JP3762507B2 - Vacuum leakage inspection method for vacuum packaged products - Google Patents

Vacuum leakage inspection method for vacuum packaged products Download PDF

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Publication number
JP3762507B2
JP3762507B2 JP35584196A JP35584196A JP3762507B2 JP 3762507 B2 JP3762507 B2 JP 3762507B2 JP 35584196 A JP35584196 A JP 35584196A JP 35584196 A JP35584196 A JP 35584196A JP 3762507 B2 JP3762507 B2 JP 3762507B2
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Japan
Prior art keywords
vacuum
weight
packaged product
inspection method
leakage
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Expired - Fee Related
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JP35584196A
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Japanese (ja)
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JPH10181720A (en
Inventor
源治 堀田
隆司 山田
浩之 猿渡
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Nippon Steel Texeng Co Ltd
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Nittetsu Elex Co Ltd
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Priority to JP35584196A priority Critical patent/JP3762507B2/en
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Description

【0001】
【発明の属する技術分野】
本発明は真空容積が比較的多い真空包装品、たとえば真空を利用した断熱パネルなどの製造工程において、製品の真空漏洩を全数検査する方法に関する。
【0002】
【従来の技術】
真空包装品は種々の分野において使用されており、特にプラスチックのラミネートフィルムの袋を真空容器とする真空包装品は従来の食品分野などに止まらず近年適用分野がますます広くなっている。たとえば硬質の発泡プラスチックの板をプラスチックなどからなるラミネートフィルムで包装し、内部を真空にした断熱パネルがある。このような断熱パネルは冷蔵庫やさらに進んでは建築物の断熱構造などにも適用が検討されている。
【0003】
このような真空包装品にあっては信頼性確保のため製品の全数について真空漏洩を検査することが必要である。従来からの検査方法は真空包装品を真空チャンバー内に入れることにより、真空不良品が膨れることで判別していた。しかしながら真空チャンバーは高価であり、とくに大型のパネルを入れるようなものは耐圧構造のため大がかりな設備になる。また大容量の真空ポンプを常時運転する必要があり、動力費も大きなものになる。
【0004】
【発明が解決しようとする課題】
本発明は上記のような断熱パネルなどの真空包装品の製造工程において、製品の真空漏洩の検査を簡単な設備で行なう方法を提供することを課題とする。
【0005】
【課題を解決するための手段】
本発明は前記課題を解決するものであって、嵩密度が0.5g/cm 以下の真空包装品について真空包装直後にその重量を測定し、さらに大気中に置いた状態で時間が経過後に再び同一の真空包装品の重量を測定して前記の前後の重量の測定値を比較し、後の測定における重量の増大によって真空の漏洩を判断することを特徴とする真空包装品の真空漏洩検査方法である。またここにおいて、前記の真空包装品が連続気泡の発泡体の板をラミネートフィルムで包装した断熱パネルであることも特徴とする。
【0006】
【発明の実施の形態】
本発明は真空包装品が真空漏洩したとき、真空容積部分に相当する空気の重量分だけ重くなることを検知するものである。窒素と酸素の比率で分配した空気の平均分子量は28.8であるから、0℃、1気圧で22.4リットルの空気の重量は28.8gとなる。したがってたとえば真空容積10リットルの真空包装品であれば完全に漏洩した場合、12.9gの重量増加となる。さらに実際には空気中の水分の影響もある。これについては水の分子量は18で酸素や窒素の分子量より小さいので単純に考えると真空漏洩による重量増加を少なくする方向に作用するように予想される。しかしながら本発明者らによる前記の断熱パネルについての実験では湿り空気の方が乾燥空気の場合より重量増加が大きい。これは断熱パネルを真空にした時点では内部の発泡体は乾燥状態にあり、これの表面積が大きいためあたかも乾燥剤のように作用して真空漏洩によって侵入した空気中の水分を吸着するためと考えられる。このため水蒸気分圧に相当する分だけ侵入した空気の圧力が減少し、さらに余計に空気が侵入することになる。
【0007】
上記の真空容積10リットルの真空包装品の例において、外容積と真空容積とがほぼ等しくかつ嵩密度が0.1g/cmとすると、全重量は1kgであるから上記の空気中の水分を無視した場合の重量増加率は約1.3%となる。この程度の重量変化は天秤式の秤量装置によって十分に測定可能である。さらにこの真空容積10リットルの真空包装品の例において、嵩密度が上記より大きい0.5g/cm 全重量が5kgなら重量増加率は0.26%、嵩密度が1g/cm で全重量が10kgなら重量増加率は0.13%となるが、0.1〜0.2%程度になると工業的な重量測定設備では限界に近いといえる。したがって本発明の真空漏洩検査方法はどんな真空包装品にも万能的に用いられるものではなく、十分な真空容積を有しかつ嵩密度が比較的小さなものに適用するのが有効である。上記の真空容積の問題であるが、たとえば食肉加工品の真空パックなどに見られるように真空の空間そのものがもともと少ないものでは真空漏洩があっても侵入する空気の分量自体がわずかであり、本発明の方法は不適当である。したがって検査対象とする真空包装品の嵩密度の範囲を上に示した0.5g/cm 以下とする。
【0008】
一方、先にも述べたような断熱パネルなどは本発明の真空漏洩検査方法が特に適している。この断熱パネルは連続気泡型、すなわち隣接する気泡同士が通気できるためすべての気泡が真空排気できる発泡体の板を、プラスチックと金属フォイルの層などからなるラミネートフィルムで包装し内部を真空にしたものである。発泡体としては硬質のプラスチックのものが一般的であるが、軽石状のセラミックスの発泡体も用いることができる。このようなものは真空容積が大きく本発明の方法が有効に適用できる。一方、大型のパネルのようなものは前記のように従来から知られている真空容器に入れる方法で検査するのは困難であるので、本発明の方法は対象物によって従来の真空漏洩検査方法と相互に補完するものといえる。
【0009】
本発明の真空漏洩検査方法は真空包装後短時間内に重量を測定した後、さらに時間経過後に再び同一の真空包装品の重量を測定する。つまり同一物品の重量を追跡して測定し、前に測定した重量と参照するものである。同じ製品の大量生産ラインにおいても重量の比較は同一物品について行なうべきである。すなわち本発明の方法は1%といったオーダーの重量の相違を問題にするのであるから、同種の製品でも個々の製品の重量のばらつきによって正確な判断ができなくなるおそれがあるからである。
【0010】
先の重量測定は真空包装直後、すなわちできるだけ早くたとえば2分以内に行なうのが好ましい。真空包装後の時間が長いと真空漏れが比較的激しい場合に先の測定時にすでに重量が増加した状態になり、後の測定における重量との差が小さくなって正確な判断が困難になるからである。後の重量測定までの時間間隔は通常の場合たとえば先の重量測定から30分程度あれば良い。真空漏洩がある場合かなり急速に空気が入り込むのが普通だからである。もちろん真空包装直後の先の重量測定から丸1日といった長時間置いてから後の測定することは差し支えない。
【0011】
上記のように前後の重量測定の時間間隔が長い場合、気温や気圧の変化に伴って空気による浮力が変化して測定誤差を生ずることになる。その率は気温が10℃変動したとして273分の10、すなわち3.7%、また気圧が10ミリバール変動したとして1%である。真空包装品の外容積と真空容積とがほぼ等しい場合において10℃の温度上昇があると、真空漏洩がなくても真空が完全に漏洩した場合に起こるべき重量変化の3.7%といった割合で重量が増加することになる。真空包装品の外容積が真空容積の2倍であれば変化は上記の倍になる。しかしながら特に同じ物品を同時に複数製造する場合においては、真空漏洩のない大部分の物品で同じような重量の変化があるので特に補正の計算をしなくても誤認することはない。
【0012】
【実施例】
内部を真空にした断熱パネルに対して本発明の真空漏洩検査方法を適用した。この断熱パネルは不飽和ポリエステル樹脂の連続気泡の発泡体をアルミニウムシートをポリエステル樹脂でコーティングしたもので包装し、真空ポンプで0.05ミリバールまで吸引しつつ封じ切ったものである。外形寸法は18mm厚×650mm幅×1500mm長で真空にしたときの重量は約1480gである。
【0013】
上記のパネルで真空漏洩がないものは事実上重量の変化がないが、真空漏洩があったものの例では、30分後の測定で19.2g(1.30%)の重量増加があった。同じものの24時間後の測定において、温度、気圧の変化による浮力の変化を補償した重量増加は真空包装直後に比べ21.7g(1.47%)であった。すなわち真空漏洩があるものは比較的短時間で真空漏洩が進行し、大部分の重量増加は初期の段階で現われることがわかる。したがって通常の場合、2回目の測定は真空包装直後の測定から30分や1時間後といった比較的短い間隔で行なっても真空漏洩を検出できる。
【0014】
上記断熱パネルを工場の生産ラインで真空漏洩検査する装置の例を図1に示す。図示しない真空包装装置で内部を真空にされた断熱パネル1は比較的低速で走行するベルトコンベア3によって図示しない製品倉庫に送られる。第1の秤量装置2はベルトコンベアの入側の真空包装装置からすぐの所にあり、ベルトコンベアの脇に設置されて断熱パネルをベルトコンベアから取り込んで重量を測定したのち、ベルトコンベアに戻すようになっている。第2の秤量装置4はベルトコンベアの出側の近くにあり、ベルトコンベアの脇に設置されて第1の秤量装置と同様な方法で断熱パネルの重量を測定するようになっている。重量測定結果は演算装置5に送られ、同一の断熱パネルの第1と第2の秤量装置での測定結果を比較するとともに第1と第2の秤量装置での重量測定の間の経過時間も記録される。
【0015】
【発明の効果】
本発明の真空包装品の真空漏洩検査方法によれば、従来の検査方法の適用が困難であった内部を真空にした断熱パネルのような大型なものの検査を簡単な設備で低コストで行なうことができる。
【図面の簡単な説明】
【図1】本発明の方法を実施するための装置の例を示す図
【符号の説明】
1 断熱パネル
2 第1の秤量装置
3 ベルトコンベア
4 第2の秤量装置
5 演算装置
[0001]
BACKGROUND OF THE INVENTION
The present invention relates to a method for inspecting all products for vacuum leakage in a manufacturing process of a vacuum packaged product having a relatively large vacuum volume, for example, a heat insulating panel using vacuum.
[0002]
[Prior art]
Vacuum packaged products are used in various fields, and in particular, vacuum packaged products using plastic laminated film bags as vacuum containers are not limited to the conventional food field and the like, and their application fields are becoming increasingly widespread in recent years. For example, there is a heat insulating panel in which a hard foam plastic plate is wrapped with a laminate film made of plastic or the like and the inside is evacuated. Application of such heat insulation panels to refrigerators and further to heat insulation structures of buildings is being studied.
[0003]
In such a vacuum packaged product, it is necessary to inspect the vacuum leakage for the total number of products in order to ensure reliability. The conventional inspection method has been identified by placing a vacuum packaged product in a vacuum chamber and expanding defective products. However, the vacuum chamber is expensive, and a large-sized panel can be a large facility because of its pressure-resistant structure. Moreover, it is necessary to always operate a large-capacity vacuum pump, resulting in a large power cost.
[0004]
[Problems to be solved by the invention]
It is an object of the present invention to provide a method for inspecting a product for vacuum leakage with simple equipment in a manufacturing process of a vacuum packaged product such as a heat insulating panel as described above.
[0005]
[Means for Solving the Problems]
The present invention solves the above-mentioned problems, and the weight of a vacuum packaged product having a bulk density of 0.5 g / cm 3 or less is measured immediately after the vacuum packaging, and is further placed in the atmosphere after a lapse of time. The vacuum leakage inspection of the vacuum packaging product characterized by measuring the weight of the same vacuum packaging product again, comparing the measured values of the weight before and after the above, and judging the leakage of the vacuum by the increase in the weight in the subsequent measurement. Is the method. Here, the vacuum packaged product is also characterized in that it is a heat insulating panel in which an open-cell foam plate is wrapped with a laminate film.
[0006]
DETAILED DESCRIPTION OF THE INVENTION
In the present invention, when a vacuum packaged product leaks, it is detected that the amount of air corresponding to the vacuum volume is increased. Since the average molecular weight of air distributed by the ratio of nitrogen and oxygen is 28.8, the weight of 22.4 liters of air at 0 ° C. and 1 atm is 28.8 g. Therefore, for example, in the case of a vacuum packaged product having a vacuum volume of 10 liters, if it completely leaks, the weight increases by 12.9 g. Furthermore, there is actually an influence of moisture in the air. Regarding this, since the molecular weight of water is 18 and smaller than the molecular weight of oxygen or nitrogen, it is expected to act in the direction of reducing the weight increase due to vacuum leakage. However, in the experiment on the above-mentioned heat insulation panel by the present inventors, the increase in weight is larger in the case of humid air than in the case of dry air. This is because the foam inside is in a dry state when the heat insulation panel is evacuated, and because it has a large surface area, it acts as a desiccant to absorb moisture in the air that has entered due to vacuum leakage. It is done. For this reason, the pressure of the air which invaded by an amount corresponding to the water vapor partial pressure is reduced, and further air enters.
[0007]
In the above example of a vacuum packaged product having a vacuum volume of 10 liters, if the outer volume and the vacuum volume are substantially equal and the bulk density is 0.1 g / cm 3 , the total weight is 1 kg. When neglected, the weight increase rate is about 1.3%. Such a change in weight can be sufficiently measured by a balance-type weighing device. Further in the example of the vacuum volume 10 l vacuum packaging, the total weight of 5kg if the weight increase is 0.26% in bulk density and the larger 0.5 g / cm 3 from the above, a volume density of 1 g / cm 3 If the total weight is 10 kg, the rate of weight increase will be 0.13%, but if it is about 0.1-0.2%, it can be said that it is close to the limit in industrial weight measuring equipment. Therefore, the vacuum leakage inspection method of the present invention is not universally used for any vacuum packaged product, and it is effective to apply it to a material having a sufficient vacuum volume and a relatively small bulk density. This is a problem with the vacuum volume described above. For example, when the vacuum space itself is small, as seen in vacuum packs for processed meat products, the amount of air that enters is small even if there is a vacuum leak. The method of the invention is inappropriate. Therefore, the range of the bulk density of the vacuum packaged product to be inspected is set to 0.5 g / cm 3 or less shown above .
[0008]
On the other hand, the vacuum leak inspection method of the present invention is particularly suitable for the heat insulating panels as described above. This thermal insulation panel is an open cell type, that is, a foam plate that can evacuate all the bubbles because adjacent bubbles can be ventilated and wrapped with a laminate film consisting of a layer of plastic and metal foil, etc., and the inside is evacuated It is. A hard plastic is generally used as the foam, but a pumice-like ceramic foam can also be used. In such a case, the vacuum volume is large and the method of the present invention can be effectively applied. On the other hand, since it is difficult to inspect a large panel like the above-described conventional method using a vacuum vessel, the method of the present invention is different from the conventional vacuum leak inspection method depending on the object. It can be said that they complement each other.
[0009]
The vacuum leakage inspection method of the present invention measures the weight within a short time after vacuum packaging, and then measures the weight of the same vacuum packaged product again after a lapse of time. That is, the weight of the same article is tracked and measured, and is referred to as the previously measured weight. Weight comparisons should be made on the same item, even on the same product mass production line. That is, since the method of the present invention makes a difference in weight of the order of 1% a problem, there is a possibility that accurate judgment cannot be made even with the same type of product due to variation in the weight of individual products.
[0010]
The previous weight measurement is preferably performed immediately after vacuum packaging, that is, as soon as possible, for example, within 2 minutes. If the time after vacuum packaging is long, if the vacuum leak is relatively severe, the weight has already increased at the time of the previous measurement, and the difference from the weight in the subsequent measurement becomes small, making accurate judgment difficult. is there. The time interval until the subsequent weight measurement is usually, for example, about 30 minutes after the previous weight measurement. This is because it is normal for air to enter very quickly when there is a vacuum leak. Of course, it is possible to measure after a long period of time such as a full day from the previous weight measurement immediately after vacuum packaging.
[0011]
As described above, when the time interval between the front and rear weight measurements is long, the buoyancy due to air changes with changes in temperature and pressure, resulting in measurement errors. The rate is 10/273, that is, 3.7% if the air temperature fluctuates by 10 ° C., or 1% if the air pressure fluctuates by 10 mbar. If the external volume of the vacuum package is almost equal to the vacuum volume, and there is a temperature rise of 10 ° C, even if there is no vacuum leak, it will be a rate of 3.7% of the weight change that should occur when the vacuum is completely leaked. The weight will increase. If the external volume of the vacuum packaged product is twice the vacuum volume, the change is twice the above. However, especially when a plurality of the same articles are manufactured at the same time, since there is a similar weight change in most articles without vacuum leakage, there is no misunderstanding even if no correction is calculated.
[0012]
【Example】
The vacuum leakage inspection method of the present invention was applied to a heat insulating panel whose inside was evacuated. This heat insulation panel is formed by packaging an open cell foam of an unsaturated polyester resin with an aluminum sheet coated with a polyester resin, and sealing it while sucking up to 0.05 mbar with a vacuum pump. The external dimensions are 18 mm thick × 650 mm wide × 1500 mm long, and the weight when vacuumed is about 1480 g.
[0013]
The above panel without vacuum leakage has virtually no change in weight, but the example with vacuum leakage has an increase in weight of 19.2 g (1.30%) after 30 minutes. In the measurement after 24 hours of the same, the increase in weight compensated for the change in buoyancy due to the change in temperature and pressure was 21.7 g (1.47%) compared to immediately after vacuum packaging. In other words, it can be seen that the vacuum leakage proceeds in a relatively short time when there is a vacuum leakage, and most of the weight increase appears in the initial stage. Therefore, in the normal case, the vacuum leakage can be detected even if the second measurement is performed at a relatively short interval such as 30 minutes or 1 hour after the measurement immediately after vacuum packaging.
[0014]
FIG. 1 shows an example of an apparatus for inspecting the heat insulation panel for a vacuum leakage in a factory production line. The heat insulation panel 1 whose inside is evacuated by a vacuum packaging device (not shown) is sent to a product warehouse (not shown) by a belt conveyor 3 that runs at a relatively low speed. The first weighing device 2 is located immediately from the vacuum packaging device on the entrance side of the belt conveyor, and is installed on the side of the belt conveyor to take the heat insulation panel from the belt conveyor, measure the weight, and then return to the belt conveyor. It has become. The second weighing device 4 is located near the exit side of the belt conveyor, and is installed on the side of the belt conveyor to measure the weight of the heat insulation panel by the same method as the first weighing device. The weight measurement result is sent to the arithmetic unit 5, and the measurement results of the first and second weighing devices of the same heat insulation panel are compared, and the elapsed time between the weight measurement by the first and second weighing devices is also compared. To be recorded.
[0015]
【The invention's effect】
According to the vacuum leakage inspection method for a vacuum packaged product of the present invention, inspection of a large-sized object such as a heat insulation panel in which the inside is evacuated, which has been difficult to apply the conventional inspection method, can be performed with simple equipment at low cost. Can do.
[Brief description of the drawings]
FIG. 1 is a diagram showing an example of an apparatus for carrying out the method of the present invention.
DESCRIPTION OF SYMBOLS 1 Thermal insulation panel 2 1st weighing apparatus 3 Belt conveyor 4 2nd weighing apparatus 5 Arithmetic unit

Claims (2)

嵩密度が0.5g/cm 以下の真空包装品について真空包装直後にその重量を測定し、さらに大気中に置いた状態で時間が経過後に再び同一の真空包装品の重量を測定して前記の前後の重量の測定値を比較し、後の測定における重量の増大によって真空の漏洩を判断することを特徴とする真空包装品の真空漏洩検査方法。For a vacuum packaged product having a bulk density of 0.5 g / cm 3 or less , the weight thereof is measured immediately after the vacuum packaging, and the weight of the same vacuum packaged product is measured again after a lapse of time in the state of being placed in the atmosphere. A vacuum leakage inspection method for a vacuum packaged product, comprising comparing the measured values of the weight before and after and determining the leakage of the vacuum based on the increase in weight in the subsequent measurement. 真空包装品が連続気泡の発泡体の板をラミネートフィルムで包装した断熱パネルであることを特徴とする請求項1に記載の真空包装品の真空漏洩検査方法。  2. The vacuum leakage inspection method for a vacuum packaged product according to claim 1, wherein the vacuum packaged product is a heat insulating panel obtained by packaging an open-cell foam board with a laminate film.
JP35584196A 1996-12-25 1996-12-25 Vacuum leakage inspection method for vacuum packaged products Expired - Fee Related JP3762507B2 (en)

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JP3762507B2 true JP3762507B2 (en) 2006-04-05

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DE10164004B4 (en) * 2001-12-28 2005-07-14 Bayerisches Zentrum für Angewandte Energieforschung e.V. Vacuum insulation panel and method for measuring the internal pressure thereof
US7343080B2 (en) * 2004-09-27 2008-03-11 Idc, Llc System and method of testing humidity in a sealed MEMS device
CN103318479A (en) * 2013-06-24 2013-09-25 苏州快吉刀片制造有限公司 Blade weight detection unit
CN117046754B (en) * 2023-10-10 2023-12-08 地立(苏州)智能装备有限公司 Packaging bottle leak hunting and weighing integrated machine

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