JP3223982U - Industrial supercritical compound extraction structure - Google Patents
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- JP3223982U JP3223982U JP2019003341U JP2019003341U JP3223982U JP 3223982 U JP3223982 U JP 3223982U JP 2019003341 U JP2019003341 U JP 2019003341U JP 2019003341 U JP2019003341 U JP 2019003341U JP 3223982 U JP3223982 U JP 3223982U
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- 238000000605 extraction Methods 0.000 title claims abstract description 49
- 150000001875 compounds Chemical class 0.000 title claims description 4
- 239000003054 catalyst Substances 0.000 claims abstract description 27
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 claims abstract description 26
- 229910002092 carbon dioxide Inorganic materials 0.000 claims abstract description 13
- 239000001569 carbon dioxide Substances 0.000 claims abstract description 13
- 239000002131 composite material Substances 0.000 claims abstract description 13
- 238000010438 heat treatment Methods 0.000 claims abstract description 5
- 238000009833 condensation Methods 0.000 claims abstract description 4
- 230000005494 condensation Effects 0.000 claims abstract description 4
- 238000003780 insertion Methods 0.000 claims description 7
- 230000037431 insertion Effects 0.000 claims description 7
- 239000000463 material Substances 0.000 claims description 7
- 238000001816 cooling Methods 0.000 claims description 6
- 239000002994 raw material Substances 0.000 abstract description 9
- 239000000284 extract Substances 0.000 abstract description 6
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 abstract 1
- 229910052799 carbon Inorganic materials 0.000 abstract 1
- 241000218236 Cannabis Species 0.000 description 3
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 3
- QHMBSVQNZZTUGM-UHFFFAOYSA-N Trans-Cannabidiol Natural products OC1=CC(CCCCC)=CC(O)=C1C1C(C(C)=C)CCC(C)=C1 QHMBSVQNZZTUGM-UHFFFAOYSA-N 0.000 description 3
- QHMBSVQNZZTUGM-ZWKOTPCHSA-N cannabidiol Chemical compound OC1=CC(CCCCC)=CC(O)=C1[C@H]1[C@H](C(C)=C)CCC(C)=C1 QHMBSVQNZZTUGM-ZWKOTPCHSA-N 0.000 description 3
- 229950011318 cannabidiol Drugs 0.000 description 3
- ZTGXAWYVTLUPDT-UHFFFAOYSA-N cannabidiol Natural products OC1=CC(CCCCC)=CC(O)=C1C1C(C(C)=C)CC=C(C)C1 ZTGXAWYVTLUPDT-UHFFFAOYSA-N 0.000 description 3
- PCXRACLQFPRCBB-ZWKOTPCHSA-N dihydrocannabidiol Natural products OC1=CC(CCCCC)=CC(O)=C1[C@H]1[C@H](C(C)C)CCC(C)=C1 PCXRACLQFPRCBB-ZWKOTPCHSA-N 0.000 description 3
- VLKZOEOYAKHREP-UHFFFAOYSA-N n-Hexane Chemical compound CCCCCC VLKZOEOYAKHREP-UHFFFAOYSA-N 0.000 description 3
- 239000002904 solvent Substances 0.000 description 3
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 2
- ATUOYWHBWRKTHZ-UHFFFAOYSA-N Propane Chemical compound CCC ATUOYWHBWRKTHZ-UHFFFAOYSA-N 0.000 description 2
- 238000000034 method Methods 0.000 description 2
- 238000000638 solvent extraction Methods 0.000 description 2
- VGGSQFUCUMXWEO-UHFFFAOYSA-N Ethene Chemical compound C=C VGGSQFUCUMXWEO-UHFFFAOYSA-N 0.000 description 1
- 239000005977 Ethylene Substances 0.000 description 1
- CYQFCXCEBYINGO-UHFFFAOYSA-N THC Natural products C1=C(C)CCC2C(C)(C)OC3=CC(CCCCC)=CC(O)=C3C21 CYQFCXCEBYINGO-UHFFFAOYSA-N 0.000 description 1
- 229910021529 ammonia Inorganic materials 0.000 description 1
- 230000000049 anti-anxiety effect Effects 0.000 description 1
- 230000001773 anti-convulsant effect Effects 0.000 description 1
- 230000003110 anti-inflammatory effect Effects 0.000 description 1
- 239000001961 anticonvulsive agent Substances 0.000 description 1
- 229960003965 antiepileptics Drugs 0.000 description 1
- 239000002249 anxiolytic agent Substances 0.000 description 1
- CYQFCXCEBYINGO-IAGOWNOFSA-N delta1-THC Chemical compound C1=C(C)CC[C@H]2C(C)(C)OC3=CC(CCCCC)=CC(O)=C3[C@@H]21 CYQFCXCEBYINGO-IAGOWNOFSA-N 0.000 description 1
- 229960004242 dronabinol Drugs 0.000 description 1
- 229940079593 drug Drugs 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 230000000857 drug effect Effects 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 235000019441 ethanol Nutrition 0.000 description 1
- 229910001385 heavy metal Inorganic materials 0.000 description 1
- 239000001294 propane Substances 0.000 description 1
- QQONPFPTGQHPMA-UHFFFAOYSA-N propylene Natural products CC=C QQONPFPTGQHPMA-UHFFFAOYSA-N 0.000 description 1
- 125000004805 propylene group Chemical group [H]C([H])([H])C([H])([*:1])C([H])([H])[*:2] 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 231100000331 toxic Toxicity 0.000 description 1
- 230000002588 toxic effect Effects 0.000 description 1
- 231100000419 toxicity Toxicity 0.000 description 1
- 230000001988 toxicity Effects 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
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Abstract
【課題】産業型超臨界複合式抽出構造を提供する。【解決手段】抽出装置に抽出対象物Ｂを抽出するための原料取付具Ａを内設し、複合触媒装置５の触媒容器５１にて補助抽出の触媒Ｃを収容し、超臨界装置６に二酸化炭素を抽出装置１１に抽出する加圧素子６２と、二酸化炭素の温度を引き上げる加熱素子６４とを有し、収集容器Ｆに収集素子を内設し、収集素子が抽出装置の収集チューブ７３に接続していて、収集チューブが収集容器の上方に対応して凝縮滴下口７５を設ける。これにより、超臨界の二酸化炭素Ｄが効率的に抽出対象物を抽出できる。【選択図】図１An industrial supercritical composite extraction structure is provided. A raw material fixture A for extracting an extraction object B is provided in an extraction device, a catalyst C for auxiliary extraction is accommodated in a catalyst container 51 of a composite catalyst device 5, and a supercritical device 6 contains carbon dioxide. It has a pressurizing element 62 that extracts carbon to the extraction device 11 and a heating element 64 that raises the temperature of carbon dioxide. A collecting element is provided in the collecting container F, and the collecting element is connected to a collecting tube 73 of the extracting device. The collection tube is provided with a condensation dripping port 75 corresponding to the upper side of the collection container. Thereby, supercritical carbon dioxide D can extract an extraction target efficiently. [Selection] Figure 1
Description
本考案は産業型超臨界複合式抽出構造に関し、特に超臨界状態の二酸化炭素を用いて、抽出対象物の加圧抽出技術分野に関する。 The present invention relates to an industrial supercritical combined extraction structure, and more particularly to the technical field of pressurized extraction of an extraction object using carbon dioxide in a supercritical state.
我々の生活に多くの薬物自体が毒性を帯びる。しかし、毒性以外に有用物がないことではない。そのうち、大麻がもっとも特色を有する。
大麻の成分には、人類に習慣性をもたらすテトラヒドロカンナビノールと習慣性を与えないカンナビジオールとを含む。そのうち、カンナビジオールには人類にとって有益性と利用価値を含まれている。薬効果の特徴は抗けいれん、抗不安、抗炎症抗等の作用を挙げられる。
Many drugs themselves are toxic to our lives. However, it is not that there are no useful substances other than toxicity. Among them, cannabis has the most characteristic features.
The components of cannabis include tetrahydrocannabinol that brings addictiveness to mankind and cannabidiol that does not add addictiveness. Among them, cannabidiol contains benefits and utility values for humanity. The characteristics of the drug effect include anticonvulsant, anti-anxiety, anti-inflammatory and other actions.
現時点、カンナビジオールの抽出について、溶剤抽出法がもっとも適切な方法と言われる。しかし、溶剤抽出法には溶剤の残留、重金属などを除去できなく、含まれている有機塩が溶剤によって破壊され、溶剤を除去するという課題が残り、大麻原料の浪費である。 At present, solvent extraction is said to be the most appropriate method for extracting cannabidiol. However, the solvent extraction method cannot remove solvent residues, heavy metals, and the like, and the organic salt contained therein is destroyed by the solvent, leaving the problem of removing the solvent, which is a waste of cannabis raw material.
本考案において、抽出装置と、自動材料供給装置と、複合触媒装置と、超臨界装置と、収集装置と、を含む、産業型超臨界複合式抽出構造が提供される。 In the present invention, an industrial supercritical composite extraction structure including an extraction device, an automatic material supply device, a composite catalyst device, a supercritical device, and a collection device is provided.
係る抽出装置の右側にピストンバルブを有し、外側は係るピストンバルブに対応してピストンローダーを有する。 The extraction device has a piston valve on the right side, and the outside has a piston loader corresponding to the piston valve.
係る自動材料供給装置に保存空間を内設し、下部に等量出力ノズルを設ける。
係る取付具搬送装置に循環ローダーを設け、循環ローダーは等量出力ノズルから係る循環ローダーに移動される。
A storage space is provided in the automatic material supply apparatus, and an equivalent output nozzle is provided in the lower part.
A circulation loader is provided in the fixture conveying apparatus, and the circulation loader is moved from the equivalent output nozzle to the circulation loader.
係る複合触媒装置に１から８の触媒容器を設け、触媒容器に触媒ポンプと、抽出装置とを接続されている。 The composite catalyst device is provided with 1 to 8 catalyst containers, and a catalyst pump and an extraction device are connected to the catalyst container.
係る超臨界装置を気体保存具につなぎ、内部に二酸化炭素を収容し、超臨界装置に加圧具を配置され、加圧具を抽出装置のベンチュリ管に接続し、ベンチュリ管に加熱素子が配置されている。 Connecting such a supercritical device to a gas storage device, containing carbon dioxide inside, placing a pressurizer in the supercritical device, connecting the pressurizer to the venturi tube of the extraction device, and placing a heating element in the venturi tube Has been.
係る収集装置に収集ローダーを内設し、収集ローダーに挿入スロットを敷設し、収集装置は収集装置の収集チューブと接続し、収集装置に収集チューブを冷却するための冷却凝縮装置を有し、収集チューブが挿入スロットの上方に対応して、凝縮滴下口を設ける。 A collecting loader is installed in the collecting device, an insertion slot is installed in the collecting loader, the collecting device is connected to the collecting tube of the collecting device, and the collecting device has a cooling condensing device for cooling the collecting tube. A tube is provided with a condensation dripping opening corresponding to the upper part of the insertion slot.
本考案において、収集装置の下方に収集ローダーを回転させるための搬送具を設け、収集装置の上方に抽出具を設け、抽出具に押上ピストン具を設け、収集装置の上方は押上ピストン具に対応する出力口仕切弁を設ける。
本考案の目的は超臨界装置を利用し、二酸化炭素を抽出装置内部で超臨界状態にした上、超臨界状態の二酸化炭素によって、抽出物を抽出する効果を実現する。
In the present invention, a conveying tool for rotating the collecting loader is provided below the collecting device, an extracting tool is provided above the collecting device, a lifting piston tool is provided on the extracting device, and the upper part of the collecting device corresponds to the pushing piston tool. An output port gate valve is provided.
The purpose of the present invention is to use a supercritical device to bring carbon dioxide into a supercritical state inside the extraction device, and to realize the effect of extracting the extract with the supercritical carbon dioxide.
本考案の産業型超臨界複合式抽出構造１が抽出装置１１と、自動材料供給装置３と、取付具搬送装置４と、複合触媒装置５と、超臨界装置６と、収集装置７とを含む。
The industrial supercritical
係る抽出装置１１に、少なくとも１つの原料取付具Ａを内設し、原料取付具Ａに抽出対象物Ｂを収容し、抽出装置１１は原料取付具Ａの右側に抽出装置１１をオンとオフ制御のピストン弁１２を有し、抽出装置１１の外側に原料取付具Ａを搬送するピストンローダー２を有する。
The
係る自動材料供給装置３に抽出対象物Ｂを取り付ける保存空間３１を有し、保存空間３１の下方に抽出対象物Ｂの出力量制御の等量出力ノズル３３を設ける。
The automatic
係る取付具搬送装置４に原料取付具Ａを等量出力ノズル３３下方に搬送して、抽出対象物Ｂを受けるための循環ローダー４１を設け、原料取付具Ａを循環ローダー４１からピストンローダー２に搬送した上、ピストンローダー２によって、抽出装置１１に送られる。
A
複合触媒装置５はメチルアルコール、エチルアルコール、ヘキサン、アンモニア、エチレン、プロパン、プロピレンと水を補助抽出ための触媒Ｃと、少なくとも８つの触媒容器５１を有し、触媒容器５１は触媒Ｃを抽出して、抽出装置１１に搬送する触媒ポンプ５２を設けられている。
The composite catalyst device 5 has a catalyst C for auxiliary extraction of methyl alcohol, ethyl alcohol, hexane, ammonia, ethylene, propane, propylene and water, and at least eight
係る超臨界装置６と気体保存具６１とを接続し、気体保存具６１の内部に二酸化炭素Ｄを収容し、超臨界装置６は気体保存具６１の二酸化炭素Ｄを抽出装置１１に抽出するため、少なくとも一つの加圧素子６２を配置し、加圧素子６２は抽出装置１１に連絡するベンチュリ管６３と連絡し、ベンチュリ管６３に二酸化炭素Ｄ温度を引き上げる加熱素子６４を設ける。
The
係る収集装置７に収集ローダー７１を内設し、収集ローダー７１に挿入スロット７２を敷設し、それぞれの挿入スロット７２に収集容器Ｆを収容し、収集装置７は少なくとも抽出装置１１につなぐ収集チューブ７３を有し、収集装置７は少なくとも収集チューブ７３を冷却するための冷却凝縮装置７４をさらに有し、収集チューブ７３が収集容器Ｆの上方に対応して少なくとも凝縮滴下口７５を設けられている（図１に示す、取付具搬送装置４図２に示す）。
A
さらに、収集装置７の下方に収集ローダー７１を回転させるための搬送具７７を設け、収集装置７の上方に抽出具７８を設け、抽出具７８に押上ピストン具７８１を設ける。搬送具７７によって、収集ローダー７１を回転させ、収集容器Ｆを抽出具７８の位置に搬送して、押上ピストン具７８１によって、収集容器Ｆを掴んで収集装置７より搬出し、収集装置７の上方が押上ピストン具７８１に対応して出力口仕切弁７１２を設ける（図１、３）。
Further, a conveying
以上の説明から分かるように、本考案の産業型超臨界複合式抽出構造１によれば、超臨界装置６を加熱して、二酸化炭素Ｄを抽出装置１１に仕込み、抽出対象物Ｂによる超臨界抽出とともに、触媒Ｃと合わせて、抽出対象物Ｂの所望成分を抽出する。このように多様性に抽出対象物Ｂを抽出できる点が本考案の優れるところである。
As can be seen from the above description, according to the industrial supercritical
Ａ 原料取付具
Ｂ 抽出対象物
Ｃ 触媒
Ｄ 二酸化炭素
Ｆ 収集容器
１ 産業型超臨界複合式抽出構造
１１ 抽出装置
１２ ピストン弁
２ ピストンローダー
３ 自動材料供給装置
３１ 保存空間
３３ 等量出力ノズル
４ 取付具搬送装置
４１ 循環ローダー
５ 複合触媒装置
５１ 触媒容器
５２ 触媒ポンプ
６ 超臨界装置
６１ 気体保存具
６２ 加圧素子
６３ ベンチュリ管
６４ 加熱素子
７ 収集装置
７１ 収集ローダー
７１２ 出力口仕切弁
７２ 挿入スロット
７３ 収集チューブ
７４ 冷却凝縮装置
７５ 凝縮滴下口
７７ 搬送具
７８ 抽出具
７８１ 押上ピストン具
A Raw material fixture B Extraction object C Catalyst D Carbon dioxide
Claims (2)
前記抽出装置の右側にピストン弁を有し、外側は前記ピストン弁に対応してピストンローダーを有し、
前記自動材料供給装置に保存空間を内設し、下部に等量出力ノズルを設け、
前記取付具搬送装置に循環ローダーを設け、前記循環ローダーが前記等量出力ノズル下方から前記ピストンローダーに位置し、
前記複合触媒装置に１ないし８の触媒容器を設け、前記触媒容器に触媒を収容し、前記触媒容器が触媒ポンプと、抽出装置とを接続し、
前記超臨界装置が気体保存具に接続し、前記気体保存具に二酸化炭素を内蔵し、前記超臨界装置に加圧素子を配置し、前記加圧素子が抽出装置のベンチュリ管と接続し、前記ベンチュリ管に加熱素子を配置し、
前記収集装置に収集ローダーを内設し、前記収集ローダーに挿入スロットを敷設し、前記収集装置が抽出装置の収集チューブと接続し、前記収集装置に収集チューブを設けられた冷却凝縮装置を有し、収集チューブが挿入スロットの上方に対応して、凝縮滴下口を設けることを特徴とする、産業型超臨界複合式抽出構造。 Including at least an extraction device, an automatic material supply device, a fixture transport device, a composite catalyst device, a supercritical device, and a collection device,
Having a piston valve on the right side of the extraction device, the outside has a piston loader corresponding to the piston valve,
A storage space is provided in the automatic material supply device, and an equal amount output nozzle is provided at the bottom,
A circulation loader is provided in the fixture conveying device, and the circulation loader is located in the piston loader from below the equivalent output nozzle,
1 to 8 catalyst containers are provided in the composite catalyst device, the catalyst is accommodated in the catalyst container, the catalyst container connects a catalyst pump and an extraction device,
The supercritical device is connected to a gas storage device, carbon dioxide is contained in the gas storage device, a pressure element is disposed in the supercritical device, the pressure element is connected to a venturi tube of an extraction device, and Place a heating element on the Venturi tube,
A collection loader is installed in the collection device, an insertion slot is laid in the collection loader, the collection device is connected to a collection tube of an extraction device, and the collection device has a cooling condensing device provided with a collection tube An industrial supercritical compound extraction structure characterized in that the collection tube is provided with a condensation dripping port corresponding to the upper part of the insertion slot.
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