JP2737376B2 - Al alloy two-stage powder forged member with high fatigue strength and high toughness - Google Patents
Al alloy two-stage powder forged member with high fatigue strength and high toughnessInfo
- Publication number
- JP2737376B2 JP2737376B2 JP22200890A JP22200890A JP2737376B2 JP 2737376 B2 JP2737376 B2 JP 2737376B2 JP 22200890 A JP22200890 A JP 22200890A JP 22200890 A JP22200890 A JP 22200890A JP 2737376 B2 JP2737376 B2 JP 2737376B2
- Authority
- JP
- Japan
- Prior art keywords
- alloy
- powder
- fatigue strength
- toughness
- powder forged
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
Description
【発明の詳細な説明】 〔産業上の利用分野〕 この発明は、原料粉末としてアトマイズAl合金粉末を
用い、これの圧粉体を2段粉末鍛造を施してAl合金製部
材を製造するに際して、前記Al合金の組成を特定するこ
とにより高疲労強度と高靭性を具備せしめたAl合金製2
段粉末鍛造部材に関するものである。DETAILED DESCRIPTION OF THE INVENTION [Industrial application field] This invention uses an atomized Al alloy powder as a raw material powder, and performs a two-stage powder forging of the green compact to produce an Al alloy member. Al alloy 2 with high fatigue strength and high toughness by specifying the composition of the Al alloy 2
It relates to a stepped powder forged member.
従来、例えば特公平2−9099号公報に記載される通
り、重量%で(以下%は重量%を示す)、 Si:8〜30%、 を含有し、さらに、 Cu,Mg,Ni,Fe,およびMnのうちの1種または2種以上:
0.1〜10%、 を含有し、残りがAlと不可避不純物からなる組成を有す
るアトマイズAl合金粉末を原料粉末として用い、これの
圧粉体に熱間鍛造を施すことにより製造されたAl合金製
粉末鍛造部材が知られている。Conventionally, for example, as described in Japanese Patent Publication No. 2-9099, Si: 8 to 30% by weight (hereinafter,% indicates weight%), and Cu, Mg, Ni, Fe, And one or more of Mn:
Atomized Al alloy powder having a composition of 0.1 to 10%, with the balance being Al and unavoidable impurities, used as a raw material powder, and an Al alloy powder produced by subjecting the green compact thereof to hot forging. Forged members are known.
また、これらの従来Al合金製粉末鍛造部材が、例えば
エンジンやコンプレッサーなどの構造部材として適用さ
れていることも知られている。It is also known that these conventional aluminum alloy powder forged members are applied as structural members such as engines and compressors.
〔発明が解決しようとする課題〕 一方、近年の各種機関の高速化および高性能化、さら
に軽量化はめざましく、これに伴ない、これらの構造部
材の使用環境は一段と苛酷さを増す傾向にあるが、従来
のAl合金製粉末鍛造部材は疲労強度および靭性が十分で
ないために、これに満足に対応することができないのが
現状である。[Problems to be Solved by the Invention] On the other hand, the speed and performance of various engines in recent years have been remarkable, and the use environment of these structural members tends to be even more severe. However, since the conventional aluminum alloy powder forged members do not have sufficient fatigue strength and toughness, it is currently impossible to satisfactorily cope with them.
そこで、本発明者等は、上述のような観点から、上記
の従来Al合金製粉末鍛造部材に着目し、これの疲労強度
と靭性の向上をはかるべく研究を行なった結果、原料粉
末として用いられるアトマイズAl合金粉末を、 Si:12〜30%、 Cu:0.1〜10%、 Fe:0.1〜10%、 Mg:0.1〜3%、 P :0.001〜0.05%、Ti:0.2〜1%、 を含有し、残りがAlと不可避不純物からなる組成を有す
るアトマイズAl合金粉末に特定し、これよりプレス成形
された粉末体に、2段の粉末鍛造、望ましくは350〜520
℃の温度での2回の密閉型鍛造を施すと、前記アトマイ
ズAl合金粉末中に合金成分として含有するPとTiが、前
記の2段の粉末鍛造作用と相まって、製造されたAl合金
製2段粉末鍛造部材の疲労強度と靭性を著しく向上させ
るように作用するという研究結果を得たのである。Therefore, the present inventors have focused on the above-mentioned conventional Al alloy powder forged member from the above-described viewpoint, and have conducted research to improve the fatigue strength and toughness thereof, and as a result, used as a raw material powder. Atomized Al alloy powder contains: Si: 12-30%, Cu: 0.1-10%, Fe: 0.1-10%, Mg: 0.1-3%, P: 0.001-0.05%, Ti: 0.2-1% Then, the remainder is specified as an atomized Al alloy powder having a composition consisting of Al and unavoidable impurities, and the powder compacted from this is subjected to two-stage powder forging, preferably 350 to 520.
When the closed die forging is performed twice at a temperature of ° C., P and Ti contained as alloy components in the atomized Al alloy powder are combined with the two-stage powder forging action described above to produce an Al alloy 2 Research results have been obtained that it acts to significantly improve the fatigue strength and toughness of a stepped powder forged member.
この発明は、上記研究結果にもとづいてなされたもの
であって、 Si:12〜30%、 Cu:0.1〜10%、 Fe:0.1〜10%、 Mg:0.1〜3%、 P :0.001〜0.05%、Ti:0.2〜1%、 を含有し、残りがAlと不可避不純物からなる組成を有す
るAl合金で構成してなる高疲労強度と高靭性を有するAl
合金製2段粉末鍛造部材に特徴を有するものである。The present invention has been made based on the above research results, and includes: Si: 12 to 30%, Cu: 0.1 to 10%, Fe: 0.1 to 10%, Mg: 0.1 to 3%, P: 0.001 to 0.05 %, Ti: 0.2 to 1%, with the balance being an Al alloy having a composition comprising Al and inevitable impurities, and having high fatigue strength and high toughness.
It is characterized by a two-stage powder forged alloy member.
つぎに、この発明のAl合金製2段粉末鍛造部材におい
て、これを構成するAl合金の成分組成を上記の通りに限
定した理由を説明する。Next, the reason why the component composition of the Al alloy constituting the aluminum alloy two-stage powder forged member of the present invention is limited as described above will be described.
(a) Si Si成分には、部材の熱膨張係数を低下させると共に、
耐摩耗性を向上させる作用があるが、その含有量が12%
未満では前記作用に所望の効果が得られず、一方、その
含有量が30%を越えると、靭性が低下し、かつ機械加工
が困難になることから、その含有量を12〜30%と定め
た。(A) Si The Si component reduces the coefficient of thermal expansion of the member,
Has the effect of improving wear resistance, but its content is 12%
If the content is less than 30%, the desired effect cannot be obtained. On the other hand, if the content exceeds 30%, the toughness decreases and machining becomes difficult, so the content is set to 12 to 30%. Was.
(b) CuおよびMg これらの成分には、2段粉末鍛造後の時効処理で、微
細なMg2SiやCu2Alなどの金属間化合物として素地中に析
出して、部材の強度を向上させる作用があるが、その含
有量が、それぞれCu:0.1%未満およびMg:0.1%未満では
所望の強度向上効果が得られず、一方その含有量がそれ
ぞれCu:10%およびMg:3%を越えると、部材の靭性が低
下するようになることから、その含有量をそれぞれCu:
0.1〜10%、Mg:0.1〜3%と定めた。(B) Cu and Mg These components are precipitated as fine intermetallic compounds such as Mg 2 Si and Cu 2 Al by aging treatment after two-stage powder forging to improve the strength of members. Although it has an effect, the desired strength improvement effect cannot be obtained if its content is less than Cu: 0.1% and Mg: less than 0.1%, respectively, while its content exceeds Cu: 10% and Mg: 3%, respectively. And, since the toughness of the member will be reduced, the content is respectively Cu:
0.1-10%, Mg: 0.1-3%.
(c) Fe Fe成分には、CuおよびMgと同様に時効処理でAl−Fe−
Si系金属間化合物として析出して、部材の強度、耐熱
性、および耐摩耗性を向上させる作用があるが、その含
有量が0.1%未満では前記作用に所望の効果が得られ
ず、一方その含有量が10%を越えると部材の靭性が低下
するようになることから、その含有量を0.1〜10%と定
めた。(C) Fe The Fe component contains Al-Fe-
It precipitates as a Si-based intermetallic compound and has the effect of improving the strength, heat resistance, and abrasion resistance of the member. However, if the content is less than 0.1%, the desired effect cannot be obtained in the above-described effect. If the content exceeds 10%, the toughness of the member decreases, so the content is set to 0.1 to 10%.
(d) PおよびTi これらの成分には、共存した状態で部材の疲労強度と
靭性を著しく向上させる作用があり、したがってPの単
独含有でも、Tiの単独含有でも所望の疲労強度と靭性を
確保することができず、またPおよびTi含有量のいずれ
かが、P:0.001%未満およびTi:0.2%未満となって前記
作用に所望の向上効果が得られず、一方PおよびTiによ
る前記作用の向上効果は、P:0.05%およびTi:1%で飽和
し、これ以上含有させてもより一層の向上効果は得られ
ないことから、経済性を考慮して、その含有量をP:0.00
1〜0.05%、Ti:0.2〜1%と定めた。(D) P and Ti These components have the effect of significantly improving the fatigue strength and toughness of the member when they coexist. Therefore, the desired fatigue strength and toughness can be ensured regardless of whether P alone or Ti is contained. And the content of P and Ti is less than 0.001% and less than 0.2% of P: less than 0.2%, so that the desired improvement effect cannot be obtained in the above-mentioned action. The effect of P is saturated with P: 0.05% and Ti: 1%, and even if the content is further increased, no further improvement effect can be obtained.
1 to 0.05%, Ti: 0.2 to 1%.
つぎに、この発明のAl合金製2段粉末鍛造部材を実施
例により具体的に説明する。Next, the aluminum alloy two-stage powder forged member of the present invention will be specifically described with reference to examples.
通常の溶解法にて、それぞれ第1表に示される成分組
成をもったAl合金溶湯を調製し、空気アトマイズ法によ
り粒度:100メッシュ以下のAl合金粉末とし、このAl合金
粉末より6ton/cm2の圧力で10mm×23mm×55mmの寸法をも
った圧粉体をプレス成形し、この圧粉体に、まず、大気
中、15℃/minの昇温速度で480℃で昇温し、この温度に
て密閉型を用い、8ton/cm2の圧力で1段目の粉末鍛造を
施して、いずれも11mm×16mm×57mmの寸法をもった理論
密度比:98%以上の1次粉末鍛造素材とし、ついで、こ
れに、同じく密閉型を用い、大気中、昇温速度:15℃/mi
n、加熱温度:480℃、圧力:8ton/cm2の同じ条件で2段目
の熱間鍛造を施して水冷し、14mm×12mm×60mmの寸法を
もった2次粉末鍛造素材とし、最終的に、これに温度:1
70℃に6時間保持の条件で時効処理を施すことにより実
質的に上記Al合金粉末と同じ成分組成をもった本発明Al
合金製2段粉末鍛造部材(以下、本発明粉末鍛造部材と
いう) 1〜19、および比較Al合金製2段粉末鍛造部材(以下、
比較粉末鍛造部材という)1〜9をそれぞれ製造した。An Al alloy melt having the component composition shown in Table 1 was prepared by a normal melting method, and was made into an Al alloy powder having a particle size of 100 mesh or less by an air atomizing method, and 6 ton / cm 2 was obtained from the Al alloy powder. A green compact having a size of 10 mm x 23 mm x 55 mm is press-molded at a pressure of, and the green compact is first heated at 480 ° C in the atmosphere at a heating rate of 15 ° C / min. In a closed mold, the first stage of powder forging was applied at a pressure of 8 ton / cm 2 to obtain a primary powder forging material with a theoretical density ratio of 98% or more, each having dimensions of 11 mm × 16 mm × 57 mm. Then, using a closed type, in the air, at a heating rate of 15 ° C./mi
n 、 Heating temperature: 480 ℃ 、 Pressure: 8ton / cm 2 under the same conditions, the second stage of hot forging, water-cooled to form a secondary powder forging material with dimensions of 14mm × 12mm × 60mm, finally In this, the temperature: 1
The present invention Al having substantially the same component composition as the Al alloy powder by subjecting to aging treatment at 70 ° C. for 6 hours.
Alloy two-stage powder forged member (hereinafter referred to as powder forged member of the present invention) 1-19, and a comparative Al alloy two-stage powder forged member (hereinafter, referred to as
1-9.
なお、比較粉末鍛造部材1〜9は、いずれもこれを構
成するAl合金における構成成分のうちのいずれかの成分
含有量(第1表に※印を付す)がこの発明の範囲から外
れたものである。Each of the comparative powder forged members 1 to 9 has a component content (marked with * in Table 1) of any of the constituent components of the Al alloy constituting the same, which is out of the scope of the present invention. It is.
ついで、この結果得られた各種の粉末鍛造部材につい
て、強度と靭性を評価する目的で、引張強さ、疲労強
度、およびシャルピー衝撃値を測定した。これらの測定
結果を第1表に示した。Next, the tensile strength, the fatigue strength, and the Charpy impact value of the various powder forged members obtained as a result were measured for the purpose of evaluating the strength and toughness. Table 1 shows the results of these measurements.
なお、疲労強度は、回転数:4000r.p.m.で片持ち回転
曲げ疲労試験を行ない、繰り返し数:1×107回まで行な
っても破壊しなかった応力をもって表わした。In addition, the fatigue strength was represented by a stress that did not break even after performing a cantilever rotating bending fatigue test at a rotation speed of 4000 rpm and repeating the test up to 1 × 10 7 times.
第1表に示される結果から、本発明粉末鍛造部材1〜
19は、特に合金成分として含有させたPおよびTiの共存
含有によって、いずれも高疲労強度と高靭性を有するの
に対して、比較粉末鍛造部材1〜9に見られるように、
Al合金の構成成分のうちのいずれかの成分含有量がこの
発明の範囲から外れると、疲労強度と靭性のうちの少な
くともいずれかの特性が劣ったものになることが明らか
である。From the results shown in Table 1, the powder forged members of the present invention 1 to 1
19 has high fatigue strength and high toughness, both due to the co-presence of P and Ti, especially as alloy components, as shown in the comparative powder forged members 1 to 9,
When the content of any one of the components of the Al alloy is out of the range of the present invention, it is apparent that at least one of the properties of fatigue strength and toughness is inferior.
上述のように。この発明のAl合金製2段粉末鍛造部材
は、高疲労強度と高靭性を有し、かつ従来のAl合金製粉
末鍛造部材と同等の高強度と低熱膨張係数を有するの
で、苛酷な条件下で運転される各種機関の構造部材とし
て用いた場合にもすぐれた性能を長期に亘って発揮する
ことなど工業上有用な特性を有するのである。As mentioned above. The Al alloy two-stage powder forged member of the present invention has high fatigue strength and high toughness, and has the same high strength and low coefficient of thermal expansion as conventional Al alloy powder forged members, so under severe conditions. It has industrially useful characteristics such as exhibiting excellent performance over a long period of time even when used as a structural member of various types of operating engines.
Claims (1)
重量%)を有するAl合金で構成したことを特徴とする高
疲労強度および高靭性を有するAl合金製2段粉末鍛造部
材。(1) Si: 12 to 30%, Cu: 0.1 to 10%, Fe: 0.1 to 10%, Mg: 0.1 to 3%, P: 0.001 to 0.05%, Ti: 0.2 to 1%. A two-stage powder forged member made of an Al alloy having high fatigue strength and high toughness, characterized in that the remainder is composed of an Al alloy having a composition of Al and unavoidable impurities (at least by weight).
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP22200890A JP2737376B2 (en) | 1990-08-23 | 1990-08-23 | Al alloy two-stage powder forged member with high fatigue strength and high toughness |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP22200890A JP2737376B2 (en) | 1990-08-23 | 1990-08-23 | Al alloy two-stage powder forged member with high fatigue strength and high toughness |
Publications (2)
Publication Number | Publication Date |
---|---|
JPH04103739A JPH04103739A (en) | 1992-04-06 |
JP2737376B2 true JP2737376B2 (en) | 1998-04-08 |
Family
ID=16775662
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP22200890A Expired - Fee Related JP2737376B2 (en) | 1990-08-23 | 1990-08-23 | Al alloy two-stage powder forged member with high fatigue strength and high toughness |
Country Status (1)
Country | Link |
---|---|
JP (1) | JP2737376B2 (en) |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN104625066A (en) * | 2015-01-30 | 2015-05-20 | 北京科技大学 | Method for manufacturing high-niobium titanium-aluminum alloy material by adopting two-step pressure infiltration |
-
1990
- 1990-08-23 JP JP22200890A patent/JP2737376B2/en not_active Expired - Fee Related
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN104625066A (en) * | 2015-01-30 | 2015-05-20 | 北京科技大学 | Method for manufacturing high-niobium titanium-aluminum alloy material by adopting two-step pressure infiltration |
Also Published As
Publication number | Publication date |
---|---|
JPH04103739A (en) | 1992-04-06 |
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