JP3762014B2 - Coloring immobilization method of biodegradable simulated bait - Google Patents
Coloring immobilization method of biodegradable simulated bait Download PDFInfo
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- JP3762014B2 JP3762014B2 JP01317297A JP1317297A JP3762014B2 JP 3762014 B2 JP3762014 B2 JP 3762014B2 JP 01317297 A JP01317297 A JP 01317297A JP 1317297 A JP1317297 A JP 1317297A JP 3762014 B2 JP3762014 B2 JP 3762014B2
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- biodegradable
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Description
【0001】
【発明の属する技術分野】
本発明は、コンニャクマンナンを素材とした生分解性擬似餌を食用色素で着色した後、有機酸緩衝液に浸漬処理し、色素を着色固定化することによって保存安定性並びに水中での溶出安定化をはかることによって環境に優しい、しかも取扱い易く色素の長期保持性のある生分解性擬似餌の提供に関する。
【0002】
【従来の技術】
今日のレジャーブームとあいまって趣味、娯楽の中でも釣りが幅広く大衆化してきた。中でもその使いやすさ、手軽さ等から幅広い年齢層でルアー(擬似餌)の使用が一段と増してきている。一方このブームの加熱で使い捨てのルアーが魚体内にそのまま残ったり、根がかり等により放置されたルアーと共に残った釣り糸が水鳥の足に絡まったりする事故が相次いでいる。こうした環境への悪影響を改善するため自然界で微生物によって分解される生分解性擬似餌が注目されている。
例えば、特開昭62ー190037号公報には多糖類と多価金属化合物を基材とする擬似餌用ゲル化組成物が開示されており、動物性真餌に近いものではあるが、水中叉は海水中での使用に耐える形態保持や安全性、特に魚類群誘引物質の中でも誘引効果を左右する色素の保持性に劣っている。
また、特開昭63ー120366号公報にはコンニャクマンナンを主成分とするコンニャク芋精粉に蚕蛹粉末等の魚類群誘引物質、着色料等を混合添加し、アルカリ処理により得るゲル組成物に蒸し処理を施した後、各種成型及び/叉は各種包装形態品の釣餌及びその製造方法が開示されている。しかし、コンニャクマンナンの凝固前に着色を施し、アルカリ処理で凝固後蒸し処理によって着色料の安定化をはかっているが根本的には着色料の固定安定化はなされておらず、また凝固前の着色では各種動物性生餌に似せた自由な色の調整は困難であり釣餌としての性能が著しく低下してしまう欠点がある。
【0003】
【発明が解決しようとする課題】
本発明は、生分解性擬似餌を生餌に酷似した着色を長時間保持させることを目的にした着色法において、着色料に食用色素として使用できる法定食用タール色素および/または天然色素を使用して、コンニャクマンナンを素材とした生分解性擬似餌の品質を損なうことなく着色、固定化することを特徴とした安全性の高い自然に優しい着色生分解性擬似餌を提供することにある。
【課題を解決するための手段】
本発明者は生餌に酷似した着色を長時間保持させることのできる着色法について種々検討を重ねた結果、弱アルカリ性に調整した食用色素の水溶液中にコンニャクマンナンを素材とした擬似餌を浸漬して色素を浸透着色させ、更に有機酸とリン酸水素二ナトリウムでpH3.8〜4.5に調整した緩衝液、好ましくはpH4.0〜4.3に調整した緩衝液に浸漬することにより本発明の目的を達成することができる着色法を見出した。
すなわち本発明は、コンニャクマンナンを素材とした擬似餌を凝固後に、弱アルカリ性に調整した食用色素水溶液中に浸漬し、浸透着色した後、有機酸緩衝液に室温で3〜7時間浸漬し色素を固定化する生分解性擬似餌の着色固定化方法である。また本発明は、コンニャクマンナンを素材とした擬似餌を凝固後に、弱アルカリ性に調整した食用色素水溶液中に浸漬し、浸透着色した後、pH3.8〜4.5の有機酸緩衝液に室温で3〜7時間浸漬し色素を固定化する方法で着色固定化された、生分解性擬似餌である。
【0004】
【発明の実施の形態】
以下、本発明の生分解性擬似餌の着色固定化方法について詳述する。
本発明で使用するコンニャクマンナンは最も多く栽培されているコンヤク芋の赤茎種の他、青茎種、シナ種等のいずれでも良く、これらから通常食用コンヤクとして供されるコンニャク芋粉を使用することができる。
このコンヤク芋粉を素材として、これに魚類群誘引物質として蚕蛹粉末、魚油類、魚粉類、魚臭性物質等のような味覚、臭覚刺激物質、蛍光物質のような視覚刺激物質、さらには必要により着色料、防腐剤等を添加混合した後アルカリ処理し、各種動物生餌に似た形状、大きさの型枠で凝固成型して擬似餌をえる。
本発明に用いられる着色料は、食品添加物として用いられる法定食用タール色素および/または天然色素であり、法定食用タール色素として好適に使用されるものとしては、カラーインデックス番号がC.I.45430(食用赤色3号)、C.I.45410(食用赤色104号)及びC.I.45440(食用赤色105号)などのキサンテン系のものを挙げることができる。また天然色素としてはクチナシ黄色素(クロセチン)、クチナシ青色素及びアナトー色素等を好適に使用することができる。更に望ましくは、これらの法定食用タール色素と天然色素とを適宜配合して使用することが好ましくその濃度、色相を自由に変化、調整することによって各種動物性生餌の色に合わせることができる。
コンニャクマンナンを素材とした生分解性擬似餌の着色はコンニャクマンナンを凝固する前にその他の魚類群誘引物質と共に添加着色することもできるが、望む各種動物性生餌の色に調整するには凝固後着色する方が好ましく、室温で上記色素の弱アルカリ性水溶液に浸漬することによって容易に実施できる。
本発明に用いられる有機酸としては、クエン酸、酒石酸、リンゴ酸及びフマル酸等が挙げられ、特にクエン酸が好ましい。
【0005】
【実施例】
以下に実施例を挙げ、本発明をさらに詳しく説明する。
[実施例1]
弱アルカリ性に調整した0.03%食用赤色3号[(株)アイゼン製]水溶液43mlと水7mlの溶液中に、コンニャクマンナン素材の成型生分解性擬似餌8本(約28g)を室温で加えて15時間浸漬した。着色された生分解性擬似餌は、水切り後室温の水50mlで速やかに洗浄して表面に付着している未着色色素を取り除き、次にpH4に調整したクエン酸緩衝液(2%クエン酸水溶液160mlと7%リン酸水素二ナトリウム40mlからなる水溶液)50mlの中に着色した生分解性擬似餌を室温で4時間浸漬して、色素を固定化後水洗して赤色に着色した。得られた着色生分解性擬似餌の各々8本を多量の水及び海水中に室温で1時間、3時間、5時間浸漬した後、着色生分解性擬似餌を取り出し充分すりつぶし、弱アルカリ性の水で残存色素を抽出し、分光光度計で比色して色素残存率を算出した。その結果、着色固定化生分解性擬似餌は品質の劣化もなく、水中または海水中での溶出試験は未固定の擬似餌に比較して表−1に示したように格段に優れていた。
【0006】
【表1】
【0007】
[実施例2]
実施例1と同様にして食用赤色3号の代わりに1%ネオグリーンK−15[(株)アイゼン製クチナシ青色素とクチナシ黄色素(クロセチン)との混合製剤]水溶液50mlを使用して着色した後、実施例1と同様にして色素を固定化し、ウオーターメロン色の着色生分解性擬似餌を得た。この色素残存率を実施例1と同様にして測定した結果を表−1にを示した。得られた着色生分解性擬似餌の性能は実施例1と同様であった。
【0008】
[実施例3]
実施例1と同様にして食用赤色3号の代わりに0.01%食用赤色3号[(株)アイゼン製]水溶液42.5mlと0.75%クロシンブル−G[(株)アイゼン製クチナシ青色素製剤]水溶液7.5mlとの混合液を使用して着色した後、実施例1と同様にして色素を固定化し、紫色の着色生分解性擬似餌を得た。この色素残存率を実施例1と同様にして測定した結果を表−1にを示した。その性能は実施例1と同様であった。
【0009】
[実施例4]
実施例1と同様にして食用赤色3号の代わりに0.01%食用赤色105号[(株)アイゼン製]水溶液7.5mlと0.25%クロシンブル−G[(株)アイゼン製クチナシ青色素製剤]水溶液5ml及び0.25%クロシンPAGコンク[(株)アイゼン製クチナシ黄色素製剤]水溶液37.5mlの混合液を使用して着色した後、実施例1と同様にして色素を固定化し、茶色の着色生分解性擬似餌を得た。この色素残存率を実施例1と同様にして測定した結果を表−1にを示した。その性能は実施例1と同様であった。
【0010】
[実施例5]
実施例1と同様にして食用赤色3号の代わりに0.01%食用赤色104号[(株)アイゼン製]水溶液8mlと0.25%クロシンPAGコンク[(株)アイゼン製クチナシ黄色素製剤]水溶液3ml及び水39mlの混合液を使用して着色した後、実施例1と同様にして色素を固定化し、ライトルビー色の着色生分解性擬似餌を得た。この色素残存率を実施例1と同様にして測定した結果を表−1にを示した。
【0011】
[比較例]
実施例1〜5の有機酸緩衝液による色素の固定化処理を省略した未固定の着色生分解性擬似餌の色素残存率を実施例1と同様にして試験した結果を表−1に示した。
その結果、着色固定化処理をおこなわなっかった場合はいずれも著しく色素は溶出した。
【0012】
【発明の効果】
本発明方法によれば、コンニャクマンナンを素材とした生分解性擬似餌を食用色素で着色でき、動物性生餌に類似した着色色素をそのまま固定化する事が可能となる。また品質を損なうこともなくしかも着色固定化した色素は水中または海水中でも長期に安定保持できその機能を充分発揮することができる。[0001]
BACKGROUND OF THE INVENTION
The present invention is a biodegradable artificial bait made of konjac mannan, colored with food dyes, then immersed in an organic acid buffer solution, and the dyes are colored and fixed to preserve storage stability and elution stability in water. environmentally friendly by to achieve, yet it relates to providing a biodegradable pseudo Niesa with long retention easy to handle dyes.
[0002]
[Prior art]
Coupled with today's leisure boom, fishing has become widespread in hobbies and entertainment. Above all, the use of lures (pseudo bait) is increasing more and more in a wide range of age groups because of its ease of use and ease of use. On the other hand, there are a number of accidents in which disposable lures remain in the fish body due to the heating of the boom, or fishing lines that remain with lures left behind by roots or the like are entangled with the feet of water birds. In order to improve such adverse environmental impacts, biodegradable simulated baits that are degraded by microorganisms in the natural world have attracted attention.
For example, Japanese Patent Application Laid-Open No. 62-190037 discloses a gel composition for a pseudo food based on a polysaccharide and a polyvalent metal compound. Is inferior in retention of the form that can withstand use in seawater and safety, especially in the retention of pigments that influence the attractiveness among fish attractants.
In JP-A-63-120366, konjac mannan powder containing konjac mannan as a main ingredient is mixed with a fish group attractant such as salmon powder and coloring agents, and steamed into a gel composition obtained by alkali treatment. After processing, various baits and / or various packaged forms of bait and methods for manufacturing the same are disclosed. However, coloring is performed before solidification of konjac mannan, and the colorant is stabilized by alkali treatment and post-coagulation steaming treatment, but the colorant is not fixed and stabilized fundamentally. In coloring, it is difficult to freely adjust the color to resemble various animal feeds, and the performance as a fishing bait is significantly reduced.
[0003]
[Problems to be solved by the invention]
The present invention uses a legal edible tar dye and / or a natural dye that can be used as a food dye in a coloring method for the purpose of maintaining a coloring that is very similar to that of a raw food for a long time. Another object of the present invention is to provide a highly safe and naturally colored biodegradable simulated bait characterized by being colored and fixed without impairing the quality of the biodegradable simulated bait made of konjac mannan.
[Means for Solving the Problems]
The present inventor has conducted various studies on a coloring method capable of maintaining a coloring very similar to that of raw food for a long time, and as a result, a pseudo food made of konjac mannan was immersed in an aqueous solution of a food color adjusted to be weakly alkaline. By immersing the dye in a buffer solution adjusted to pH 3.8 to 4.5 with an organic acid and disodium hydrogen phosphate, preferably immersed in a buffer solution adjusted to pH 4.0 to 4.3. We have found a coloring method that can achieve the object of the invention.
That is, the present invention, after solidifying a pseudo bait made of konjac mannan as a raw material , immersing it in an edible dye aqueous solution adjusted to weak alkalinity, osmotically coloring , and then immersing the dye in an organic acid buffer at room temperature for 3-7 hours This is a color immobilization method for immobilizing biodegradable simulated bait. In addition, the present invention is a method in which a pseudo bait made of konjac mannan is coagulated, dipped in an aqueous edible dyestuff adjusted to weak alkalinity, osmotically colored , and then placed in an organic acid buffer having a pH of 3.8 to 4.5 at room temperature. It is a biodegradable simulated bait that is colored and fixed by a method in which it is immersed for 3 to 7 hours to fix the pigment.
[0004]
DETAILED DESCRIPTION OF THE INVENTION
Hereinafter, the coloring immobilization method of the biodegradable simulated bait of the present invention will be described in detail.
The konjac mannan used in the present invention may be any of the most commonly cultivated red stalks of konjac koji, blue stalks, cinnamons, etc., and konjac koji flour usually used as edible konjac is used. be able to.
This konjac flour is used as a material, and as a fish group attractant, taste, odor stimulating substances such as salmon powder, fish oils, fish meals, fish odorous substances, and other visual stimulating substances such as fluorescent substances are necessary. colorants, and alkali treatment was added and mixed a preservative or the like, shape similar to various animals live food, obtain the pseudo Niesa solidified molded in mold sizes by.
The colorant used in the present invention is a legal edible tar dye and / or a natural dye used as a food additive. A color index number of C.I. I. 45430 (edible red No. 3), C.I. I. 45410 (edible red 104) and C.I. I. And xanthene-based compounds such as 45440 (edible red No. 105). As natural pigments, gardenia yellow pigment (crocetin), gardenia blue pigment, annatto pigment and the like can be suitably used. More desirably, these legal edible tar pigments and natural pigments are preferably blended and used as appropriate, and can be adjusted to the color of various animal diets by freely changing and adjusting the concentration and hue.
Coloring of biodegradable simulated bait made from konjac mannan can be added and colored with other fish group attractants before solidifying konjac mannan, but it can be solidified to adjust the color of various animal live bait as desired. Post-coloring is preferred, and it can be easily carried out by immersing in a weakly alkaline aqueous solution of the dye at room temperature.
Examples of the organic acid used in the present invention include citric acid, tartaric acid, malic acid and fumaric acid, and citric acid is particularly preferable.
[0005]
【Example】
The following examples further illustrate the present invention.
[Example 1]
In a solution of a weakly alkaline 0.03% Food Red No. 3, which was adjusted to soluble [Corp. Aizen] solution 43ml and water 7 ml, molded biodegradable pseudo Niesa eight konjak mannan material (about 28 g) at room temperature In addition, it was immersed for 15 hours. Colored biodegradable pseudo Niesa was removes the uncolored pigments attached to the surface by quickly washed with 50ml of water at room temperature after draining, then citrate buffer adjusted to pH 4 (2% citric acid biodegradable pseudo Niesa colored in an aqueous solution 160ml of an aqueous solution consisting of 7% disodium hydrogen phosphate 40 ml) 50 ml was immersed for 4 hours at room temperature, was colored red by washing after immobilization of the dye. 1 hour at room temperature, respectively eight to a large amount of water and in sea water of the resulting colored biodegradable pseudo Niesa, 3 hours, was immersed for 5 hours, sufficient ground removed colored biodegradable pseudo Niesa, weakly alkaline The remaining pigment was extracted with water and colorimetrically measured with a spectrophotometer to calculate the pigment remaining rate. As a result, coloring fixed metaplastic degradable pseudo Niesa without deterioration of quality, the dissolution test in water or seawater have much better as shown in Table 1 in comparison with the unfixed pseudo Niesa It was.
[0006]
[Table 1]
[0007]
[Example 2]
In the same manner as in Example 1, instead of food red No. 3, coloring was performed using 50 ml of an aqueous solution of 1% Neogreen K-15 [mixed preparation of gardenia blue pigment made by Eisen Co., Ltd. and gardenia yellow pigment (crocetin)]. after, in the same manner as in example 1 was immobilized dye to obtain a colored biodegradable pseudo Niesa of water melon color. The results of measuring the dye residual ratio in the same manner as in Example 1 are shown in Table 1. Obtained colored biodegradable pseudo Niesa performance was similar to Example 1.
[0008]
[Example 3]
In the same manner as in Example 1, 42.5 ml of 0.01% edible red No. 3 [manufactured by Eisen Co., Ltd.] and 0.75% Closmmble-G [Eisen Co., Ltd. gardenia blue pigment, instead of Edible Red No. 3 after coloring using a mixed solution of formulation] aqueous solution 7.5 ml, the dye is immobilized in the same manner as in example 1 to obtain a colored biodegradable pseudo Niesa purple. The results of measuring the dye residual ratio in the same manner as in Example 1 are shown in Table 1. The performance was the same as in Example 1.
[0009]
[Example 4]
In the same manner as in Example 1, in place of Food Red No. 3, 0.01 ml of Food Red No. 105 [manufactured by Eisen Co., Ltd.], 7.5 ml of an aqueous solution and 0.25% Closmmble-G [Keishinashi Blue Pigment manufactured by Eisen Co., Ltd. Formulation] After coloring using a mixed solution of 5 ml of an aqueous solution and 37.5 ml of a 0.25% crocin PAG conch [Euzen Kuchinashi Yellow Dye Formulation] aqueous solution, the dye was immobilized in the same manner as in Example 1, to obtain a colored biodegradable pseudo Niesa of brown. The results of measuring the dye residual ratio in the same manner as in Example 1 are shown in Table 1. The performance was the same as in Example 1.
[0010]
[Example 5]
In the same manner as in Example 1, instead of Edible Red No. 3, 0.01% Edible Red No. 104 [manufactured by Eisen Co., Ltd.] 8 ml of an aqueous solution and 0.25% Crocin PAG Conk [Euzen Co. after coloring using a mixed solution of aqueous solution 3ml, and water 39 ml, the dye is immobilized in the same manner as in example 1 to obtain a colored biodegradable pseudo Niesa write ruby. The results of measuring the dye residual ratio in the same manner as in Example 1 are shown in Table 1.
[0011]
[Comparative example]
Shows the results of testing in the residual rate of the dye unfixed coloring biodegradable pseudo Niesa is omitted immobilization treatment of the dye with an organic acid buffer solution of Example 1-5 in the same manner as in Example 1 in Table 1 It was.
As a result, the dye was remarkably eluted in all cases where the color immobilization treatment was not performed.
[0012]
【The invention's effect】
According to the method of the present invention, a biodegradable simulated bait made of konjac mannan can be colored with a food dye, and a colored dye similar to animal live bait can be immobilized as it is. In addition, the coloring and fixing dyes can be stably maintained in water or seawater for a long period of time without deteriorating the quality, and can fully exhibit their functions.
Claims (7)
Priority Applications (1)
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JP01317297A JP3762014B2 (en) | 1997-01-10 | 1997-01-10 | Coloring immobilization method of biodegradable simulated bait |
Applications Claiming Priority (1)
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JP01317297A JP3762014B2 (en) | 1997-01-10 | 1997-01-10 | Coloring immobilization method of biodegradable simulated bait |
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JPH10191840A JPH10191840A (en) | 1998-07-28 |
JP3762014B2 true JP3762014B2 (en) | 2006-03-29 |
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JP01317297A Expired - Fee Related JP3762014B2 (en) | 1997-01-10 | 1997-01-10 | Coloring immobilization method of biodegradable simulated bait |
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