JP3333557B2 - How to make persimmon wine - Google Patents
How to make persimmon wineInfo
- Publication number
- JP3333557B2 JP3333557B2 JP24047792A JP24047792A JP3333557B2 JP 3333557 B2 JP3333557 B2 JP 3333557B2 JP 24047792 A JP24047792 A JP 24047792A JP 24047792 A JP24047792 A JP 24047792A JP 3333557 B2 JP3333557 B2 JP 3333557B2
- Authority
- JP
- Japan
- Prior art keywords
- persimmon
- wine
- juice
- persimmon wine
- gelatin
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
Description
【0001】[0001]
【産業上の利用分野】本発明は、劣化の遅い柿ワインの
製造法に関する。BACKGROUND OF THE INVENTION 1. Field of the Invention The present invention relates to a method for producing persimmon wine having a slow deterioration.
【0002】[0002]
【従来の技術】従来柿を原料として柿果汁を作り、ブド
ウ果汁からワインを作ると同様に柿果汁から柿ワインが
製造できることは公知である。また柿の果実には、フェ
ノール性物質、例えばカテキン、縮合型タンニン、フラ
ボノイドなどが多量に存在していることは公知である。2. Description of the Related Art It is known that persimmon juice can be produced from persimmon juice in the same manner as persimmon juice is made from persimmon as a raw material and wine is made from grape juice. It is known that persimmon fruits contain a large amount of phenolic substances such as catechin, condensed tannin, and flavonoids.
【0003】[0003]
【発明が解決しようとする課題】従来の柿ワインは劣化
が早いため、短期間のうちに褐変し、香味も損なわれて
しまう。Since the conventional persimmon wine deteriorates quickly, it browns in a short period of time and the flavor is impaired.
【0004】[0004]
【課題を解決するための手段】本発明者は、柿ワイン製
造工程上、柿果汁の段階または柿ワイン醸成後に、柿果
汁または柿ワインに含まれるフェノール性物質を除去ま
たは低減することにより、柿ワインの劣化が遅くなるこ
とを見出し、本発明を完成するに至った。本発明は、柿
を用いて柿ワインを製造する方法において、柿果汁もし
くは柿ワインに含まれるフェノール性物質と結合または
吸着できる物質で柿果汁もしくは柿ワインを処理するこ
とを特徴とする柿ワインの製造法に関する。Means for Solving the Problems In the persimmon wine production process, the present inventor removed or reduced the phenolic substances contained in persimmon juice or persimmon wine at the stage of persimmon juice or after brewing persimmon wine, thereby improving persimmon wine. The present inventors have found that the deterioration of wine is delayed, and have completed the present invention. The present invention provides a method for producing persimmon wine using persimmon, wherein persimmon juice or persimmon wine is treated with a substance capable of binding or adsorbing to a phenolic substance contained in persimmon juice or persimmon wine. Related to manufacturing method.
【0005】以下、本発明を詳細に説明する。本発明に
おける柿果汁もしくは柿ワインに含まれるフェノール性
物質と結合または吸着できる物質としては、例えばゼラ
チン、アルブミン、カゼイン、グロブリン、グルテリ
ン、プロラミンなどのタンパク質(好ましくはゼラチ
ン、アルブミン)あるいはシリカゾル、シリカゲル、シ
リカ粉末など(好ましくはコロイド状シリカゾル)があ
げられ、これらを単独または2種以上組み合わせて用い
ればよい。Hereinafter, the present invention will be described in detail. Examples of the substance capable of binding or adsorbing to the phenolic substance contained in the persimmon juice or persimmon wine in the present invention include proteins such as gelatin, albumin, casein, globulin, glutelin, and prolamin (preferably gelatin, albumin) or silica sol, silica gel, Examples thereof include silica powder and the like (preferably colloidal silica sol), and these may be used alone or in combination of two or more.
【0006】また、本発明における柿果汁もしくは柿ワ
インを処理するとは、柿果汁もしくは柿ワインに、フェ
ノール性物質と結合または吸着できる物質を接触させれ
ばよく、例えば、柿果汁もしくは柿ワインにフェノール
性物質と結合または吸着できる物質を混合し、ついで遠
心分離、ろ過などによりフェノール性物質と結合または
吸着できる物質を除去する方法、あるいはシリカゲル、
カラギーナン等の担体あるいは膜などにフェノール性物
質と結合または吸着できる物質を固定化し、これに柿果
汁または柿ワインを通す方法などがあげられる。The treatment of persimmon juice or persimmon wine in the present invention may be achieved by bringing persimmon juice or persimmon wine into contact with a substance capable of binding or adsorbing a phenolic substance. A method of mixing a substance capable of binding or adsorbing with a phenolic substance by mixing a substance capable of binding or adsorbing with a phenolic substance, or silica gel,
A method in which a substance capable of binding or adsorbing to a phenolic substance is immobilized on a carrier such as carrageenan or a membrane, and persimmon juice or persimmon wine is passed through the immobilized substance.
【0007】本発明に用いる柿品種は富有、次郎、駿
河、禅寺丸、平核無、会津身不知など甘柿、渋柿を問わ
ずいずれの品種も用いることができる。柿果汁は、柿を
破砕した際得られる果汁または柿を搾汁したものが用い
られ、柿ワインとしてはその柿果汁を酵母で発酵させた
ものを用いればよい。処理に用いるフェノール性物質と
結合または吸着できる物質、例えばゼラチンは市販の粉
末のものを用いればよい。アルブミンについては、市販
の粉末アルブミンの他、鶏卵白を用いることもできる。
コロイド状シリカゾルには様々な市販品があり、いずれ
も用いることができるが、コポロック300TM(大塚化学
社製)が効果の上で優れている。As the persimmon variety used in the present invention, any variety such as Fuyu, Jiro, Suruga, Zenjimaru, Hiraganashi, Aizu Shiranu and other persimmons and astringent persimmons can be used. As the persimmon juice, juice obtained by crushing the persimmon or squeezed persimmon is used. As persimmon wine, persimmon juice obtained by fermenting the persimmon juice with yeast may be used. As a substance capable of binding or adsorbing to the phenolic substance used in the treatment, for example, gelatin, a commercially available powder may be used. As for albumin, chicken egg white can be used in addition to commercially available powdered albumin.
There are various commercially available colloidal silica sols, and any of them can be used. Copoloc 300 ™ (manufactured by Otsuka Chemical Co., Ltd.) is superior in effect.
【0008】ゼラチンあるいはアルブミンの添加量は、
柿果汁、柿ワインいずれの場合も、それぞれ、5 〜1000
mg/lであるが、望ましくは30〜200mg/l である。コロイ
ド状シリカゾルの添加量は、0.03〜2ml/l であるが、望
ましくは0.2 〜1.0ml/l である。処理に用いるフェノー
ル性物質と結合または吸着できる物質、例えばゼラチ
ン、アルブミンまたはコロイド状シリカゾルなどをそれ
ぞれ単独で使うかあるいは併用するかについては、柿果
汁または柿ワインのフェノール性物質含量さらにはフェ
ノールの成分組成によって異なるが、柿果汁処理、柿ワ
イン処理いずれの場合も、概して、ゼラチンとコロイド
状シリカゾルを併用した場合に効果が優れている。[0008] The amount of gelatin or albumin added is
In the case of persimmon juice and persimmon wine, 5-1000 each
mg / l, preferably 30-200 mg / l. The addition amount of the colloidal silica sol is from 0.03 to 2 ml / l, preferably from 0.2 to 1.0 ml / l. The substance capable of binding or adsorbing with the phenolic substance used in the treatment, such as gelatin, albumin or colloidal silica sol, is used alone or in combination, depending on the phenolic substance content of persimmon juice or persimmon wine and also the phenol component. Although different depending on the composition, in both cases of persimmon juice treatment and persimmon wine treatment, the effect is generally excellent when gelatin and colloidal silica sol are used in combination.
【0009】処理温度は、柿果汁または柿ワインが凍結
しない温度ならいずれも用いることができるが、好適に
は5〜25℃である。処理期間は、柿果汁、柿ワインのフ
ェノール性物質の組成、含量によっても異なるが、通常
2〜18時間であり、15時間ぐらいが望ましい。以下に本
発明の実施例を示す。The treatment temperature may be any temperature at which the persimmon juice or persimmon wine does not freeze, but is preferably 5 to 25 ° C. The treatment period varies depending on the composition and content of phenolic substances in persimmon juice and persimmon wine, but usually
It is 2 to 18 hours, preferably about 15 hours. Hereinafter, examples of the present invention will be described.
【0010】[0010]
実施例1 禅寺丸種柿50kgを破砕した後搾汁し、約35リットルの柿
果汁を得た。この柿果汁にピロ亜硫酸カリウム100mg/l
、酒石酸4g/lを加え、ペクチナーゼ標品スミチ−ムS
PC(新日本化学社製)を200mg/l 添加して、攪はん後1
5℃で放置した。24時間後に柿果汁を遠心し、清澄柿果
汁約30リットルを得た。この清澄柿果汁に、同じ柿果汁
中あらかじめ20℃で3 日間培養したワイン酵母サッカロ
マイセス・セレビシエ(Saccharomyces cerevisiae)KY
-5700株〔化学と生物,28, 800(1990)〕の培養液を酒母
として1.5 リットル加え、15℃で発酵を行った。Example 1 After crushing 50 kg of Zenji-maru seed persimmon, the juice was squeezed to obtain about 35 liters of persimmon juice. 100 mg / l potassium pyrosulfite in this persimmon juice
, Tartaric acid 4 g / l, and pectinase standard Sumitime S
Add 200mg / l PC (manufactured by Shin Nippon Chemical Co., Ltd.)
It was left at 5 ° C. After 24 hours, the persimmon juice was centrifuged to obtain about 30 liters of clear persimmon juice. Saccharomyces cerevisiae KY, a wine yeast cultured in the same persimmon juice at 20 ° C for 3 days in advance,
1.5 liters of a culture solution of -5700 strain [Chemistry and Organisms, 28 , 800 (1990)] was added as fermenter and fermentation was carried out at 15 ° C.
【0011】発酵開始後10日目に、ピロ亜硫酸カリウム
160mg/lをモロミに添加し、遠心分離を行って発酵を停
止させ、柿ワイン約29リットルを得た。この柿ワインを
2等分して一方に、コロイド状シリカゾル コポロック
300TM を0.5ml/l 加えて攪はんした後、少量の温水で溶
解したゼラチン粉末を50mg/l添加して混ぜ、攪はんを止
めて16時間放置した。次に、オリ部分がなるべく混入し
ないように分離した上澄約13リットルに、0.5g/lのベン
トナイト(関東ベントナイト鉱業社製)を加えて攪はん
後、一晩放置し、濾過を行って、柿ワイン(シリカゾル
−ゼラチン処理)約12リットルを得た。一方、残りの半
量については、シリカゾル−ゼラチン処理を行わずに、
0.5g/lのベントナイトを添加して攪はん後、一晩放置
し、濾過を行って、柿ワイン(無処理)約14リットルを
得た。Ten days after the start of fermentation, potassium pyrosulfite
160 mg / l was added to moromi, and the fermentation was stopped by centrifugation to obtain about 29 liters of persimmon wine. Divide this persimmon wine into two equal parts, and add colloidal silica sol
After 0.5 ml / l of 300 TM was added and the mixture was stirred, 50 mg / l of gelatin powder dissolved in a small amount of warm water was added and mixed, the stirring was stopped, and the mixture was allowed to stand for 16 hours. Next, 0.5 g / l of bentonite (manufactured by Kanto Bentonite Mining Co., Ltd.) was added to about 13 liters of the supernatant separated so that the ori portion was not mixed as much as possible. After stirring, the mixture was allowed to stand overnight and filtered. And about 12 liters of persimmon wine (silica sol-gelatin treatment). On the other hand, for the other half, without silica sol-gelatin treatment,
After stirring by adding 0.5 g / l of bentonite, the mixture was allowed to stand overnight and filtered to obtain about 14 liters of persimmon wine (untreated).
【0012】得られた柿ワインのシリカゾル−ゼラチン
処理前および処理後における総フェノール含量を測定し
た。結果を第1表に示す。The total phenol content of the persimmon wine before and after the silica sol-gelatin treatment was measured. The results are shown in Table 1.
【0013】[0013]
【表1】 [Table 1]
【0014】さらに醸成した柿ワインの分析値と官能評
価結果を第2表に示す。なお、劣化の指標としてOD
430nm 1cm を測定した。30℃で 3ケ月保存をしてもOD
430nm 1cm の値が0.10を超えない場合、劣化が遅いこと
を意味する。また、官能評価は熟練した7名よりなるパ
ネルを用いて行った。[0014] Analytical values and sensory evaluation of the further brewed persimmon wine
The results are shown in Table 2. Note that OD is an indicator of deterioration.
430nm 1cmWas measured. OD even after storage at 30 ℃ for 3 months
430nm 1cmIf the value does not exceed 0.10, the deterioration is slow
Means In addition, the sensory evaluation was performed by a
This was performed using a flannel.
【0015】[0015]
【表2】 [Table 2]
【0016】さらに、これら両区の柿ワインを、720ml
ボルドー型ビンにつめ、スクリューキャップを打栓し
て、5℃および30℃において、保存テストを行った。そ
の結果を第3表に示す。[0016] Furthermore, 720 ml of persimmon wine of these two districts
Storage tests were performed at 5 ° C. and 30 ° C., packed in a Bordeaux bottle, stoppered with a screw cap. Table 3 shows the results.
【0017】[0017]
【表3】 [Table 3]
【0018】実施例2 富有柿50kgを破砕した後搾汁して得た約37リットルの柿
果汁に、ピロ亜硫酸カリウム150mg/l 、酒石酸4.2g/lを
加え、スミチームSPC200mg/lを添加して15℃で16時間放
置した後、上澄約31リットルを分離した。この上澄を2
等分して一方にコロイド状シリカゾル コポロック300TM
1.2ml/l 、少量の温水で溶解したゼラチン粉末0.8mg/l
をこの順で攪はんしながら加え、攪はんを止めてから1
5℃において8時間放置した後、上清約12.5リットルを
得た。得られた柿果汁のシリカゾル−ゼラチン処理前お
よび処理後における総フェノール含量を測定した。結果
を第4表に示す。Example 2 To about 37 liters of persimmon juice obtained by crushing and squeezing 50 kg of Fuyu persimmon, 150 mg / l of potassium pyrosulfite and 4.2 g / l of tartaric acid were added, and 200 mg / l of Sumizyme SPC was added. After standing at 15 ° C. for 16 hours, about 31 liters of supernatant was separated. This supernatant is
Equally divided into colloidal silica sol, Copoloc 300 TM
1.2ml / l, gelatin powder 0.8mg / l dissolved in a small amount of warm water
While stirring in this order.
After standing at 5 ° C. for 8 hours, about 12.5 liters of supernatant was obtained. The total phenol content of the obtained persimmon juice before and after the silica sol-gelatin treatment was measured. The results are shown in Table 4.
【0019】[0019]
【表4】 [Table 4]
【0020】このシリカゾル−ゼラチン処理柿果汁と他
方の無処理柿果汁に、無処理柿果汁中であらかじめ20
℃、3日間培養したワイン酵母サッカロマイセス・セレ
ビシエ(Saccharomyces cerevisiae)プリーズ・ド・
ムース株を酒母として、それぞれ0.63リットル、0.78リ
ットルずつ加え、15℃で発酵を行った。発酵開始後12日
目に、各々、ピロ亜硫酸カリウム160mg/l をモロミに添
加し、遠心分離を行って発酵を停止させ、ベントナイト
0.6g/lを加えて、一晩放置し、濾過を行って柿ワインを
得た。処理柿果汁および無処理柿果汁から醸成された柿
ワインは、各々約11リットルおよび約13リットルであっ
た。The silica sol-gelatin-treated persimmon juice and the other untreated persimmon juice are mixed in advance with the untreated persimmon juice.
℃, 3 days of culture wine yeast Saccharomyces cerevisiae (Saccharomyces cerevisiae) Please de
0.63 liter and 0.78 liter of the mousse strain were added to the mother, respectively, and fermentation was performed at 15 ° C. On the 12th day after the start of fermentation, 160 mg / l of potassium pyrosulfite was added to the moromi, and the fermentation was stopped by centrifugation.
0.6 g / l was added, the mixture was allowed to stand overnight, and filtered to obtain persimmon wine. Persimmon wines brewed from treated and untreated persimmon juice were about 11 liters and about 13 liters, respectively.
【0021】醸成された柿ワインの分析値を第5表に示
した。なお、官能評価は熟練した7名よりなるパネルを
用いて行った。The analytical values of the brewed persimmon wine are shown in Table 5. In addition, the sensory evaluation was performed using the panel which consists of seven skilled people.
【0022】[0022]
【表5】 [Table 5]
【0023】次に、これら2種の柿ワインについて、 7
20mlボルドー型ビン中で5℃および30℃における保存テ
ストを行った。その結果を、第6表に示した。Next, about these two kinds of persimmon wines,
Storage tests were performed at 5 ° C. and 30 ° C. in 20 ml Bordeaux bottles. The results are shown in Table 6.
【0024】[0024]
【表6】 [Table 6]
【0025】[0025]
【発明の効果】本発明の方法によれば、劣化の遅い柿ワ
インを製造することができる。According to the method of the present invention, persimmon wine with a slow deterioration can be produced.
───────────────────────────────────────────────────── フロントページの続き (72)発明者 山本 秀城 山梨県山梨市小原西791 (72)発明者 西牧 憲一 山梨県塩山市西野原419 (72)発明者 北野 一好 山梨県甲府市大里町1098 審査官 伏見 邦彦 (56)参考文献 特開 昭60−27376(JP,A) 特開 昭60−180574(JP,A) 特開 平2−268676(JP,A) 特開 昭58−71883(JP,A) (58)調査した分野(Int.Cl.7,DB名) C12G 1/00 - 3/14 C12H 1/00 - 1/22 JICSTファイル(JOIS) 食品関連文献情報(食ネット)──────────────────────────────────────────────────続 き Continued on the front page (72) Inventor Hideki Yamamoto 791 Ohara Nishi, Yamanashi City, Yamanashi Prefecture (72) Inventor Kenichi Nishimaki 419, Nishinohara, Enzan City, Yamanashi Prefecture (72) Inventor Kazuyoshi Kitano 1098 Osatocho, Kofu City, Yamanashi Prefecture Examiner Kunihiko Fushimi (56) References JP-A-60-27376 (JP, A) JP-A-60-180574 (JP, A) JP-A-2-268676 (JP, A) JP-A-58-71883 (JP) , A) (58) Fields surveyed (Int. Cl. 7 , DB name) C12G 1/00-3/14 C12H 1/00-1/22 JICST file (JOIS) Food-related literature information (food net)
Claims (1)
いて、ゼラチンまたはアルブミンとコロイド状シリカゾ
ルとを併用して柿果汁または柿ワインを処理することを
特徴とする柿ワインの製造法。1. A method for producing persimmon wine using persimmon, comprising: gelatin or albumin and colloidal silica.
Preparation of persimmon wine, characterized in that in combination with Le processing the persimmon juice or persimmon wine.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP24047792A JP3333557B2 (en) | 1992-09-09 | 1992-09-09 | How to make persimmon wine |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP24047792A JP3333557B2 (en) | 1992-09-09 | 1992-09-09 | How to make persimmon wine |
Publications (2)
Publication Number | Publication Date |
---|---|
JPH0690730A JPH0690730A (en) | 1994-04-05 |
JP3333557B2 true JP3333557B2 (en) | 2002-10-15 |
Family
ID=17060101
Family Applications (1)
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JP24047792A Expired - Fee Related JP3333557B2 (en) | 1992-09-09 | 1992-09-09 | How to make persimmon wine |
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Country | Link |
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JP (1) | JP3333557B2 (en) |
Families Citing this family (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
IT1303918B1 (en) * | 1998-06-05 | 2001-03-01 | Esseco S P A | BEVERAGE CLARIFICATION METHOD |
JP4500078B2 (en) * | 2004-03-24 | 2010-07-14 | 奈良県 | Extract method of persimmon tannin and persimmon tannin extracted by this method |
CN114806410A (en) * | 2021-01-21 | 2022-07-29 | 肖清风 | Method for preparing persimmon paint |
-
1992
- 1992-09-09 JP JP24047792A patent/JP3333557B2/en not_active Expired - Fee Related
Also Published As
Publication number | Publication date |
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JPH0690730A (en) | 1994-04-05 |
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