JP2823891B2 - Method for producing composition for hair - Google Patents
Method for producing composition for hairInfo
- Publication number
- JP2823891B2 JP2823891B2 JP1213145A JP21314589A JP2823891B2 JP 2823891 B2 JP2823891 B2 JP 2823891B2 JP 1213145 A JP1213145 A JP 1213145A JP 21314589 A JP21314589 A JP 21314589A JP 2823891 B2 JP2823891 B2 JP 2823891B2
- Authority
- JP
- Japan
- Prior art keywords
- hair
- melanin
- producing
- melanin pigment
- tyrosinase
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
Description
【発明の詳細な説明】 〔産業上の利用分野〕 本発明は、白髪の一時染色に関し、特に、メラニンを
含有する毛髪用組成物の製造方法に関する。Description: TECHNICAL FIELD The present invention relates to temporary dyeing of gray hair, and more particularly to a method for producing a hair composition containing melanin.
従来の髪の染色法は、メラニンを除くための過酸化水
素による脱色過程と、染色剤の酸化による髪の染色過程
がある。Conventional hair dyeing methods include a bleaching process with hydrogen peroxide to remove melanin and a hair dyeing process with oxidation of a dye.
しかしながら、前記従来の髪の染色法は、毛髪の損傷
が甚だしく、また、操作も煩雑という欠点があった。However, the conventional hair dyeing method has the drawbacks that the hair is seriously damaged and the operation is complicated.
そこで、本発明は、髪を損傷せず、皮膚、衣類等を汚
さず、髪の染色の操作が簡便で、染色仕上りが自然であ
るメラニン含有毛髪用組成物の製造方法を提供するもの
である。Therefore, the present invention provides a method for producing a melanin-containing hair composition that does not damage hair, does not stain skin, clothing, and the like, is easy to dye hair, and has a natural dyeing finish. .
本発明は、天然色素メラニンを酵素反応により製造
し、その高分子アニオン性を利用して一行程で染色する
ので、髪を損傷せず、色調も自然である。メラニンはも
ともと髪のなかにあるものであり、髪に親和性を有し髪
を染めるが、皮膚には親和性が少なく染めない特性があ
る。In the present invention, the natural pigment melanin is produced by an enzymatic reaction and is dyed in one step by utilizing its high molecular anionicity, so that the hair is not damaged and the color tone is natural. Melanin is originally present in hair and has an affinity for hair and dyes hair, but has a property of having low affinity for skin and not dyeing.
本発明の毛髪用組成物の製造方法は、椎茸が生産する
チロシナーゼの生成能がある担糸菌の菌体または培養液
から得たチロシナーゼ含有液をジフェノール及びチロシ
ンに作用せしめてメラニン色素を生成せしめ、キトサン
酢酸塩を作用させて得られたメラニン色素を毛髪化粧料
に添加することを特徴とする。The method for producing a hair composition of the present invention comprises producing a melanin pigment by reacting a tyrosinase-containing solution obtained from a cell or a culture of a filamentous fungus capable of producing tyrosinase produced by shiitake mushrooms with diphenol and tyrosine. It is characterized by adding melanin pigment obtained by acting chitosan acetate to hair cosmetics.
チロシナーゼ含有液の製造は、担糸菌として使用する
椎茸100gに対して水400mlを加え、菌体をミキサーで切
断してチロシナーゼを抽出する。次にろ別してろ液を酵
素液とする。In the production of a tyrosinase-containing solution, 400 ml of water is added to 100 g of shiitake mushrooms used as a fungi, and the cells are cut with a mixer to extract tyrosinase. Then, the mixture is filtered to obtain an enzyme solution.
１％カテコール、0.5％チロシンを含む液に対し30vol
％の酵素液を入れて、30℃において通気しつつ撹拌し、
酵素反応を進めると、１日後にはドーパキノンによる赤
褐色、３日後には黒色のメラニン色素を生成する。30vol for liquid containing 1% catechol and 0.5% tyrosine
% Enzyme solution, stirred at 30 ° C with aeration,
When the enzymatic reaction proceeds, a red-brown color is produced by dopaquinone after one day, and a black melanin pigment is formed after three days.
メラニン色素は（−）荷電の高分子色素であるから、
これに（＋）荷電の凝集剤を添加すると、メラニンは凝
集沈殿するので分離採取することができる。Since melanin pigment is a (-) charged polymer pigment,
When a (+) charged flocculant is added to this, melanin flocculates and precipitates and can be separated and collected.
このようにして得られたメラニン色素を養毛剤、ポマ
ード、ヘアクリーム等の毛髪化粧料に添加して黒色養毛
料を製造する。これら養毛料は髪を損傷せず、白髪を自
然に染め、黒髪を一層さえた美しさにする。染色は水洗
で落ちないが、シャンプーによる水洗では少し落ちる。The melanin pigment thus obtained is added to hair cosmetics such as hair tonics, pomades, and hair creams to produce black hair tonics. These hair nourishes do not damage the hair, dye gray hair naturally and make black hair more beautiful. Dyeing does not come off with water washing, but it does come off a little with water washing with shampoo.
次に実施例について示す。 Next, examples will be described.
１）メラニン色素の製造 椎茸100gを裁断し、これに水400mlを加えて、４℃、1
8時間チロシナーゼを抽出し、抽出液270mlを得る。この
抽出液75mlに水400ml、カテコール4g、チロシン1.5gを
添加し、30℃にて通気しつつ６日間酵素反応を行わしめ
ると、液は赤褐色から黒色に変わりメラニンが生成す
る。次に、カチオン性高分子凝集剤キトサン酢酸塩15mg
を加えて、18時間置きメラニンを凝集せしめ採取し6.1g
を得た。1) Production of melanin pigment 100 g of shiitake mushrooms were cut, and 400 ml of water was added thereto.
Extract tyrosinase for 8 hours to obtain 270 ml of extract. 400 ml of water, 4 g of catechol, and 1.5 g of tyrosine are added to 75 ml of the extract, and the enzyme reaction is carried out for 6 days while aerating at 30 ° C. Next, the cationic polymer flocculant chitosan acetate 15 mg
, Add 18 hours and aggregate melanin to collect 6.1 g
I got
２）養毛剤の製造 メラニン色素10gをセチルトリメチル、アンモニウム
クロライド0.1溶液100mlに添加すると良く溶解する。次
にキトサン酢酸塩1gを加えて溶解せしめ養毛剤とする。
髪は洗髪した後半乾燥し、この養毛剤を塗布し乾燥する
と髪は天然の黒色に染まる。毛髪は手触りが柔らかく感
触も良い。2) Manufacture of hair restorer When 10 g of melanin pigment is added to 100 ml of 0.1 solution of cetyltrimethyl and ammonium chloride, it dissolves well. Next, 1 g of chitosan acetate is added and dissolved to obtain a hair restorer.
The hair is dried in the latter half of the hair washing, and the hair is dyed a natural black color when the hair tonic is applied and dried. The hair feels soft and feels good.
３）ポマード 下記の処法によりポマードを製造する。3) Pomade Pomade is produced by the following method.
固形パラフィン ６％ ワセリン 52％ オリーブ油 28％ メラニン色素（水分90％） ５％ 流動パラフィン 11％ 香料 適量 ４）ヘアクリーム,5）ポマード 公知方法によりそれぞれ製造し、メラニン色素（水分
10％）を５ないし10％添加する。Solid paraffin 6% Vaseline 52% Olive oil 28% Melanin pigment (moisture 90%) 5% Liquid paraffin 11% Flavor appropriate amount 4) Hair cream, 5) Pomade Manufacture melanin pigment (moisture)
5% to 10%).
メラニン色素を毛髪化粧料に添加することにより、白
髪を天然の黒色に染色して、毛髪を損傷することなく染
色することが可能な毛髪用組成物を製造することができ
る。この組成物は毛髪を選択的に染色するが、皮膚を染
めず、また衣類等を汚すことが無く、従来のこの種の製
品にない特徴がある。By adding a melanin pigment to hair cosmetics, it is possible to produce a hair composition capable of dyeing gray hair with natural black color and dyeing without damaging the hair. Although this composition selectively dyes hair, it does not stain skin, does not stain clothing, etc., and has features not found in conventional products of this type.
Claims (1)
る担糸菌の菌体または培養液から得たチロシナーゼ含有
液をジフェノール及びチロシンに作用せしめてメラニン
色素を生成せしめ、キトサン酢酸塩を作用させて得られ
たメラニン色素を毛髪化粧料に添加することを特徴とす
る毛髪用組成物の製造方法。1. A tyrosinase-containing solution obtained from a fungus body or a culture solution of a filamentous fungus capable of producing tyrosinase produced by shiitake mushrooms, is allowed to act on diphenol and tyrosine to form a melanin pigment, and a chitosan acetate is used. A method for producing a hair composition, comprising adding a melanin pigment obtained by the above to a hair cosmetic.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP1213145A JP2823891B2 (en) | 1989-08-19 | 1989-08-19 | Method for producing composition for hair |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP1213145A JP2823891B2 (en) | 1989-08-19 | 1989-08-19 | Method for producing composition for hair |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPH0377813A JPH0377813A (en) | 1991-04-03 |
| JP2823891B2 true JP2823891B2 (en) | 1998-11-11 |
Family
ID=16634326
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP1213145A Expired - Fee Related JP2823891B2 (en) | 1989-08-19 | 1989-08-19 | Method for producing composition for hair |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JP2823891B2 (en) |
Families Citing this family (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US6036729A (en) * | 1995-12-22 | 2000-03-14 | Novo Nordisk A/S | Enzymatic method for textile dyeing |
| US5972042A (en) * | 1995-12-22 | 1999-10-26 | Novo Nordisk A/S | Method for dyeing a material with a dyeing system which contains an enzymatic oxidizing agent |
| ITMI991896A1 (en) * | 1999-09-09 | 2001-03-09 | Carlo Ghisalberti | MELANINES AND VEGETABLE PIGMENTS |
| JP4955920B2 (en) * | 2004-12-08 | 2012-06-20 | 花王株式会社 | Hair dye composition |
| JP4788200B2 (en) * | 2005-06-02 | 2011-10-05 | 日本精工株式会社 | Self-aligning roller bearing assembly method |
| JP4739909B2 (en) * | 2005-10-25 | 2011-08-03 | 株式会社マキタ | Work tools |
| CN106420678B (en) * | 2016-09-30 | 2019-04-23 | 广东轻工职业技术学院 | Aryl compound containing phenolic hydroxyl group is used as tyrosinase activator and its application |
Family Cites Families (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS6169718A (en) * | 1985-08-24 | 1986-04-10 | Hidetoshi Tsuchida | Dyeing agent composition |
| JPS62282598A (en) * | 1987-04-24 | 1987-12-08 | Amano Pharmaceut Co Ltd | Method for determining total bilirubin and reagent composition for determination |
| US4855144A (en) * | 1987-10-23 | 1989-08-08 | Advanced Polymer Systems | Synthetic melanin aggregates |
-
1989
- 1989-08-19 JP JP1213145A patent/JP2823891B2/en not_active Expired - Fee Related
Also Published As
| Publication number | Publication date |
|---|---|
| JPH0377813A (en) | 1991-04-03 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| LAPS | Cancellation because of no payment of annual fees |