JP3437308B2 - Heat treatment furnace for semiconductor manufacturing equipment - Google Patents

Heat treatment furnace for semiconductor manufacturing equipment

Info

Publication number
JP3437308B2
JP3437308B2 JP01751695A JP1751695A JP3437308B2 JP 3437308 B2 JP3437308 B2 JP 3437308B2 JP 01751695 A JP01751695 A JP 01751695A JP 1751695 A JP1751695 A JP 1751695A JP 3437308 B2 JP3437308 B2 JP 3437308B2
Authority
JP
Japan
Prior art keywords
valve
temperature
reaction tube
heat treatment
semiconductor manufacturing
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
JP01751695A
Other languages
Japanese (ja)
Other versions
JPH08191075A (en
Inventor
英二 保坂
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Hitachi Kokusai Electric Inc
Original Assignee
Hitachi Kokusai Electric Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Hitachi Kokusai Electric Inc filed Critical Hitachi Kokusai Electric Inc
Priority to JP01751695A priority Critical patent/JP3437308B2/en
Publication of JPH08191075A publication Critical patent/JPH08191075A/en
Application granted granted Critical
Publication of JP3437308B2 publication Critical patent/JP3437308B2/en
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Description

【発明の詳細な説明】Detailed Description of the Invention

【0001】[0001]

【産業上の利用分野】本発明は半導体製造装置の熱処理
炉、特に高温で熱処理を行う半導体製造装置の熱処理炉
に関するものである。
BACKGROUND OF THE INVENTION 1. Field of the Invention The present invention relates to a heat treatment furnace for semiconductor manufacturing equipment, and more particularly to a heat treatment furnace for semiconductor manufacturing equipment which performs heat treatment at a high temperature.

【0002】[0002]

【従来の技術】半導体製造過程でウェーハの水素アニー
ル処理を行う工程があり、このアニール処理を行う従来
の熱処理炉を図3に於いて説明する。
2. Description of the Related Art There is a step of performing a hydrogen annealing process on a wafer in a semiconductor manufacturing process, and a conventional heat treatment furnace for performing this annealing process will be described with reference to FIG.

【0003】筒状のヒータ1内に反応管2が設けられ、
該反応管2内にはウェーハ3が水平姿勢で多段に装填さ
れたボート4が装入される。前記反応管2の内壁に沿っ
て立設されたノズル5は第1流量調整器6、第1バルブ
7を介して窒素ガス供給源(図示せず)に接続され、又
前記ノズル5は第2流量調整器8、第2バルブ9を介し
て水素ガス供給源(図示せず)に接続されている。又前
記反応管2の下端には排気管10が接続され、該排気管
10は第3バルブ11を介して図示しない排気装置に接
続され、又前記排気管10の第3バルブ11の上流側に
は第4バルブ12を介して排気ポンプ13が連通してい
る。
A reaction tube 2 is provided in a cylindrical heater 1.
A boat 4 loaded with wafers 3 in a horizontal posture in multiple stages is loaded in the reaction tube 2. A nozzle 5 provided upright along the inner wall of the reaction tube 2 is connected to a nitrogen gas supply source (not shown) through a first flow rate regulator 6 and a first valve 7, and the nozzle 5 is a second nozzle. It is connected to a hydrogen gas supply source (not shown) via the flow rate regulator 8 and the second valve 9. Further, an exhaust pipe 10 is connected to a lower end of the reaction pipe 2, the exhaust pipe 10 is connected to an exhaust device (not shown) through a third valve 11, and the exhaust pipe 10 is connected to an upstream side of the third valve 11. Is connected to an exhaust pump 13 via a fourth valve 12.

【0004】水素アニール処理は高温下で水素ガスを流
通させ、ウェーハの水素アニール処理を行うが、水素ガ
スの特性上、酸素が混入したまま温度を上昇させると爆
発の危険がある。この為、処理を行う前に、前記第1バ
ルブ7、第2バルブ9、第3バルブ11を閉じ、前記第
4バルブ12を開き前記排気ポンプ13により反応管2
内を一度真空引きし、炉内の酸素を充分に除去してから
第4バルブ12を閉じ、前記第1バルブ7を開いて窒素
ガスを供給し、前記反応管2内を大気圧迄復圧した後、
第1バルブ7を閉じ、前記第2バルブ9、第3バルブ1
1を開いて水素ガスを供給する。水素ガスにより窒素ガ
スを押出す形で炉内を水素ガス雰囲気にし、アニール処
理を行う。
In the hydrogen annealing treatment, hydrogen gas is circulated at a high temperature to perform hydrogen annealing treatment on the wafer. However, due to the characteristics of hydrogen gas, there is a danger of explosion if the temperature is raised while oxygen is mixed. Therefore, before processing, the first valve 7, the second valve 9, and the third valve 11 are closed, the fourth valve 12 is opened, and the reaction tube 2 is opened by the exhaust pump 13.
The inside of the furnace is evacuated once to sufficiently remove oxygen in the furnace, then the fourth valve 12 is closed, the first valve 7 is opened to supply nitrogen gas, and the pressure inside the reaction tube 2 is restored to atmospheric pressure. After doing
The first valve 7 is closed, and the second valve 9 and the third valve 1 are closed.
Open 1 to supply hydrogen gas. Annealing is performed in a hydrogen gas atmosphere in the furnace by extruding nitrogen gas with hydrogen gas.

【0005】[0005]

【発明が解決しようとする課題】従来水素アニール処理
は、炉内温度400〜450℃で行っているが、炉内温
度を1100〜1200℃の高温で行う場合もある。と
ころが炉内温度が1100〜1200℃では反応管の剛
性、強度が低下するので、前記した様に反応管内部を窒
素ガスに置換する過程で反応管内を減圧すると、減圧時
に反応管が変形する虞れがあった。従って、従来の半導
体製造装置の熱処理炉では高温での水素アニール処理は
できないという問題があった。
Conventionally, the hydrogen annealing treatment is carried out at a furnace temperature of 400 to 450 ° C., but it may be carried out at a furnace temperature of 1100 to 1200 ° C. However, when the temperature in the furnace is 1100 to 1200 ° C., the rigidity and strength of the reaction tube decrease. Therefore, if the pressure inside the reaction tube is reduced in the process of replacing the inside of the reaction tube with nitrogen gas as described above, the reaction tube may be deformed during the pressure reduction. There was Therefore, there is a problem that the hydrogen annealing treatment at a high temperature cannot be performed in the conventional heat treatment furnace of the semiconductor manufacturing apparatus.

【0006】本発明は斯かる実情に鑑み、減圧工程を含
む高温での熱処理を行える様にしようとするものであ
る。
In view of the above situation, the present invention intends to enable heat treatment at a high temperature including a pressure reducing step.

【0007】[0007]

【課題を解決するための手段】本発明は、反応管内に不
活性ガスを導入する管路途中に設けられたバルブと、減
圧経路の途中に設けられた他のバルブと、反応管の温度
を検出する温度検出器と、該温度検出器と設定温度とを
比較し、検出温度が設定温度以上に高い場合に信号を発
する温度コントローラとを具備し、該温度コントローラ
からの信号が発せられた場合に、前記他のバルブを閉塞
し、前記バルブを開放する様構成し、或は更に反応管の
内部圧力と大気圧との差圧を検出する大気圧ゲージを設
け、差圧が等しくなった時に不活性ガスを導入する管路
途中に設けられたバルブを閉塞する様構成した半導体製
造装置の熱処理炉に係るものである。
According to the present invention, the temperature of a reaction tube and a valve provided in the middle of a pipe for introducing an inert gas into a reaction tube, another valve provided in the middle of a depressurization path, are controlled. When a temperature detector for detecting and a temperature controller for comparing the temperature detector with a set temperature and issuing a signal when the detected temperature is higher than the set temperature are provided, and a signal from the temperature controller is issued In addition, the other valve is closed and the valve is opened, or an atmospheric pressure gauge for detecting the differential pressure between the internal pressure of the reaction tube and the atmospheric pressure is provided, and when the differential pressure becomes equal, The present invention relates to a heat treatment furnace of a semiconductor manufacturing apparatus configured to close a valve provided in the middle of a pipeline for introducing an inert gas.

【0008】[0008]

【作用】減圧途中に反応管の強度の低下が問題となる温
度迄上昇した場合に、減圧経路の途中に設けられた他の
バルブを閉塞し、減圧を停止し、或は更に不活性ガスを
導入する管路途中に設けられたバルブを開いて不活性ガ
スを導入して反応管内を復圧し、反応管への外圧を低
減、或は除去して反応管の損傷を防止する。
[Function] When the temperature of the reaction tube rises to a temperature at which reduction of the strength of the reaction tube becomes a problem during depressurization, the other valve provided in the depressurization path is closed to stop the depressurization, or further inert gas is added. A valve provided in the middle of the introducing pipe is opened to introduce an inert gas to restore the pressure in the reaction tube and reduce or remove the external pressure to the reaction tube to prevent damage to the reaction tube.

【0009】[0009]

【実施例】以下、図面を参照しつつ本発明の一実施例を
説明する。
DETAILED DESCRIPTION OF THE PREFERRED EMBODIMENTS An embodiment of the present invention will be described below with reference to the drawings.

【0010】図1中、図3中で示したものと同一のもの
には同符号を付し、その説明を省略する。
In FIG. 1, the same parts as those shown in FIG. 3 are designated by the same reference numerals and the description thereof will be omitted.

【0011】主コントローラ15を第1スイッチボック
ス16を介して前記第1バルブ7に接続し、第2スイッ
チボックス17を介して前記第3バルブ11に接続し、
第3スイッチボックス18を介して第4バルブ12にそ
れぞれ接続する。前記第3スイッチボックス18は第4
スイッチボックス21に接続されると共に該第4スイッ
チボックス21は前記第1スイッチボックス16に接続
される。
The main controller 15 is connected to the first valve 7 via a first switch box 16, and is connected to the third valve 11 via a second switch box 17.
Each of them is connected to the fourth valve 12 via the third switch box 18. The third switch box 18 has a fourth
The fourth switch box 21 is connected to the switch box 21, and the fourth switch box 21 is connected to the first switch box 16.

【0012】前記反応管2の温度を測定する熱電対等の
温度検出器19を前記ヒータ1を貫通して設け、該温度
検出器19に温度コントローラ20を接続し、該温度コ
ントローラ20は前記第3スイッチボックス18に接続
する。前記排気管10に大気圧ゲージ22を設け、該大
気圧ゲージ22には前記第4スイッチボックス21を接
続する。
A temperature detector 19 such as a thermocouple for measuring the temperature of the reaction tube 2 is provided through the heater 1, and a temperature controller 20 is connected to the temperature detector 19, and the temperature controller 20 is connected to the third controller. Connect to the switch box 18. An atmospheric pressure gauge 22 is provided on the exhaust pipe 10, and the fourth switch box 21 is connected to the atmospheric pressure gauge 22.

【0013】前記温度コントローラ20には前記反応管
2の強度が低下する温度を設定値23、例えば該反応管
2の材質が石英であるとすると850℃を設定入力して
おく。通常の作動では前記主コントローラ15からの開
閉指令信号により前記第1バルブ7、第2バルブ9、第
3バルブ11、第4バルブ12が開閉される。
The temperature controller 20 is preset with a set temperature 23 at which the strength of the reaction tube 2 decreases, for example, 850 ° C. when the material of the reaction tube 2 is quartz. In normal operation, the first valve 7, the second valve 9, the third valve 11, and the fourth valve 12 are opened / closed by an opening / closing command signal from the main controller 15.

【0014】次に、ウェーハ3の処理開始時の減圧工程
に於ける作動について説明する。
Next, the operation of the depressurizing process at the start of processing the wafer 3 will be described.

【0015】前記第1バルブ7、第2バルブ9、第3バ
ルブ11を閉じ、前記第4バルブ12を開いて前記排気
ポンプ13により反応管2内を減圧する。減圧過程の反
応管2の温度を前記温度検出器19が検出し、検出結果
は前記温度コントローラ20に入力される。該温度コン
トローラ20では検出結果と前記設定値23とを比較
し、比較の結果、設定値23より温度検出器19の検出
値が大きいと、前記温度コントローラ20より前記第3
スイッチボックス18に第4バルブ12の閉塞信号が発
せられると共に前記第4スイッチボックス21を介して
前記第1スイッチボックス16に第1バルブ7の開放信
号が発せられる。又、温度コントローラ20は前記設定
値23より温度検出器19の検出値が大きいとアラーム
信号を発して作業者等に警告を発する。
The first valve 7, the second valve 9, and the third valve 11 are closed, the fourth valve 12 is opened, and the exhaust pump 13 depressurizes the reaction tube 2. The temperature detector 19 detects the temperature of the reaction tube 2 during the depressurization process, and the detection result is input to the temperature controller 20. The temperature controller 20 compares the detection result with the set value 23. As a result of the comparison, if the detected value of the temperature detector 19 is larger than the set value 23, the temperature controller 20 outputs the third value.
A signal for closing the fourth valve 12 is issued to the switch box 18, and an opening signal for the first valve 7 is issued to the first switch box 16 via the fourth switch box 21. Further, when the detected value of the temperature detector 19 is larger than the set value 23, the temperature controller 20 issues an alarm signal to warn an operator or the like.

【0016】而して、第4バルブ12が閉塞され、反応
管2内の排気が停止すると共に前記第1バルブ7が開い
て窒素ガスが導入され、減圧が停止されると同時に昇圧
が行われ、反応管2の損傷、変形が防止される。更に、
前記反応管2内の圧力は前記大気圧ゲージ22及び第4
スイッチボックス21により監視され、大気圧となった
時点で第4スイッチボックス21から第1スイッチボッ
クス16に閉塞信号が出されて第1バルブ7が閉塞さ
れ、反応管2内が過加圧となることが防止される。
Thus, the fourth valve 12 is closed, the exhaust in the reaction tube 2 is stopped, the first valve 7 is opened to introduce the nitrogen gas, and the pressure reduction is stopped and the pressure rise is performed at the same time. The damage and deformation of the reaction tube 2 are prevented. Furthermore,
The pressure in the reaction tube 2 is equal to that of the atmospheric pressure gauge 22 and the fourth pressure gauge.
Monitored by the switch box 21, when the atmospheric pressure is reached, a closing signal is output from the fourth switch box 21 to the first switch box 16, the first valve 7 is closed, and the inside of the reaction tube 2 is over-pressurized. Is prevented.

【0017】該上記実施例では第1スイッチボックス1
6、第2スイッチボックス17、第3スイッチボックス
18、第4スイッチボックス21を主コントローラ15
と第1バルブ7、第3バルブ11、第4バルブ12の間
に介在させ、減圧時の反応管2の損傷防止作動を強制的
に行わせたが、斯かる損傷防止作動も前記主コントロー
ラ15により行う様にしてもよい。
In the above embodiment, the first switch box 1
6, the second switch box 17, the third switch box 18, the fourth switch box 21 to the main controller 15
And the first valve 7, the third valve 11, and the fourth valve 12 are interposed to forcefully perform the damage prevention operation of the reaction tube 2 at the time of decompression. It may be performed by.

【0018】図2は主コントローラ15による損傷防止
作動を行わせる他の実施例を示しており、温度コントロ
ーラ20からの信号、前記大気圧ゲージ22とからの信
号が前記主コントローラ15に入力される様になってお
り、温度コントローラ20は前記設定値23より温度検
出器19の検出値が大きいと前記主コントローラ15に
信号を出力し、該主コントローラ15は前記第4バルブ
12を閉塞し、前記第1バルブ7を開放し、排気を停止
させると共に窒素ガスを反応管2内に導入する。更に、
反応管2内が大気圧になったことを前記大気圧ゲージ2
2が検出すると主コントローラ15は前記第1バルブ7
を閉塞する。
FIG. 2 shows another embodiment in which the damage prevention operation is carried out by the main controller 15. The signal from the temperature controller 20 and the signal from the atmospheric pressure gauge 22 are inputted to the main controller 15. The temperature controller 20 outputs a signal to the main controller 15 when the detected value of the temperature detector 19 is larger than the set value 23, and the main controller 15 closes the fourth valve 12, The first valve 7 is opened, the exhaust is stopped, and nitrogen gas is introduced into the reaction tube 2. Furthermore,
The atmospheric pressure gauge 2 indicates that the inside of the reaction tube 2 is at atmospheric pressure.
2 is detected, the main controller 15 causes the first valve 7
To block.

【0019】尚、上記温度検出器19は熱電対以外の光
検出による温度測定に代えてもよい等適宜変更が可能で
あることは言う迄もなく、窒素ガスはアルゴンガス等の
他の不活性ガスに代えてもよく、又本発明は横型炉に実
施可能なことも勿論である。
Needless to say, the temperature detector 19 may be changed as appropriate, such as temperature measurement by light detection other than a thermocouple, and nitrogen gas may be other inert gas such as argon gas. Of course, the gas may be used, and the present invention can be applied to a horizontal furnace.

【0020】[0020]

【発明の効果】以上述べた如く本発明によれば、高温熱
処理に於ける反応管の損傷を防止することができ、半導
体製造装置の熱処理炉に於ける高温熱処理を可能とし、
又強制的な保護作動が行われるので操作ミスによる反応
管の損傷を防止できる等の優れた効果を発揮する。
As described above, according to the present invention, it is possible to prevent the damage of the reaction tube in the high temperature heat treatment, and enable the high temperature heat treatment in the heat treatment furnace of the semiconductor manufacturing apparatus.
Further, since the protective operation is compulsorily performed, it is possible to prevent the damage of the reaction tube due to the operation mistake, and the like, which is an excellent effect.

【図面の簡単な説明】[Brief description of drawings]

【図1】本発明の一実施例を示す概略図説明図である。FIG. 1 is a schematic diagram illustrating an embodiment of the present invention.

【図2】本発明の他の実施例を示す概略図説明図であ
る。
FIG. 2 is a schematic diagram illustrating another embodiment of the present invention.

【図3】従来例を示す概略図説明図である。FIG. 3 is a schematic diagram illustrating a conventional example.

【符号の説明】[Explanation of symbols]

1 ヒータ 2 反応管 7 第1バルブ 10 排気管 11 第3バルブ 12 第4バルブ 19 温度検出器 20 温度コントローラ 22 大気圧ゲージ 1 heater 2 reaction tubes 7 First valve 10 exhaust pipe 11 third valve 12th valve 19 Temperature detector 20 Temperature controller 22 Atmospheric pressure gauge

Claims (2)

(57)【特許請求の範囲】(57) [Claims] 【請求項1】 反応管内に不活性ガスを導入する管路途
中に設けられたバルブと、減圧経路の途中に設けられた
他のバルブと、反応管の温度を検出する温度検出器と、
該温度検出器と設定温度とを比較し、検出温度が設定温
度以上に高い場合に信号を発する温度コントローラとを
具備し、該温度コントローラからの信号が発せられた場
合に、前記他のバルブを閉塞し、前記バルブを開放する
様構成したことを特徴とする半導体製造装置の熱処理
炉。
1. A valve provided in the middle of a pipeline for introducing an inert gas into the reaction tube, another valve provided in the middle of the decompression path, and a temperature detector for detecting the temperature of the reaction tube.
A temperature controller that compares the temperature detector with a set temperature and issues a signal when the detected temperature is higher than the set temperature; and when the signal from the temperature controller is issued, the other valve is turned on. A heat treatment furnace of a semiconductor manufacturing apparatus, which is configured to be closed and the valve is opened.
【請求項2】 反応管の内部圧力と大気圧との差圧を検
出する大気圧ゲージを設け、差圧が等しくなった時に不
活性ガスを導入する管路途中に設けられたバルブを閉塞
する様構成した請求項1の半導体製造装置の熱処理炉。
2. An atmospheric pressure gauge for detecting the pressure difference between the internal pressure of the reaction tube and the atmospheric pressure is provided, and a valve provided in the middle of the conduit for introducing the inert gas when the pressure difference becomes equal is closed. The heat treatment furnace of the semiconductor manufacturing apparatus according to claim 1, which is configured as described above.
JP01751695A 1995-01-09 1995-01-09 Heat treatment furnace for semiconductor manufacturing equipment Expired - Lifetime JP3437308B2 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP01751695A JP3437308B2 (en) 1995-01-09 1995-01-09 Heat treatment furnace for semiconductor manufacturing equipment

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP01751695A JP3437308B2 (en) 1995-01-09 1995-01-09 Heat treatment furnace for semiconductor manufacturing equipment

Publications (2)

Publication Number Publication Date
JPH08191075A JPH08191075A (en) 1996-07-23
JP3437308B2 true JP3437308B2 (en) 2003-08-18

Family

ID=11946134

Family Applications (1)

Application Number Title Priority Date Filing Date
JP01751695A Expired - Lifetime JP3437308B2 (en) 1995-01-09 1995-01-09 Heat treatment furnace for semiconductor manufacturing equipment

Country Status (1)

Country Link
JP (1) JP3437308B2 (en)

Also Published As

Publication number Publication date
JPH08191075A (en) 1996-07-23

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