On the other hand, when the particulate matter trapped in the cell wall 61b exceeds a certain amount, the honeycomb filter 60 is clogged. Therefore, the honeycomb filter 60 is burned by a burner or an electric heater, and the honeycomb filter 60 is regenerated.

ハニカムフィルタ60で捕捉したパティキュレートを燃焼して再生する際に、燃焼熱が金属製の収納容器64から放散すると、ハニカムフィルタ60の再生が困難となることがある。これを防止するため、図5(a)(b)に示すように、流入側の流路端部51dと流出側の流路端部51eとに、封止材52d、52eによる交互封止に加え、外周壁51a近傍の同じ流路51cを封止材55d、55eで封止し、封止した流路51cを保温空間55とするハニカムフィルタ50が提案されている(例えば、特許文献1(特開平5−118211号公報)参照)。なお、51はハニカム構造体、51bはセル壁、D51は流路端部51f(51g)の外径を示す。   When the particulate matter captured by the honeycomb filter 60 is burned and regenerated, if the combustion heat is dissipated from the metal storage container 64, the regeneration of the honeycomb filter 60 may be difficult. In order to prevent this, as shown in FIGS. 5A and 5B, the inflow side flow path end 51d and the outflow side flow path end 51e are alternately sealed with the sealing materials 52d and 52e. In addition, a honeycomb filter 50 is proposed in which the same flow path 51c in the vicinity of the outer peripheral wall 51a is sealed with sealing materials 55d and 55e, and the sealed flow path 51c is used as a heat retaining space 55 (for example, Patent Document 1 ( JP, 5-118211, A). In addition, 51 is a honeycomb structure, 51b is a cell wall, D51 shows the outer diameter of the flow-path edge part 51f (51g).

本出願人も特許文献2(特開2003−126629号公報)として、図5(a)(b)に示すように、外周壁51a近傍の流路51cの両端部51d、51eを各々封止材55d、55eで封止し、ハニカムフィルタ50の端面からの、この封止材55d、55eの長さ(L55)をハニカムフィルタ50の全長(L51)の8.2%以下、かつ、外周壁51a近傍の両端を封止している流路51cを、外周壁51aから中心に向かって、最大5×(隔壁ピッチ)の長さ(B55)とするハニカムフィルタ50を提案している。本出願人の特許文献2によれば、ハニカムフィルタ50の端面からの封止材55d、55eの長さ(L55)を、ハニカムフィルタ50の全長(L51)の8.2%以下、好ましくは、3.3%以下とすることで、パティキュレートの燃焼熱が金属製の収納容器に放散するのを抑え、また捕集したパティキュレートの燃え残りを少なくすることができる。さらに、両端が封止されている流路を、ハニカムフィルタ端面の外周壁から中心に向かって、最大5×(隔壁ピッチ)の長さ(B55)、好ましくは、最大3×(隔壁ピッチ)の長さ(B55)とすることで、相対的にフィルタ機能を有するセル壁の割合を多くして、ハニカムフィルタの圧力損失を最小限に抑えることができるとしている。   As shown in FIGS. 5 (a) and 5 (b), the applicant of the present invention also discloses, as Patent Document 2 (Japanese Patent Laid-Open No. 2003-126629), both end portions 51d and 51e of the flow path 51c in the vicinity of the outer peripheral wall 51a. 55d and 55e are sealed, and the length (L55) of the sealing material 55d and 55e from the end face of the honeycomb filter 50 is 8.2% or less of the total length (L51) of the honeycomb filter 50, and the outer peripheral wall 51a. A honeycomb filter 50 is proposed in which the flow path 51c sealing both ends in the vicinity has a length (B55) of 5 × (partition wall pitch) at the maximum from the outer peripheral wall 51a toward the center. According to Patent Document 2 of the present applicant, the length (L55) of the sealing materials 55d and 55e from the end face of the honeycomb filter 50 is 8.2% or less of the total length (L51) of the honeycomb filter 50, preferably By setting it as 3.3% or less, it can suppress that the combustion heat of a particulate is dissipated to a metal storage container, and can reduce the unburned residue of the collected particulate. Furthermore, the flow path sealed at both ends is directed from the outer peripheral wall of the honeycomb filter end face toward the center at a length (B55) of a maximum of 5 × (partition wall pitch), preferably a maximum of 3 × (partition wall pitch). By setting the length (B55), the ratio of cell walls having a filter function can be relatively increased, and the pressure loss of the honeycomb filter can be minimized.

ここで、図5に示すハニカムフィルタ50の外周壁51a近傍の流路51cの両端部51d、51eを各々封止材55d、55eで封止する方法は、特許文献3に記載されている方法をもとに次のように行うことができる。例えば、コージェライトを形成するセラミック材料で、ハニカム構造体51を作製し、図3に示すハニカム構造体51と封止用フィルム30の斜視図のように、ハニカム構造体51の流路端部51d(51e)を封止用フィルム30で覆って粘着する。そして、封止用フィルム30に、流路端部51d(51e)の封止すべき流路を市松模様並びに外周壁51a近傍の流路に、レーザなど熱による溶融で多数の貫通孔30a、30bを形成する。
次に、図示しないが、ハニカム構造体51の流路端部51d(51e)を、封止材が含有するスラリーに浸漬させ、スラリーを封止用フィルム30の貫通孔30a、30bを通じて流路端部51d(51e)の流路51cに浸入させる。そして、スラリーを硬化させると共に封止用フィルム30を除去する。以上の工程により、ハニカムフィルタ50を得ることができる。この時、封止用フィルム30は、図3に示すように、ハニカム構造体51の流路端部の外周寸法より大きいものを用いている。また、図4に示すように、ハニカム構造体51の流路とほぼ同じ形状の市販の使い捨ての粘着シート40を用いる提案もある(例えば、特許文献4(特開2001−300922号公報)、参照)。なお、図4で、51cは流路、51d(51e)は流路端部、30a、30bは貫通孔を示す。
Here, the method described in Patent Document 3 is used as the method of sealing both end portions 51d and 51e of the flow path 51c in the vicinity of the outer peripheral wall 51a of the honeycomb filter 50 shown in FIG. 5 with the sealing materials 55d and 55e, respectively. It can be done as follows. For example, a honeycomb structure 51 is made of a ceramic material forming cordierite, and a flow path end 51d of the honeycomb structure 51 is shown in a perspective view of the honeycomb structure 51 and the sealing film 30 shown in FIG. (51e) is covered with the sealing film 30 and adhered. Then, a plurality of through holes 30a and 30b are melted by heat such as a laser into a checkered pattern and a flow path in the vicinity of the outer peripheral wall 51a in the sealing film 30 and a flow path to be sealed at the flow path end 51d (51e). Form.
Next, although not shown, the flow path end 51d (51e) of the honeycomb structure 51 is immersed in the slurry contained in the sealing material, and the slurry is passed through the through holes 30a and 30b of the sealing film 30. It penetrates into the flow path 51c of the part 51d (51e). Then, the slurry is cured and the sealing film 30 is removed. Through the above steps, the honeycomb filter 50 can be obtained. At this time, as shown in FIG. 3, the sealing film 30 is larger than the outer peripheral dimension of the flow path end portion of the honeycomb structure 51. Moreover, as shown in FIG. 4, there is also a proposal to use a commercially available disposable adhesive sheet 40 having substantially the same shape as the flow path of the honeycomb structure 51 (see, for example, Patent Document 4 (Japanese Patent Application Laid-Open No. 2001-300922)). ). In FIG. 4, 51c denotes a flow path, 51d (51e) denotes a flow path end, and 30a and 30b denote through holes.

さらに、特許文献5には、セラミックハニカムフィルタ50の外周壁51a近傍の流路51cを封止する方法として次のように記載されている。セラミックハニカム構造体61の流路61cの所定の開口部が封止されているセラミックハニカムフィルタ60の両端面にフィルムを貼り、外周壁51a近傍の流路端部で封止されていない流路端部に相当するフィルム部分に貫通孔を形成し、ついで、この貫通孔より充填材を導入する。または、外周壁51a近傍の流路51cを除く端面61d(61e)を適当なマスク材で覆い、外周壁51a近傍の流路51cで封止されていない流路端部に充填材を圧入して外周壁51a近傍の流路51cの両端部が封止されたハニカムフィルタ50を得ることができる。   Further, Patent Document 5 describes the following as a method of sealing the flow path 51c in the vicinity of the outer peripheral wall 51a of the ceramic honeycomb filter 50. A film end is attached to both end faces of the ceramic honeycomb filter 60 in which a predetermined opening of the flow path 61c of the ceramic honeycomb structure 61 is sealed, and the flow path end is not sealed at the flow path end near the outer peripheral wall 51a. A through hole is formed in the film portion corresponding to the portion, and then a filler is introduced from the through hole. Alternatively, the end face 61d (61e) except for the flow path 51c in the vicinity of the outer peripheral wall 51a is covered with an appropriate mask material, and a filler is pressed into the end of the flow path that is not sealed by the flow path 51c in the vicinity of the outer peripheral wall 51a. A honeycomb filter 50 in which both ends of the flow path 51c in the vicinity of the outer peripheral wall 51a are sealed can be obtained.

特開平5−118211号公報JP-A-5-118211 特開2003−126629号公報JP 2003-126629 A 特開2002−28915号公報JP 2002-28915 A 特開2001−300922号公報Japanese Patent Laid-Open No. 2001-300922 特公平1−47206号公報JP-B-1-47206

しかしながら、ハニカムフィルタにおいて、パティキュレートを燃焼して再生する際に生じる燃焼熱が、金属製の収納容器に放散するのを抑制する、図5に示すような保温空間55を形成しようとした場合、特許文献1、2には、ハニカム構造体外周壁近傍の同一流路の両端部を封止材で封止する具体的方法、特に封止部を形成する際に、封止材が流路に入らないようにするマスクの具体的な構造や形成方法についての記載がなかった。そこで、保温空間55を形成するために、外周壁近傍の同一流路の両端部を封止材で封止する方法として、特許文献3に記載されている封止用フィルム30をハニカム構造体の端面に貼り付け、目封止材で閉塞すべき流路に位置するフィルムにレーザ光などによる熱により貫通孔を形成して、この貫通孔を通じて目封止材スラリーを浸入させる方法や、特許文献4に記載されている粘着シート40の所定の流路に対応した位置に孔をあけてマスクを作成し、マスクにあけられた穴から目封止スラリーを充填する方法を採用した場合、以下のような問題が生じた。これら特許文献3及び4の方法では、封止用フィルム30や粘着シート40の所定の位置にレーザなどの方法で貫通孔をあける必要があることから、ハニカム構造体外周壁近傍に保温空間55を形成する目的で、外周壁近傍の同一流路の両端部を封止材で封止しようとした場合、封止材用フィルム30や、粘着シート40の外周壁近傍の流路に相当する全ての位置にレーザなどで貫通孔を形成させる必要がある。そのため、貫通孔をあけるための時間が長くなるという問題があった。すなわち、ハニカム構造体の中心部の流路では、封止材用フィルム30や、粘着シート40に対し、市松模様になるよう交互に貫通孔を形成しているのに対して、外周壁近傍では、隣接する流路全てに相当する位置に貫通孔を形成する必要があるからである。更に具体的に言えば、市松模様になるよう交互に貫通孔を形成する場合に比べ、外周壁近傍では貫通孔を形成すべき流路数が2倍となり、かつ、円の面積は直径の2乗に比例することから、外周壁に近いほど、流路数が多くなるからである。
また、特許文献5に記載されているように、外周壁近傍を除く端面を適当なマスク材で覆い、外周壁近傍の流路で封止されていない流路端部に封止材を圧入する場合には次のような問題が生じた。フィルムやマスク材でハニカムフィルタ端面を覆う際に、マスク材の位置決めが正しく行われなかった場合、外周壁近傍で封止されるべき流路数に偏りが生じ、外周壁近傍で最外周部から中心部へ形成される保温空間数に偏りが生じ、保温空間数の少ない部位から再生時の燃焼熱が金属製の収納容器に放散してしまうという問題があった。さらに、フィルムやマスク材が流路端部から剥がれた場合、封止しない流路に封止材が流れ込み、流路を交互に封止されなくなり、排気ガスが通過できない流路が生じ、圧力損失が大きくなるという問題が生じた。
However, in the honeycomb filter, when it is attempted to form a heat retaining space 55 as shown in FIG. 5 that suppresses the combustion heat generated when the particulates are burned and regenerated to dissipate into the metal storage container, In Patent Documents 1 and 2, a specific method of sealing both ends of the same flow path in the vicinity of the outer peripheral wall of the honeycomb structure with a sealing material, particularly when the sealing part is formed, the sealing material enters the flow path. There was no description about the specific structure and forming method of the mask to be eliminated. Therefore, as a method of sealing both ends of the same flow path in the vicinity of the outer peripheral wall with a sealing material in order to form the heat retaining space 55, the sealing film 30 described in Patent Document 3 is used for the honeycomb structure. A method in which through holes are formed in a film positioned in a flow path to be sealed with a plugging material by heat from a laser beam and the like, and a plugging material slurry is infiltrated through the through holes. When a method of filling a plugging slurry from a hole made in the mask by making a hole at a position corresponding to a predetermined flow path of the pressure-sensitive adhesive sheet 40 described in No. 4 is as follows: Such a problem occurred. In these methods of Patent Documents 3 and 4, since it is necessary to make a through hole in a predetermined position of the sealing film 30 or the adhesive sheet 40 by a method such as a laser, a heat insulating space 55 is formed in the vicinity of the outer peripheral wall of the honeycomb structure. In order to seal both ends of the same flow path near the outer peripheral wall with a sealing material, all the positions corresponding to the sealing material film 30 and the flow path near the outer peripheral wall of the adhesive sheet 40 It is necessary to form a through hole with a laser or the like. Therefore, there has been a problem that the time for opening the through-hole becomes long. That is, in the flow path at the center of the honeycomb structure, through-holes are alternately formed in the checker film 30 and the pressure-sensitive adhesive sheet 40 so as to have a checkered pattern. This is because it is necessary to form through holes at positions corresponding to all the adjacent flow paths. More specifically, compared to the case where the through holes are alternately formed so as to form a checkered pattern, the number of flow paths in which the through holes are to be formed is doubled in the vicinity of the outer peripheral wall, and the area of the circle is 2 of the diameter. This is because the number of flow paths increases as the distance from the outer wall increases.
Moreover, as described in Patent Document 5, the end surface except for the vicinity of the outer peripheral wall is covered with an appropriate mask material, and the sealing material is press-fitted into the end of the flow path that is not sealed by the flow path near the outer peripheral wall. In such cases, the following problems occurred. If the mask material is not positioned correctly when the honeycomb filter end face is covered with a film or mask material, the number of channels to be sealed near the outer peripheral wall will be biased, and from the outermost peripheral portion near the outer peripheral wall. There is a problem in that the number of heat insulation spaces formed in the central portion is biased, and the heat of combustion during regeneration is dissipated from a portion having a small number of heat insulation spaces to a metal storage container. Furthermore, when the film or mask material is peeled off from the end of the flow path, the sealing material flows into the flow path that is not sealed, and the flow path is not alternately sealed, resulting in a flow path through which exhaust gas cannot pass, resulting in pressure loss. The problem that becomes larger.

本発明の課題は、ハニカム構造体の流路端部を封止するハニカムフィルタにおいて、フィルタ再生時の燃焼熱が、金属製の収納容器に放散するのを抑制することができる保温空間が形成されたハニカムフィルタとするために、外周壁近傍の流路の両端部を封止材で封止する際に、保温空間が均一に形成でき、封止位置へ貫通孔を形成する時間を短縮できる封止用フィルム、およびこれを用いたハニカムフィルタの製造方法を得ることにある。   An object of the present invention is to form a heat insulation space capable of suppressing the heat of combustion at the time of filter regeneration from being dissipated into a metal storage container in a honeycomb filter that seals the flow path end of a honeycomb structure. Therefore, when sealing both ends of the flow path near the outer peripheral wall with a sealing material, a heat insulating space can be formed uniformly and the time required for forming a through hole at the sealing position can be shortened. It is to obtain a film for stopping and a method for producing a honeycomb filter using the same.

上記課題を解決する為、本発明者は、鋭意検討の結果、封止用フィルムの最適な形状とその構造を見出した。
具体的に、本発明の封止用フィルムは、ハニカム構造体の流路端部を封止するハニカムフィルタの製造に用いる封止用フィルムであって、前記流路端部の外周形状と、少なくとも一部の周部の形状とを概略一致させた剥離紙と、該剥離紙に前記ハニカム構造体の端部の外周形状よりも小さい形状とした貼着フィルムを、貼着していることを特徴とする。
上記構成とすることで、外周壁近傍で流路の両端部を封止する範囲を除いて封止用フィルムで覆うことができるので、従来技術のように外周壁近傍で流路の両端部を封止する範囲のフィルムに貫通孔を形成する必要が無く、フィルムに貫通孔を形成させる時間を短縮することができる。また、剥離紙の少なくとも一部の周部で、ハニカム構造体の流路端部の外周と正確に位置決めできるので、外周壁近傍の同じ流路の両端を封止している範囲のばらつきをなくすことができ、外周壁近傍の保温空間が均一に形成され、パティキュレートの燃焼熱が金属製の収納容器へ放散するのを防ぐことのできるハニカムフィルタを得ることができる。
ここで、貼着フィルムは、ハニカム構造体の端部の外周よりも小さい相似形状とし、図1(a)(c)に示すように、ハニカム構造体の流路端部51d、51eの外周形状に概略一致している剥離紙の周部11a、11b、11cから、一定間隔を有する位置で剥離紙に貼着されていることが好ましい。貼着フィルムが、流路端部の外周形状に、少なくとも一部の周部の形状とを概略一致している剥離紙の周部11a、11b、11cから、一定間隔を有する位置で剥離紙に貼着されていることで、貼着フィルムが、流路端部に貼着された際に、貼着フィルムの中心が、流路端部の外周形状の中心と略同心に貼着される。これにより、外周壁近傍の同じ流路の両端を封止する範囲のばらつきをなくすことができる。このとき、貼着フィルムの中心と流路端部の外周形状の中心とのずれは、ハニカム構造体のセルピッチの1倍以下であることが好ましく、これにより、外周壁近傍の同じ流路の両端を封止する範囲のばらつきをなくすことができ、外周壁近傍の保温空間が均一に形成され、パティキュレートの燃焼熱が金属製の収納容器へ放散するのを防ぐことのできるハニカムフィルタを得ることができるのである。
なお、剥離紙の周部は、ハニカム構造体の流路端部の外形と同じ形状、例えば、ハニカム構造体の流路端部の外形が円、楕円であれば、剥離紙も同じ形状の円、楕円にすれば、ハニカム構造体に対して何れの方向にもあわせることができ、作製も容易である。一方、剥離紙の周部を、ハニカム構造体の流路端部の外周に少なくとも3個所をあわせた形状であれば、円形状以外でもよく、略三角形状、略四角形状などの略多角形状として、剥離紙を節約することもできる。
In order to solve the above problems, the present inventor has found the optimum shape and structure of the sealing film as a result of intensive studies.
Specifically, the sealing film of the present invention is a sealing film used for manufacturing a honeycomb filter for sealing a flow path end portion of a honeycomb structure, and the outer peripheral shape of the flow path end portion is at least A release paper in which the shape of a part of the peripheral portion is approximately matched, and an adhesive film having a shape smaller than the outer peripheral shape of the end portion of the honeycomb structure is attached to the release paper. And
By adopting the above configuration, the both ends of the flow path can be covered with a sealing film except in the range of sealing both ends of the flow path near the outer peripheral wall. There is no need to form through holes in the film to be sealed, and the time for forming the through holes in the film can be shortened. In addition, since at least a part of the periphery of the release paper can be accurately positioned with the outer periphery of the channel end of the honeycomb structure, variations in the range in which both ends of the same channel near the outer peripheral wall are sealed are eliminated. Thus, a honeycomb filter can be obtained in which the heat insulation space in the vicinity of the outer peripheral wall is uniformly formed and the combustion heat of the particulates can be prevented from being diffused into the metal storage container.
Here, the sticking film has a similar shape smaller than the outer periphery of the end portion of the honeycomb structure, and as shown in FIGS. 1A and 1C, the outer peripheral shape of the flow path end portions 51d and 51e of the honeycomb structure body. Is preferably attached to the release paper at a position having a predetermined interval from the peripheral portions 11a, 11b, and 11c of the release paper that substantially coincide with each other. Sticking the film, the outer peripheral shape of the flow path end portion, at least a portion of the periphery of the shape and the substantially aligned to have release paper peripheral portion 11a, 11b, from 11c, the release paper at a position having a predetermined distance By being stuck, when the sticking film is stuck on the flow path end, the center of the sticking film is stuck substantially concentrically with the center of the outer peripheral shape of the flow path end. Thereby, the dispersion | variation in the range which seals the both ends of the same flow path near an outer peripheral wall can be eliminated. At this time, the difference between the center of the adhesive film and the center of the outer peripheral shape of the end of the flow path is preferably not more than one time the cell pitch of the honeycomb structure, and thereby both ends of the same flow path near the outer peripheral wall. A honeycomb filter capable of eliminating the variation in the sealing range, forming a uniform heat-retaining space in the vicinity of the outer peripheral wall, and preventing the combustion heat of the particulate from being dissipated into the metal storage container is obtained. Can do it.
Note that the periphery of the release paper has the same shape as the outer shape of the flow path end of the honeycomb structure, for example, if the outer shape of the flow path end of the honeycomb structure is a circle or an ellipse, the release paper also has the same shape . If it is made into an ellipse, it can be adjusted in any direction with respect to the honeycomb structure, and production is also easy. On the other hand, as long as the peripheral portion of the release paper has a shape in which at least three locations are combined with the outer periphery of the flow path end of the honeycomb structure, it may be other than a circular shape, and may be a substantially polygonal shape such as a substantially triangular shape or a substantially rectangular shape. Also, you can save release paper.

本発明の封止用フィルムにおいて、前記剥離紙は、該剥離紙を複数に分離する手段を有することが好ましい。剥離紙を複数に分離する手段を有することで、剥離紙から貼着フィルムをハニカム構造体の流路端部に貼着する際、フィルムの位置決めが正しく行われる。これは、複数の分離手段のうちのひとつの分離手段で剥離紙の1部分を分離するとともに、貼着フィルムから剥離し、貼着フィルムの1部分をハニカム構造体の流路端部に貼りつけ、これにより、貼着フィルムが流路端部に固定され、次に、残りの分離手段で剥離紙を分離して、貼着フィルムから剥離し、貼着フィルムを貼り付けるからである。また、貼着フィルムからの剥離紙の剥離が容易となる。剥離紙を複数に分離する手段として、剥離紙にミシン目、或いは、切り目等を入れることができる   In the sealing film of the present invention, the release paper preferably has means for separating the release paper into a plurality of pieces. By having means for separating the release paper into a plurality of pieces, the film is correctly positioned when the adhesive film is attached from the release paper to the end of the flow path of the honeycomb structure. This means that one part of the release paper is separated by one of a plurality of separation means, and the part is peeled off from the adhesive film, and the part of the adhesive film is attached to the end of the channel of the honeycomb structure. This is because the sticking film is fixed to the end of the flow path, and then the release paper is separated by the remaining separating means, peeled off from the sticking film, and stuck to the sticking film. Moreover, peeling of the release paper from the sticking film becomes easy. As a means for separating the release paper into a plurality, perforations or cuts can be made in the release paper

本発明の封止用フィルムにおいて、前記貼着フィルムは、0.03〜3.0mmの厚さで、その材質がポリプロピレン、ポリエチレン、アクリル、オレフィンから選択されることが好ましい。ポリプロピレン、ポリエチレン、アクリル、オレフィンから選択され、その厚さが0.03以上であれば貼着前後の強度が確保され、3.0mm以下であればレーザーなどにより貫通孔の形成が容易となる。   In the sealing film of the present invention, the adhesive film preferably has a thickness of 0.03 to 3.0 mm, and the material thereof is selected from polypropylene, polyethylene, acrylic, and olefin. If it is selected from polypropylene, polyethylene, acrylic, and olefin, and its thickness is 0.03 or more, the strength before and after sticking is secured, and if it is 3.0 mm or less, formation of a through hole is facilitated by a laser or the like.

本発明の封止用フィルムにおいて、前記貼着フィルムの貼着材の粘着力が2N/25mm以上であることが好ましい。貼着フィルムの粘着力が2N/25mm未満であると、ハニカム構造体の流路端部に貼り付けた場合に、剥がれやすくなってずれたり、封止材を浸入させる際に、封止しない流路に封止材が流れ込み、流路を交互に封止できなくなる。好ましくは4N/25mm以上であれば良い。
そして、前記貼着フィルムの貼着材が、0.01〜1.0mmの厚さで、その材質がアクリルゴム、スチレンブタジエンゴム等のゴムを基剤とする材料であることが好ましい。貼着フィルムの貼着材が0.01〜1.0mmの厚さで、その材質がゴムを基剤とする材料であると、ハニカム構造体の流路端部に貼り付けた場合、貼着フィルムの貼着材が柔軟に変形し、ハニカム構造体の端部の形状に合わせて貼り付き、貼着フィルムがハニカム構造体の端部により密着できるようになる。そのため、貼着フィルムが剥がれ難くなるのでずれることがなく、さらに、封止材を浸入させる際に、封止しない流路に封止材が流れ込み、流路を交互に封止できなくなることが生じ難くなるのである。
In the sealing film of the present invention, the adhesive strength of the adhesive material of the adhesive film is preferably 2 N / 25 mm or more. When the adhesive strength of the adhesive film is less than 2 N / 25 mm, it is easy to peel off when it is attached to the end of the flow path of the honeycomb structure, or when the sealing material is infiltrated, it is not sealed. The sealing material flows into the path, and the flow path cannot be alternately sealed. Preferably it should just be 4N / 25mm or more.
And it is preferable that the adhesive material of the said adhesive film is 0.01-1.0 mm in thickness, and the material is a material based on rubbers, such as an acrylic rubber and a styrene butadiene rubber. When the sticking material of the sticking film has a thickness of 0.01 to 1.0 mm and the material is a material based on rubber, sticking to the end of the channel of the honeycomb structure is sticking The adhesive material for the film is flexibly deformed and adhered in accordance with the shape of the end portion of the honeycomb structure, so that the adhesive film can be more closely attached to the end portion of the honeycomb structure. For this reason, the sticking film is difficult to peel off, so that it does not shift. Further, when the sealing material is infiltrated, the sealing material flows into the unsealed flow path, and the flow paths cannot be alternately sealed. It becomes difficult.

次に、本別発明は、外周壁と該外周壁の内側に複数の流路を有するハニカム構造体を作製した後、該ハニカム構造体の流路端部を封止するハニカムフィルタの製造方法において、
前記流路端部の外周形状と、少なくとも一部の周部の形状とを一致させた剥離紙と、該剥離紙に前記ハニカム構造体の端部の外周形状よりも小さい形状とした貼着フィルムを、貼着している封止用フィルムの剥離紙で前記ハニカム構造体の流路端部を覆う工程;
前記剥離紙を前記貼着フィルムから分離すると共に、該貼着フィルムを前記ハニカム構造体の流路端部に貼着し残置する工程;
前記貼着フィルムの前記ハニカム構造体の流路端部が交互に封止される位置に貫通孔を形成する工程;
含むことを特徴とする。これらの工程を含むことにより、外周壁近傍で流路の両端部を封止する範囲を除いて封止用フィルムで覆うので、従来技術のように外周壁近傍で流路の両端部を封止する範囲のフィルムに貫通孔を形成する必要が無くなり、フィルムに貫通孔を形成させる時間を短縮することができる。さらに、剥離紙の少なくとも一部の周部で、ハニカム構造体の流路端部の外周と正確に位置決めできるので、外周壁近傍の両端を封止している範囲のばらつきをなくすことができ、外周壁近傍の保温空間が均一に形成され、パティキュレートの燃焼熱が金属製の収納容器へ放散することを防ぐことができる。
Next, the present invention relates to a method for manufacturing a honeycomb filter in which a honeycomb structure having a plurality of flow paths inside an outer peripheral wall and the outer peripheral wall is manufactured, and then a flow path end of the honeycomb structure is sealed. ,
And the outer peripheral shape of the flow path ends, stuck films and release paper is matched with the shape of at least part of the peripheral portion, a shape smaller than the outer peripheral shape of the end portion of the honeycomb structure to the release paper Covering the flow path end of the honeycomb structure with the release paper of the sealing film that is adhered;
Separating the release paper from the sticking film, and sticking the sticking film to the flow path end of the honeycomb structure;
Forming a through hole at a position where the flow path ends of the honeycomb structure of the adhesive film are alternately sealed;
It is characterized by including. By including these steps, the both ends of the flow path are covered with a sealing film except in the vicinity of the outer peripheral wall, so that both ends of the flow path are sealed near the outer peripheral wall as in the prior art. This eliminates the need to form through-holes in the film in the range, thereby reducing the time for forming the through-holes in the film. Furthermore, since at least a part of the periphery of the release paper can be accurately positioned with the outer periphery of the end of the flow path of the honeycomb structure, it is possible to eliminate variations in the range in which both ends near the outer peripheral wall are sealed, The heat insulation space in the vicinity of the outer peripheral wall is formed uniformly, and the heat of combustion of the particulates can be prevented from being dissipated to the metal storage container.

本発明の封止用フィルムによれば、外周壁近傍で流路の両端部を封止する範囲を除いて封止用フィルムで覆って、外周壁近傍の流路の両端部を封止し、外周壁近傍の同じ流路の両端を封止している範囲のばらつきをなくすことができるので、パティキュレートの燃焼熱が金属製の収納容器に放散するのを抑える保温空間が均一に形成され、また、外周壁近傍の封止位置への貫通孔を形成する時間を短縮することができる。   According to the sealing film of the present invention, except for the range of sealing both ends of the flow path in the vicinity of the outer peripheral wall, covered with the sealing film, sealing both ends of the flow path in the vicinity of the outer peripheral wall, Since it is possible to eliminate variations in the range of sealing both ends of the same flow path in the vicinity of the outer peripheral wall, a heat insulation space that suppresses the diffusion of particulate combustion heat to the metal storage container is uniformly formed, Moreover, the time for forming the through hole to the sealing position in the vicinity of the outer peripheral wall can be shortened.

(実施の形態1)
図1は、実施の形態1の封止用フィルム10の模式図であり、(a)は正面図、(b)は側面図、(c)は変形例の正面図を示す。図1(a)(b)の封止用フィルム10は、図5に示すようなハニカム構造体51の流路端部51d(51e)を封止するハニカムフィルタ(50)の製造に用いる封止用フィルム10であって、ハニカム構造体51の流路端部51d(51e)の外周形状と、周部11a〜11cの形状とを一致させた外径D11の剥離紙11と、この剥離紙11に貼着材13で貼着して、ハニカム構造体51の流路端部51d(51e)の外周形状よりも小さい形状の外径D12とした貼着フィルム12を、剥離紙の周部11a〜11cから、一定間隔を有する位置で同心に貼り着けている。剥離紙11は、剥離紙11を2つに分離する切り目14を有する。貼着フィルム12は、0.05mm厚さのポリプロピレンを選択している。
(Embodiment 1)
1A and 1B are schematic views of a sealing film 10 according to Embodiment 1, wherein FIG. 1A is a front view, FIG. 1B is a side view, and FIG. 1C is a front view of a modification. 1 (a) and 1 (b) is a sealing film 10 used for manufacturing a honeycomb filter (50) for sealing the flow path end portion 51d (51e) of a honeycomb structure 51 as shown in FIG. A release paper 11 having an outer diameter D11 in which the outer peripheral shape of the flow path end portion 51d (51e) of the honeycomb structure 51 is matched with the shapes of the peripheral portions 11a to 11c, and the release paper 11 by sticking with stuck material 13, the adhered film 12 that the outer diameter D12 of the smaller shape than the outer peripheral shape of the flow passage end portion 51d of the honeycomb structure 51 (51e), the circumferential portion of the release paper 11a~ From 11c, it sticks concentrically at a position having a fixed interval. The release paper 11 has a cut 14 that separates the release paper 11 into two. As the adhesive film 12, 0.05 mm thick polypropylene is selected.

図1の封止用フィルム10によれば、剥離紙11の外径D11でハニカム構造体51の流路端部51d(51e)の外周と正確に位置決めし、貼着フィルム12で、ハニカム構造体51の流路端部51d(51e)の外周壁51a近傍で流路の両端部を封止する範囲を除いてばらつくことなく覆うことができる。また、剥離紙11は、分離手段である切り目14により、貼着フィルム12からの剥離が容易となる。   According to the sealing film 10 of FIG. 1, the outer diameter D11 of the release paper 11 is accurately positioned with respect to the outer periphery of the flow path end portion 51d (51e) of the honeycomb structure 51. The flow path end portion 51d (51e) can be covered without variation except in the vicinity of the outer peripheral wall 51a except for the range where both ends of the flow channel are sealed. Further, the release paper 11 can be easily peeled off from the adhesive film 12 by the cut 14 which is a separating means.

なお、剥離紙11の周部11a〜11bは、ハニカム構造体51の流路端部51d(51e)の外周51f(51g)と少なくとも3個所をあわせておけば、円形状以外でもよく、図1(c)に示すように、略三角形状や略四角形状などの多角形状として、剥離紙を節約することも可能である。   The peripheral portions 11a to 11b of the release paper 11 may have a shape other than the circular shape as long as at least three locations are combined with the outer periphery 51f (51g) of the flow path end portion 51d (51e) of the honeycomb structure 51, as shown in FIG. As shown in (c), it is possible to save the release paper as a polygonal shape such as a substantially triangular shape or a substantially rectangular shape.

(実施の形態2)
図2(a)〜(f)は、ハニカムフィルタの製造工程を示す模式図であり、(b)〜(d)での左側は各工程での側面図、右側は各工程での平面図、(e)はこの工程の側面図、(f)はこの工程の平面図を示す。これを製造工程順に説明する。
(Embodiment 2)
Fig.2 (a)-(f) is a schematic diagram which shows the manufacturing process of a honey-comb filter, The left side in (b)-(d) is a side view in each process, The right side is a top view in each process, (E) is a side view of this process, and (f) is a plan view of this process. This will be described in the order of the manufacturing process.

先ず、原料を配合して坏土とし、これをハニカム構造にする金型で押出成形し、乾燥し、さらに1400℃の温度で焼成し、コージェライト質からなり、図5に示す、外周壁51aの流路端部51d(51e)の外形D51が250mm、長さ(L51)が200mm、セル壁厚0.3mm、セル壁ピッチ1.5mm(44セル/cm)で、外周壁51aの内側に各々直交するセル壁51bにより形成された複数の流路51cを有するハニカム構造体51を作製した。 First, raw materials are blended to form a clay, which is extruded with a die having a honeycomb structure, dried, further fired at a temperature of 1400 ° C., made of cordierite, and shown in FIG. The flow path end 51d (51e) has an outer shape D51 of 250 mm, a length (L51) of 200 mm, a cell wall thickness of 0.3 mm, a cell wall pitch of 1.5 mm (44 cells / cm 2 ), and an inner side of the outer peripheral wall 51a. A honeycomb structure 51 having a plurality of flow paths 51c formed by cell walls 51b orthogonal to each other was produced.

(a)封止用フィルムの準備
図1(a)(b)の封止用フィルム10を準備した。図1の封止用フィルム10は、ハニカム構造体51の流路端部51d(51e)の外径D51と同じ、外径D11が250mmの剥離紙11と、この剥離紙11に、ハニカム構造体51の外周壁51aから2つ目までの流路を除いた外径D12が242mmの貼着フィルム12とを同心に貼着材13で貼着し、剥離紙11には切り目14を設けた。貼着フィルム12は、0.05mm厚さのポリプロピレンを選択した。この粘着フィルムは粘着力が7.3N/25mm、保持力が0.5mm/30分、であった。
(A) Preparation of sealing film The sealing film 10 shown in FIGS. 1A and 1B was prepared. 1 is the same as the outer diameter D51 of the flow path end 51d (51e) of the honeycomb structure 51, and the release paper 11 has an outer diameter D11 of 250 mm. The adhesive film 12 having an outer diameter D12 of 242 mm excluding the second flow path from the outer peripheral wall 51a of 51 was attached concentrically with the adhesive material 13, and the release paper 11 was provided with cuts 14. As the adhesive film 12, 0.05 mm thick polypropylene was selected. This adhesive film had an adhesive force of 7.3 N / 25 mm and a holding force of 0.5 mm / 30 minutes.

(b)剥離紙で流路端部を覆う
次に、封止用フィルム10の剥離紙11の外径D11を、ハニカム構造体51の外形D51にあわせて流路端部51d(51e)を覆う。このとき、剥離紙11によりハニカム構造体51の流路端部51d(51e)と正確に位置決めでき、また貼着フィルム12でハニカム構造体51の外周壁51a近傍の封止範囲を除いて覆い、流路端部51d(51e)に貼着することができる。
(B) Covering the end of the flow path with release paper Next, the outer diameter D11 of the release paper 11 of the sealing film 10 is matched with the outer shape D51 of the honeycomb structure 51 to cover the flow path end 51d (51e). . At this time, the release paper 11 can accurately position the channel end 51d (51e) of the honeycomb structure 51, and the adhesive film 12 covers the honeycomb structure 51 except for the sealing range in the vicinity of the outer peripheral wall 51a, It can be attached to the channel end 51d (51e).

(c)剥離紙を貼着フィルムから分離しハニカム構造体に残置
次に、剥離紙11−1を、切り目14を使って貼着フィルム12から分離して、剥離紙11−1と貼着されていた部分の貼着フィルム12をハニカム構造体31の流路端部51d(51e)に貼着させ、次いで、残った剥離紙11−2を切り目14より貼着フィルム12から分離して剥離紙11−2と貼着されていた部分の貼着フィルム12をハニカム構造体31の流路端部51d(51e)に貼着させ残置した。このとき、貼着フィルム12の中心と流路端部51d(51e)の外周形状の中心とのずれは0.8mmであった。
(C) Separate the release paper from the adhesive film and leave it in the honeycomb structure. Next, the release paper 11-1 is separated from the adhesive film 12 using the cut line 14, and is attached to the release paper 11-1. The pasted adhesive film 12 was adhered to the channel end 51d (51e) of the honeycomb structure 31, and then the remaining release paper 11-2 was separated from the adhesive film 12 through the cut line 14 to release the release paper. The part of the adhesive film 12 that had been attached to 11-2 was attached to the channel end 51d (51e) of the honeycomb structure 31 and was left behind. At this time, the deviation between the center of the adhesive film 12 and the center of the outer peripheral shape of the flow path end 51d (51e) was 0.8 mm.

(d)貼着フィルムに貫通孔を形成
次に、ハニカム構造体51の流路端部51d(51e)の交互に封止する位置の貼着フィルム12に、レーザを照射し、貼着フィルム12に貫通孔12aを形成した。この時、貼着フィルム12の外周端面部で、貼着フィルム12がハニカム構造体の流路を完全に覆っていない流路は、全て貫通孔12bを形成することとした。この結果、外周壁近傍の封止位置への貫通孔12aの形成は行わなかったので、形成すべき貫通孔の数が約7%減り、貫通孔を形成する時間も短縮することができた。
(D) Forming a through-hole in the adhesive film Next, the adhesive film 12 at the position where the flow path end portions 51d (51e) of the honeycomb structure 51 are alternately sealed is irradiated with a laser so that the adhesive film 12 is sealed. The through-hole 12a was formed in. At this time, all the flow paths in which the adhesive film 12 does not completely cover the flow path of the honeycomb structure in the outer peripheral end surface portion of the adhesive film 12 are formed as the through holes 12b. As a result, since the through holes 12a were not formed at the sealing position near the outer peripheral wall, the number of through holes to be formed was reduced by about 7%, and the time for forming the through holes could be shortened.

(e)貫通孔に封止材を充填
次に、ハニカム構造体51の流路端部51d(51e)を、封止材が含有するスラリー25に浸漬させ、スラリー25を貼着フィルム12の貫通孔12aを通じて、流路端部51d(51e)に充填させた。さらに、ハニカム構造体51を加熱し、流路端部51d(51f)に侵入したスラリーを硬化させると共に貼着フィルム12を燃焼して除去した。
(E) Filling the through hole with the sealing material Next, the flow path end 51d (51e) of the honeycomb structure 51 is immersed in the slurry 25 contained in the sealing material, and the slurry 25 penetrates the adhesive film 12. The channel end 51d (51e) was filled through the hole 12a. Further, the honeycomb structure 51 was heated to cure the slurry that entered the flow path end 51d (51f), and the adhesive film 12 was removed by burning.

(f)ハニカムフィルタ
以上の工程により、ハニカム構造体51の流路端部51d(51e)の外周壁51aから2目の長さ(D55)が封止材55d(55e)で封止され、さらにその内側に市松模様に封止材52d(52e)で封止されたハニカムフィルタ50となった。このようなハニカムフィルタ50は、外周壁近傍での最外周部から中心部へ形成される保温空間55が均一に形成されているので、パティキュレートの燃焼熱が金属製の収納容器に放散するのを抑えることができる。
(F) Honeycomb filter Through the above steps, the second length (D55) from the outer peripheral wall 51a of the flow path end 51d (51e) of the honeycomb structure 51 is sealed with the sealing material 55d (55e). The honeycomb filter 50 was sealed inside with a sealing material 52d (52e) in a checkered pattern. In such a honeycomb filter 50, the heat insulating space 55 formed from the outermost peripheral portion in the vicinity of the outer peripheral wall to the central portion is uniformly formed, so that the combustion heat of the particulate is dissipated in the metal storage container. Can be suppressed.

(実施の形態3)
実施の形態2と同様に図5に示すハニカム構造体51を作製した。
次に、実施の形態2と同様に図1(a)(b)の封止用フィルム10を準備した。ただし、貼着材13には、0.5mmの厚さでアクリルゴムを基剤とした貼着材を塗布したものを用いた。
次いで、実施の形態2と同様に図2(b)〜(e)の工程で、ハニカム構造体51の流路端部51d(51e)に、スラリー25を貼着フィルム12の貫通孔12aを通じて、流路端部51d(51e)に充填させた。この時、封止用フィルムの貼着材13が、0.5mmの厚さでスチレンブタジエンゴムを基剤とした貼着材であったので、封止用フィルムがハニカム構造体51の流路端部51d(51e)の形状に合わせて貼り付き、封止用フィルムがハニカム構造体の端部に密着したので、封止しない流路に封止材が流れ込むことがなく、流路を交互に封止できなくなることはなかった。
そして、以上の工程により、ハニカム構造体51の流路端部51d(51e)の外周壁51aから2目の長さ(D55)が封止材55d(55e)で封止され、さらにその内側に市松模様に封止材52d(52e)で封止されたハニカムフィルタ50を得た。
このハニカムフィルタ50は、外周壁近傍での最外周部から中心部へ形成される保温空間55が均一に形成されているので、パティキュレートの燃焼熱が金属製の収納容器に放散するのを抑えることができる。
(Embodiment 3)
A honeycomb structure 51 shown in FIG. 5 was produced in the same manner as in the second embodiment.
Next, the sealing film 10 shown in FIGS. 1A and 1B was prepared as in the second embodiment. However, the adhesive material 13 was applied with an adhesive material based on acrylic rubber with a thickness of 0.5 mm.
Next, in the steps of FIGS. 2B to 2E as in the second embodiment, the slurry 25 is passed through the through holes 12a of the sticking film 12 to the flow path end portion 51d (51e) of the honeycomb structure 51. The flow path end 51d (51e) was filled. At this time, since the sealing film adhesive 13 was an adhesive having a thickness of 0.5 mm and a styrene butadiene rubber as a base, the sealing film was the end of the flow path of the honeycomb structure 51. Since the sealing film adheres to the end of the honeycomb structure, the sealing material does not flow into the non-sealed flow path, and the flow paths are sealed alternately. I couldn't stop it.
Then, through the above steps, the second length (D55) from the outer peripheral wall 51a of the flow path end 51d (51e) of the honeycomb structure 51 is sealed with the sealing material 55d (55e), and further inside thereof A honeycomb filter 50 sealed in a checkered pattern with a sealing material 52d (52e) was obtained.
In this honeycomb filter 50, the heat insulation space 55 formed from the outermost peripheral part in the vicinity of the outer peripheral wall to the central part is uniformly formed, so that the combustion heat of the particulates is prevented from being diffused into the metal storage container. be able to.

実施の形態1の封止用フィルム10の模式図であり、(a)は正面図、(b)は側面図、(c)は変形例の正面図を示す。It is a schematic diagram of the film 10 for sealing of Embodiment 1, (a) is a front view, (b) is a side view, (c) shows the front view of a modification. (a)〜(f)は、ハニカムフィルタの製造工程を示す模式図であり、(b)〜(d)での左側は各工程での側面図、右側は各工程での平面図、(e)はこの工程の側面図、(f)はこの工程の平面図を示す。(A)-(f) is a schematic diagram which shows the manufacturing process of a honey-comb filter, The left side in (b)-(d) is a side view in each process, The right side is a top view in each process, (e ) Is a side view of this process, and (f) is a plan view of this process. 従来の、ハニカム構造体51と封止用フィルム30の斜視図である。FIG. 3 is a perspective view of a conventional honeycomb structure 51 and a sealing film 30. 従来の、ハニカム構造体51の流路端部51d(51e)の外形とほぼ同じ形状の市販の使い捨ての粘着シート40を用いる斜視図である。It is a perspective view using the conventional commercially available disposable adhesive sheet 40 of the substantially same shape as the external shape of the flow-path edge part 51d (51e) of the honeycomb structure 51. FIG. 外周壁51a近傍の同じ流路51cを封止材55d、55eで封止し、封止した流路51cを保温空間55とするハニカムフィルタ50であり、(a)は正面図、(b)は断面図を示す。The same flow path 51c in the vicinity of the outer peripheral wall 51a is sealed with sealing materials 55d and 55e, and the sealed flow path 51c is used as a heat retaining space 55. (a) is a front view and (b) is a front view. A cross-sectional view is shown. 従来のハニカムフィルタの一例の模式図を示し、(a)は正面図、(b)は断面図である。The schematic diagram of an example of the conventional honey-comb filter is shown, (a) is a front view, (b) is sectional drawing.

符号の説明Explanation of symbols

10、30:封止用フィルム
11:剥離紙
11a〜11c:周部
12:貼着フィルム
13:貼着材
14:切り目
12a、12b、30a、30b:貫通孔
40:粘着シート
50、60:ハニカムフィルタ
51、61:ハニカム構造体
51a、61a:外周壁
51b、61b:セル壁
51c、61c:流路
51d、51e、61d、61e:流路端部
51f、51g:(流路端部)外周
52d、52e、55d、55e、62d、62e:封止材
55:保温空間
64:収納容器
63a〜63c:把持部材
65a、65b、65c:排気ガス
B55:ハニカムフィルタ端面からの長さ
D11、D12:外径
D51:外形
L51:全長
L52:長さ
DESCRIPTION OF SYMBOLS 10, 30: Film for sealing 11: Release paper 11a-11c: Peripheral part 12: Adhesive film 13: Adhesive material 14: Cut 12a, 12b, 30a, 30b: Through-hole 40: Adhesive sheet 50, 60: Honeycomb Filters 51, 61: Honeycomb structures 51a, 61a: Outer peripheral walls 51b, 61b: Cell walls 51c, 61c: Channels 51d, 51e, 61d, 61e: Channel ends 51f, 51g: (Channel ends) outer periphery 52d , 52e, 55d, 55e, 62d, 62e: Sealing material 55: Thermal insulation space 64: Storage container 63a to 63c: Gripping members 65a, 65b, 65c: Exhaust gas B55: Length from honeycomb filter end face D11, D12: Outside Diameter D51: Outline L51: Full length L52: Length

Claims (6)

ハニカム構造体の流路端部を封止するハニカムフィルタの製造に用いる封止用フィルムであって、前記流路端部の外周形状と、少なくとも一部の周部の形状とを概略一致させた剥離紙と、該剥離紙に前記ハニカム構造体の端部の外周形状よりも小さい形状とした貼着フィルムを、貼着材で貼着していることを特徴とする封止用フィルム。 The flow passage end portion of the honeycomb structure to a sealing film for use in manufacturing the honeycomb filter for sealing an outer peripheral shape of the flow path ends, were substantially aligned with the shape of at least part of the peripheral portion A sealing film, wherein a release paper and an adhesive film having a shape smaller than an outer peripheral shape of an end portion of the honeycomb structure are attached to the release paper with an adhesive material. 前記貼着フィルムは、ハニカム構造体の端部の外周よりも小さい相似形状とし、前記剥離紙の周部から、一定間隔を有する位置で剥離紙に貼着されていることを特徴とする請求項1に記載の封止用フィルム。 The sticking film has a similar shape smaller than the outer periphery of the end portion of the honeycomb structure, and is stuck to the release paper at a certain interval from the periphery of the release paper. 2. The sealing film according to 1. 前記剥離紙は、該剥離紙を複数に分離する手段を備えていることを特徴とする請求項1または請求項2に記載の封止用フィルム。 The sealing film according to claim 1, wherein the release paper includes means for separating the release paper into a plurality of pieces. 前記貼着フィルムは、0.03〜3.0mmの厚さで、その材質が、ポリプロピレン、ポリエチレン、アクリル、オレフィンから選択されることを特徴とする請求項1ないし請求項3のいずれかに記載の封止用フィルム。 The said sticking film is 0.03-3.0 mm in thickness, The material is selected from a polypropylene, polyethylene, an acryl, and an olefin, The Claim 1 thru | or 3 characterized by the above-mentioned. Sealing film. 前記貼着材が、0.01〜1.0mmの厚さで、その材質がゴムを基剤とする材料であることを特徴とする請求項4に記載の封止用フィルム。 The sealing film according to claim 4, wherein the adhesive material has a thickness of 0.01 to 1.0 mm, and the material thereof is a material based on rubber. 外周壁と該外周壁の内側に複数の流路を有するハニカム構造体を作製した後、該ハニカム構造体の流路端部を封止するハニカムフィルタの製造方法において、
前記流路端部の外周形状と、少なくとも一部の周部の形状とを一致させた剥離紙と、該剥離紙に前記ハニカム構造体の端部の外周形状よりも小さい形状とした貼着フィルムを貼着している封止用フィルムの該剥離紙で前記ハニカム構造体の流路端部を覆う工程;
前記剥離紙を前記貼着フィルムから分離すると共に、該貼着フィルムを前記ハニカム構造体の流路端部に貼着し残置する工程;
前記貼着フィルムの前記ハニカム構造体の流路端部が交互に封止される位置に貫通孔を形成する工程;
含むことを特徴とするハニカムフィルタの製造方法。
In a method for manufacturing a honeycomb filter in which a honeycomb structure having a plurality of flow paths inside an outer peripheral wall and the outer peripheral wall is manufactured, and then a flow path end of the honeycomb structure is sealed.
And the outer peripheral shape of the flow path ends, stuck films and release paper is matched with the shape of at least part of the peripheral portion, a shape smaller than the outer peripheral shape of the end portion of the honeycomb structure to the release paper Covering the end of the flow path of the honeycomb structure with the release paper of the sealing film to which is attached;
Separating the release paper from the sticking film, and sticking the sticking film to the flow path end of the honeycomb structure;
Forming a through hole at a position where the flow path ends of the honeycomb structure of the adhesive film are alternately sealed;
The manufacturing method of the honey-comb filter characterized by including.
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JPH0147206B2 (en) * 1981-09-14 1989-10-12 Ngk Insulators Ltd
JPH0245481B2 (en) * 1981-07-15 1990-10-09 Corning Glass Works
JP2002028915A (en) * 2000-05-12 2002-01-29 Denso Corp Method for manufacturing ceramic honeycomb structure and through hole forming device
JP2003320517A (en) * 2002-04-30 2003-11-11 Ngk Insulators Ltd Method for manufacturing honeycomb structure
JP2005048084A (en) * 2003-07-30 2005-02-24 Nippon Carbide Ind Co Inc Adhesive sheet and method for producing porous laminated structure

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Publication number Priority date Publication date Assignee Title
JPH0245481B2 (en) * 1981-07-15 1990-10-09 Corning Glass Works
JPH0147206B2 (en) * 1981-09-14 1989-10-12 Ngk Insulators Ltd
JP2002028915A (en) * 2000-05-12 2002-01-29 Denso Corp Method for manufacturing ceramic honeycomb structure and through hole forming device
JP2003320517A (en) * 2002-04-30 2003-11-11 Ngk Insulators Ltd Method for manufacturing honeycomb structure
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