JP4384900B2 - Polymer flocculant powder dissolution equipment - Google Patents

Polymer flocculant powder dissolution equipment Download PDF

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JP4384900B2
JP4384900B2 JP2003408580A JP2003408580A JP4384900B2 JP 4384900 B2 JP4384900 B2 JP 4384900B2 JP 2003408580 A JP2003408580 A JP 2003408580A JP 2003408580 A JP2003408580 A JP 2003408580A JP 4384900 B2 JP4384900 B2 JP 4384900B2
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polymer flocculant
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池田正義
東真裕
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株式会社トーケミ
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Description

本発明は、溶解槽での高分子凝集剤等粉末の水等の溶媒液による溶解操作中に所謂ままこの発生を防止するために、前記溶解操作の予備操作として用いる溶解装置に関するものである。   The present invention relates to a dissolution apparatus used as a preliminary operation of the dissolution operation in order to prevent the occurrence of the so-called generation during the dissolution operation of a powder such as a polymer flocculant in a dissolution tank with a solvent such as water.

前記のままこの発生を防止するために、溶解槽内の上方に定量供給口を設け、該定量供給口から供給される高分子凝集剤等の粉末に接触させてこれを前記溶解槽内に湿気(水気)を伴って分散させ、溶媒液と容易に馴染み易くするようにした装置は公知であり、具体的には、スプレーノズルを用いて、噴霧状の分散用水(水膜)を得てこれを前記高分子凝集剤粉末に接触させたり、或いは傾斜板上に水を供給することによって分散用水(水膜)を得、該分散用水上に高分子凝集剤粉末を落下接触させるようにした構造のものがある(特許文献1)。   In order to prevent this occurrence as it is, a fixed amount supply port is provided above the dissolution tank and brought into contact with powder such as a polymer flocculant supplied from the fixed amount supply port, and this is put in the dissolution tank with moisture. A device that is dispersed with (water) and easily adapted to a solvent solution is known. Specifically, spray water is used to obtain sprayed dispersion water (water film). A structure in which water for dispersion (water film) is obtained by bringing the polymer flocculant powder into contact with the polymer flocculant powder or by supplying water onto the inclined plate, and the polymer flocculant powder is brought into drop contact with the dispersion water (Patent Document 1).

特開2001−887603号公報JP 2001-877603 A

前記従来例中のスプレーノズル方式のものはノズルが水などの溶媒液中の異物によって詰り、該ノズルを通じて噴出する液量が変化し易く、従って分散用水のパターンが容易に変化し、高分子凝集剤粉末の良好な分散状態を必ずしも得られず、このため、スプレーノズルの保守に十分配慮する必要がある。また、傾斜板方式のものは、傾斜板の傾斜を利用して該板上に供給される分散水(溶媒液)を分散させて水膜を得、水膜の、いわば広がりによって高分子凝集剤粉末を分散させるものであるから、水膜の広がりには自ら制約があり、分散水の供給量の少しの変化によって分散効果が変わり、また、傾斜板に粉末が容易に堆積するおそれがある。   In the conventional spray nozzle type, the nozzle is clogged with foreign matter in a solvent liquid such as water, and the amount of liquid ejected through the nozzle is easily changed. Therefore, it is not always possible to obtain a good dispersion state of the agent powder. For this reason, it is necessary to sufficiently consider the maintenance of the spray nozzle. In addition, in the inclined plate type, a water film is obtained by dispersing the dispersed water (solvent liquid) supplied onto the plate using the inclination of the inclined plate, and the polymer flocculant is formed by the so-called spread of the water film. Since the powder is dispersed, the spread of the water film is restricted by itself, and the dispersion effect is changed by a slight change in the supply amount of the dispersed water, and the powder may easily deposit on the inclined plate.

本発明は、斯様な従来例の欠点に着目し、粉末を分散させるための好適な液膜を得られる、斬新な構造の溶解装置を提供すべく創案したものである。   The present invention has been devised to provide a melting apparatus with a novel structure that can obtain a suitable liquid film for dispersing powder, paying attention to the disadvantages of such conventional examples.

溶解槽内の上方に定量供給口を設け、該定量供給口から供給される高分子凝集剤等の粉末に接触してこれを前記溶解槽内に分散させる、溶媒液の液膜の形成装置を備えた高分子凝集剤等粉末の溶解装置において、前記形成装置を、前記定量供給口側の、前方側の一半の周端が円弧状を成し、上面が曲面状の液膜形成材を、前記溶解槽へ前記溶媒液を落下供給する注液口の直下に前方下りに傾斜させて配置して構成したものである。 An apparatus for forming a liquid film of a solvent solution, which is provided with a quantitative supply port above the dissolution tank and contacts the powder such as a polymer flocculant supplied from the quantitative supply port and disperses the powder in the dissolution tank. In the apparatus for dissolving powder such as a polymer flocculant provided, the forming device is a liquid film forming material having a circular shape on the front side and a curved surface on the front side, on the quantitative supply port side , The solvent solution is dropped into the dissolution tank and is arranged so as to be inclined forward and downward just below the liquid inlet.

本発明によれば、供給材の凹曲面状の上面に注入口から分散用水を落下させるものであるから該上面形によって分散用水は供給材位置から水膜となって拡散し、定量供給口からの高分子凝集剤等の粉末は該分散水に伴われて確実に分散され、ままこ発生防止のための予備操作を確実に行うことができる。   According to the present invention, since the water for dispersion is dropped from the inlet to the upper surface of the concave surface of the feed material, the water for dispersion diffuses as a water film from the position of the feed material due to the shape of the upper surface, and from the quantitative feed port. The powder such as the polymer flocculant is reliably dispersed along with the dispersed water, so that a preliminary operation for preventing the occurrence of the litter can be reliably performed.

図面は本発明に係る高分子凝集剤等粉末の溶解装置の一実施例を示し、図1は略示説明図、図2は図1の一部拡大図である。   The drawings show one embodiment of the powder dissolving apparatus for polymer flocculant and the like according to the present invention, FIG. 1 is a schematic explanatory view, and FIG. 2 is a partially enlarged view of FIG.

図中、1は撹拌機を省略して示した溶解槽(図面は一部を示している)、2は該溶解槽1の上方に配置した粉末の収容部で、該収容部2の排出口2aから予め設定した定量の(一定時間、一定量の)粉末が排出され、前記溶解槽1内の溶解部1a上に設置した液膜形成装置3で形成される液膜に落下、接触するようにしてある。   In the figure, reference numeral 1 is a dissolution tank with a stirrer omitted (the drawing shows a part thereof), and 2 is a powder storage part arranged above the dissolution tank 1, and an outlet of the storage part 2 A predetermined amount (a certain amount of time, a certain amount) of powder is discharged from 2a so as to drop and come into contact with the liquid film formed by the liquid film forming apparatus 3 installed on the dissolution part 1a in the dissolution tank 1. It is.

なお、実施例の収容部2は粉末を定量的に排出口(切出し方式などにより排出量を調節できるようにしてある)2aより粉末が排出するようにしてあるが(従って、溶解槽1の上方に配置されることになる)、予め設定した所望量の粉末をエアーを利用して前記液膜形成装置3で形成される液膜S部に送り込むようなものでも良く(もっとも、液膜は溶媒液で形成したものであることは勿論である)、この場合は、溶解槽と別体にして、例えば、案内管(粉末押送用の)で両者を連通させることになる。   In addition, although the container 2 in the embodiment quantitatively discharges the powder from the discharge port 2a (the discharge amount can be adjusted by a cutting method or the like) 2a (therefore, above the dissolution tank 1). In other words, a desired amount of powder set in advance may be sent to the liquid film S formed by the liquid film forming apparatus 3 using air (however, the liquid film is a solvent). In this case, it is separated from the dissolution tank, and for example, both are communicated by a guide tube (for powder feeding).

前記液膜形成装置3によって形成されて液膜Sとなる溶媒液は、前記溶解槽1の上方に設置した定水位槽4と該液膜形式装置3との間に介在させた導通路5を通じて前記定水位槽4から供給される。   The solvent liquid which is formed by the liquid film forming apparatus 3 and becomes the liquid film S passes through a conduction path 5 interposed between the constant water level tank 4 installed above the dissolution tank 1 and the liquid film type apparatus 3. Supplied from the constant water level tank 4.

導通路5は、前記溶解槽1と通じる上端の導入口5aを前記定水位槽4内の上下方向の中間位置に配置し、下端の注液口5bを前記液膜形成装置3の直上に配置して定水位槽4の隣接位置に設け(実施例では管体を定水位槽4に装入配設して隣接位置に設けてある)、前記注液口5bを、定水位槽4内に装置した図示省略したレベルスイッチに連係して開閉するようにし、レベルスイッチからの指令信号によって開放して溶解槽1からの分散溶媒液を注液口5bから排出し、前記の通り、前記液膜形式装置3に供給して液膜とする。   The conducting path 5 has an upper inlet port 5 a communicating with the dissolution tank 1 disposed at an intermediate position in the vertical direction in the constant water level tank 4, and a lower liquid inlet 5 b disposed immediately above the liquid film forming apparatus 3. Then, it is provided at a position adjacent to the constant water level tank 4 (in the embodiment, the pipe body is inserted and disposed in the constant water level tank 4 and provided at the adjacent position), and the liquid injection port 5b is provided in the constant water level tank 4 It opens and closes in conjunction with the level switch (not shown) of the apparatus, is opened by a command signal from the level switch, and the dispersed solvent liquid from the dissolution tank 1 is discharged from the liquid injection port 5b. The liquid is supplied to the format device 3 to form a liquid film.

定水位槽4は、導通路5の前記導入口5aより下方位置に設けた供液口8を通じて溶媒液供給源13から調節弁12を介して溶媒液が注入、供給されるようになっており、越流堰9(管体を定水位槽4内に装入配設して構成してあるが、その構造は自由に選択すれば良い)を備えて当該定水位槽4、すなわち溶媒液を一定の水位において収容する槽(タンク)を構成せしめ、越流堰(仕切り材)9の上端9aを前記導入口5aより上方に位置させ、越流堰9を溶媒液が流下する状態時には前記レベルスイッチの注液口5bの開放指示により前記導入口5aを通じて導通路5内に溶媒液が流れる関係にしてある。   In the constant water level tank 4, the solvent liquid is injected and supplied from the solvent liquid supply source 13 through the control valve 12 through the liquid supply port 8 provided below the introduction port 5 a of the conduction path 5. , The overflow weir 9 (which is constructed by charging and arranging the pipe body in the constant water level tank 4, but the structure may be freely selected), and the constant water level tank 4, that is, the solvent liquid A tank (tank) that accommodates at a constant water level is constructed, the upper end 9a of the overflow weir (partition material) 9 is positioned above the introduction port 5a, and the level when the solvent liquid flows down the overflow weir 9 In response to an instruction to open the liquid injection port 5b of the switch, the solvent liquid flows into the conduction path 5 through the introduction port 5a.

前記レベルスイッチは、この越流堰9の上端9a位置まで供液口8から供給される溶媒液の水位が上昇したとき、これを検知して前記注液口5bの開放と同時又は時間差を於いて前記収容部2の排出口2aを開放状態にさせ、収容部2から前記液膜S部へと粉末を供給する。   The level switch detects when the water level of the solvent liquid supplied from the liquid supply port 8 rises to the position of the upper end 9a of the overflow weir 9, and detects this when the liquid injection port 5b is opened or at a time difference. Then, the discharge port 2a of the container 2 is opened, and the powder is supplied from the container 2 to the liquid film S part.

また、前記越流堰9から流下する溶媒液は分流路10を通じて前記溶解槽1の溶解部1aに連通させ、前記供液口8は系路中に前記の通り調節弁12を介して溶媒液供給源13に連通させてある。   Further, the solvent liquid flowing down from the overflow weir 9 is communicated with the dissolving portion 1a of the dissolution tank 1 through the diversion channel 10, and the liquid supply port 8 is connected to the solvent liquid via the control valve 12 in the system path as described above. It is in communication with a supply source 13.

しかして、溶媒液供給源13からの調節弁12を通じての定水位槽4への溶媒液供給量(定水位槽4から排出される量とほぼ等量)を調節弁12で設定し、該溶媒液供給量に見合う粉末の排出口2aからの排出量を収容部2において設定して供給源13から溶媒液を送ると、調節弁12で設定した量の溶媒液が定水位槽4の給液口8を通じて送り込まれる。   Thus, the supply amount of the solvent liquid from the solvent liquid supply source 13 to the constant water level tank 4 through the adjustment valve 12 (almost equal to the amount discharged from the constant water level tank 4) is set by the adjustment valve 12, and the solvent When the amount of powder discharged from the discharge port 2 a corresponding to the amount of liquid supplied is set in the storage unit 2 and the solvent liquid is sent from the supply source 13, the amount of solvent liquid set by the control valve 12 is supplied to the constant water level tank 4. It is sent through the mouth 8.

そして、定水位槽4の越流堰9の上端位置まで該溶媒液の水位が上昇すると、レベルスイッチはこれを検知して導通路5の注液口5bと収容部2の排出口2aを開放し、注液口5bを通じて定水位槽4内の溶媒液は導通路5を経て分散溶媒液となって液膜形式装置3に供給され液膜Sとなって溶解槽1の溶解部1aへと流(落)下し、他方、レベルスイッチ6の指令によって排出口2aが開放され、かつ、該排出口2aを通じて排出可能状態にある粉末は、収容部2内に装置した排出装置によって定量的に排出口2aから排出され液膜形成装置3で形成される液膜S部に落下、接触し、液膜Sにいわば伴われて溶解部1a中に供給される。   Then, when the water level of the solvent liquid rises to the upper end position of the overflow weir 9 of the constant water level tank 4, the level switch detects this and opens the liquid injection port 5 b of the conduction path 5 and the discharge port 2 a of the storage unit 2. Then, the solvent liquid in the constant water level tank 4 is supplied to the liquid film type device 3 through the conduction path 5 and supplied to the liquid film type device 3 through the liquid inlet 5b, and becomes the liquid film S to the dissolving part 1a of the dissolving tank 1. On the other hand, the discharge port 2a is opened by the command of the level switch 6, and the powder that can be discharged through the discharge port 2a is quantitatively measured by the discharge device installed in the container 2. The liquid film S is discharged from the discharge port 2a and falls on and comes into contact with the liquid film S formed by the liquid film forming apparatus 3, and is supplied to the dissolving part 1a along with the liquid film S.

また、供液口8からは、導通路5を経て定水位槽4より排出される分散溶媒液の量より大量の溶媒液が定水位槽4に供給されるようにしてあるので、定水位槽4中に供給された溶媒液はいわば分流して越流堰9を超えて流下し、分流路10を経て溶解部1aと供給され、溶解部1a中に粉末が混合した溶媒液が適宜の水位になった時点で撹拌機を作動させることによって粉末は溶媒液によって溶解され、溶液を得るのである。   In addition, since a large amount of solvent liquid is supplied from the liquid supply port 8 to the constant water level tank 4 through the conduction path 5 than the amount of the dispersed solvent liquid discharged from the constant water level tank 4, the constant water level tank The solvent liquid supplied in 4 is divided so that it flows down over the overflow weir 9, and is supplied to the dissolving part 1a via the diversion channel 10, and the solvent liquid mixed with the powder in the dissolving part 1a has an appropriate water level. At this point, by operating the stirrer, the powder is dissolved by the solvent solution to obtain a solution.

そして、定水位槽4乃至溶解槽1への溶媒液の供給量が一定であるから、該供給量に対応させて粉末の供給量を設定することにより溶解槽1には一定濃度の溶解液が形成され、溶解槽1中より当該溶解液を取り出しつつ溶解液を連続的に得られるのである。   And since the supply amount of the solvent liquid to the constant water level tank 4 thru | or the dissolution tank 1 is constant, the dissolution liquid of a fixed density | concentration is set to the dissolution tank 1 by setting the supply amount of a powder corresponding to this supply amount. Thus, the solution can be continuously obtained while taking out the solution from the dissolution tank 1.

なお、例えば、溶媒液を水道水としたときは、供給源である元栓から送り込まれる水道水はその押送圧力が変化して調節弁12を通じての供給量が変わる場合があるが、そのようなときは溶水供給源13である前記元栓と前記調節弁12との間に圧力調整弁を設けて押送圧力を一定にさせ、調節弁12で設定した定量の水を定水位槽4へと供給できる。   For example, when the solvent liquid is tap water, tap water fed from the main plug that is the supply source may change its supply pressure and the supply amount through the control valve 12 may change. Can provide a constant amount of water set by the control valve 12 to the constant water level tank 4 by providing a pressure adjustment valve between the main plug as the dissolved water supply source 13 and the control valve 12 to make the pressure constant. .

前記液膜形式装置3は、前記導通路5を構成する導通管5Aに上下調節自在にして組付けた支持材14の下端に取付けた液膜形成材15を備え、液膜形成材15は上面を曲面状に凹ませた楕円状の輪郭形体を、前記供給口2a側の前方下りに傾斜させて構成し、曲面状の上面に溶媒液(分散液)を連続的に落下させることにより、その形態によって該形成材15の周辺に液膜Sが形成されるようにしたものである。 The liquid film forming apparatus 3 includes a liquid film forming material 15 attached to the lower end of a support material 14 that is assembled to the conducting pipe 5A constituting the conducting path 5 so as to be adjustable in the vertical direction. Is formed by inclining forward and downward on the supply port 2a side, and by continuously dropping the solvent liquid (dispersion liquid) on the curved upper surface, The liquid film S is formed around the forming material 15 depending on the form.

液膜形成材は円形状の輪郭形態を備えたものでも良く、傾斜に沿う側を長軸としたとき、長軸と短軸の長さの割合が1:1〜1:2の関係にあって、支持材14による片持ち状態における傾斜角度が水平状態を0度としたき、−15〜−20°の範囲が理想的な液膜を得られる。   The liquid film forming material may have a circular contour shape, and the ratio of the length of the major axis to the minor axis is 1: 1 to 1: 2 when the side along the slope is the major axis. Thus, an ideal liquid film can be obtained when the inclination angle in the cantilever state by the support member 14 is 0 degree in the horizontal state and is in the range of -15 to -20 °.

また、この液膜Sに対する粉体の接触は、形成材15の前方の液膜S部分で行われるから、形成材15全体が、円形や楕円形の輪郭形を備えていることは必ずしも必要としないものと考えられ、形成材15の前方側の一半の周端が円弧形(輪郭形)になっていれば良く、上面の曲面状も実施例のように中央部を凹ませた形態とは逆に突出させた形態でも不都合はない。   Further, since the powder contact with the liquid film S is performed in the liquid film S portion in front of the forming material 15, it is not always necessary that the entire forming material 15 has a circular or elliptical outline. The half of the front end of the forming material 15 only needs to have an arc shape (contour shape), and the curved surface shape of the upper surface of the forming material 15 has a shape in which the central portion is recessed as in the embodiment. There is no inconvenience even if it is made to protrude in the opposite direction.

なお、ここでいう前方側の一半とは厳密に一半である必要はなく、前端を含む前方側という意味である。   In addition, the front half here does not need to be exactly half, but means the front side including the front end.

略示説明図。Abbreviation explanatory drawing. 図1の一部拡大図。The partially expanded view of FIG.

符号の説明Explanation of symbols

1 溶解槽
2a 定量供給口
3 形成装置
5b 注液口
15 液膜形成材
DESCRIPTION OF SYMBOLS 1 Dissolution tank 2a Fixed supply port 3 Formation apparatus 5b Injection port 15 Liquid film formation material

Claims (1)

溶解槽内の上方に定量供給口を設け、該定量供給口から供給される高分子凝集剤等の粉末に接触してこれを前記溶解槽内に分散させる、溶媒液の液膜の形成装置を備えた高分子凝集剤等粉末の溶解装置において、前記形成装置を、前記定量供給口側の、前方側の一半の周端が円弧状を成し、上面が曲面状の液膜形成材を、前記溶解槽へ前記溶媒液を落下供給する注液口の直下に前方下りに傾斜させて配置して構成した、高分子凝集剤等粉末の溶解装置。 An apparatus for forming a liquid film of a solvent solution, which is provided with a quantitative supply port above the dissolution tank and contacts the powder such as a polymer flocculant supplied from the quantitative supply port and disperses the powder in the dissolution tank. In the apparatus for dissolving powder such as a polymer flocculant provided, the forming device is a liquid film forming material having a circular shape on the front side and a curved surface on the front side, on the quantitative supply port side , An apparatus for dissolving powder such as a polymer flocculant, which is arranged to be inclined forward and downward immediately below a liquid injection port for dropping and supplying the solvent liquid to the dissolution tank.
JP2003408580A 2003-12-08 2003-12-08 Polymer flocculant powder dissolution equipment Expired - Lifetime JP4384900B2 (en)

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JP4384900B2 true JP4384900B2 (en) 2009-12-16

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JP4855051B2 (en) * 2005-11-14 2012-01-18 株式会社トーケミ Polymer flocculant powder disperser
JP4745935B2 (en) 2006-10-10 2011-08-10 株式会社ヨシカワ Flocculant dissolver
KR101676046B1 (en) * 2010-09-29 2016-11-14 가부시키가이샤 요시카와 Apparatus for dissolving flocculant

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