JP2020103116A - Method for producing beverage - Google Patents

Method for producing beverage Download PDF

Info

Publication number
JP2020103116A
JP2020103116A JP2018244467A JP2018244467A JP2020103116A JP 2020103116 A JP2020103116 A JP 2020103116A JP 2018244467 A JP2018244467 A JP 2018244467A JP 2018244467 A JP2018244467 A JP 2018244467A JP 2020103116 A JP2020103116 A JP 2020103116A
Authority
JP
Japan
Prior art keywords
grain powder
beverage
tea
grain
raw material
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
JP2018244467A
Other languages
Japanese (ja)
Other versions
JP6921052B2 (en
Inventor
有希子 池上
Yukiko Ikegami
有希子 池上
遼 伊藤
Ryo Ito
遼 伊藤
孝平 森田
Kohei Morita
孝平 森田
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Asahi Soft Drinks Co Ltd
Original Assignee
Asahi Soft Drinks Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Asahi Soft Drinks Co Ltd filed Critical Asahi Soft Drinks Co Ltd
Priority to JP2018244467A priority Critical patent/JP6921052B2/en
Publication of JP2020103116A publication Critical patent/JP2020103116A/en
Application granted granted Critical
Publication of JP6921052B2 publication Critical patent/JP6921052B2/en
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Landscapes

  • Tea And Coffee (AREA)
  • Non-Alcoholic Beverages (AREA)

Abstract

To provide a method for producing a beverage, capable of producing a beverage which contains grain powder and is excellent in redispersion properties of sediments of the grain powder.SOLUTION: A method for producing a beverage containing a beverage dispersion medium and grain powder includes: a grain powder production step of bringing a starch content of raw material grain powder as the raw material of the grain powder to 30 mass% or more, subjecting at least one of amylase treatment and cellulase treatment to the raw material grain powder after dispersing the raw material grain powder in an aqueous medium, and obtaining the grain powder dispersed in the aqueous medium; and a mixing step of mixing the grain powder dispersed in the aqueous medium and obtained in the grain powder production step with the beverage dispersion medium.SELECTED DRAWING: None

Description

本発明は、飲料の製造方法に関する。 The present invention relates to a method for producing a beverage.

穀物茶飲料等の茶飲料は、その甘み、苦味や渋み等の風味により、消費者に幅広く受け入れられている。このような茶飲料は、風味等の特性の改良が重ねられている。例えば、特許文献1では、0.009重量%以上のでんぷん質と、平均粒子径が1μm以下の抹茶や煎茶等の超微粉砕茶葉とを含有する穀物茶飲料とすることで、穀類の持つまろやかさや香味を損なわずに、穀類由来のベタツキ感を抑制した、すっきりとした後味を有する穀類茶飲料とする技術が開示されている。また、特許文献2には、穀物原料の抽出液及び食物繊維を含有し、穀物原料に対する食物繊維の重量比率(食物繊維/穀物原料)が0.02〜3.00であり、不溶性粒子の平均粒子径が10〜70μmである穀物茶飲料とすることで、食物繊維の添加による香味バランスの欠如及び性状劣化を抑制した穀物茶飲料とする技術が開示されている。また、特許文献3には、茶葉を夾雑ペクチナーゼ活性の少ない特定のセルラーゼで処理して抽出した特定濃度の茶酵素処理エキスと、抹茶とを混合した茶飲料とすることで、抹茶のザラツキ、雑味、沈殿が抑制された抹茶入り茶飲料とする技術が開示されている。 Tea beverages such as grain tea beverages are widely accepted by consumers due to their sweetness, flavors such as bitterness and astringency. Such tea beverages have been repeatedly improved in characteristics such as flavor. For example, in Patent Document 1, the mellowness of grains is obtained by providing a grain tea beverage containing 0.009% by weight or more of starch and an ultrafinely ground tea leaf such as matcha or sencha having an average particle size of 1 μm or less. A technique for producing a cereal tea beverage having a refreshing aftertaste in which a sticky feeling derived from cereals is suppressed without impairing the pod flavor is disclosed. Moreover, in patent document 2, the extract of a grain raw material and a dietary fiber are contained, the weight ratio of the dietary fiber to the grain raw material (dietary fiber/grain raw material) is 0.02 to 3.00, and the average of insoluble particles. A technique is disclosed in which a grain tea beverage having a particle size of 10 to 70 μm is used to suppress the lack of flavor balance and the deterioration of properties due to the addition of dietary fiber. Further, in Patent Document 3, tea leaves are treated with a specific concentration of a tea enzyme-treated extract obtained by treating tea leaves with a specific cellulase having a small amount of contaminated pectinase activity, and a tea beverage is prepared by mixing matcha tea, thereby producing a matcha and a miscellaneous matcha. A technique for producing a tea beverage containing matcha in which taste and precipitation are suppressed is disclosed.

特開2009−082086号公報JP, 2009-082086, A 特開2017−127332号公報JP, 2017-127332, A 特開2013−055906号公報JP, 2013-055906, A

上記特許文献1〜3では、茶飲料の風味等の特性を改良するために、茶飲料に、抹茶や煎茶等の茶葉粉末や不溶性固形分等の成分を配合しているが、配合された成分が茶飲料に不溶である場合は、該成分は茶飲料の容器の底に沈殿する。このように、特性の改良のための成分が沈殿した茶飲料は、飲用する直前に振とうされて沈殿物が茶飲料中に再分散されて飲用されるのが通常である。 In the above Patent Documents 1 to 3, in order to improve the characteristics such as the flavor of the tea beverage, the tea beverage is blended with components such as tea leaf powder and insoluble solids such as green tea and green tea, but the blended components. If is insoluble in the tea beverage, the ingredient will settle to the bottom of the tea beverage container. As described above, the tea beverage in which the component for improving the characteristics is precipitated is usually shaken immediately before drinking, and the precipitate is redispersed in the tea beverage for drinking.

しかしながら、例えばコクやボディ感の向上等のために、穀物粉末を茶飲料に配合すると、配合された穀物粉末の沈殿物の再分散性が悪い場合があるという問題がある。沈殿物の再分散性が悪い場合は、繰り返し振とうしなくてはならない。
なお、配合された穀物粉末の沈殿物の再分散性が悪い場合があるという問題は、茶飲料に限らず、その他の飲料においても、同様に存在する。
However, when the grain powder is blended with a tea beverage in order to improve the richness and body sensation, there is a problem that the redispersibility of the blended grain powder precipitate may be poor. If the redispersibility of the precipitate is poor, it must be shaken repeatedly.
In addition, the problem that the redispersibility of the precipitate of the blended grain powder may be poor is not limited to tea beverages, and similarly exists in other beverages.

本発明は、上記の状況に鑑みてなされたものであり、穀物粉末を含み該穀物粉末の沈殿物の再分散性に優れた飲料を製造することができる飲料の製造方法を提供することを目的とする。 The present invention has been made in view of the above circumstances, and an object of the present invention is to provide a method for producing a beverage, which contains a grain powder and is excellent in redispersibility of a precipitate of the grain powder. And

本発明者らは、デンプン含有量が30質量%以上の原料穀物粉末を水性媒体に分散した後に、原料穀物粉末に対してアミラーゼ処理及びセルラーゼ処理の少なくとも一方を施して水性媒体に分散した穀物粉末を得て、これを飲料用分散媒と混合することにより、飲料に含まれる穀物粉末の沈殿の再分散性を向上できることを見出し、本発明を完成するに至った。より具体的には、本発明は以下のものを提供する。 The present inventors disperse a raw material grain powder having a starch content of 30% by mass or more in an aqueous medium, and then subject at least one of an amylase treatment and a cellulase treatment to the raw material grain powder to disperse the grain powder in an aqueous medium. Then, it was found that the redispersibility of the precipitation of the grain powder contained in the beverage can be improved by mixing this with a dispersion medium for beverage, and completed the present invention. More specifically, the present invention provides the following.

(1) 飲料用分散媒と穀物粉末とを含む飲料の製造方法であって、前記穀物粉末の原料である原料穀物粉末のデンプン含有量が30質量%以上であり、前記原料穀物粉末を水性媒体に分散した後に、前記原料穀物粉末に対してアミラーゼ処理及びセルラーゼ処理の少なくとも一方を施して、前記水性媒体に分散した前記穀物粉末を得る穀物粉末製造工程と、前記穀物粉末製造工程で得られた前記水性媒体に分散した前記穀物粉末と前記飲料用分散媒とを混合する混合工程とを有する、飲料の製造方法。 (1) A method for producing a beverage containing a dispersion medium for beverages and a grain powder, wherein the raw material grain powder, which is a raw material of the grain powder, has a starch content of 30% by mass or more, and the raw grain powder is an aqueous medium. And then subjected to at least one of amylase treatment and cellulase treatment to the raw material grain powder, to obtain the grain powder dispersed in the aqueous medium, a grain powder manufacturing step, obtained in the grain powder manufacturing step A method for producing a beverage, comprising a mixing step of mixing the grain powder dispersed in the aqueous medium and the beverage dispersion medium.

(2) 前記飲料用分散媒が茶抽出液であり、前記飲料が茶飲料である、(1)に記載の飲料の製造方法。 (2) The method for producing a beverage according to (1), wherein the beverage dispersion medium is a tea extract, and the beverage is a tea beverage.

本発明によれば、デンプン含有量が30質量%以上の原料穀物粉末を水性媒体に分散した後に、原料穀物粉末に対してアミラーゼ処理及びセルラーゼ処理の少なくとも一方を施して穀物粉末を得て、これを飲料用分散媒と混合することにより、穀物粉末を含み該穀物粉末の沈殿物の再分散性に優れた飲料を製造することができる。 According to the present invention, a raw material grain powder having a starch content of 30% by mass or more is dispersed in an aqueous medium, and then the raw material grain powder is subjected to at least one of amylase treatment and cellulase treatment to obtain a grain powder. By mixing with a dispersion medium for beverages, it is possible to produce a beverage containing grain powder and having excellent redispersibility of the precipitate of the grain powder.

以下、本発明の実施形態について詳細に説明する。なお、本発明は以下の実施形態に限定されない。 Hereinafter, embodiments of the present invention will be described in detail. The present invention is not limited to the embodiments below.

<飲料の製造方法>
本実施の形態に係る飲料の製造方法は、飲料用分散媒と穀物粉末とを含む飲料を製造するものである。そして、本実施の形態に係る飲料の製造方法は、穀物粉末の原料である原料穀物粉末のデンプン含有量が30質量%以上であり、この原料穀物粉末を水性媒体に分散した後に、原料穀物粉末に対してアミラーゼ処理及びセルラーゼ処理の少なくとも一方を施して、水性媒体に分散した穀物粉末を得る穀物粉末製造工程と、穀物粉末製造工程で得られた水性媒体に分散した穀物粉末と飲料用分散媒とを混合する混合工程とを有する。
<Beverage manufacturing method>
The beverage manufacturing method according to the present embodiment is for manufacturing a beverage containing a beverage dispersion medium and grain powder. Then, in the method for producing a beverage according to the present embodiment, the raw material grain powder, which is a raw material of the grain powder, has a starch content of 30% by mass or more, and after the raw material grain powder is dispersed in an aqueous medium, the raw material grain powder is obtained. To at least one of amylase treatment and cellulase treatment to obtain a grain powder dispersed in an aqueous medium, a grain powder manufacturing process, the grain powder dispersed in the aqueous medium obtained in the grain powder manufacturing process and a dispersion medium for beverages And a mixing step of mixing and.

本実施の形態に係る飲料の製造方法で製造される飲料としては、例えば、茶飲料(緑茶飲料、紅茶飲料、中国茶飲料、ブレンド茶飲料等)、コーヒー飲料、野菜飲料、果汁飲料、乳飲料、アルコール飲料、スポーツドリンク等、種々の飲料が挙げられる。飲料として茶飲料を製造する場合を例に、以下に本実施の形態に係る飲料の製造方法について詳細に説明する。 Examples of the beverage produced by the method for producing a beverage according to the present embodiment include, for example, tea beverages (green tea beverage, black tea beverage, Chinese tea beverage, blended tea beverage, etc.), coffee beverage, vegetable beverage, fruit juice beverage, milk beverage. , Various drinks such as alcoholic drinks and sports drinks. The method for producing a beverage according to the present embodiment will be described in detail below, taking the case of producing a tea beverage as a beverage as an example.

(飲料用分散媒)
茶飲料が含む飲料用分散媒は、茶抽出液である。「茶抽出液」とは、茶飲料の素材(ベース)となる抽出液であり、茶抽出液の原料(茶原料)を、必要に応じて焙煎した後、抽出溶媒を用いて抽出した抽出液である。
茶抽出液として穀物抽出液を用いる場合は、穀物茶飲料が得られる。穀物抽出液の原料穀物としては、穀物茶飲料の原料として通常用いられる穀物を使用でき、大麦、発芽大麦、小麦等の麦類、玄米、発芽玄米等の米類、大豆、小豆、黒豆等の豆類、ハトムギ、トウモロコシ、芋、あわ、キビ等が挙げられる。穀物抽出液は穀物由来の甘みが良好である。穀物抽出液の原料穀物としては、甘みの観点から、大麦、ハトムギや、玄米が好ましい。穀物抽出液は、抽出液の原料穀物から抽出液を得るために通常採用される抽出方法によって得られる。
(Beverage dispersion medium)
The beverage dispersion medium contained in the tea beverage is a tea extract. "Tea extract" is an extract that becomes the material (base) of tea beverages, and the raw material of the tea extract (tea raw material) is roasted if necessary and then extracted using an extraction solvent. It is a liquid.
When a grain extract is used as the tea extract, a grain tea beverage can be obtained. As the raw material grain of the grain extract, grains usually used as a raw material for grain tea beverages can be used, such as barley, germinated barley, wheat such as wheat, brown rice, germinated brown rice and other rice, soybeans, red beans, black beans and the like. Beans, pearl barley, corn, potatoes, bubbles, millet and the like can be mentioned. The grain extract has good sweetness derived from grains. From the viewpoint of sweetness, barley, pearl barley and brown rice are preferable as raw material grains for the grain extract. The grain extract is obtained by an extraction method usually adopted for obtaining an extract from a raw material grain of the extract.

茶抽出液として、穀物以外の茶原料の抽出液を用いてもよい。穀物以外の茶原料の抽出液を得る茶原料としては、Camellia属(C.sinensis、C.assamica等)の茶葉(緑茶葉、紅茶葉、半発酵茶葉)、ビワの葉、桑の葉、エゴマの葉、クマザサの葉、柿の葉、アマチャヅルの葉、アシタバの葉、ドクダミの葉、シソの葉、ヨモギの葉、杜仲葉、グァバ葉、月見草、大麦若葉、カワラケツメイ等の葉類、ナツメ、クコ、ユズ、ミカン、レモン等の果実類、チコリーの根、タンポポの根、ゴボウの根や、エビスグサの種子(ケツメイシ)を乾燥等させたものが挙げられる。 As the tea extract, an extract of tea raw material other than grain may be used. Examples of the tea raw material for obtaining an extract of tea raw materials other than grains include tea leaves of the genus Camellia (C. sinensis, C. assamica, etc.) (green tea leaves, black tea leaves, semi-fermented tea leaves), loquat leaves, mulberry leaves, and sesame seeds. Leaves, leaves of Kumazasa, leaves of persimmon, leaves of Achacha, leaves of Ashitaba, leaves of Dokudami, leaves of Perilla, leaves of mugwort, leaves of Tonaka leaves, guava leaves, evening primroses, young barley leaves, kawara-ketsumei, etc., dates, jujube, Examples include fruits such as wolfberry, yuzu, mandarin, and lemon, chicory root, dandelion root, burdock root, and dried Ebisugusa seeds (Ketsumeishi).

茶抽出液として、茶原料を1種のみ用いても、2種以上を用いてもよい。 As the tea extract, one kind of tea raw material may be used, or two or more kinds thereof may be used.

(穀物粉末)
茶飲料が含む穀物粉末は、穀物粉末の原料穀物を必要に応じて焙煎した後、粉砕して得られる粉末状の穀物である原料穀物粉末を、詳しくは後述する方法によりアミラーゼ処理やセルラーゼ処理した穀物粉末(以下、酵素処理済み穀物粉末ともいう)である。
穀物粉末の原料穀物としては、穀物茶飲料の原料として通常用いられる穀物を使用でき、大麦、発芽大麦、小麦等の麦類、玄米、発芽玄米等の米類、大豆、小豆、黒豆等の豆類、トウモロコシ、芋、あわ、キビ、ハトムギ等が挙げられる。穀物粉末の原料穀物としては、おいしさや味わいの観点からは、大麦、玄米や、トウモロコシ、ハトムギが好ましい。但し、本実施の形態においては、原料穀物粉末のデンプン含有量が30質量%以上になる原料穀物を用いる。
(Grain powder)
The grain powder contained in the tea beverage is a raw grain powder that is a powdery grain obtained by roasting the raw grain powder of the grain powder, if necessary, and amylase treatment or cellulase treatment by the method described later in detail. Grain powder (hereinafter, also referred to as enzyme-treated grain powder).
As the raw material grain of the grain powder, grains usually used as a raw material for grain tea beverages can be used, such as barley, germinated barley, wheat and other wheat, brown rice, germinated brown rice and other rice, soybeans, red beans, black beans and other beans. , Corn, potato, foam, millet, pearl barley and the like. From the viewpoint of taste and taste, barley, brown rice, corn, and adlay are preferable as raw material grains for grain powder. However, in the present embodiment, a raw material grain in which the starch content of the raw material grain powder is 30% by mass or more is used.

茶飲料が含む茶抽出液や穀物粉末の配合割合は、特に限定されない。本実施の形態の茶飲料が含む茶抽出液は、例えば、茶飲料に対して茶抽出液の茶原料を0.1g/L以上30.0g/L以下の配合割合で抽出された抽出液である。また、本実施の形態の茶飲料が含む穀物粉末は、茶飲料に対して、例えば0.01g/L以上1.0g/L以下であり、0.05g/L以上であることが好ましく、0.1g/L以上であることがより好ましく、また、0.5g/L以下であることが好ましく、0.3g/L以下であることがより好ましい。なお、上記配合割合は、茶抽出液の茶原料や穀物粉末について、乾燥物(焙煎物)での量として記載してある。 The blending ratio of the tea extract or grain powder contained in the tea beverage is not particularly limited. The tea extract contained in the tea beverage of the present embodiment is, for example, an extract obtained by extracting the tea raw material of the tea extract into the tea beverage at a mixing ratio of 0.1 g/L or more and 30.0 g/L or less. is there. Further, the grain powder contained in the tea beverage of the present embodiment is, for example, 0.01 g/L or more and 1.0 g/L or less, preferably 0.05 g/L or more, with respect to the tea beverage, 0 0.1 g/L or more is more preferable, 0.5 g/L or less is preferable, and 0.3 g/L or less is more preferable. The above blending ratio is described as the amount of the tea raw material or the grain powder of the tea extract in a dried product (roasted product).

茶飲料は、本発明の効果を阻害しない範囲で、一般的な茶飲料に通常用いられる他の添加剤等を含んでいてもよい。添加剤の含有量は得ようとする効果に応じて適宜設定できる。茶飲料が含んでいてもよい添加剤としては、例えば酸化防止剤、香料、各種エステル類、有機酸類、有機酸塩類、無機酸類、無機酸塩類、無機塩類、色素類、乳化剤、保存料、調味料、品質安定剤等が挙げられる。 The tea beverage may contain other additives ordinarily used in general tea beverages, as long as the effects of the present invention are not impaired. The content of the additive can be appropriately set depending on the effect to be obtained. Examples of additives that the tea beverage may include include, for example, antioxidants, flavors, various esters, organic acids, organic acid salts, inorganic acids, inorganic acid salts, inorganic salts, pigments, emulsifiers, preservatives, and seasonings. Materials, quality stabilizers and the like.

(穀物粉末製造工程)
穀物粉末製造工程では、原料穀物粉末を水性媒体に分散した後に、原料穀物粉末に対してアミラーゼ処理及びセルラーゼ処理の少なくとも一方を施して、水性媒体に分散した穀物粉末、すなわち、穀物粉末が水性媒体に分散した穀物粉末分散液を得る。
(Cereal powder manufacturing process)
In the grain powder manufacturing process, after the raw grain powder is dispersed in an aqueous medium, at least one of amylase treatment and cellulase treatment is applied to the raw grain powder, and the grain powder dispersed in the aqueous medium, that is, the grain powder is an aqueous medium. To obtain a cereal powder dispersion.

本実施の形態において用いる、穀物粉末の原料としての原料穀物粉末は、デンプン含有量が30質量%以上である。デンプン含有量が30質量%以上の原料穀物粉末を用いると、穀物粉末の沈殿物の再分散性が悪くなるが、本実施の形態の製造方法で製造することにより、穀物粉末の沈殿物の再分散性を向上することができる。 The raw material grain powder used as the raw material of the grain powder used in the present embodiment has a starch content of 30% by mass or more. When the raw material grain powder having a starch content of 30% by mass or more is used, the redispersibility of the grain powder precipitate is deteriorated. However, when the raw material grain powder is produced by the production method of the present embodiment, the grain powder precipitate is redispersed. The dispersibility can be improved.

原料穀物粉末のデンプン含有量は、30質量%以上であればよく、例えば、40質量%以上でもよく、50質量%以上でもよく、60質量%以上でもよい。上限値は特に限定されないが、例えば95質量%以下である。 The starch content of the raw material grain powder may be 30 mass% or more, for example, 40 mass% or more, 50 mass% or more, and 60 mass% or more. The upper limit is not particularly limited, but is 95% by mass or less, for example.

原料穀物粉末のデンプン含有量は、酵素法定量で測定する。本明細書では、F−キットスターチ(製品番号;207748;ロッシュ/R−バイオファーム社製)によって、後述する実施例に記載の方法で測定する。なお、測定には乾燥した状態(例えば焙煎後)の原料穀物粉末を供する。 The starch content of the raw grain flour is measured by the enzymatic method. In the present specification, F-kit starch (product number: 207748; manufactured by Roche/R-Biopharm) is used for measurement by the method described in Examples below. In addition, the raw material grain powder in a dried state (for example, after roasting) is used for the measurement.

原料穀物粉末は、原料穀物を粉砕することで得られる。原料穀物を粉砕する方法は特に限定されず、例えば、ジェットミル、ボールミル、ビーズミル、遊星ミル、ハンマーミル、ピンミル、ロールミル、カッターミル、ホモゲナイザー、フレンチプレス等を用いて粉砕することができる。なお、粉砕処理に供する原料穀物は、焙煎後の穀物を用いることが好ましい。 The raw grain powder is obtained by crushing the raw grain. The method for crushing the raw material grain is not particularly limited, and for example, it can be crushed using a jet mill, a ball mill, a bead mill, a planetary mill, a hammer mill, a pin mill, a roll mill, a cutter mill, a homogenizer, a French press or the like. In addition, it is preferable to use the grain after roasting as a raw grain used for a grinding process.

穀物粉末の原料穀物を焙煎する方法は、一般的な焙煎方法を採用可能であり、例えば、熱風焙煎、直火焙煎、砂炒焙煎、遠赤外焙煎等が挙げられる。焙煎工程を有さなくてもよいが、香ばしさ等を付与できる観点から、焙煎工程を有することが好ましい。 As a method for roasting the raw material grain of the grain powder, a general roasting method can be adopted, and examples thereof include hot air roasting, direct-fire roasting, sand roasting, and far infrared roasting. Although it is not necessary to have a roasting step, it is preferable to have a roasting step from the viewpoint of imparting flavor and the like.

原料穀物粉末を分散させる水性媒体としては、水や、水に各種添加剤(例えば、pH調整剤)を添加した水溶液が挙げられる。 Examples of the aqueous medium in which the raw material grain powder is dispersed include water and an aqueous solution obtained by adding various additives (for example, a pH adjusting agent) to water.

原料穀物粉末を水性媒体に分散させる方法は特に限定されず、分散後に、原料穀物粉末に対してアミラーゼ処理やセルラーゼ処理が行えるように、原料穀物粉末が分散できればよい。 The method of dispersing the raw grain powder in the aqueous medium is not particularly limited, and it is sufficient that the raw grain powder can be dispersed so that the raw grain powder can be subjected to amylase treatment or cellulase treatment after the dispersion.

原料穀物粉末に対してアミラーゼ処理する方法は特に限定されない。例えば原料穀物粉末が分散された水性媒体に、アミラーゼを添加すればよい。アミラーゼ処理の温度(水性媒体の温度)は、例えば30℃以上80℃以下、好ましくは45℃以上70℃以下である。また、アミラーゼ処理の時間は、例えば1分以上3時間以下、好ましくは10分以上1時間以下である。
アミラーゼは、デンプンの構成成分であるアミロース、アミロペクチンやグリコーゲンを分解できる酵素である。アミラーゼとしては、α−アミラーゼ、β−アミラーゼ、グルコアミラーゼ、イソアミラーゼ等が挙げられる。アミラーゼとして、市販品を用いてもよい。
原料穀物粉末に対してアミラーゼ処理することにより、原料穀物粉末中のデンプンが分解される。
The method of amylase treatment of the raw grain powder is not particularly limited. For example, amylase may be added to an aqueous medium in which the raw grain powder is dispersed. The temperature of the amylase treatment (temperature of the aqueous medium) is, for example, 30° C. or higher and 80° C. or lower, preferably 45° C. or higher and 70° C. or lower. The amylase treatment time is, for example, 1 minute or more and 3 hours or less, preferably 10 minutes or more and 1 hour or less.
Amylase is an enzyme that can decompose amylose, amylopectin, and glycogen, which are constituents of starch. Examples of the amylase include α-amylase, β-amylase, glucoamylase and isoamylase. A commercially available product may be used as the amylase.
By subjecting the raw grain powder to amylase treatment, the starch in the raw grain powder is decomposed.

原料穀物粉末に対してセルラーゼ処理する方法は特に限定されない。例えば原料穀物粉末が分散された水性媒体に、セルラーゼを添加すればよい。セルラーゼ処理の温度(水性媒体の温度)は、例えば30℃以上80℃以下、好ましくは45℃以上70℃以下である。また、セルラーゼ処理の時間は、例えば1分以上3時間以下、好ましくは10分以上1時間以下である。
セルラーゼは、セルロースのグリコキシド結合を分解できる酵素である。セルラーゼとして、市販品を用いてもよい。
原料穀物粉末に対してセルラーゼ処理することにより、原料穀物粉末中のセルロースが分解される。
The method of cellulase treatment of the raw grain powder is not particularly limited. For example, cellulase may be added to an aqueous medium in which the raw grain powder is dispersed. The temperature of the cellulase treatment (temperature of the aqueous medium) is, for example, 30° C. or higher and 80° C. or lower, preferably 45° C. or higher and 70° C. or lower. The cellulase treatment time is, for example, 1 minute or more and 3 hours or less, preferably 10 minutes or more and 1 hour or less.
Cellulase is an enzyme capable of degrading the glycoxide bond of cellulose. A commercially available product may be used as the cellulase.
By subjecting the raw material grain powder to cellulase treatment, the cellulose in the raw material grain powder is decomposed.

アミラーゼ及びセルラーゼを併用してもよく、また、アミラーゼ及びセルラーゼの少なくとも一方とその他の酵素とを併用してもよい。 Amylase and cellulase may be used in combination, or at least one of amylase and cellulase may be used in combination with other enzyme.

(混合工程)
混合工程では、穀物粉末製造工程で得られた水性媒体に分散した穀物粉末と飲料用分散媒とを混合する。
まず、飲料用分散媒としての茶抽出液を準備する。茶抽出液は、茶抽出液の原料(茶原料)から、抽出溶媒を用いて得られる。抽出に供する茶原料は、焙煎後のものであることが好ましい。
(Mixing process)
In the mixing step, the grain powder dispersed in the aqueous medium obtained in the grain powder manufacturing step is mixed with the beverage dispersion medium.
First, a tea extract as a dispersion medium for beverages is prepared. The tea extract is obtained from the raw material of the tea extract (tea raw material) using an extraction solvent. The tea raw material used for extraction is preferably that after roasting.

なお、複数の茶原料を用いる場合、例えば、複数の茶原料をそれぞれ単独で抽出してもよいし、複数の茶原料を予め混合して抽出してもよい。製造効率の観点から、複数の穀物原料の全てを予め混合して抽出することが好ましい。 When using a plurality of tea raw materials, for example, the plurality of tea raw materials may be extracted individually, or the plurality of tea raw materials may be mixed in advance and extracted. From the viewpoint of production efficiency, it is preferable to premix and extract all of the plurality of grain raw materials.

抽出方法としては一般的な抽出方法を採用可能であり、例えば、水蒸気蒸留、液化炭酸ガス抽出、アルコール抽出、熱水抽出等の従来公知の抽出方法を用いることができる。また、抽出に用いる抽出溶媒の種類は、特に限定されないが、水を抽出溶媒とする場合は、脱イオン交換処理精製したもの又は蒸留水を用いることが好ましい。これらは、安価、手軽であり、且つ安全に調製し抽出設備に供することができる。水以外の抽出溶媒としては、エタノールやその他の親水性有機溶媒が挙げられる。また、抽出溶媒に対して、抽出効率化の目的で、食品添加物のいわゆる炭酸塩(炭酸水素ナトリウム(重曹)等)、リン酸塩、アスコルビン酸塩、アスコルビン酸等を適宜添加してもよい。 As the extraction method, a general extraction method can be adopted, and for example, a conventionally known extraction method such as steam distillation, liquefied carbon dioxide extraction, alcohol extraction, hot water extraction and the like can be used. The type of extraction solvent used for extraction is not particularly limited, but when water is used as the extraction solvent, it is preferable to use deionized exchange-treated and purified water or distilled water. These are inexpensive and convenient, and can be safely prepared and supplied to the extraction equipment. Examples of the extraction solvent other than water include ethanol and other hydrophilic organic solvents. For the purpose of improving the extraction efficiency, so-called carbonates (sodium hydrogen carbonate (sodium bicarbonate) etc.), phosphates, ascorbates, ascorbic acid etc. of food additives may be appropriately added to the extraction solvent. ..

抽出温度は、特に限定されないが、例えば、80℃以上100℃以下であることが好ましい。上記温度範囲で抽出を行えば、抽出効率が高い。抽出時間も特に限定されないが、5分以上60分以下の範囲内で行うことが好ましい。上記抽出時間で抽出物を得れば、熱による風味変化や香気成分の散逸を抑えつつ、甘味、香ばしさの各成分を抽出しやすい傾向にある。これにより、嗜好性に優れた茶飲料が得やすくなる。 The extraction temperature is not particularly limited, but is preferably 80° C. or higher and 100° C. or lower, for example. If extraction is performed within the above temperature range, extraction efficiency is high. The extraction time is not particularly limited, but it is preferably performed within the range of 5 minutes or more and 60 minutes or less. If the extract is obtained in the above extraction time, the sweetness and fragrance components tend to be easily extracted while suppressing the change in flavor and the dissipation of aroma components due to heat. This makes it easier to obtain a tea beverage with excellent palatability.

飲料用分散媒としての茶抽出液と、水性媒体に分散した穀物粉末とを混合する方法は特に限定されない。必要に応じて、水や添加物を添加してもよい。なお、複数の抽出液を得た場合は、該複数の抽出液を水性媒体に分散した穀物粉末と混合すればよい。 The method for mixing the tea extract as a beverage dispersion medium and the grain powder dispersed in the aqueous medium is not particularly limited. You may add water and an additive as needed. When a plurality of extracts are obtained, the plurality of extracts may be mixed with grain powder dispersed in an aqueous medium.

(殺菌工程及び容器充填工程)
混合工程の後、殺菌工程や容器充填工程を経ることが好ましい。
殺菌工程では、加熱等により、茶抽出液及び穀物粉末等を殺菌する。また、容器充填工程では、茶抽出液及び穀物粉末等を容器に充填する。金属缶や瓶のように容器に充填後、加熱殺菌できる場合は、レトルト殺菌(加圧加熱処理:110〜140℃、1〜数十分間)により製造できる。ペットボトルや紙容器のようにレトルト殺菌できないものについては、予めレトルト殺菌と同等の殺菌条件、例えばプレート式熱交換機等で超高温加熱処理(UHT殺菌:110〜150℃、1〜数十秒間)し、一定の温度まで冷却後、容器に充填する等の方法が選択できる。容器充填工程の方法としては、例えば、アセプティック(無菌)充填法、ホットパック充填法等が挙げられる。
(Sterilization process and container filling process)
After the mixing step, it is preferable to go through a sterilization step and a container filling step.
In the sterilization step, the tea extract, grain powder and the like are sterilized by heating or the like. Further, in the container filling step, the container is filled with the tea extract, grain powder and the like. When it can be sterilized by heating after being filled in a container such as a metal can or a bottle, it can be produced by retort sterilization (pressure heating treatment: 110 to 140° C., 1 to several tens of minutes). For items that cannot be sterilized by retort, such as PET bottles and paper containers, sterilization conditions equivalent to those for retort sterilization, such as ultra-high temperature heat treatment using a plate heat exchanger (UHT sterilization: 110 to 150°C, 1 to several tens of seconds) However, a method of filling the container after cooling to a certain temperature can be selected. Examples of the method for the container filling step include an aseptic (sterile) filling method and a hot pack filling method.

上記茶飲料の製造方法の各工程に用いられる装置や条件は、通常茶飲料の製造工程に採用されるものを使用できる。 As the apparatus and conditions used in each step of the above-mentioned tea beverage manufacturing method, those usually employed in the tea beverage manufacturing step can be used.

ここで、茶飲料が含む穀物粉末は、茶抽出液に溶解しない。したがって、製造から時間が経過した茶飲料、例えば販売時の茶飲料では、穀物粉末が沈殿した沈殿物が生じる。本実施の形態で製造される茶飲料においては、この穀物粉末の沈殿物の再分散性が良く、例えば茶飲料の容器を軽く振とうすることにより容易に再分散させることができる。 Here, the cereal powder contained in the tea beverage does not dissolve in the tea extract. Therefore, in a tea beverage which has passed the time since production, for example, a tea beverage at the time of sale, a precipitate in which grain powder is precipitated is generated. In the tea beverage produced in the present embodiment, the redispersibility of the grain powder precipitate is good, and the tea beverage can be easily redispersed by lightly shaking the container.

一方、水性媒体に分散した原料穀物粉末に対してアミラーゼ処理やセルラーゼ処理を施していない穀物粉末を茶飲料に配合すると、穀物粉末の沈殿物の再分散性が悪く、茶飲料の容器を繰り返し振とうしないと沈殿物を再分散できない。このことは、穀物粉末においては、原料穀物粉末に含まれるデンプン及び殻皮や果皮に含まれるセルロースが穀物粉末表面に露出した状態になっていて、製造中に施される高温加熱(例えば殺菌処理)によってデンプンがα化(糊化)してセルロースと付着しやすくなり、そのため穀物粉末同士が固着することによると推測される。 On the other hand, if the grain powder that has not been subjected to amylase treatment or cellulase treatment is mixed into the tea beverage for the raw grain powder dispersed in the aqueous medium, the redispersibility of the grain powder precipitate is poor and the tea beverage container is repeatedly shaken. Otherwise, the precipitate cannot be redispersed. This means that in the grain powder, the starch contained in the raw material grain powder and the cellulose contained in the shells and pericarps are exposed on the surface of the grain powder, and the high temperature heating (for example, sterilization treatment) performed during the production is performed. It is speculated that due to (), starch is pregelatinized (gelatinized) and easily adheres to cellulose, which causes the grain powders to stick to each other.

これに対し、本実施の形態においては、穀物粉末に対して予めアミラーゼ処理やセルラーゼ処理を行っている。したがって、本実施の形態においては、アミラーゼ処理によりデンプン鎖が短くなるか、セルラーゼ処理によりセルロース鎖が短くなった穀物粉末を用いるため、デンプンとセルロースが付着し難くなり、穀物同士の固着が抑制されて、再分散性が向上すると推測される。 On the other hand, in the present embodiment, amylase treatment and cellulase treatment are performed on the grain powder in advance. Therefore, in the present embodiment, since starch powder is shortened by amylase treatment or cellulose powder is shortened by cellulase treatment, it becomes difficult for starch and cellulose to adhere to each other, and adhesion between grains is suppressed. Therefore, it is presumed that the redispersibility is improved.

このように、本実施の形態においては、穀物粉末を含み穀物粉末の沈殿物の再分散性に優れた茶飲料を製造することができるため、例えば穀物粉末の沈殿物の再分散性に優れ且つコクやボディ感の向上等の特性が改良された飲料を提供することができる。 Thus, in the present embodiment, since it is possible to produce a tea beverage containing grain powder and excellent in redispersibility of the precipitate of grain powder, for example, excellent redispersibility of the precipitate of grain powder and It is possible to provide a beverage having improved characteristics such as improved body feeling and body feeling.

<飲料用分散媒に添加される、穀物粉末が水性媒体に分散した穀物粉末分散液の製造方法、及び、酵素処理済み穀物粉末の製造方法>
本実施の形態に係る上記飲料の製造方法における穀物粉末製造工程と同様の方法で、飲料用分散媒に添加される、穀物粉末が水性媒体に分散した穀物粉末分散液や、酵素処理済み穀物粉末を製造することができる。
<Method for producing grain powder dispersion liquid in which grain powder is dispersed in an aqueous medium, and method for producing enzyme-treated grain powder, which is added to a dispersion medium for beverages>
In the same manner as the grain powder manufacturing step in the method for producing a beverage according to the present embodiment, the grain powder is added to the beverage dispersion medium, the grain powder dispersion of the grain powder dispersed in an aqueous medium, enzyme-treated grain powder. Can be manufactured.

具体的には、前者の飲料用分散媒に添加される、穀物粉末が水性媒体に分散した穀物粉末分散液の製造方法は、穀物粉末の原料である原料穀物粉末のデンプン含有量が30質量%以上であり、この原料穀物粉末を水性媒体に分散した後に、原料穀物粉末に対してアミラーゼ処理及びセルラーゼ処理の少なくとも一方を施して、穀物粉末が水性媒体に分散した穀物粉末分散液を得る穀物粉末分散液製造工程を有する。穀物粉末分散液製造工程は、上記穀物粉末製造工程と同様であり、穀物粉末、飲料用分散媒等は、上記<飲料の製造方法>において記載されたものと同様である。 Specifically, the former method of producing a grain powder dispersion liquid in which grain powder is dispersed in an aqueous medium, which is added to a beverage dispersion medium, has a starch content of 30% by mass of the raw material grain powder as a raw material of the grain powder. The above is, after the raw material grain powder is dispersed in an aqueous medium, at least one of amylase treatment and cellulase treatment is applied to the raw grain powder to obtain a grain powder dispersion liquid in which the grain powder is dispersed in an aqueous medium. It has a dispersion liquid manufacturing process. The grain powder dispersion liquid manufacturing process is the same as the grain powder manufacturing process, and the grain powder, the beverage dispersion medium, and the like are the same as those described in the above <Beverage manufacturing method>.

また、後者の飲料用分散媒に添加される酵素処理済み穀物粉末の製造方法は、穀物粉末の原料である原料穀物粉末のデンプン含有量が30質量%以上であり、この原料穀物粉末を水性媒体に分散した後に、原料穀物粉末に対してアミラーゼ処理及びセルラーゼ処理の少なくとも一方を施して、穀物粉末が水性媒体に分散した穀物粉末分散液を得る穀物粉末分散液製造工程と、穀物粉末分散液製造工程で得られた穀物粉末分散液から穀物粉末を回収する穀物粉末回収工程とを有する。穀物粉末分散液製造工程は、上記飲料用分散媒に添加される、穀物粉末が水性媒体に分散した穀物粉末分散液の製造方法における穀物粉末分散液製造工程と同様である。また、穀物粉末回収工程において、穀物粉末分散液製造工程で得られた穀物粉末分散液から穀物粉末(酵素処理済み穀物粉末)を回収する方法は、特に限定されず、例えば穀物粉末分散液を濾過する方法や、遠心分離やスプレードライ、凍結乾燥等の、穀物粉末分散液から分散媒を除去する方法が挙げられる。 Further, in the latter method for producing an enzyme-treated grain powder added to a dispersion medium for beverage, the starch content of the raw grain powder, which is a raw material of the grain powder, is 30% by mass or more, and the raw grain powder is an aqueous medium. And then at least one of amylase treatment and cellulase treatment on the raw material grain powder to obtain a grain powder dispersion liquid in which the grain powder is dispersed in an aqueous medium. And a grain powder collecting step of collecting grain powder from the grain powder dispersion liquid obtained in the step. The grain powder dispersion liquid producing step is the same as the grain powder dispersion liquid producing step in the method for producing a grain powder dispersion liquid in which grain powder is dispersed in an aqueous medium, which is added to the beverage dispersion medium. In the grain powder collecting step, the method for collecting grain powder (enzyme-treated grain powder) from the grain powder dispersion obtained in the grain powder dispersion manufacturing step is not particularly limited, and for example, the grain powder dispersion is filtered. And a method of removing the dispersion medium from the grain powder dispersion liquid, such as centrifugation, spray drying, and freeze drying.

これらの製造方法で得られる穀物粉末分散液中の穀物粉末や、酵素処理済み穀物粉末は、沈殿物の再分散性に優れている。したがって、該穀物粉末分散液や酵素処理済み穀物粉末を各種飲料用分散媒に配合することにより、穀物粉末の沈殿物の再分散性に優れ且つコクやボディ感の向上等の特性が改良された飲料を得ることができる。 The grain powder in the grain powder dispersion obtained by these production methods and the grain powder subjected to the enzyme treatment are excellent in the redispersibility of the precipitate. Therefore, by blending the grain powder dispersion liquid or the enzyme-treated grain powder in a dispersion medium for various beverages, the redispersibility of the precipitate of the grain powder is excellent and the properties such as the richness and the body feeling are improved. You can get a drink.

以下、実施例を示し、本発明を具体的に説明するが、本発明はこれらの実施例に限定されるものではない。 Hereinafter, the present invention will be specifically described with reference to examples, but the present invention is not limited to these examples.

[茶飲料1〜17]
<茶抽出液(飲料用分散媒)の作製>
ドリップ抽出器を用い、焙煎後の大麦を、10g/Lとなる配合割合で、20倍量のお湯(90℃)で30分間浸漬抽出し、濾過して、茶抽出液を得た。
<穀物粉末の作製>
焙煎後の大麦、トウモロコシ、玄米、ハトムギを、それぞれ粉砕して、原料穀物粉末(大麦粉末、トウモロコシ粉末、玄米粉末、ハトムギ粉末)を得た。
また、得られた各原料穀物粉末について、それぞれデンプン含有量を、以下の方法で測定した。結果を表1に示す。
[Tea beverages 1-17]
<Preparation of tea extract (dispersion medium for beverages)>
Using a drip extractor, the barley after roasting was subjected to immersion extraction with 20 times the amount of hot water (90° C.) for 30 minutes at a blending ratio of 10 g/L, followed by filtration to obtain a tea extract.
<Production of grain powder>
The roasted barley, corn, brown rice, and adlay were crushed to obtain raw grain powder (barley powder, corn powder, brown rice powder, adlay powder).
In addition, the starch content of each of the obtained raw material grain powders was measured by the following method. The results are shown in Table 1.

(デンプン含有量の測定)
F−キットスターチ(製品番号;207748;ロッシュ/R−バイオファーム社製)を用いて、以下の方法により各原料穀物粉末のデンプン含有量を測定した。
<前処理>
F−キットスターチ取扱説明書(8.試料の調整法、8.1.DMSO(ジメチルスルホキシド)及びHClによるスターチの可溶化に記載の方法)に基づいて処理した。具体的には、以下の手順で処理して、F−キットスターチでの測定試料(試料溶液)を調整した。
(1)試料である原料穀物粉末を0.2mm径のふるいにかけて均一化する。
(2)ふるい後の原料穀物粉末について、100mg〜1gを正確に秤量する。(スターチ量として70mgまで)
(3)20mLのジメチルスルホキシド及び5mLの塩酸(8mol/L)を加え、ときどき撹拌しながら60℃30分間加温する。
(4)室温(25℃)に急冷する。
(5)水酸化ナトリウム水溶液(8mol/L)5mLを加える。
(6)クエン酸緩衝液(0.112mol/Lクエン酸と0.112mol/Lクエン酸三ナトリウムの混合液)を加えて100mLに定容する。
(7)濾過した濾液0.10mL又は0.20mLをF−キットでの測定試料とする。(スターチ濃度が6〜70mg/100mLとなるよう、0.10〜0.20mlの範囲で試料量を調整する)
(Measurement of starch content)
Using F-kit starch (product number: 207748; Roche/R-Biopharm), the starch content of each raw material grain powder was measured by the following method.
<Pretreatment>
Processing was performed according to the F-kit starch instruction manual (8. Preparation of samples, 8.1. Method described in solubilization of starch with DMSO (dimethyl sulfoxide) and HCl). Specifically, the sample was processed by the following procedure to prepare a measurement sample (sample solution) with F-kit starch.
(1) A raw material grain powder as a sample is passed through a sieve having a diameter of 0.2 mm to make it uniform.
(2) Regarding the raw material grain powder after sieving, 100 mg to 1 g is accurately weighed. (Up to 70 mg of starch)
(3) Add 20 mL of dimethylsulfoxide and 5 mL of hydrochloric acid (8 mol/L), and heat at 60° C. for 30 minutes with occasional stirring.
(4) Rapidly cool to room temperature (25°C).
(5) Add 5 mL of sodium hydroxide aqueous solution (8 mol/L).
(6) Add a citrate buffer solution (mixture of 0.112 mol/L citric acid and 0.112 mol/L trisodium citrate) to bring the volume to 100 mL.
(7) Use 0.10 mL or 0.20 mL of the filtered filtrate as a measurement sample with the F-kit. (Adjust the sample amount in the range of 0.10 to 0.20 ml so that the starch concentration is 6 to 70 mg/100 mL)

(A)試料溶液0.10〜0.20mLに対し、溶液1を0.20mL混和し、55〜60℃(温浴中)で15分間インキュベーションした。その後、試料を温浴から取り出し、室温に戻してから、蒸留水を試料と蒸留水の合計量が1.10mLとなるように加え、溶液2を1.00mL秤取し、混和して、約3分後に波長340nmにおける吸光度EA1を測定した。さらに、懸濁液3を0.02mL混和し、約10〜15分後に波長340nmにおける吸光度EA2を測定した。そして、吸光度ΔEA(=吸光度EA2−吸光度EA1)を算出した。 (A) 0.20 mL of the solution 1 was mixed with 0.10 to 0.20 mL of the sample solution and incubated at 55 to 60° C. (in a warm bath) for 15 minutes. Then, the sample was taken out of the warm bath and returned to room temperature, and then distilled water was added so that the total amount of the sample and distilled water was 1.10 mL, and 1.00 mL of solution 2 was weighed and mixed to obtain about 3 mL. After a minute, the absorbance EA1 at a wavelength of 340 nm was measured. Further, 0.02 mL of the suspension 3 was mixed, and after about 10 to 15 minutes, the absorbance EA2 at a wavelength of 340 nm was measured. Then, the absorbance ΔEA (=absorbance EA2-absorbance EA1) was calculated.

(B)溶液1 0.20mLに対し、蒸留水0.10mLを混和し、55〜60℃(温浴中)で15分間インキュベーションした。その後、温浴から取り出し、室温に戻してから、蒸留水を1.00mL及び溶液2を1.00mL秤取し、混和して、約3分後に波長340nmにおける吸光度EB1を測定した。さらに、懸濁液3を0.02mL混和し、約10〜15分後に波長340nmにおける吸光度EB2を測定した。そして、吸光度ΔEB(=吸光度EB2−吸光度EB1)を算出した。 (B) Solution 1 (0.20 mL) was mixed with distilled water (0.10 mL) and incubated at 55 to 60° C. (in a warm bath) for 15 minutes. Then, after taking out from a warm bath and returning to room temperature, 1.00 mL of distilled water and 1.00 mL of solution 2 were weighed and mixed, and after about 3 minutes, the absorbance EB1 at a wavelength of 340 nm was measured. Further, 0.02 mL of the suspension 3 was mixed, and after about 10 to 15 minutes, the absorbance EB2 at a wavelength of 340 nm was measured. Then, the absorbance ΔEB (=absorbance EB2−absorbance EB1) was calculated.

上記(A)(B)において使用した溶液は、下記の通りである。
溶液1:「F−キット スターチ」のビン1(約100mg凍結乾燥品:クエン酸バッファー、pH約4.6;酵素アミログルコシダーゼ(AGS)約84Uを蒸留水6mLで溶解した溶液。
溶液2:「F−キット スターチ」のビン2(約5g粉末;トリエタノールアミンバッファー、pH約7.6;ニコチンアミドアデニンジヌクレオチドリン酸(NADP)約75mg:アデノシン三リン酸(ATP)約190mg;Mg2SO4)を蒸留水27mLで溶解した溶液。
懸濁液3:「F−キット スターチ」のビン3(0.7ml懸濁液:ヘキソキナーゼ(HK)約200U;グルコース‐6‐リン酸デヒドロゲナーゼ(G6P−DH)約100U)
The solutions used in the above (A) and (B) are as follows.
Solution 1: Bottle 1 of "F-Kit Starch" (about 100 mg lyophilized product: citrate buffer, pH about 4.6; solution in which about 84 U of enzyme amyloglucosidase (AGS) was dissolved in 6 mL of distilled water.
Solution 2: "F-Kit Starch" bottle 2 (about 5 g powder; triethanolamine buffer, pH about 7.6; nicotinamide adenine dinucleotide phosphate (NADP) about 75 mg: adenosine triphosphate (ATP) about 190 mg) A solution of Mg2SO4) dissolved in 27 mL of distilled water.
Suspension 3: Bottle 3 of "F-Kit Starch" (0.7 ml suspension: hexokinase (HK) about 200 U; glucose-6-phosphate dehydrogenase (G6P-DH) about 100 U)

そして、ΔE=ΔEA−ΔEBを算出し、次式によりデンプン成分の含有量を算出した。結果を表1に示す。
試料溶液中のデンプンの含有量(mg/100mL)=0.597×ΔE×100
原料穀物粉末中のデンプンの含有量(mg/g)=試料溶液中のデンプン含有量/原料穀物粉末採取量(g)
(式中、原料穀物粉末採取量は、前処理における(2)で秤量した原料穀物粉末の量である。)
Then, ΔE=ΔEA−ΔEB was calculated, and the content of the starch component was calculated by the following formula. The results are shown in Table 1.
Content of starch in sample solution (mg/100 mL) = 0.597 x ΔE x 100
Content of starch in raw grain powder (mg/g)=starch content in sample solution/collection amount of raw grain powder (g)
(In the formula, the amount of raw grain powder collected is the amount of raw grain powder weighed in (2) in the pretreatment.)

また、得られた各原料穀物粉末に対して、原料穀物粉末を100倍量の水に分散させて、表1に示す酵素試薬を添加し、恒温水槽にて50℃1時間保持する、酵素処理を施した。これにより、酵素処理された穀物粉末の水分散液を得た。下記に酵素試薬として用いたアミラーゼ(α−アミラーゼ)、セルラーゼ、ヘミセルラーゼ、プロテアーゼ及びその使用量を記載する。
・α−アミラーゼ((富士フイルム和光純薬製、α-Amylase)、250000Unit、水に対する使用量:0.0006g/L)
・セルラーゼ((MPバイオメディカル製、Cellulase)、42700Unit、水に対する使用量:0.0076g/L)
・ヘミセルラーゼ((メルク製、Hemicellulase from Aspergillus niger)、60000Unit、水に対する使用量:0.0179g/L)
・プロテアーゼ((富士フイルム和光純薬製、Protease)、1500Unit、水に対する使用量:0.048g/L)
Further, with respect to each of the obtained raw material grain powders, the raw material grain powders were dispersed in 100 times the amount of water, the enzyme reagents shown in Table 1 were added, and the mixture was kept in a constant temperature water bath at 50° C. for 1 hour. Was applied. As a result, an aqueous dispersion of the grain powder that had been treated with the enzyme was obtained. The amylase (α-amylase), cellulase, hemicellulase, protease used as enzyme reagents and the amounts used are described below.
・Α-Amylase ((Fujifilm Wako Pure Chemical Industries, α-Amylase), 250,000Unit, water usage: 0.0006g/L)
・Cellulase ((MP Biomedical, Cellulase), 42700Unit, water usage: 0.0076g/L)
・Hemicellulase ((Merck, Hemicellulase from Aspergillus niger), 60000Unit, usage in water: 0.0179g/L)
・Protease ((Fujifilm Wako Pure Chemical Industries, Protease), 1500Unit, water usage: 0.048g/L)

<穀物茶飲料の作製>
<茶抽出液(飲料用分散媒)の作製>で得られた各茶抽出液に、得られる茶飲料1Lに対して、穀物粉末の含有量が0.3g/Lになるように、<穀物粉末の作製>で得られた酵素処理された穀物粉末の水分散液を混合した後、アスコルビン酸ナトリウム及び炭酸水素ナトリウム(重曹)を添加して、水で規定量にフィルアップした。アスコルビン酸ナトリウムは得られる茶飲料1Lに対して0.4g/L、炭酸水素ナトリウム(重曹)は得られる茶飲料1Lに対して0.1g/Lになるように添加した。なお、これらの濃度は、全て最終的に得られた茶飲料における濃度である。
得られた各茶飲料を、超高温加熱処理(UHT)法にて殺菌し、それぞれ500mLのPETボトルにアセプティック(無菌)充填し、茶飲料1〜17を得た。
<Production of grain tea beverage>
To each tea extract obtained in <Preparation of tea extract (dispersion medium for beverage)>, the content of grain powder was 0.3 g/L for 1 L of the obtained tea beverage, <grain Preparation of powder> After mixing the aqueous dispersion of the enzyme-treated grain powder obtained in <1.>, sodium ascorbate and sodium hydrogen carbonate (baking soda) were added, and water was filled up to a specified amount. Sodium ascorbate was added in an amount of 0.4 g/L with respect to 1 L of the obtained tea beverage, and sodium hydrogen carbonate (sodium bicarbonate) was added in an amount of 0.1 g/L with respect to 1 L of the obtained tea beverage. In addition, all of these concentrations are the concentrations in the finally obtained tea beverage.
Each of the obtained tea beverages was sterilized by an ultra-high temperature heat treatment (UHT) method, and each 500 mL PET bottle was aseptically (sterile) filled to obtain tea beverages 1 to 17.

[茶飲料18]
穀物粉末を用いなかったこと以外は、上記茶飲料1と同様して、茶飲料18を得た。
[Tea drink 18]
A tea beverage 18 was obtained in the same manner as the tea beverage 1 except that the grain powder was not used.

[茶飲料19(参考例)]
<緑茶抽出液の作製>
浸漬撹拌抽出機を用い、焙煎後の緑茶葉を、7g/Lとなる配合割合で、30倍量のお湯(70℃)で7分間浸漬抽出し、濾過して、緑茶抽出液を得た。
<緑茶粉末の作製>
焙煎後の緑茶を粉砕して、緑茶粉末を得た。得られた緑茶粉末を、100倍量の水に分散させて、緑茶粉末の水分散液を得た。
[Tea drink 19 (reference example)]
<Preparation of green tea extract>
Using a dipping and stirring extractor, the green tea leaves after roasting were dipped and extracted in 30 times the amount of hot water (70° C.) for 7 minutes at a blending ratio of 7 g/L and filtered to obtain a green tea extract. ..
<Preparation of green tea powder>
The green tea after roasting was crushed to obtain green tea powder. The obtained green tea powder was dispersed in 100 times the amount of water to obtain an aqueous dispersion of green tea powder.

<緑茶飲料の作製>
茶抽出液の代わりに緑茶抽出液を用い、酵素処理された穀物粉末の水分散液の代わりに緑茶粉末の水分散液を用いたこと以外は、上記茶飲料1と同様にして、茶飲料19を得た。
<Production of green tea beverage>
A tea beverage 19 was prepared in the same manner as the tea beverage 1 except that a green tea extract was used in place of the tea extract and an aqueous dispersion of green tea powder was used in place of the aqueous dispersion of enzyme-treated grain powder. Got

(再分散性の評価)
得られた茶飲料1〜19を、4℃で2週間静置した。この4℃で2週間の静置により、穀物粉末を含む茶飲料1〜17では穀物粉末がPETボトルの底に沈殿しており、また、緑茶粉末を含む茶飲料19では緑茶粉末がPETボトルの底に沈殿していた。
この4℃で2週間の静置後、PETボトルを手で上下回転(1回転/1秒間)させて、沈殿物が完全に分散するまでの回転数を調べた。結果を表1に示す。
(Evaluation of redispersibility)
The obtained tea beverages 1 to 19 were allowed to stand at 4°C for 2 weeks. By allowing this to stand at 4° C. for 2 weeks, the tea powders 1 to 17 containing the cereal powder have the cereal powder settled to the bottom of the PET bottle, and the tea drink 19 containing the green tea powder has the green tea powder to the PET bottle. It had settled to the bottom.
After standing at 4° C. for 2 weeks, the PET bottle was manually rotated up and down (1 rotation/1 second) to examine the number of rotations until the precipitate was completely dispersed. The results are shown in Table 1.

Figure 2020103116
Figure 2020103116

上記に示すように、原料穀物粉末のデンプン含有量が30質量以上でありアミラーゼ処理又はセルラーゼ処理が施された穀物粉末を添加した茶飲料2〜3、7〜8及び11〜12では、酵素処理を施さない又はヘミセルラーゼ処理やプロテアーゼ処理を施した茶飲料1、4〜6及び9〜10及び13よりも回転数が顕著に少なく、沈殿の再分散性に優れていることが確認された。
一方、原料穀物粉末のデンプン含有量が30質量%未満である茶飲料14〜17では、酵素処理の有無や酵素の種類によらず、沈殿の再分散性ほぼ同じであった。
なお、緑茶粉末を緑茶抽出液に添加した茶飲料19では、酵素処理を施さなくても再分散性に優れていた。
As described above, in the tea beverages 2-3, 7-8, and 11-12 in which the starch content of the raw material cereal powder is 30 mass or more and the cereal powder subjected to the amylase treatment or the cellulase treatment is added, the enzyme treatment is performed. It was confirmed that the number of revolutions was remarkably smaller than that of the tea beverages 1, 4 to 6 and 9 to 10 and 13 which were not subjected to the treatment or which were treated with the hemicellulase or the protease, and were excellent in redispersibility of the precipitate.
On the other hand, in the tea beverages 14 to 17 in which the starch content of the raw material grain powder was less than 30% by mass, the redispersibility of precipitation was almost the same regardless of the presence or absence of enzyme treatment and the type of enzyme.
The tea beverage 19 in which green tea powder was added to the green tea extract was excellent in redispersibility even without the enzymatic treatment.

Claims (2)

飲料用分散媒と穀物粉末とを含む飲料の製造方法であって、
前記穀物粉末の原料である原料穀物粉末のデンプン含有量が30質量%以上であり、
前記原料穀物粉末を水性媒体に分散した後に、前記原料穀物粉末に対してアミラーゼ処理及びセルラーゼ処理の少なくとも一方を施して、前記水性媒体に分散した前記穀物粉末を得る穀物粉末製造工程と、
前記穀物粉末製造工程で得られた前記水性媒体に分散した前記穀物粉末と前記飲料用分散媒とを混合する混合工程とを有する、飲料の製造方法。
A method for producing a beverage containing a beverage dispersion medium and grain powder,
The starch content of the raw material grain powder which is the raw material of the grain powder is 30% by mass or more,
After dispersing the raw grain powder in an aqueous medium, at least one of amylase treatment and cellulase treatment for the raw grain powder, to obtain the grain powder dispersed in the aqueous medium, a grain powder manufacturing step,
A method for producing a beverage, comprising a mixing step of mixing the grain powder obtained in the grain powder production step and dispersed in the aqueous medium, and the beverage dispersion medium.
前記飲料用分散媒が茶抽出液であり、前記飲料が茶飲料である、請求項1に記載の飲料の製造方法。 The method for producing a beverage according to claim 1, wherein the beverage dispersion medium is a tea extract, and the beverage is a tea beverage.
JP2018244467A 2018-12-27 2018-12-27 Beverage manufacturing method Active JP6921052B2 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP2018244467A JP6921052B2 (en) 2018-12-27 2018-12-27 Beverage manufacturing method

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP2018244467A JP6921052B2 (en) 2018-12-27 2018-12-27 Beverage manufacturing method

Publications (2)

Publication Number Publication Date
JP2020103116A true JP2020103116A (en) 2020-07-09
JP6921052B2 JP6921052B2 (en) 2021-08-18

Family

ID=71447642

Family Applications (1)

Application Number Title Priority Date Filing Date
JP2018244467A Active JP6921052B2 (en) 2018-12-27 2018-12-27 Beverage manufacturing method

Country Status (1)

Country Link
JP (1) JP6921052B2 (en)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP7105349B1 (en) * 2021-09-02 2022-07-22 アサヒ飲料株式会社 beverage
JP7134318B1 (en) 2021-09-02 2022-09-09 アサヒ飲料株式会社 beverage

Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2009142184A (en) * 2007-12-13 2009-07-02 Gun Ei Chem Ind Co Ltd beta-GLUCAN-CONTAINING BEVERAGE
JP2010063382A (en) * 2008-09-09 2010-03-25 T Hasegawa Co Ltd Method for producing plant extract
WO2013173869A1 (en) * 2012-05-23 2013-11-28 Climax Holdings Pty Limited Cereal based beverage
JP2013252113A (en) * 2012-06-08 2013-12-19 T Hasegawa Co Ltd Taste improver for cereal-containing food and beverage
JP2014027895A (en) * 2012-07-31 2014-02-13 Suntory Beverage & Food Ltd Production method of saccharified liquid of barley
JP2017127332A (en) * 2017-05-01 2017-07-27 株式会社 伊藤園 Dietary fiber-containing grain tea beverage production process and property deterioration suppression method
JP2018042521A (en) * 2016-09-16 2018-03-22 群栄化学工業株式会社 β-GLUCAN-CONTAINING BEVERAGE AND METHOD FOR PRODUCING THE SAME
JP2018102308A (en) * 2018-02-28 2018-07-05 長谷川香料株式会社 Taste improvement agent for food/beverage product

Patent Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2009142184A (en) * 2007-12-13 2009-07-02 Gun Ei Chem Ind Co Ltd beta-GLUCAN-CONTAINING BEVERAGE
JP2010063382A (en) * 2008-09-09 2010-03-25 T Hasegawa Co Ltd Method for producing plant extract
WO2013173869A1 (en) * 2012-05-23 2013-11-28 Climax Holdings Pty Limited Cereal based beverage
JP2013252113A (en) * 2012-06-08 2013-12-19 T Hasegawa Co Ltd Taste improver for cereal-containing food and beverage
JP2014027895A (en) * 2012-07-31 2014-02-13 Suntory Beverage & Food Ltd Production method of saccharified liquid of barley
JP2018042521A (en) * 2016-09-16 2018-03-22 群栄化学工業株式会社 β-GLUCAN-CONTAINING BEVERAGE AND METHOD FOR PRODUCING THE SAME
JP2017127332A (en) * 2017-05-01 2017-07-27 株式会社 伊藤園 Dietary fiber-containing grain tea beverage production process and property deterioration suppression method
JP2018102308A (en) * 2018-02-28 2018-07-05 長谷川香料株式会社 Taste improvement agent for food/beverage product

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP7105349B1 (en) * 2021-09-02 2022-07-22 アサヒ飲料株式会社 beverage
JP7134318B1 (en) 2021-09-02 2022-09-09 アサヒ飲料株式会社 beverage
JP2023036212A (en) * 2021-09-02 2023-03-14 アサヒ飲料株式会社 beverage

Also Published As

Publication number Publication date
JP6921052B2 (en) 2021-08-18

Similar Documents

Publication Publication Date Title
JP5101913B2 (en) Containerized mixed tea beverage
JP5449661B2 (en) Cereal tea drink
EP2476317B1 (en) Almond drinks and methods for their production
JP5981235B2 (en) Taste improving agent for cereal-containing foods and drinks
JP5868787B2 (en) Taste improving agent for cacao flavored food and drink
JP6921052B2 (en) Beverage manufacturing method
JP6309214B2 (en) Roasted tea beverage
JP6187572B2 (en) soda drink
JP4257323B2 (en) Azuki bean beverage and production method thereof
TW201106869A (en) Tea leaves for green tea drink extraction
JP6921051B2 (en) How to make grain tea beverages, grain tea beverages and how to adjust the bitterness of grain tea beverages
TWI735190B (en) Powdered foods containing edible plants, and food and beverages containing them
JP6921038B2 (en) How to make sterilized grain tea beverages, sterilized grain tea beverages and how to improve the taste-correlated appearance of sterilized grain tea beverages
EP1838160A1 (en) Method for making a food composition with a preservative free enhancer and a food composition
WO2015129648A1 (en) Method for manufacturing packaged coffee beverage
JP6218035B2 (en) Coffee beverage containing fine powder of roasted coffee beans and malt extract
CN108065011A (en) A kind of preparation method of concentrated coffee
JP5155093B2 (en) Containerized brown rice tea beverage
TWI679939B (en) Beverage and method for inhibiting agglomeration of beverage
CN116058413B (en) Oolong tea milk beverage and preparation method thereof
JP4038537B1 (en) Method for increasing the content of quercetin in onion skin, method for improving the taste of onion skin, fermented onion skin obtained therefrom and health food comprising the same
JP6994937B2 (en) Grain mixed tea beverage and its manufacturing method
JP2014176355A (en) Method for preparing corn tea
JP2022096085A (en) Packed barley extract-containing beverage, method for producing the beverage, and method for sweetening the beverage
JP2023034772A (en) Green beverage

Legal Events

Date Code Title Description
A621 Written request for application examination

Free format text: JAPANESE INTERMEDIATE CODE: A621

Effective date: 20201217

A871 Explanation of circumstances concerning accelerated examination

Free format text: JAPANESE INTERMEDIATE CODE: A871

Effective date: 20201217

A975 Report on accelerated examination

Free format text: JAPANESE INTERMEDIATE CODE: A971005

Effective date: 20210205

A131 Notification of reasons for refusal

Free format text: JAPANESE INTERMEDIATE CODE: A131

Effective date: 20210224

A521 Request for written amendment filed

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20210419

TRDD Decision of grant or rejection written
A01 Written decision to grant a patent or to grant a registration (utility model)

Free format text: JAPANESE INTERMEDIATE CODE: A01

Effective date: 20210629

A61 First payment of annual fees (during grant procedure)

Free format text: JAPANESE INTERMEDIATE CODE: A61

Effective date: 20210727

R150 Certificate of patent or registration of utility model

Ref document number: 6921052

Country of ref document: JP

Free format text: JAPANESE INTERMEDIATE CODE: R150