JP3550109B2 - Melt blown nonwoven spinning die - Google Patents

Melt blown nonwoven spinning die Download PDF

Info

Publication number
JP3550109B2
JP3550109B2 JP2001180145A JP2001180145A JP3550109B2 JP 3550109 B2 JP3550109 B2 JP 3550109B2 JP 2001180145 A JP2001180145 A JP 2001180145A JP 2001180145 A JP2001180145 A JP 2001180145A JP 3550109 B2 JP3550109 B2 JP 3550109B2
Authority
JP
Japan
Prior art keywords
spinning
nozzle
hot air
air discharge
slits
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
JP2001180145A
Other languages
Japanese (ja)
Other versions
JP2002371427A (en
Inventor
満 末冨
Original Assignee
有限会社末富エンジニアリング
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by 有限会社末富エンジニアリング filed Critical 有限会社末富エンジニアリング
Priority to JP2001180145A priority Critical patent/JP3550109B2/en
Priority to CN 02122292 priority patent/CN1270002C/en
Publication of JP2002371427A publication Critical patent/JP2002371427A/en
Application granted granted Critical
Publication of JP3550109B2 publication Critical patent/JP3550109B2/en
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

Links

Images

Landscapes

  • Spinning Methods And Devices For Manufacturing Artificial Fibers (AREA)
  • Nonwoven Fabrics (AREA)

Description

【0001】
【発明の技術分野】
この発明は、不織布をメルトブロー法で製造する際に用いる紡糸ダイに関する。
【0002】
【従来の技術】
メルトブロー法は、概略図5に示すように、ホッパー1に投入された原料チップを押出機2で加熱溶融し、ダイ3に供給して紡出し、紡出した短繊維を捕集ネットから成るコンベア4上にシート状に堆積させ、これをコンベア4から剥離しながら、カレンダロール5を通過させた後、巻取機6で巻き取って不織布を製造する方法である。
【0003】
【発明の課題】
上記ダイ3は、紡糸口3aから吐出された溶融ポリマーを熱風吐出口3bから噴出した高温エヤーで紡出するようになっているが、紡糸口3aからの溶融ポリマーの吐出量と高温エヤーの吐出量に微妙なバランスが必要であって、任意の径の繊維を紡出すること、特に細い径の繊維を紡出することが難しく、バルキー性の高い風合の良い不織布を得ることが出来なかった。さらに、多量の熱風を送る必要があるため、エネルギーコストが高くつく問題があった。
【0004】
そこで本発明者は、溶融ポリマーを押し出すノズルの先端近辺に、熱風吐出スリットを配置し、その下流に大量の冷風を吐出するスリットを配置して溶融ポリマーを延伸するようにした紡糸ダイを提案している(特開2000−336517号公報)。このような紡糸ダイを用いると細径の繊維より成るバルキー性の高い不織布が得られることが確認されているが、冷風吐出スリットの吐出端直下に、急激な冷風吐出によって渦流が生じ、紡出された繊維表面に渦流の影響で凹凸が生じ、時には紡出口に引掛り、紡糸効率を低下させる問題が生じている。
【0005】
この発明の課題は、前記渦流の発生を防止し、滑らかな表面を有する繊維を効率よく紡出することができる紡糸ダイを提供することである。
【0006】
【課題の解決手段】
上記の課題を解決するために、この発明は、溶融ポリマーを押し出すノズルの先端近辺に、一対の熱風吐出スリットを前記ノズルを中心に対向配置し、この冷風吐出スリットの下流に一対の冷風吐出スリットを前記ノズルを中心に対向配置した紡糸ダイにおいて、前記冷風が吐出する紡出口の内端部に通気スリット又は通気孔列を対向して設けたことを特徴とする。また、前記熱風吐出スリットと冷風吐出スリットとの間に、外気に通じる一対のスリットを前記ノズルを中心に対向配置しておくのが好ましい。
【0007】
【実施の形態】
以下、この発明の実施形態を図1乃至図4に基づいて説明する。図示のように、紡糸パック10の下端に紡糸ダイ20が取り付けられている。紡糸パック10は、2分割された本体11a、11bをボルト12で結合したものであって、本体11a、11bの上部には、ポリプロピレン樹脂、ポリエステル樹脂、ナイロン(商標)樹脂等の溶融ポリマーの注入口13が設けられ、下部には熱風の送入口14a、14bが設けられている。また、側面には、押え板16a、16bによって、パネルヒーター15a、15bが当接している。
【0008】
前記紡糸ダイ20には、前記ポリマー注入口13に続くポリマー通路17の先端に複数のノズル21が一列に設けられ、このノズル21の先端21aは、熱風室22a、22bからの熱風を吐出する対向配置された一対の吐出スリット23a、23bの中央に臨んでいる。また、前記熱風室22a、22bは前記熱風送入口14a、14bに通路24a、24bを介して連通している。
【0009】
前記熱風吐出スリット23a、23bから一定の間隔Sをあけて、冷風室25a、25bと一対の冷風吐出スリット26a、26bが前記ノズル21を中心に対向配置され、前記冷風室25a、25bは冷風送入口27a、27bに連通している。そして冷風吐出スリット26a、26bの前方は、紡出口29になっている。また、間隔Sは、ノズル21の先端近辺に、外気(随伴流)の吸引スリット28a、28bを形成している。この間隔Sは、2〜10mm程度が好ましい。
【0010】
図2に明瞭に示されているように、上記紡出口29の内端から一定の間隔Sをあけて紡出口29間と外気を連通する通気スリット30a、30bが紡出口29の全長にわたって対向して形成されている。この間隔Sは1〜10mm程度が好ましい。また、図3に示すように、通気スリット30a、30bに代えて通気孔列30c、30dを対向して設けてもよい。通気孔列30c、30dを形成する場合は、ダイ20の長さ方向に狭い間隔で多数の通気孔を設け、紡出口29に開口する内端に、溝31a、31bを紡出口29の全長にわたって設けておくのがよい。
【0011】
いま、ノズル21から溶融ポリマーを押し出すと、溶融ポリマーの両側からその押し出し方向に傾斜した一対の熱風吐出スリット23a、23bを通して吹き出される熱風に挟まれるように引き出され、さらに冷風吐出スリット26a、26bから冷風が大量に吐出されるため、前記ノズル21から押し出された溶融ポリマーが負圧で急激に吸引延伸されると同時に結晶化が進行する。このとき、熱風の温度は200〜300℃、冷風の温度は10〜30℃程度が好ましく、風量は冷風に対して熱風が5〜20%程度が好ましい。例えば冷風が100〜250m/秒であると、熱風は5〜50m/秒程度である。即ち、ここでは、熱風はノズル21から押し出された溶融ポリマーが急速に冷却しない程度に加熱するだけでよく、冷風によって生じる負圧で急激に延伸して細径繊維が形成される。そして冷風の急激な吐出によって、紡出口29の内端付近で生じる渦流は通気スリット30a、30b又は通気孔列30c、30dによって消滅し、滑らかな表面を有する繊維が紡出される。なお、冷風吐出スリット26a、26bも、熱風吐出スリット23a、23bと同様に紡出口29の方向に下降する傾斜をもたせておく。また、随伴流を生じるスリット28a、28bを形成しておけば、風量の節減を果すことができる。
【0012】
【発明の効果】
この発明によれば、以上のように、ノズルで押し出した溶融ポリマーが冷却しない程度の少量の熱風で加熱したものを、大量の冷風による負圧で延伸し、その際に生じる渦流をなくするようにしたので、細径で表面の滑らかな繊維が得られ、それによってバルキー性の高い風合のよい不織布が得られる。
【0013】
また、紡出口での繊維の引掛りなどがなくなるため、従来より吐出ポリマーを多くすることができ生産性が向上する。
【図面の簡単な説明】
【図1】この発明の紡糸ダイを組み込んだ紡糸パックを示す横断面図
【図2】紡糸ダイの拡大断面図
【図3】紡糸ダイの部分拡大断面図
【図4】紡糸ダイの斜視図
【図5】従来のメルトブロー法による不織布の製造方法を示す一部横断概略線図
【符号の説明】
1 ホッパー
2 押出機
3 ダイ
3a 紡糸口
3b 熱風吐出口
4 コンベア
5 カレンダロール
6 巻取機
10 紡糸パック
11a、11b 本体
12 ボルト
13 注入口
14a、14b 送入口
15a、15b パネルヒーター
16a、16b 押え板
17 通路
20 紡糸ダイ
21 ノズル
21a ノズルの先端
22a、22b 熱風室
23a、23b 熱風吐出スリット
24a、24b 通路
25a、25b 冷風室
26a、26b 冷風吐出スリット
27a、27b 冷風送入口
28a、28b 吸引スリット
29 紡出口
30a、30b 通気スリット
30c、30d 通気孔列
31a、31b 溝
、S 間隔
[0001]
TECHNICAL FIELD OF THE INVENTION
The present invention relates to a spinning die used when manufacturing a nonwoven fabric by a melt blow method.
[0002]
[Prior art]
In the melt blow method, as shown in FIG. 5, a raw material chip put into a hopper 1 is heated and melted by an extruder 2, supplied to a die 3 and spun, and the spun short fibers are conveyed from a collecting net. This is a method of manufacturing a nonwoven fabric by depositing the sheet on a sheet 4, passing the sheet through a calendar roll 5 while separating the sheet from the conveyor 4, and winding the sheet by a winder 6.
[0003]
[Problems of the Invention]
The die 3 spins the molten polymer discharged from the spinning port 3a with the high-temperature air jetted from the hot-air discharging port 3b, and discharges the molten polymer from the spinning port 3a and discharges the high-temperature air. A delicate balance is required in the amount, and it is difficult to spun fibers with an arbitrary diameter, especially with small diameter fibers, and it is not possible to obtain a bulky nonwoven fabric with a good feel. Was. In addition, a large amount of hot air needs to be sent, so that there is a problem in that energy costs are high.
[0004]
Therefore, the present inventor has proposed a spinning die in which a hot air discharge slit is arranged near the tip of a nozzle for extruding a molten polymer, and a slit for discharging a large amount of cold air is arranged downstream of the slit to stretch the molten polymer. (JP-A-2000-336517). It has been confirmed that using such a spinning die, a nonwoven fabric having a high bulky property composed of small-diameter fibers can be obtained. Irregularities are generated on the surface of the woven fiber under the influence of the vortex, and sometimes the fiber is caught at the spinning outlet, which causes a problem of lowering the spinning efficiency.
[0005]
An object of the present invention is to provide a spinning die capable of preventing the occurrence of the vortex and efficiently spinning a fiber having a smooth surface.
[0006]
[Means for solving the problem]
In order to solve the above-mentioned problem, the present invention provides a pair of hot air discharge slits disposed near the tip of a nozzle for extruding a molten polymer, with a pair of hot air discharge slits opposed to each other around the nozzle. In a spinning die in which the nozzles are arranged opposite to each other, a vent slit or a row of vent holes is provided at an inner end of a spinning outlet from which the cool air is discharged . Also, between the hot air discharge slit and the cold air discharge slit, preferably a pair of slits communicating with the ambient air keep to face disposed about said nozzle.
[0007]
Embodiment
Hereinafter, an embodiment of the present invention will be described with reference to FIGS. As shown, a spinning die 20 is attached to the lower end of the spin pack 10. The spinning pack 10 is obtained by joining body parts 11a and 11b divided into two parts with bolts 12, and a molten polymer such as a polypropylene resin, a polyester resin, and a nylon (trademark) resin is provided on the upper parts of the body parts 11a and 11b. An inlet 13 is provided, and hot air inlets 14a and 14b are provided below. Panel heaters 15a and 15b are in contact with the side surfaces by holding plates 16a and 16b.
[0008]
The spinning die 20 is provided with a plurality of nozzles 21 in a row at the tip of a polymer passage 17 following the polymer injection port 13, and the tip 21 a of the nozzle 21 is opposed to discharge hot air from the hot air chambers 22 a and 22 b. It faces the center of the arranged pair of discharge slits 23a and 23b. The hot air chambers 22a and 22b communicate with the hot air inlets 14a and 14b via passages 24a and 24b.
[0009]
Open the hot air discharge slit 23a, a constant from 23b spacing S 1, cold air chamber 25a, 25b and a pair of cool air discharge slits 26a, 26b are opposed around the nozzle 21, the cold air chamber 25a, 25b is cold It communicates with the inlets 27a and 27b. The front of the cold air discharge slits 26a, 26b is a spinning outlet 29. The distance S 1 is near the tip of the nozzle 21, the suction slit 28a of the outside air (accompanying flow) to form a 28b. The spacing S 1 is about 2~10mm are preferred.
[0010]
As clearly shown in FIG. 2, opposite the vent slits 30a communicating between spinning outlet 29 and the outside air from the inner end at a certain distance S 2 of the spinning outlet 29, 30b is over the entire length of the spinning outlet 29 It is formed. The spacing S 2 about 1~10mm are preferred. Further, as shown in FIG. 3, instead of the ventilation slits 30a and 30b, ventilation hole rows 30c and 30d may be provided to face each other. When forming the air hole rows 30c and 30d, a large number of air holes are provided at narrow intervals in the length direction of the die 20, and grooves 31a and 31b are formed at the inner end opening to the spinning outlet 29 over the entire length of the spinning outlet 29. It is good to provide.
[0011]
Now, when the molten polymer is extruded from the nozzle 21, the molten polymer is drawn out from both sides of the molten polymer so as to be sandwiched by the hot air blown out through a pair of hot air discharge slits 23a, 23b inclined in the extrusion direction, and further cooled air discharge slits 26a, 26b. , A large amount of cold air is discharged from the nozzle 21, so that the molten polymer extruded from the nozzle 21 is rapidly drawn and drawn under negative pressure, and at the same time, crystallization proceeds. At this time, the temperature of the hot air is preferably 200 to 300 ° C., the temperature of the cold air is preferably about 10 to 30 ° C., and the amount of the hot air is preferably about 5 to 20% of the cold air. For example, when the cool air is 100 to 250 m / sec, the hot air is about 5 to 50 m / sec. That is, in this case, the hot air only needs to be heated to such an extent that the molten polymer extruded from the nozzle 21 does not rapidly cool, and is rapidly drawn by the negative pressure generated by the cool air to form fine fibers. Then, the vortex generated near the inner end of the spinning outlet 29 due to the rapid discharge of the cool air is extinguished by the ventilation slits 30a, 30b or the row of ventilation holes 30c, 30d, and a fiber having a smooth surface is spun. The cold air discharge slits 26a and 26b are also inclined so as to descend in the direction of the spinning outlet 29 similarly to the hot air discharge slits 23a and 23b. In addition, if the slits 28a and 28b that generate the entrained flow are formed, the air volume can be reduced.
[0012]
【The invention's effect】
According to the present invention, as described above, what is heated with a small amount of hot air that does not cool the molten polymer extruded by the nozzle, is stretched by negative pressure due to a large amount of cold air, and the vortex generated at that time is eliminated. As a result, fibers having a small diameter and a smooth surface can be obtained, whereby a nonwoven fabric having a high bulkiness and a good feel can be obtained.
[0013]
In addition, since the fiber is not caught at the spinning outlet, the amount of the discharged polymer can be increased as compared with the related art, thereby improving the productivity.
[Brief description of the drawings]
FIG. 1 is a cross-sectional view showing a spinning pack incorporating a spinning die of the present invention. FIG. 2 is an enlarged cross-sectional view of the spinning die. FIG. 3 is a partially enlarged cross-sectional view of the spinning die. FIG. 5 is a schematic partial cross-sectional view showing a conventional method for producing a nonwoven fabric by a melt blow method.
DESCRIPTION OF SYMBOLS 1 Hopper 2 Extruder 3 Die 3a Spinning port 3b Hot air discharge port 4 Conveyor 5 Calendar roll 6 Winding machine 10 Spinning pack 11a, 11b Main body 12 Bolt 13 Inlet 14a, 14b Inlet 15a, 15b Panel heater 16a, 16b Pressing plate 17 Passage 20 Spinning die 21 Nozzle 21a Nozzle tip 22a, 22b Hot air chamber 23a, 23b Hot air discharge slit 24a, 24b Passage 25a, 25b Cold air chamber 26a, 26b Cold air discharge slit 27a, 27b Cold air inlet 28a, 28b Suction slit 29 Spinning outlet 30a, 30b ventilation slits 30c, 30d vent columns 31a, 31b groove S 1, S 2 interval

Claims (2)

溶融ポリマーを押し出すノズルの先端近辺に、一対の熱風吐出スリットを前記ノズルを中心に対向配置し、その下流に一対の冷風吐出スリットを前記ノズルを中心に対向配置した紡糸ダイにおいて、前記冷風が吐出する紡出口の内端部に通気スリット又は通気孔列を設けたことを特徴とするメルトブロー式不織布の紡糸ダイ。Near the tip of the nozzle that extrudes the molten polymer, a pair of hot air discharge slits are arranged facing each other around the nozzle, and a pair of cool air discharge slits is arranged downstream thereof at a spinning die where the cold air is discharged. A melt-blowing nonwoven spinning die, characterized in that a vent slit or a row of vent holes is provided at the inner end of the spinning outlet. 前記熱風吐出スリットと冷風吐出スリットの間に、外気に通じる一対のスリットを前記ノズルを中心に対向配置した請求項に記載のメルトブロー式不織布の紡糸ダイ。The spinning die for a melt-blown nonwoven fabric according to claim 1 , wherein a pair of slits communicating with the outside air is disposed between the hot air discharge slit and the cool air discharge slit so as to face each other around the nozzle.
JP2001180145A 2001-06-14 2001-06-14 Melt blown nonwoven spinning die Expired - Fee Related JP3550109B2 (en)

Priority Applications (2)

Application Number Priority Date Filing Date Title
JP2001180145A JP3550109B2 (en) 2001-06-14 2001-06-14 Melt blown nonwoven spinning die
CN 02122292 CN1270002C (en) 2001-06-14 2002-06-04 Spinning plate used in non-woven fabric production

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP2001180145A JP3550109B2 (en) 2001-06-14 2001-06-14 Melt blown nonwoven spinning die

Publications (2)

Publication Number Publication Date
JP2002371427A JP2002371427A (en) 2002-12-26
JP3550109B2 true JP3550109B2 (en) 2004-08-04

Family

ID=19020607

Family Applications (1)

Application Number Title Priority Date Filing Date
JP2001180145A Expired - Fee Related JP3550109B2 (en) 2001-06-14 2001-06-14 Melt blown nonwoven spinning die

Country Status (2)

Country Link
JP (1) JP3550109B2 (en)
CN (1) CN1270002C (en)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US7662534B2 (en) 2006-09-11 2010-02-16 Ricoh Company Ltd. Apparatus for producing toner precursor, and method for the same, fibrous toner precursor, apparatus for producing toner, and method for producing electrophotographic toner and fine resin particles
US7879268B2 (en) 2006-11-10 2011-02-01 Ricoh Company Limited Apparatus and method for manufacturing particulate resin

Families Citing this family (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2006285198A (en) * 2005-03-09 2006-10-19 Hosokawa Funtai Gijutsu Kenkyusho:Kk Toner particle, apparatus for manufacturing toner particle, and method for manufacturing toner particle
KR101265364B1 (en) * 2005-05-23 2013-05-20 쓰리엠 이노베이티브 프로퍼티즈 컴파니 Methods and apparatus for meltblowing of polymeric material utilizing fluid flow from an auxiliary manifold
JP2008096974A (en) * 2006-09-11 2008-04-24 Ricoh Co Ltd Apparatus for producing toner precursor and method for the same, fibrous toner precursor, apparatus for producing toner and electrophotographic toner
CN101922052B (en) * 2010-05-14 2011-11-30 上海天洋热熔胶有限公司 Spinneret plate for producing hot melt adhesive net film
KR20130111591A (en) * 2010-12-06 2013-10-10 미쓰이 가가쿠 가부시키가이샤 Melt-blown nonwoven fabric, and production method and device for same
JP6049967B2 (en) * 2012-10-30 2016-12-21 株式会社化繊ノズル製作所 Ultra fine fiber nonwoven manufacturing equipment
CN103114341A (en) * 2013-02-22 2013-05-22 昆山鸿福泰环保科技有限公司 Spinning nozzle for processing PP (polypropylene) filter elements
JP6171072B1 (en) * 2016-11-14 2017-07-26 関西電子株式会社 Resin fiber manufacturing method, nozzle head and manufacturing apparatus used therefor
CN111850713A (en) * 2020-08-04 2020-10-30 南通大学 Split type double-groove melt-blowing die head for preparing superfine fibers
CN112251909A (en) * 2020-09-21 2021-01-22 江苏惠沣环保科技有限公司 Manufacturing process of high-low temperature integrally-formed hot-melt net film
CN112481819B (en) * 2020-11-23 2021-12-03 舒城娃娃乐儿童用品有限公司 Preparation method of hard cotton
CN112981722B (en) * 2021-01-26 2023-03-28 广东蒙泰高新纤维股份有限公司 Method for preparing lithium ion battery diaphragm by sea island COPET-PP composite negative pressure spinning

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US7662534B2 (en) 2006-09-11 2010-02-16 Ricoh Company Ltd. Apparatus for producing toner precursor, and method for the same, fibrous toner precursor, apparatus for producing toner, and method for producing electrophotographic toner and fine resin particles
US7879268B2 (en) 2006-11-10 2011-02-01 Ricoh Company Limited Apparatus and method for manufacturing particulate resin

Also Published As

Publication number Publication date
CN1270002C (en) 2006-08-16
JP2002371427A (en) 2002-12-26
CN1392297A (en) 2003-01-22

Similar Documents

Publication Publication Date Title
JP3335949B2 (en) Melt blown nonwoven spinning die
JP3550109B2 (en) Melt blown nonwoven spinning die
KR100560589B1 (en) Cold Air Meltblown Apparatus and Process
US4406850A (en) Spin pack and method for producing conjugate fibers
US6013223A (en) Process and apparatus for producing non-woven webs of strong filaments
US5260003A (en) Method and device for manufacturing ultrafine fibres from thermoplastic polymers
JP3704522B2 (en) Equipment for continuous production of nonwoven fiber webs
US20070202769A1 (en) Device and method for melt spinning fine non-woven fibers
CA2417872C (en) Process and system for producing multicomponent spunbonded nonwoven fabrics
JPH07102408A (en) Melt-blow spinneret
US20100099321A1 (en) Process and apparatus for the production of nonwoven fabrics from extruded filaments
US5439364A (en) Apparatus for delivering and depositing continuous filaments by means of aerodynamic forces
CZ305342B6 (en) Process for producing nonwoven fabrics and apparatus for making the same
JPH03174008A (en) Method for production of synthetic yarn and/or fiber in the course of manufacture of spinning fleece from thermoplastic plastic and spinning nozzle unit
JP2009536693A (en) Apparatus for melt spinning row filaments
US6814555B2 (en) Apparatus and method for extruding single-component liquid strands into multi-component filaments
US20050233018A1 (en) Device for the production of multicomponent fibers or filaments, in particular bicomponent fibers or filaments
JPH04228606A (en) Method and apparatus for manufacturing very fine thread of melt-spinnable synthetic material
JP3560568B2 (en) Melt blown nonwoven spinning die
CN214244808U (en) Manufacturing equipment of double-component spun-bonded non-woven fabric
CN108323175B (en) Method for producing resin fiber, nozzle head used for the method, and production apparatus
CN112281226B (en) A shower nozzle module and device for producing melt-blown non-woven fabrics
WO2019198397A1 (en) Spinneret and method of manufacturing fiber web
JP2003278070A (en) Method and machine for producing web with unidirectionally arranged filaments
JPS61119705A (en) Production of multifilament

Legal Events

Date Code Title Description
A977 Report on retrieval

Free format text: JAPANESE INTERMEDIATE CODE: A971007

Effective date: 20031222

A131 Notification of reasons for refusal

Free format text: JAPANESE INTERMEDIATE CODE: A131

Effective date: 20040120

A521 Written amendment

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20040305

TRDD Decision of grant or rejection written
A01 Written decision to grant a patent or to grant a registration (utility model)

Free format text: JAPANESE INTERMEDIATE CODE: A01

Effective date: 20040330

A61 First payment of annual fees (during grant procedure)

Free format text: JAPANESE INTERMEDIATE CODE: A61

Effective date: 20040422

R150 Certificate of patent or registration of utility model

Free format text: JAPANESE INTERMEDIATE CODE: R150

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

FPAY Renewal fee payment (event date is renewal date of database)

Free format text: PAYMENT UNTIL: 20080430

Year of fee payment: 4

FPAY Renewal fee payment (event date is renewal date of database)

Free format text: PAYMENT UNTIL: 20090430

Year of fee payment: 5

LAPS Cancellation because of no payment of annual fees