JP4375665B2 - Friction stir welding tool - Google Patents

Friction stir welding tool Download PDF

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JP4375665B2
JP4375665B2 JP2004005564A JP2004005564A JP4375665B2 JP 4375665 B2 JP4375665 B2 JP 4375665B2 JP 2004005564 A JP2004005564 A JP 2004005564A JP 2004005564 A JP2004005564 A JP 2004005564A JP 4375665 B2 JP4375665 B2 JP 4375665B2
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friction stir
stir welding
joined
probe pin
rotor
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JP2005199281A (en
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実 阪野
正和 坂本
英俊 藤井
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Description

この発明は、アルミニウム、アルミニウム合金、マグネシウム合金、銅合金、チタン合金などの金属材料で構成された被接合部材相互を摩擦攪拌接合させるのに使用する摩擦攪拌接合用ツールに係り、特に、長期にわたって被接合部材相互を摩擦攪拌接合させることができるようにすると共に、被接合部材相互を適切に接合できるようにした点に特徴を有するものである。   The present invention relates to a friction stir welding tool used for friction stir welding of members to be joined made of a metal material such as aluminum, aluminum alloy, magnesium alloy, copper alloy, titanium alloy and the like. The present invention is characterized in that the members to be joined can be friction stir welded together and the members to be joined can be joined appropriately.

アルミニウム、アルミニウム合金、マグネシウム合金、銅合金、チタン合金などの金属材料で構成された被接合部材相互を接合させるにあたり、従来においては一般に、電気抵抗溶接、アーク溶接、ガス溶接などの溶接による方法が用いられている。   Conventionally, in joining members to be joined made of metal materials such as aluminum, aluminum alloy, magnesium alloy, copper alloy, and titanium alloy, conventionally, methods such as electric resistance welding, arc welding, and gas welding are generally used. It is used.

また、近年においては、このような溶接に代えて、摩擦攪拌接合によって被接合部材相互を接合させることが提案されている。   In recent years, it has been proposed to join members to be joined by friction stir welding instead of such welding.

ここで、摩擦攪拌接合によって被接合部材相互を接合させるにあたっては、一般に、図1に示すように、外周にねじ部(図示せず)が設けられたプローブピン12が回転子11の先端面11aから延出された摩擦攪拌接合用ツール10を用い、この摩擦攪拌接合用ツール10を高速で回転させながら、回転子11の先端面11aから延出された上記のプローブピン12を被接合部材1相互の接合部1aに圧入させると共に回転子11の先端面11aを接触させ、この状態で、摩擦攪拌接合用ツール10を被接合部材1の接合部1aに沿って移動させながら、被接合部材1相互を接合部1aに沿って順々に接合させるようになっている。   Here, in joining the members to be joined by friction stir welding, generally, as shown in FIG. 1, the probe pin 12 provided with a screw portion (not shown) on the outer periphery is the tip surface 11 a of the rotor 11. Using the friction stir welding tool 10 extended from the above, the probe pin 12 extended from the tip end surface 11a of the rotor 11 is rotated while rotating the friction stir welding tool 10 at a high speed. The members to be joined 1 are pressed into the mutual joining portions 1a and the tip end surface 11a of the rotor 11 is brought into contact, and the friction stir welding tool 10 is moved along the joining portions 1a of the members to be joined 1 in this state. They are joined together in sequence along the joint 1a.

すなわち、この摩擦攪拌接合用ツール10においては、上記のように高速で回転する回転子11やプローブピン12と被接合部材1との摩擦熱により、被接合部材1を塑性流動化させ、流動化された被接合部材1をその接合部1aにおいてプローブピン12の外周に設けられたねじ部により攪拌させるようにし、その後、これを冷却させて被接合部材1相互を接合部1aにおいて接合させるようになっている。   That is, in the friction stir welding tool 10, the member 1 to be joined is plastically fluidized and fluidized by the frictional heat between the rotor 11 and the probe pin 12 rotating at a high speed and the member 1 to be joined as described above. The joined member 1 is agitated by a screw portion provided on the outer periphery of the probe pin 12 at the joining portion 1a, and then cooled to join the joined members 1 at the joining portion 1a. It has become.

そして、このように摩擦攪拌接合により被接合部材1相互を接合させる場合、溶接に比べて、低温で被接合部材1相互を接合させることができ、接合時の熱変形や酸化による接合不良が抑制されると共に、接合部1a全体が均一に接合されるようなり、さらに異種材料の接合も容易に行えるという利点がある。   And when joining the to-be-joined members 1 mutually by friction stir welding in this way, the to-be-joined members 1 can be joined at low temperature compared with welding, and the joining defect by thermal deformation and oxidation at the time of joining is suppressed. In addition, there is an advantage that the entire joint portion 1a is uniformly joined, and that different materials can be joined easily.

ここで、上記の摩擦攪拌接合用ツール10における回転子11やプローブピン12を構成する材料としては、一般に工具鋼やダイス鋼が使用されていた。   Here, as a material constituting the rotor 11 and the probe pin 12 in the friction stir welding tool 10 described above, tool steel and die steel are generally used.

しかし、上記のように摩擦攪拌接合用ツール10を高速で回転させて、プローブピン12を被接合部材1相互の接合部に圧入させると共に回転子11の先端面を被接合部材1に接触させ、摩擦熱により被接合部材1を塑性流動化させるようにした場合、流動化された被接合部材1が回転子11やプローブピン12に溶着したり、回転子11やプローブピン12が高温になって激しく摩耗すると共に、連続して摩擦攪拌接合を行った場合、回転子11やプローブピン12が座屈したり、接合された被接合部材1の接合部1aが熱変形したりするという問題が生じた。   However, as described above, the friction stir welding tool 10 is rotated at a high speed so that the probe pin 12 is press-fitted into the joint between the members to be joined 1 and the tip surface of the rotor 11 is brought into contact with the member 1 to be joined. When the joined member 1 is plastically fluidized by frictional heat, the fluidized joined member 1 is welded to the rotor 11 or the probe pin 12, or the rotor 11 or the probe pin 12 becomes high temperature. When the friction stir welding is performed continuously, the rotor 11 and the probe pin 12 are buckled or the bonded portion 1a of the bonded member 1 is thermally deformed. .

このため、近年においては、被接合部材を強制的に冷却しながら摩擦攪拌接合させるようにしたものや(例えば、特許文献1参照。)、上記のプローブピンをFe−Cr合金で構成したもの(例えば、特許文献2参照。)が提案されている。   For this reason, in recent years, the members to be joined are subjected to friction stir welding while forcibly cooling the members to be joined (see, for example, Patent Document 1), and the probe pins are made of an Fe—Cr alloy ( For example, see Patent Document 2).

しかし、上記のように被接合部材を強制的に冷却しながら摩擦攪拌接合させるようにした場合、被接合部材の接合部分が熱変形するのが抑制されるが、依然として、流動化された被接合部材が回転子やプローブピンに溶着したり、回転子やプローブピンが激しく摩耗するという問題があった。   However, when the friction stir welding is performed while forcibly cooling the member to be bonded as described above, it is possible to suppress the thermal deformation of the bonded portion of the member to be bonded. There is a problem in that the member is welded to the rotor or the probe pin, and the rotor or the probe pin is worn extremely.

また、プローブピンをFe−Cr合金で構成した場合においても、依然として、流動化された被接合部材が回転子やプローブピンに溶着したり、回転子やプローブピンが摩耗する等の問題があった。
特開平11−226757号公報 特開2000−343243号公報
Further, even when the probe pin is made of an Fe—Cr alloy, there are still problems such as the fluidized member to be welded to the rotor and the probe pin, and the rotor and the probe pin being worn. .
JP-A-11-226757 JP 2000-343243 A

この発明は、被接合部材相互を摩擦攪拌接合させるのに使用する摩擦攪拌接合用ツールにおける上記のような問題を解決することを課題とするものである。   This invention makes it a subject to solve the above problems in the tool for friction stir welding used for friction stir welding of to-be-joined members.

すなわち、この発明においては、摩擦攪拌接合用ツールを高速で回転させ、プローブピンを被接合部材の接合部に圧入させると共に回転子の先端面を被接合部材に接触させ、摩擦熱により被接合部材を塑性流動化させ、この状態で接合部に沿ってプローブピンを移動させて、被接合部材を接合部において摩擦攪拌接合させる場合に、回転子やプローブピンに流動化された被接合部材が溶着したり、回転子やプローブピンが摩耗するのを十分に抑制すると共に、連続して摩擦攪拌接合を行った場合に、回転子やプローブピンが座屈したり、接合された被接合部材の接合部分が熱変形したりするのを抑制し、長期にわたって被接合部材を摩擦攪拌接合させることができるようにすると共に、被接合部材を接合部において適切に接合できるようにすることを課題とするものである。   That is, in this invention, the friction stir welding tool is rotated at a high speed, the probe pin is press-fitted into the joined portion of the member to be joined, and the tip surface of the rotor is brought into contact with the member to be joined, and the member to be joined is caused by frictional heat. When the probe pin is moved along the joint in this state and the member to be joined is subjected to friction stir welding at the joint, the fluidized member to be welded to the rotor or the probe pin is welded. Or the wear of the rotor or probe pin is sufficiently suppressed, and when the friction stir welding is continuously performed, the rotor or probe pin buckles or is joined to the joined parts to be joined. It is possible to prevent the member from being thermally deformed, to allow the member to be joined to be friction stir welded over a long period of time, and to appropriately join the member to be joined at the joint. It it is an object of.

この発明においては、上記のような課題を解決するため、回転する回転子11の先端面11aから延出されたプローブピン12を、被接合部材1の接合部1aに圧入させ、接合部1aに沿ってプローブピン12移動させて、接合部1aにおいて被接合部材を摩擦攪拌接合させる摩擦攪拌接合用ツールにおいて、少なくとも上記の被接合部材1と接触するプローブピン12及び回転子11の部分を、Coを5〜18重量%含有し、且つ熱伝導率が60W/m・K以上であるWC系の超硬合金で構成した。 In the present invention, in order to solve the above-described problems, the probe pin 12 extended from the distal end surface 11a of the rotating rotor 11 is press-fitted into the joint 1a of the member 1 to be joined, and the joint 1a is inserted into the joint 1a. In the friction stir welding tool for moving the probe pin 12 along the friction stir welding of the member to be joined at the joint 1a, at least the probe pin 12 and the rotor 11 in contact with the member to be joined 1 are the containing 5 to 18 wt%, and the thermal conductivity was composed of cemented carbide WC-based is 60 W / m · K or more.

この発明における摩擦攪拌接合用ツールのように、少なくとも被接合部材と接触するプローブピン及び回転子の部分を、Coを5〜18重量%含有するWC系の超硬合金で構成すると、被接合部材とプローブピンや回転子との親和性が低くなり、この摩擦攪拌接合用ツールを高速で回転させ、プローブピンを被接合部材の接合部に圧入させると共に回転子の先端面を接触させて、摩擦熱により被接合部材を塑性流動化させる場合に、流動化された被接合部材がプローブピンや回転子に溶着するのが抑制されると共に、摩擦によるプローブピンや回転子の摩耗も少なくなる。   As in the friction stir welding tool according to the present invention, at least the probe pin and the rotor that are in contact with the member to be joined are composed of a WC-based cemented carbide containing 5 to 18% by weight of Co. The friction stir welding tool is rotated at high speed, the probe pin is press-fitted into the joint of the member to be joined, and the tip of the rotor is brought into contact with the friction stir welding tool. When the member to be welded is plastically fluidized by heat, the fluidized member to be welded is suppressed from welding to the probe pin and the rotor, and wear of the probe pin and the rotor due to friction is reduced.

また、上記のように熱伝導率が60W/m・K以上の超硬合金を用いると、連続して摩擦攪拌接合を行った場合においても、熱がプローブピンや回転子を通して効率よく外部に拡散・放出されるようになり、回転子やプローブピンが座屈したり、接合された被接合部材の接合部が熱変形したりするのが抑制されるようになる。 In addition, when a cemented carbide with a thermal conductivity of 60 W / m · K or more is used as described above , even when friction stir welding is continuously performed, heat is efficiently diffused to the outside through the probe pin and the rotor. -It will be discharge | released and it will become possible to suppress that a rotor and a probe pin buckle and that the junction part of the to-be-joined member to be joined thermally deforms.

この結果、この発明における摩擦攪拌接合用ツールを使用すると、長期にわたって被接合部材を摩擦攪拌接合させることができるようになると共に、被接合部材相互が適切に接合されるようになる。   As a result, when the friction stir welding tool according to the present invention is used, the members to be welded can be friction stir welded over a long period of time, and the members to be joined can be joined appropriately.

以下、この発明の実施形態に係る摩擦攪拌接合用ツールを添付図面に基づいて具体的に説明する。   Hereinafter, a friction stir welding tool according to an embodiment of the present invention will be specifically described with reference to the accompanying drawings.

この実施形態に係る摩擦攪拌接合用ツール10においては、図2に示すように、回転子11の先端面11aからプローブピン12を延出させる一方、このプローブピン12と反対側に、回転装置(図示せず)に取り付けられる径大になったシャンク部13を設け、上記のプローブピン12の外周に摩擦攪拌接合用ツール10の回転方向とは逆ねじれになったねじ部12aを形成すると共に、上記の回転子11の先端面11aを外周側からプローブピン12が設けられた中心に向けて凹むように形成している。   In the friction stir welding tool 10 according to this embodiment, as shown in FIG. 2, the probe pin 12 is extended from the tip end surface 11 a of the rotor 11, while the rotating device ( A shank portion 13 having a large diameter to be attached to the probe pin 12 is provided, and a thread portion 12a that is reversely twisted in the rotational direction of the friction stir welding tool 10 is formed on the outer periphery of the probe pin 12, The tip surface 11a of the rotor 11 is formed to be recessed from the outer peripheral side toward the center where the probe pin 12 is provided.

ここで、この実施形態における摩擦攪拌接合用ツール10においては、図3に示すように、上記の回転子11とプローブピン12とシャンク部13全体とを、Coを5〜18重量%含有するWC系の超硬合金で一体に形成している。なお、Coの含有量が5〜18重量%になったWC系の超硬合金を用いるのは、Coの含有量が5重量%未満であると、この摩擦攪拌接合用ツール10が折損しやすくなる一方、Coの含有量が18重量%を越えると、摩擦攪拌接合により被接合部材1相互を接合させる場合に、回転子11やプローブピン12に被接合部材1が溶着しやすくなるためである。   Here, in the friction stir welding tool 10 in this embodiment, as shown in FIG. 3, the rotator 11, the probe pin 12, and the entire shank portion 13 are WC containing 5 to 18 wt% Co. It is integrally formed of a cemented carbide. The WC cemented carbide having a Co content of 5 to 18% by weight is used because the friction stir welding tool 10 is easily broken when the Co content is less than 5% by weight. On the other hand, if the Co content exceeds 18% by weight, the member 1 to be bonded is easily welded to the rotor 11 or the probe pin 12 when the members to be bonded 1 are bonded to each other by friction stir welding. .

そして、この実施形態における摩擦攪拌接合用ツール10を用いて被接合部材1を接合部1aにおいて摩擦攪拌接合させるにあたっては、従来の摩擦攪拌接合用ツール10と同様に、図1に示すように、この摩擦攪拌接合用ツール10を高速で回転させながら、上記のプローブピン12を被接合部材1相互の接合部1aに圧入させると共に、回転子11の先端面11aを接触させ、回転する回転子11やプローブピン12と被接合部材1との摩擦熱により、接合部1aにおける被接合部材1を塑性流動化させる。そして、このように流動化された被接合部材1をプローブピン12の外周に設けられたねじ部12aにより攪拌させ、この状態で摩擦攪拌接合用ツール10を被接合部材1の接合部1aに沿って移動させて、被接合部材1相互を接合部1aに沿って順々に接合させるようにする。   Then, in the friction stir welding of the member 1 to be welded at the joint 1a using the friction stir welding tool 10 in this embodiment, as in the conventional friction stir welding tool 10, as shown in FIG. While rotating the friction stir welding tool 10 at a high speed, the probe pin 12 is press-fitted into the joint 1a between the members 1 to be joined, and the tip 11a of the rotor 11 is brought into contact with the rotor 11 to rotate. Further, the member 1 to be joined in the joining portion 1a is plastically fluidized by frictional heat between the probe pin 12 and the member 1 to be joined. Then, the fluidized member 1 thus fluidized is agitated by the screw portion 12a provided on the outer periphery of the probe pin 12, and the friction stir welding tool 10 is moved along the joint 1a of the member 1 in this state. The members to be joined 1 are joined together in order along the joining portion 1a.

ここで、この実施形態における摩擦攪拌接合用ツール10においては、上記のように回転子11とプローブピン12とシャンク部13全体とを、Coを5〜18重量%含有するWC系の超硬合金で一体に形成しているため、被接合部材1とプローブピン12や回転子11との親和性が低く、上記のようにして被接合部材1を接合部1aに沿って摩擦攪拌接合させる場合に、被接合部材1がプローブピン12や回転子11に溶着するのが抑制されると共に、摩擦によるプローブピン12や回転子11の摩耗も少なくなる。   Here, in the friction stir welding tool 10 in this embodiment, as described above, the rotor 11, the probe pin 12, and the entire shank portion 13 are WC-based cemented carbide containing 5 to 18% by weight of Co. In the case where the member 1 to be joined and the probe pin 12 or the rotor 11 have low affinity, the member 1 to be joined is friction stir welded along the joint 1a as described above. The welded member 1 is suppressed from being welded to the probe pin 12 and the rotor 11, and the wear of the probe pin 12 and the rotor 11 due to friction is reduced.

また、プローブピン12や回転子11やシャンク部13における熱伝導率が大幅に高くなり、連続して摩擦攪拌接合を行った場合においても、熱がプローブピン12や回転子11やシャンク部13を通して効率よく外部に拡散・放出されるようになり、プローブピン12や回転子11が座屈したり、接合された被接合部材1の接合部1aが熱変形するのが抑制される。   Further, the thermal conductivity in the probe pin 12, the rotor 11, and the shank portion 13 is significantly increased. Even when the friction stir welding is continuously performed, heat is transmitted through the probe pin 12, the rotor 11, and the shank portion 13. It is efficiently diffused / released to the outside, and the probe pin 12 and the rotor 11 are prevented from buckling and the joined portion 1a of the joined member 1 to be joined is prevented from being thermally deformed.

また、この実施形態における摩擦攪拌接合用ツール10において、流動化された被接合部材1をプローブピン12の外周に設けられたねじ部12aにより攪拌させる場合に、このねじ部12aが上記のように摩擦攪拌接合用ツール10の回転方向とは逆ねじれになっているため、流動化された被接合部材1がねじ部12aの作用により下方に押し付けられるようになり、また回転子11の先端面11aを上記のように外周側からプローブピン12が設けられた中心に向けて凹むように形成しているため、流動化された被接合部材1が接合部1aから外側に流れ出るのが抑制されるようになり、空洞などが形成されることなく、被接合部材1相互が接合部1aにおいて均一に接合されるようになる。   Further, in the friction stir welding tool 10 in this embodiment, when the fluidized member 1 is agitated by the screw portion 12a provided on the outer periphery of the probe pin 12, the screw portion 12a is as described above. Since the direction of rotation of the friction stir welding tool 10 is opposite to the rotational direction, the fluidized member 1 is pressed downward by the action of the screw portion 12a, and the tip end surface 11a of the rotor 11 is pressed. Is recessed from the outer peripheral side toward the center where the probe pin 12 is provided as described above, so that the fluidized joined member 1 is prevented from flowing out from the joining portion 1a. Thus, the members 1 to be joined can be uniformly joined at the joint 1a without forming a cavity or the like.

なお、この実施形態における摩擦攪拌接合用ツール10においては、回転子11とプローブピン12とシャンク部13全体とを上記のような超硬合金で一体に形成したため、上記のように熱がプローブピン12や回転子11やシャンク部13を通して効率よく外部に拡散・放出されるようになるが、材料コストが高くつくようになる。このため、図4に示すように、回転子11とプローブピン12とシャンク部13の一部13aを上記のような超硬合金で一体に形成する一方、シャンク部13の残りの部分13bを工具鋼やダイス鋼で構成し、これらをろう付け等により接合させ、上記の超硬合金の部分を少なくして、コストを低減させることも可能である。   In the friction stir welding tool 10 in this embodiment, since the rotor 11, the probe pin 12, and the entire shank portion 13 are integrally formed of the above cemented carbide, the heat is generated as described above. 12 and the rotor 11 and the shank portion 13 are efficiently diffused and discharged to the outside, but the material cost is high. Therefore, as shown in FIG. 4, the rotor 11, the probe pin 12, and a part 13 a of the shank part 13 are integrally formed of the above cemented carbide, while the remaining part 13 b of the shank part 13 is formed as a tool. It is also possible to reduce the cost by using steel or die steel and joining them by brazing or the like to reduce the above-mentioned cemented carbide portion.

さらに、図5に示すように、長く伸びた回転子11とプローブピン12とを上記のような超硬合金で一体に形成すると共に、長く伸びた回転子11の後部側に係止部11bを切り欠き形成する一方、工具鋼やダイス鋼で構成されたシャンク部13に、係止部11bが設けられた上記の回転子11の後部側を挿入させる収容部13cを設け、この収容部13c内に回転子11の後部側を挿入させると共に、収容部13c内に挿入された回転子11の係止部11bにねじ14を押し付けて、回転子11とプローブピン12とが一体に形成されたものをシャンク部13に固定させるようにすることも可能である。このようにすると、超硬合金の部分を少なくしてコストを低減させることができ、また回転子11やプローブピン12が摩耗した場合等においても、長く伸びた回転子11とプローブピン12とが一体に形成されたものだけを簡単に交換することができ、さらにコストが低減されると共に、プローブピン12の径や長さ等を変更させたものを複数準備しておき、これを適宜変更させて使用することもできるようになる。   Further, as shown in FIG. 5, the elongated rotor 11 and the probe pin 12 are integrally formed of the above cemented carbide, and a locking portion 11 b is provided on the rear side of the elongated rotor 11. While the notch is formed, a housing portion 13c for inserting the rear side of the rotor 11 provided with the locking portion 11b is provided in the shank portion 13 made of tool steel or die steel. The rotor 11 and the probe pin 12 are integrally formed by inserting the screw 14 against the engaging portion 11b of the rotor 11 inserted into the accommodating portion 13c. Can be fixed to the shank portion 13. In this way, the cost can be reduced by reducing the portion of the cemented carbide, and even when the rotor 11 and the probe pin 12 are worn out, the rotor 11 and the probe pin 12 that are elongated are formed. It is possible to easily replace only the one formed integrally, further reducing the cost, and preparing a plurality of probe pins 12 with different diameters, lengths, etc., and changing them accordingly. Can also be used.

また、この実施形態における摩擦攪拌接合用ツール10において、被接合部材1と接触するプローブピン12や回転子11の部分をTiN,TiCN,TiAlN,CrN,DLC(ダイヤモンドライクカーボン)等で被覆すると、上記のようにして被接合部材1相互を摩擦攪拌接合させる場合に、回転子11やプローブピン12に被接合部材1が溶着するのがより一層抑制されるようになる。   Further, in the friction stir welding tool 10 in this embodiment, when the portions of the probe pin 12 and the rotor 11 that are in contact with the member to be joined 1 are covered with TiN, TiCN, TiAlN, CrN, DLC (diamond-like carbon), etc., When the members 1 to be joined are friction stir welded as described above, the welding of the members 1 to the rotor 11 and the probe pins 12 is further suppressed.

次に、この発明の実施例に係る具体的な摩擦攪拌接合用ツールを用いて被接合部材を接合させた場合と比較例の摩擦攪拌接合用ツールを用いて被接合部材を接合させた場合とを比較し、この発明の実施例に係る摩擦攪拌接合用ツールが優れていることを明らかにする。   Next, the case where the member to be joined is joined using the specific friction stir welding tool according to the embodiment of the present invention and the case where the member to be joined is joined using the friction stir welding tool of the comparative example And the friction stir welding tool according to the embodiment of the present invention is clarified.

(実施例1)
実施例1においては、WCの平均粒度が2〜3μm、ロックウェル硬度AスケールHRAが88.5、熱伝導率が67W/m・KになったCoが12重量%含有されたWC系の超硬合金を用い、上記の実施形態に示すように、回転子11とプローブピン12とシャンク部13全体とを上記の超硬合金で一体に形成した摩擦攪拌接合用ツールを作製した。なお、熱伝導率については、レーザーフラッシュにより測定した。
Example 1
In Example 1, the average particle size of WC is 2 to 3 μm, the Rockwell hardness A scale HRA is 88.5, and the thermal conductivity is 67 W / m · K. Using a hard alloy, as shown in the above embodiment, a friction stir welding tool in which the rotor 11, the probe pin 12, and the entire shank portion 13 were integrally formed of the above cemented carbide was produced. The thermal conductivity was measured with a laser flash.

(実施例2)
実施例2においては、WCの平均粒度が2〜3μm、ロックウェル硬度AスケールHRAが91.5、熱伝導率が72W/m・KになったCoが7重量%含有されたWC系の超硬合金を用い、それ以外は、上記の実施例1の場合と同様にして摩擦攪拌接合用ツールを作製した。
(Example 2)
In Example 2, the average particle size of WC is 2 to 3 μm, Rockwell hardness A scale HRA is 91.5, and the thermal conductivity is 72 W / m · K. A friction stir welding tool was prepared in the same manner as in Example 1 except that a hard alloy was used.

参考例1
参考例1においては、WCの平均粒度が0.8μm、ロックウェル硬度AスケールHRAが92.0、熱伝導率が47W/m・KになったCoが13重量%含有されたWC系の超硬合金を用い、それ以外は、上記の実施例1の場合と同様にして摩擦攪拌接合用ツールを作製した。
( Reference Example 1 )
In Reference Example 1 , the average particle size of WC is 0.8 μm, the Rockwell hardness A scale HRA is 92.0, and the thermal conductivity is 47 W / m · K. A friction stir welding tool was prepared in the same manner as in Example 1 except that a hard alloy was used.

(実施例
実施例においては、WCの平均粒度が5μm、ロックウェル硬度AスケールHRAが87.0、熱伝導率が71W/m・KになったCoが10重量%含有されたWC系の超硬合金を用い、それ以外は、上記の実施例1の場合と同様にして摩擦攪拌接合用ツールを作製した。
(Example 3 )
In Example 3 , a WC cemented carbide containing WC with a mean particle size of 5 μm, Rockwell hardness A scale HRA of 87.0, and thermal conductivity of 71 W / m · K containing 10 wt% Co. Otherwise, a friction stir welding tool was prepared in the same manner as in Example 1 above.

(実施例
実施例においては、WCの平均粒度が2〜3μm、ロックウェル硬度AスケールHRAが87.5、熱伝導率が63W/m・KになったCoが15重量%含有されたWC系の超硬合金を用い、それ以外は、上記の実施例1の場合と同様にして摩擦攪拌接合用ツールを作製した。
(Example 4 )
In Example 4 , the average particle size of WC is 2 to 3 μm, the Rockwell hardness A scale HRA is 87.5, and the thermal conductivity is 63 W / m · K. A friction stir welding tool was prepared in the same manner as in Example 1 except that a hard alloy was used.

(比較例1)
比較例1においては、ロックウェル硬度CスケールHRCが57、熱伝導率が24W/m・Kの工具鋼を用い、それ以外は、上記の実施例1の場合と同様にして摩擦攪拌接合用ツールを作製した。
(Comparative Example 1)
In Comparative Example 1, a tool for friction stir welding was used in the same manner as in Example 1 except that tool steel having Rockwell hardness C scale HRC of 57 and thermal conductivity of 24 W / m · K was used. Was made.

(比較例2)
比較例2においては、WCの平均粒度が2〜3μm、ロックウェル硬度AスケールHRAが85.5、熱伝導率が58W/m・KになったCoが20重量%含有されたWC系の超硬合金を用い、それ以外は、上記の実施例1の場合と同様にして摩擦攪拌接合用ツールを作製した。
(Comparative Example 2)
In Comparative Example 2, a WC super-particle containing 20 wt% Co having an average particle size of WC of 2 to 3 μm, Rockwell hardness A scale HRA of 85.5, and thermal conductivity of 58 W / m · K. A friction stir welding tool was prepared in the same manner as in Example 1 except that a hard alloy was used.

(比較例3)
比較例3においては、WCの平均粒度が4〜5μm、ロックウェル硬度AスケールHRAが84.0、熱伝導率が68W/m・KになったCoが22重量%含有されたWC系の超硬合金を用い、それ以外は、上記の実施例1の場合と同様にして摩擦攪拌接合用ツールを作製した。
(Comparative Example 3)
In Comparative Example 3, the average particle size of WC is 4-5 μm, Rockwell hardness A scale HRA is 84.0, and the thermal conductivity is 68 W / m · K. A friction stir welding tool was prepared in the same manner as in Example 1 except that a hard alloy was used.

そして、被接合部材1として、厚みが4mmになったJIS5000系のアルミニウムで構成された板材を、図6に示すように四角筒状に折り曲げて両端部を突き合わせ、突き合わせた接合部1aの長さが300mmになったものを使用し、上記の実施例1及び比較例1の各摩擦攪拌接合用ツールを用い、回転数1200rpm、送り速度300mm/minの条件で、上記の被接合部材1における接合部1aを摩擦攪拌接合させるようにした。   Then, as a member 1 to be joined, a plate material made of JIS 5000 aluminum having a thickness of 4 mm is folded into a rectangular tube shape as shown in FIG. Using the friction stir welding tools of Example 1 and Comparative Example 1 described above, and joining in the member 1 to be joined under the conditions of a rotational speed of 1200 rpm and a feed rate of 300 mm / min. Part 1a was friction stir welded.

この結果、比較例1の摩擦攪拌接合用ツールにおいては、プローブピン12や回転子11の先端面11aに被接合部材1の溶着があり、約1500個の被接合部材1を摩擦攪拌接合させた時点で、プローブピン12の先端及びねじ部12aの摩耗が大きくなって寿命になった。これに対して、実施例1の摩擦攪拌接合用ツールにおいては、プローブピン12に被接合部材1が殆ど溶着することなく、約10000個の被接合部材1を摩擦攪拌接合させることができた。   As a result, in the friction stir welding tool of Comparative Example 1, the welded member 1 was welded to the probe pin 12 or the tip surface 11a of the rotor 11, and about 1500 welded members 1 were friction stir welded. At that time, wear of the tip of the probe pin 12 and the threaded portion 12a increased, and the service life was reached. On the other hand, in the friction stir welding tool of Example 1, approximately 10,000 welded members 1 could be friction stir welded with almost no welded member 1 welded to the probe pin 12.

また、被接合部材1として、厚みが3mmになったJIS6000系のアルミニウムで構成された板材を、図7に示すように2枚突き合わせ、突き合わせた接合部1aの長さが3mになったものを使用し、上記の実施例1〜5及び比較例1〜3の各摩擦攪拌接合用ツールを用い、回転数1500rpm、送り速度1000mm/minの条件で、上記の被接合部材1における接合部1aを摩擦攪拌接合させるようにした。   In addition, as the member 1 to be joined, two plate members made of JIS 6000 series aluminum having a thickness of 3 mm are butted as shown in FIG. 7, and the length of the joined portion 1a is 3 m. Using the above-mentioned tools for friction stir welding in Examples 1 to 5 and Comparative Examples 1 to 3 above, the joining portion 1a in the above-mentioned joined member 1 is used under the conditions of a rotational speed of 1500 rpm and a feed rate of 1000 mm / min. Friction stir welding was performed.

この結果、比較例1の摩擦攪拌接合用ツールにおいては、摩擦攪拌接合させた接合部1aの合計長さが約3000m(約1000個の接合)になった時点で、プローブピン12の先端及びねじ部12aの摩耗が大きくなって寿命になった。これに対して、実施例1の摩擦攪拌接合用ツールにおいては、接合部1aの合計長さが約15000m(約5000個の接合)になるまで摩擦攪拌接合させることができた。   As a result, in the friction stir welding tool of Comparative Example 1, when the total length of the joints 1a subjected to the friction stir welding reaches about 3000 m (about 1000 joints), the tip of the probe pin 12 and the screw The wear of the portion 12a was increased and the service life was reached. On the other hand, in the friction stir welding tool of Example 1, the friction stir welding could be performed until the total length of the joint portion 1a reached about 15000 m (about 5000 pieces).

また、上記のようにして実施例1〜4、参考例1及び比較例1〜3の各摩擦攪拌接合用ツールを用い、被接合部材1における接合部1aを摩擦攪拌接合させた場合において、各摩擦攪拌接合用ツールにおけるプローブピン12や回転子11の先端面11aへの被接合部材1の溶着の有無を調べると共に、被接合部材1の接合部1aにおける変形を調べ、比較例1の摩擦攪拌接合用ツールを用いた場合における変形量を1とした指数で、各摩擦攪拌接合用ツールを用いた場合における変形量を算出し、その結果を下記の表1に示した。 In addition, when using the friction stir welding tools of Examples 1 to 4, Reference Example 1 and Comparative Examples 1 to 3 as described above, the joint 1a in the member to be joined 1 was friction stir welded. In the friction stir welding tool, the presence or absence of welding of the member 1 to be welded to the probe pin 12 or the tip surface 11a of the rotor 11 is examined, and the deformation in the joint 1a of the member 1 to be welded is examined. The deformation amount when each friction stir welding tool was used was calculated by an index with the deformation amount when the welding tool was used as 1, and the results are shown in Table 1 below.

Figure 0004375665
Figure 0004375665

この結果から明らかなように、Coを含有するWC系の超硬合金を用いた実施例1〜4、参考例1及び比較例2,3の各摩擦攪拌接合用ツールを用いた場合、工具鋼を用いた比較例1の摩擦攪拌接合用ツールに比べて、摩擦攪拌接合させた被接合部材1における接合部1aの変形量が少なくなっており、特に、熱伝導率が60W/m・K以上の超硬合金を用いた実施例1〜4及び比較例3の各摩擦攪拌接合用ツールを用いた場合には、その変形量がさらに少なくなっていた。 As is clear from this result, when the friction stir welding tools of Examples 1 to 4, Reference Example 1 and Comparative Examples 2 and 3 using WC-based cemented carbide containing Co are used, tool steel Compared to the friction stir welding tool of Comparative Example 1 using the above, the amount of deformation of the joined portion 1a in the joined member 1 subjected to friction stir welding is reduced, and in particular, the thermal conductivity is 60 W / m · K or more. When the friction stir welding tools of Examples 1 to 4 and Comparative Example 3 using the above cemented carbides were used, the amount of deformation was further reduced.

また、Coの含有量が18重量%以下のWC系の超硬合金を用いた実施例1〜4及び参考例1の各摩擦攪拌接合用ツールを用いた場合、工具鋼を用いた比較例1の摩擦攪拌接合用ツールや、Coの含有量が18重量%を越えるWC系の超硬合金を用いた比較例2,3の各摩擦攪拌接合用ツールに比べて、プローブピン12や回転子11の先端面11aへの被接合部材1の溶着が少なくなっていた。
Further, when the friction stir welding tools of Examples 1 to 4 and Reference Example 1 using a WC-based cemented carbide having a Co content of 18% by weight or less were used, Comparative Example 1 using tool steel Compared to the friction stir welding tool of No. 1 and the friction stir welding tools of Comparative Examples 2 and 3 using a WC cemented carbide with a Co content exceeding 18% by weight, the probe pin 12 and the rotor 11 are compared. The welded member 1 was less welded to the tip surface 11a.

摩擦攪拌接合用ツールを用いて被接合部材相互を接合部において摩擦攪拌接合させる状態を示した概略説明図である。It is the schematic explanatory drawing which showed the state which joins to-be-joined members in a friction stir welding in a junction part using the tool for friction stir welding. この発明の一実施形態に係る摩擦攪拌接合用ツールの概略正面図である。It is a schematic front view of the tool for friction stir welding which concerns on one Embodiment of this invention. 同実施形態に係る摩擦攪拌接合用ツールの概略断面図である。It is a schematic sectional drawing of the tool for friction stir welding concerning the embodiment. 同実施形態に係る摩擦攪拌接合用ツールの第1の変更例を示した概略断面図である。It is the schematic sectional drawing which showed the 1st modification of the tool for friction stir welding which concerns on the same embodiment. 同実施形態に係る摩擦攪拌接合用ツールの第2の変更例を示した概略断面図である。It is the schematic sectional drawing which showed the 2nd modification of the tool for friction stir welding which concerns on the same embodiment. この発明の実施例及び比較例の摩擦攪拌接合用ツールを用いて摩擦攪拌接合させる第1の被接合部材を示した斜視図である。It is the perspective view which showed the 1st to-be-joined member made to friction stir weld using the tool for friction stir welding of the Example and comparative example of this invention. この発明の実施例及び比較例の摩擦攪拌接合用ツールを用いて摩擦攪拌接合させる第2の被接合部材を示した斜視図である。It is the perspective view which showed the 2nd to-be-joined member made to friction stir weld using the tool for friction stir welding of the Example and comparative example of this invention.

符号の説明Explanation of symbols

1 被接合部材
1a 接合部
10 摩擦攪拌接合用ツール
11 回転子
11a 回転子の先端面
12 プローブピン
13 シャンク部
DESCRIPTION OF SYMBOLS 1 To-be-joined member 1a Joining part 10 Friction stir welding tool 11 Rotor 11a End face of rotor 12 Probe pin 13 Shank part

Claims (1)

回転する回転子11の先端面11aから延出されたプローブピン12を、被接合部材1の接合部1aに圧入させ、この接合部1aに沿ってプローブピン12を移動させて、接合部1aにおいて被接合部材1を摩擦攪拌接合させる摩擦攪拌接合用ツールにおいて、少なくとも上記の被接合部材1と接触するプローブピン12及び回転子11の部分を、Coを5〜18重量%含有し、且つ熱伝導率が60W/m・K以上であるWC系の超硬合金で構成したことを特徴とする摩擦攪拌接合用ツール。 The probe pin 12 extended from the front end surface 11a of the rotating rotor 11 is press-fitted into the joint portion 1a of the member 1 to be joined, and the probe pin 12 is moved along the joint portion 1a. In the friction stir welding tool for friction stir welding the member 1 to be joined, at least the probe pin 12 and the rotor 11 in contact with the member 1 to be joined contain 5 to 18% by weight of Co and heat conduction A friction stir welding tool comprising a WC cemented carbide having a rate of 60 W / m · K or more.
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