JP2019033735A - Method for manufacturing food powder - Google Patents

Method for manufacturing food powder Download PDF

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JP2019033735A
JP2019033735A JP2017164839A JP2017164839A JP2019033735A JP 2019033735 A JP2019033735 A JP 2019033735A JP 2017164839 A JP2017164839 A JP 2017164839A JP 2017164839 A JP2017164839 A JP 2017164839A JP 2019033735 A JP2019033735 A JP 2019033735A
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oil
drying
food
food powder
emulsifier
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JP6994143B2 (en
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中村 直樹
Naoki Nakamura
直樹 中村
本間 亮介
Ryosuke Honma
亮介 本間
秀樹 玉井
Hideki Tamai
秀樹 玉井
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Ikeda Shokken KK
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Abstract

To provide a food powder excellent in dryability and solubility and having good flavor and taste in a solution after dissolution without feeling powder-likeness, and a method for manufacturing the same.SOLUTION: The method for manufacturing a food powder includes drying a liquid food using an oil-in-water type emulsified material obtained by emulsifying oil-and-fat and an emulsifier solution as a drying aid. The oil-and-fat is 0.2-20 pts.wt. to 1 pts.wt. of an emulsifier; a solid content in the oil-in-water type emulsified material is 0.2-5 pts.wt. to 1 pts.wt. of a solid content in the liquid food; and the emulsifier is a water-soluble polymer compound, and the liquid food is a plant extract.SELECTED DRAWING: None

Description

本発明は、食品粉末及び該粉末の製造方法に関する。  The present invention relates to a food powder and a method for producing the powder.

液状食品の乾燥粉末化において、例えば野菜類エキスや果実類エキスといった植物エキスで、粉末化について、種々の検討がなされている。  In dry pulverization of liquid foods, various studies have been made on pulverization with plant extracts such as vegetable extracts and fruit extracts.

特許文献1には、アミロペクチンからなる澱粉類のα−アミラーゼ加水分解処理物であってDE値2〜5の冷水易溶性デキストリンを、野菜類及び/又はスパイス類水性抽出物に添加溶解したのち乾燥することを特徴とする野菜類及び/又はスパイス類水性抽出物の粉末化法が開示され、特許文献2には、香味野菜をアルコール水溶液で抽出する工程において抽出液のアルコール濃度が10〜50(W/W)%となるように抽出を行い、次工程で抽出液に粉末化基材を添加した後粉末化することを特徴とする香味野菜エキス粉末の製造法が開示されている。  Patent Document 1 discloses that an α-amylase hydrolyzed product of starch composed of amylopectin, a cold water-soluble dextrin having a DE value of 2 to 5, is added to and dissolved in vegetables and / or spices aqueous extracts and then dried. Patent Document 2 discloses a method for pulverizing vegetables and / or spices aqueous extract characterized in that, in the step of extracting flavored vegetables with an aqueous alcohol solution, the alcohol concentration of the extract is 10 to 50 ( A method for producing a flavored vegetable extract powder is disclosed, in which extraction is performed so as to be (W / W)%, and powdered base material is added to the extract in the next step and then pulverized.

しかしながら、何れの方法においても乾燥助剤としてデキストリン等の澱粉分解物を使用しているため、得られる粉末は水溶解性が低く、さらに溶解後の溶液は粉っぽさが感じられた。  However, in any of the methods, since a starch decomposition product such as dextrin is used as a drying aid, the resulting powder has low water solubility, and the solution after dissolution feels powdery.

特開昭59−205932号公報JP 59-205932 A 特許第4304622号公報Japanese Patent No. 4304622

本発明は、乾燥性が良く、溶解性に優れ、溶解後の溶液において香り及び味が良く、かつ粉っぽさが感じられない食品粉末及び該粉末の製造方法を提供するものである。  The present invention provides a food powder having good drying properties, excellent solubility, good aroma and taste in the solution after dissolution, and no powdery feeling, and a method for producing the powder.

本発明者らは、上記課題を解決するために検討した結果、油脂と乳化剤溶液とを乳化処理してなる水中油型乳化物を乾燥助剤として、液状食品を乾燥することで、溶解性に優れた食品粉末が製造できることを見出し、本発明に至った。  As a result of investigations to solve the above-mentioned problems, the present inventors have made an oil-in-water emulsion obtained by emulsifying oils and fats and an emulsifier solution as drying aids, thereby drying the liquid food to make it soluble. The present inventors have found that an excellent food powder can be produced and have reached the present invention.

すなわち、本発明は、以下の[1]〜[11]の態様に関する。
[1]油脂と乳化剤溶液とを乳化処理してなる水中油型乳化物を乾燥助剤として、液状食品を乾燥することを特徴とする、食品粉末の製造方法。
[2]乳化剤1重量部に対し油脂0.2〜20重量部を含む、[1]記載の食品粉末の製造方法。
[3]液状食品中の固形分1重量部に対し水中油型乳化物中の固形分が0.2〜5重量部である、[1]又は[2]記載の食品粉末の製造方法。
[4]乳化剤が水溶性高分子化合物である、[1]〜[3]の何れかに記載の食品粉末の製造方法。
[5]液状食品が植物エキスである、[1]〜[4]の何れかに記載の食品粉末の製造方法。
[6][1]〜[5]の何れかに記載の製造方法により得られる、食品粉末。
[7]油脂と乳化剤溶液とを乳化処理してなる水中油型乳化物由来の固形分を乾燥助剤として含む、食品粉末。
[8]乳化剤1重量部に対し油脂0.2〜20重量部を含む、[7]記載の食品粉末。
[9]食品粉末を100重量%とした場合に、水中油型乳化物の固形分を20〜80重量%含む[7]又は[8]記載の食品粉末。
[10]乳化剤が水溶性高分子化合物である、[7]〜[9]の何れかに記載の食品粉末。
[11]植物エキス由来の固形分を含む、[7]〜[10]の何れかに記載の食品粉末。
That is, the present invention relates to the following aspects [1] to [11].
[1] A method for producing a food powder, comprising drying a liquid food using an oil-in-water emulsion obtained by emulsifying an oil and fat and an emulsifier solution as a drying aid.
[2] The method for producing a food powder according to [1], comprising 0.2 to 20 parts by weight of fat / oil with respect to 1 part by weight of the emulsifier.
[3] The method for producing a food powder according to [1] or [2], wherein the solid content in the oil-in-water emulsion is 0.2 to 5 parts by weight relative to 1 part by weight of the solid content in the liquid food.
[4] The method for producing a food powder according to any one of [1] to [3], wherein the emulsifier is a water-soluble polymer compound.
[5] The method for producing a food powder according to any one of [1] to [4], wherein the liquid food is a plant extract.
[6] A food powder obtained by the production method according to any one of [1] to [5].
[7] A food powder containing, as a drying aid, a solid content derived from an oil-in-water emulsion obtained by emulsifying an oil and fat and an emulsifier solution.
[8] The food powder according to [7], comprising 0.2 to 20 parts by weight of fats and oils relative to 1 part by weight of the emulsifier.
[9] The food powder according to [7] or [8], wherein the solid content of the oil-in-water emulsion is 20 to 80% by weight when the food powder is 100% by weight.
[10] The food powder according to any one of [7] to [9], wherein the emulsifier is a water-soluble polymer compound.
[11] The food powder according to any one of [7] to [10], comprising a solid content derived from a plant extract.

本発明の食品粉末の製造方法は、乾燥性が良いため、水分の低い粉末を効率的に製造することができ、さらに、得られる粉末は水等への溶解時に溶解性に優れると共に、溶解後の溶液は香りや味が良く、持続性もあり、かつ粉っぽさが感じられない点で優れているため、力価の高い調味料として、また飲料用粉末として最適である。  The method for producing a food powder of the present invention can efficiently produce a powder with low moisture because it has good drying properties. Further, the obtained powder has excellent solubility when dissolved in water and the like, and after dissolution This solution is excellent in that it has a good aroma and taste, is durable and does not feel powdery, and is therefore suitable as a seasoning with a high potency and as a powder for beverages.

本発明の食品粉末は、油脂と乳化剤溶液とを乳化処理してなる水中油型乳化物を乾燥助剤として、液状食品を乾燥することで得られる。  The food powder of the present invention can be obtained by drying a liquid food using an oil-in-water emulsion obtained by emulsifying oil and fat and an emulsifier solution as a drying aid.

本発明の乾燥助剤は、水中油型乳化物であればよく、油脂と乳化剤溶液とを乳化処理することで得られ、液状食品の乾燥時に用いることができる。例えば、水に乳化剤を溶解した後、油脂を加えて乳化処理し、液状食品と混合してもよく、液状食品に乳化剤を溶解した後、油脂を加えて乳化処理してもよく、液状食品の添加時期は特に限定されないが、液状食品中の固形分1重量部に対し水中油型乳化物中の固形分が0.2〜5重量部が好ましく、0.3〜4重量部がより好ましく、0.5〜3重量部がさらに好ましい。液状食品中の固形分に対して水中油型乳化物中の固形分が少な過ぎると乾燥助剤として機能し難く、多過ぎると食品粉末の力価が弱くなる。なお、デキストリン、糖アルコール、乳糖等、一般的な乾燥助剤として使用され、乳化処理に利用しない物質の添加は、液状食品中の固形分1重量部に対し0.5以下が好ましく、0.3以下がより好ましく、0.2以下がさらに好ましく、含まないのが特に好ましい。  The drying aid of the present invention may be any oil-in-water emulsion, and can be obtained by emulsifying an oil and fat and an emulsifier solution, and can be used when drying a liquid food. For example, after the emulsifier is dissolved in water, it is emulsified by adding fat and oil, and may be mixed with liquid food. After the emulsifier is dissolved in the liquid food, it may be emulsified by adding fat and oil. Although the addition time is not particularly limited, the solid content in the oil-in-water emulsion is preferably 0.2 to 5 parts by weight, more preferably 0.3 to 4 parts by weight with respect to 1 part by weight of the solid content in the liquid food. 0.5-3 weight part is further more preferable. If the solid content in the oil-in-water emulsion is too small relative to the solid content in the liquid food, it will be difficult to function as a drying aid, and if too much, the titer of the food powder will be weak. The addition of substances that are used as general drying aids such as dextrin, sugar alcohol, and lactose and are not used for the emulsification treatment is preferably 0.5 or less relative to 1 part by weight of the solid content in the liquid food. 3 or less is more preferable, 0.2 or less is more preferable, and it is particularly preferable not to include it.

乳化処理は、一般的な乳化方法で行うことができ、高圧ホモジナイザー、コロイドミル、超音波乳化機、ホモミキサー、ホモディスパー等の乳化装置を例示でき、二種類以上の装置を組み合わせてもよい。また、乳化処理時に流動性があれば特に限定されないが、乳化処理前に加熱工程を含むのが好ましく、例えば40〜100℃、50〜80℃等の加熱が例示できる。  The emulsification treatment can be performed by a general emulsification method, and examples thereof include an emulsification apparatus such as a high-pressure homogenizer, a colloid mill, an ultrasonic emulsifier, a homomixer, and a homodisper, and two or more kinds of apparatuses may be combined. Moreover, it will not specifically limit if there exists fluidity at the time of an emulsification process, However, It is preferable to include a heating process before an emulsification process, for example, heating of 40-100 degreeC, 50-80 degreeC etc. can be illustrated.

乳化剤は、乳化作用を有し、本発明の水中油型乳化物が得られる化合物であれば特に限定されないが、水溶性高分子化合物が好ましく、平均分子量1000以上がより好ましく、平均分子量2000以上がさらに好ましく、例えば、大豆蛋白質等の植物性蛋白質、カゼイン等の乳蛋白質、ゼラチン等の畜肉蛋白質、卵白等の卵蛋白質、オクテニルコハク酸澱粉ナトリウムやアラビアガム等の多糖類等が例示でき、2種類以上の乳化剤を組み合わせて用いてもよい。  The emulsifier has an emulsifying action and is not particularly limited as long as it is a compound from which the oil-in-water emulsion of the present invention can be obtained, but is preferably a water-soluble polymer compound, more preferably an average molecular weight of 1000 or more, and an average molecular weight of 2000 or more. More preferred examples include vegetable proteins such as soybean protein, milk proteins such as casein, livestock meat proteins such as gelatin, egg proteins such as egg white, polysaccharides such as sodium octenyl succinate starch and gum arabic, and the like. These emulsifiers may be used in combination.

油脂は、本発明の水中油型乳化物が得られれば特に限定されず、豚脂、鶏油、牛脂、魚油、バター等の動物性油脂、大豆油、ゴマ油、落花生油、トウモロコシ油、菜種油、米油、ヤシ油、パーム油等の植物性油脂、硬化油等が例示でき、2種類以上の油を組み合わせて用いてもよい。また、予め香味素材存在下で加熱して香味油として用いてもよく、香味素材としては、油脂に香り付けできる素材であれば特に限定されないが、果実類、野菜類、種実類、肉類、魚介類、香辛料、調味料等が例示できる。水中油型乳化組成物中の油脂含量は、乳化剤1重量部に対し油脂0.2〜20重量部が好ましく、0.3〜15重量部がより好ましく、0.5〜10重量部がさらに好ましい。  Fats and oils are not particularly limited as long as the oil-in-water emulsion of the present invention is obtained, animal fats such as pork fat, chicken oil, beef tallow, fish oil, butter, soybean oil, sesame oil, peanut oil, corn oil, rapeseed oil, Examples thereof include vegetable oils such as rice oil, coconut oil, and palm oil, and hardened oil, and two or more kinds of oils may be used in combination. Moreover, it may be used in the presence of a flavoring material in advance and used as a flavoring oil. The flavoring material is not particularly limited as long as it is a material that can be scented with fats and oils, but fruits, vegetables, seeds, meats, seafood Examples include spices, spices and seasonings. The fat content in the oil-in-water emulsion composition is preferably 0.2 to 20 parts by weight, more preferably 0.3 to 15 parts by weight, and even more preferably 0.5 to 10 parts by weight with respect to 1 part by weight of the emulsifier. .

本発明では、水中油型乳化物を乾燥助剤として含む液状食品を乾燥用原液として乾燥することで食品粉末が得られる。水中油型乳化物の平均粒子径は、本発明の食品粉末が得られれば特に限定されないが、5μm以下が好ましく、3μm以下がより好ましく、2μm以下がさらに好ましい。また、乾燥用原液中の固形分は、本発明の食品粉末が得られれば特に限定されないが、5重量%以上が好ましく、10重量%以上がより好ましく、20〜50重量%がさらに好ましい。乾燥方法としては、噴霧乾燥、ドラムドライ、エアードライ、真空及び/又は凍結乾燥等から目的に応じて適宜選択できる。  In the present invention, a food powder is obtained by drying a liquid food containing an oil-in-water emulsion as a drying aid as a stock solution for drying. The average particle size of the oil-in-water emulsion is not particularly limited as long as the food powder of the present invention is obtained, but is preferably 5 μm or less, more preferably 3 μm or less, and even more preferably 2 μm or less. Further, the solid content in the drying undiluted solution is not particularly limited as long as the food powder of the present invention is obtained, but is preferably 5% by weight or more, more preferably 10% by weight or more, and further preferably 20 to 50% by weight. The drying method can be appropriately selected depending on the purpose from spray drying, drum drying, air drying, vacuum and / or freeze drying.

本発明に記載の液状食品は、特に限定されないが、例えば、野菜類、果実類等の植物エキスが例示でき、植物を搾汁、抽出等して、皮、種子等をろ過等により除去し、濃縮していてもよい。また、野菜類、果実類、豆類、穀類等の酵素処理液及び/又は発酵液、蜂蜜含有液等でもよく、単糖、二糖、有機酸、アミノ酸等、低分子物質を含み乾燥助剤なしでは乾燥困難な天然由来の液状食品が例示できる。  Although the liquid food according to the present invention is not particularly limited, for example, vegetable extracts such as vegetables and fruits can be exemplified, and the plants are squeezed and extracted, and the skin, seeds, and the like are removed by filtration or the like, It may be concentrated. In addition, enzyme treatment liquids such as vegetables, fruits, beans, cereals and / or fermentation liquids, honey-containing liquids, etc. may be used, and they contain low molecular substances such as monosaccharides, disaccharides, organic acids, amino acids, etc. Then, naturally-derived liquid foods that are difficult to dry can be exemplified.

本発明では、前記方法で、水中油型乳化物由来の固形分を乾燥助剤として含む、液状食品の乾燥品である食品粉末を製造できる。本方法は乾燥性が良く、得られる食品粉末は溶解性に優れ、溶解後の溶液は香り、味とも良く、かつ粉っぽさが感じられないという優れた効果を有する。食品粉末の水分含量は、10重量%以下が好ましく、9重量%以下がより好ましく、8重量%以下がさらに好ましい。食品粉末は、水中油型乳化物由来の固形分を含み、食品粉末を100重量%とした場合に、水中油型乳化物の固形分を20〜80重量%含むのが好ましく、30〜70重量%含むのがより好ましい。また、食品粉末は、植物エキス由来の固形分を含む植物エキス粉末であるのが好ましく、食品粉末を100重量%とした場合に、植物エキスの固形分を20〜80重量%含むのが好ましく、30〜70重量%含むのがより好ましい。  In this invention, the said method can manufacture the food powder which is a dried product of a liquid food containing the solid content derived from an oil-in-water emulsion as a drying aid. This method has good drying properties, the resulting food powder is excellent in solubility, the solution after dissolution is good in fragrance and taste, and has an excellent effect that no powderiness is felt. The water content of the food powder is preferably 10% by weight or less, more preferably 9% by weight or less, and still more preferably 8% by weight or less. The food powder contains a solid content derived from the oil-in-water emulsion, and when the food powder is 100% by weight, the solid content of the oil-in-water emulsion is preferably 20 to 80% by weight, preferably 30 to 70%. % Is more preferable. The food powder is preferably a plant extract powder containing a solid content derived from a plant extract. When the food powder is 100% by weight, the solid content of the plant extract is preferably 20 to 80% by weight, It is more preferable to contain 30 to 70% by weight.

以下、実施例を示して本発明を具体的に説明するが、本発明は以下の例によって限定されるものではない。尚、本発明において、%は別記がない限り全て重量%である。  EXAMPLES Hereinafter, although an Example is shown and this invention is demonstrated concretely, this invention is not limited by the following examples. In the present invention, all percentages are by weight unless otherwise specified.

水道水300gに、乳化剤として大豆タンパク質(フジプロ(登録商標)F、不二製油株式会社製)15g及び植物エキスとしてニンニク抽出液(ガーリックエキスAK−3393、固形分:62%、池田糖化工業株式会社製)130gを加えて80℃で加熱溶解した後、油脂として精製パーム油(不二製油株式会社製)60gを加えて混合した。次いで、高圧ホモジナイザーを用いて乳化処理(40MPa)することで、水中油型乳化組成物及びニンニク抽出液を含む乾燥用原液480gを得た。乾燥用原液のうち100gをチャンバー温度85℃の条件で噴霧乾燥することにより、ニンニクエキス粉末25g(実施品1)を得た。  300 g of tap water, 15 g of soy protein (Fujipro (registered trademark) F, manufactured by Fuji Oil Co., Ltd.) as an emulsifier and garlic extract (garlic extract AK-3393, solid content: 62%, Ikeda Saccharification Co., Ltd.) as a plant extract (Manufactured) After adding 130 g and heating and dissolving at 80 ° C., 60 g of refined palm oil (Fuji Oil Co., Ltd.) was added and mixed as an oil. Next, 480 g of a stock solution for drying containing an oil-in-water emulsion composition and a garlic extract was obtained by emulsification (40 MPa) using a high-pressure homogenizer. 100 g of the stock solution for drying was spray-dried under conditions of a chamber temperature of 85 ° C. to obtain 25 g of garlic extract powder (Example Product 1).

[比較例1−1]
乳化処理を実施しない以外は、実施例1と同様に処理し、大豆タンパク質、精製パーム油及びニンニク抽出液を含む乾燥用原液480gを得た。乾燥用原液のうち100gをチャンバー温度85℃の条件で噴霧乾燥したが、乾燥性が悪く、ニンニクエキス粉末は得られなかった。
[Comparative Example 1-1]
Except not implementing an emulsification process, it processed similarly to Example 1 and obtained 480g of undiluted | stock solutions for drying containing a soy protein, refined palm oil, and a garlic extract. 100 g of the drying stock solution was spray-dried at a chamber temperature of 85 ° C., but the drying property was poor and garlic extract powder was not obtained.

[比較例1−2]
水道水300gに、乾燥助剤として澱粉分解物(パインデックス(登録商標)#2、松谷化学工業株式会社製)75g及び植物エキスとしてニンニク抽出液(ガーリックエキスAK−3393、固形分:62%)130gを加えて80℃で加熱溶解することで、澱粉分解物及びニンニク抽出液を含む乾燥用原液480gを得た。乾燥用原液のうち100gをチャンバー温度85℃の条件で噴霧乾燥することにより、ニンニクエキス粉末25g(比較品1−2)を得た。
[Comparative Example 1-2]
300 g of tap water, 75 g of starch decomposition product (Paindex (registered trademark) # 2, Matsutani Chemical Co., Ltd.) as a drying aid and garlic extract (garlic extract AK-3393, solid content: 62%) as a plant extract 130 g was added and dissolved by heating at 80 ° C. to obtain 480 g of a drying stock solution containing a starch degradation product and a garlic extract. By spray-drying 100 g of the stock solution for drying under the condition of a chamber temperature of 85 ° C., 25 g of garlic extract powder (Comparative product 1-2) was obtained.

[比較例1−3]
乳化剤として大豆レシチン(レシオン(登録商標)P、理研ビタミン株式会社製)を使用する以外は、実施例1と同様に処理し、大豆レシチン、精製パーム油及びニンニク抽出液を含む乾燥用原液480gを得た。乾燥用原液のうち100gをチャンバー温度85℃の条件で噴霧乾燥したが、乾燥性が悪く、ニンニクエキス粉末は得られなかった。
[Comparative Example 1-3]
Except for using soybean lecithin (Recion (registered trademark) P, manufactured by Riken Vitamin Co., Ltd.) as an emulsifier, the same treatment as in Example 1 was carried out, and 480 g of a drying stock solution containing soybean lecithin, purified palm oil and garlic extract was used. Obtained. 100 g of the drying stock solution was spray-dried at a chamber temperature of 85 ° C., but the drying property was poor and garlic extract powder was not obtained.

水道水280gに、乳化剤としてオクテニルコハク酸澱粉ナトリウム(エマルスター(登録商標)500A、松谷化学工業株式会社製)45gを加えて80℃で加熱溶解した後、油脂として精製パーム油45gを加えて混合した。次いで、高圧ホモジナイザーを用いて乳化処理(40MPa)した後、植物エキスとしてトマト抽出液(トマトエキスAK−3967、固形分:45%、池田糖化工業株式会社製)135gを加えて混合するこをで、水中油型乳化組成物及びトマト抽出液を含む乾燥用原液480gを得た。乾燥用原液のうち100gをチャンバー温度80℃の条件で噴霧乾燥することにより、トマトエキス粉末20g(実施品2)を得た。  To 280 g of tap water, 45 g of sodium octenyl succinate (Emalstar (registered trademark) 500A, manufactured by Matsutani Chemical Industry Co., Ltd.) 45 g as an emulsifier was added and dissolved by heating at 80 ° C. Then, 45 g of purified palm oil was added and mixed as an oil. Next, after emulsification (40 MPa) using a high-pressure homogenizer, 135 g of tomato extract (tomato extract AK-3967, solid content: 45%, manufactured by Ikeda Saccharification Co., Ltd.) is added and mixed as a plant extract. 480 g of a stock solution for drying containing an oil-in-water emulsion composition and a tomato extract was obtained. By spray-drying 100 g of the stock solution for drying at a chamber temperature of 80 ° C., 20 g of tomato extract powder (Example product 2) was obtained.

[比較例2−1]
乳化処理を実施しない以外は、実施例2と同様に処理し、オクテニルコハク酸澱粉ナトリウム、精製パーム油及びトマト抽出液を含む乾燥用原液480gを得た。乾燥用原液のうち100gをチャンバー温度80℃の条件で噴霧乾燥したが、乾燥性が悪く、トマトエキス粉末は得られなかった。
[Comparative Example 2-1]
Except not implementing an emulsification process, it processed similarly to Example 2 and obtained 480g of undiluted | stock solutions for drying containing a sodium octenyl succinate starch, refine | purified palm oil, and a tomato extract. 100 g of the stock solution for drying was spray-dried under conditions of a chamber temperature of 80 ° C., but the drying property was poor, and tomato extract powder was not obtained.

[比較例2−2]
水道水280gに、乾燥助剤としてオクテニルコハク酸澱粉ナトリウム(エマルスター(登録商標)500A)90gを加えて80℃で加熱溶解した後、植物エキスとしてトマト抽出液(トマトエキスAK−3967、固形分:45%)135gを加えて混合することで、オクテニルコハク酸澱粉ナトリウム及びトマト抽出液を含む乾燥用原液480gを得た。乾燥用原液のうち100gをチャンバー温度80℃の条件で噴霧乾燥することにより、トマトエキス粉末20g(比較品2−2)を得た。
[Comparative Example 2-2]
After adding 90 g of starch octenyl succinate (Emalstar (registered trademark) 500A) as a drying aid to 280 g of tap water and heating and dissolving at 80 ° C., a tomato extract (tomato extract AK-3967, solid content: 45) is obtained as a plant extract. %) 135 g was added and mixed to obtain 480 g of a drying stock solution containing sodium octenyl succinate starch and tomato extract. By spray-drying 100 g of the stock solution for drying at a chamber temperature of 80 ° C., 20 g of tomato extract powder (Comparative product 2-2) was obtained.

水道水230gに、乳化剤としてオクテニルコハク酸澱粉ナトリウム(エマルスター(登録商標)500A)45gを加えて80℃で加熱溶解した後、油脂として精製パーム油45gを加えて混合した。次いで、高圧ホモジナイザーを用いて乳化処理(40MPa)した後、植物エキスとして濃縮ピーチ混濁果汁(固形分:35%、日本果実加工株式会社製)190gを加えて混合することで、水中油型乳化組成物及び濃縮ピーチ混濁果汁を含む乾燥用原液500gを得た。乾燥用原液のうち100gをチャンバー湿度80℃の条件で噴霧乾燥することにより、桃エキス粉末25g(実施品3)を得た。  After adding 45 g of starch octenyl succinate sodium (Emalstar (registered trademark) 500A) as an emulsifier to 230 g of tap water and heating and dissolving at 80 ° C., 45 g of purified palm oil was added as an oil and mixed. Next, after emulsification (40 MPa) using a high-pressure homogenizer, 190 g of concentrated peach turbid juice (solid content: 35%, manufactured by Nippon Fruit Processing Co., Ltd.) as a plant extract is added and mixed, so that an oil-in-water emulsion composition 500 g of a drying stock solution containing the product and concentrated peach turbid juice was obtained. 100 g of the stock solution for drying was spray-dried under conditions of a chamber humidity of 80 ° C. to obtain 25 g of peach extract powder (Example Product 3).

[比較例3−1]
乳化処理を実施しない以外は、実施例3と同様に処理し、オクテニルコハク酸澱粉ナトリウム、精製パーム油及び濃縮ピーチ混濁果汁を含む乾燥用原液500gを得た。乾燥用原液のうち100gをチャンバー温度80℃の条件で噴霧乾燥したが、乾燥性が悪く、桃エキス粉末は得られなかった。
[Comparative Example 3-1]
Except not implementing an emulsification process, it processed similarly to Example 3 and obtained 500 g of drying stock solutions containing a sodium octenyl succinate starch, refined palm oil, and concentrated peach turbid fruit juice. 100 g of the stock solution for drying was spray-dried at a chamber temperature of 80 ° C., but the drying property was poor and peach extract powder was not obtained.

[比較例3−2]
水道水230gに、乾燥助剤としてオクテニルコハク酸澱粉ナトリウム(エマルスター(登録商標)500A)及び澱粉分解物(パインデックス(登録商標)#2)を各45g加えて80℃で加熱溶解した後、植物エキスとして濃縮ピーチ混濁果汁(固形分:35%)190gを加えて混合することで、オクテニルコハク酸澱粉ナトリウム、澱粉分解物及び濃縮ピーチ混濁果汁を含む乾燥用原液500gを得た。乾燥用原液のうち100gをチャンバー温度80℃の条件で噴霧乾燥することにより、桃エキス粉末25g(比較品3−2)を得た。
[Comparative Example 3-2]
To 230 g of tap water, 45 g each of sodium octenyl succinate starch (Emalstar (registered trademark) 500A) and starch degradation product (Paindex (registered trademark) # 2) were added as drying aids and dissolved at 80 ° C. As a result, 190 g of concentrated peach turbid juice (solid content: 35%) was added and mixed to obtain 500 g of a drying stock solution containing sodium octenyl succinate starch, a starch degradation product and concentrated peach turbid juice. 100 g of the stock solution for drying was spray-dried at a chamber temperature of 80 ° C. to obtain 25 g of peach extract powder (Comparative product 3-2).

[評価試験]
実施例1、2及び3の乾燥用原液について、粒度分布測定装置(SALD−2200、株式会社島津製作所製)を用いて乳化粒子の平均粒子径を測定した。また、実施品1〜3、並びに比較品1−2、2−2及び3−2について、常圧加熱乾燥法(105℃、5時間)にて水分を測定した。さらに、実施品1〜3、並びに比較品1−2、2−2及び3−2について、熱湯100gに各5gを加えて溶解させる際の溶解性を評価するともに、官能評価を実施した。官能評価は、各溶液について、香りの強弱、旨味及びコク味(実施品1、比較品1−2、実施品2及び比較品2−2)又は甘味の持続性(実施品3及び比較品3−2)の強弱、並びに粉っぽさの有無を評価した。結果を表1に示す。
[Evaluation test]
About the undiluted | stock solution for drying of Examples 1, 2, and 3, the average particle diameter of the emulsion particle | grains was measured using the particle size distribution measuring apparatus (SALD-2200, Shimadzu Corporation make). Moreover, about the implementation products 1-3 and the comparison products 1-2, 2-2, and 3-2, the water | moisture content was measured with the atmospheric pressure heating drying method (105 degreeC, 5 hours). Furthermore, about the implementation products 1-3, and the comparison products 1-2, 2-2, and 3-2, while evaluating the solubility at the time of making 5 g each add to 100 g hot water and making it melt | dissolve, sensory evaluation was implemented. The sensory evaluation is as follows. For each solution, the fragrance intensity, umami and richness (practical product 1, comparative product 1-2, practical product 2 and comparative product 2-2) or sweetness persistence (practical product 3 and comparative product 3). -2), and the presence or absence of powderiness was evaluated. The results are shown in Table 1.

Figure 2019033735
Figure 2019033735

実施例1〜3の乾燥用原液中の乳化粒子は0.68〜1.39μmで、何れも2μm以下と微細で、乳化処理を行うことで、乾燥用原液中に微細な乳化物を含んでいることが分かった。一方、乳化処理を行わなかった比較例1−1、2−1及び3−1は、実施例1〜3と同じ原料であっても乾燥性が悪く食品粉末が得られなかった。植物エキスに単に乳化剤と油脂を添加するだけでは粉末が得られず、乳化処理を行って乳化物とすることで、乾燥助剤となり得ることが分かった。また、比較例1−3は乳化処理を行ったにも関わらず乾燥性が悪く食品粉末が得られなかった。乳化剤として水溶性高分子化合物を用いた乳化物が、乾燥助剤として好ましいことが分かった。  The emulsified particles in the drying undiluted solutions of Examples 1 to 3 are 0.68 to 1.39 μm, all of which are as fine as 2 μm or less, and by carrying out an emulsification treatment, the drying undiluted solution contains a fine emulsion. I found out. On the other hand, Comparative Examples 1-1, 2-1 and 3-1 which were not subjected to the emulsification treatment were poor in drying property even if they were the same raw materials as in Examples 1 to 3, and no food powder was obtained. It has been found that powders cannot be obtained simply by adding emulsifiers and fats and oils to a plant extract, and can be used as a drying aid by emulsifying them to give an emulsion. Moreover, although the comparative example 1-3 performed the emulsification process, drying property was bad and the food powder was not obtained. It was found that an emulsion using a water-soluble polymer compound as an emulsifier is preferable as a drying aid.

実施品1は比較品1−2のニンニクエキス粉末に比べ水分含量が低く、実施品2は比較品2−2のトマトエキス粉末に比べ水分含量が低く、また実施品3は比較品3−2の桃エキス粉末に比べ水分含量が低く、何れも、各比較品に比べ実施品の方が乾燥性が良好だった。さらに、各比較品に比べ実施品の方が、水への溶解性も良好だった。よって、乳化物を乾燥助剤とする方が、澱粉分解物及び/又は加工澱粉であるオクテニルコハク酸澱粉ナトリウムを乾燥助剤とするよりも、乾燥性が良く、かつ溶解性も良いことが分かった。  Practical product 1 has a lower water content than garlic extract powder of comparative product 1-2, Practical product 2 has a lower water content than tomato extract powder of comparative product 2-2, and Practical product 3 has a comparative product 3-2. The water content was lower than that of the peach extract powder, and in each case, the dried product was better in drying than the comparative products. Furthermore, compared with each comparative product, the implementation product had better solubility in water. Therefore, it was found that the use of the emulsion as a drying aid has better drying properties and better solubility than the use of sodium octenyl succinate, which is a starch degradation product and / or processed starch, as a drying aid. .

粉末溶解後の官能評価として、実施品1〜3、並びに比較品1−2、2−2及び3−2について、香りは何れも強かったが、旨味及びコク味は実施品1及び2が強く、比較品1−2及び2−2は弱く、甘味の持続性は実施品3が強く、比較品3−2は弱かった。さらに、実施品1〜3は何れも粉っぽさが無かったのに対し、比較品1−2、2−2及び3−2は何れも粉っぽかった。よって、乳化物を乾燥助剤とする方が、澱粉分解物及び/又は加工澱粉であるオクテニルコハク酸澱粉ナトリウムを乾燥助剤とするよりも、旨味やコク味が良く、甘味の持続性もあり、かつ粉っぽさが感じられないことが分かった。  As the sensory evaluation after powder dissolution, the scents were strong for the products 1 to 3 and the comparative products 1-2, 2-2 and 3-2, but the umami and rich taste were strong for the products 1 and 2. Comparative products 1-2 and 2-2 were weak, and the sustainability of sweetness was strong in execution product 3, and comparative product 3-2 was weak. Furthermore, all of the implementation products 1 to 3 were not powdery, whereas the comparison products 1-2, 2-2 and 3-2 were all powdery. Therefore, it is better to use the emulsion as a drying aid than to use octenyl succinate sodium starch, which is a starch degradation product and / or processed starch, as a drying aid, and has a good sweetness and sustaining sweetness. And it turned out that powdery feeling is not felt.

以上より、植物エキスは、粉末化において乾燥助剤を必要とし、さらに単に乳化剤と油脂を添加するだけではなく、乳化処理を行って水中油型乳化物として乾燥助剤にすることで、乾燥性が良く、さらに、得られる粉末は水等への溶解性に優れ、溶解後の溶液は香り、味とも良く、かつ粉っぽさが感じられないという優れた効果を有することが分かった。  From the above, the plant extract requires a drying aid in pulverization, and not only simply adding emulsifiers and fats but also emulsifying treatment to form a drying aid as an oil-in-water emulsion. Furthermore, it was found that the obtained powder was excellent in solubility in water and the like, and the solution after dissolution had a good scent and taste and had an excellent effect that the powderiness was not felt.

Claims (11)

油脂と乳化剤溶液とを乳化処理してなる水中油型乳化物を乾燥助剤として、液状食品を乾燥することを特徴とする、食品粉末の製造方法。  A method for producing a food powder, comprising drying a liquid food using an oil-in-water emulsion obtained by emulsifying an oil and fat and an emulsifier solution as a drying aid. 乳化剤1重量部に対し油脂0.2〜20重量部を含む、請求項1記載の食品粉末の製造方法。  The manufacturing method of the food powder of Claim 1 containing fats and oils 0.2-20 weight part with respect to 1 weight part of emulsifiers. 液状食品中の固形分1重量部に対し水中油型乳化物中の固形分が0.2〜5重量部である、請求項1又は2に記載の食品粉末の製造方法。  The manufacturing method of the food powder of Claim 1 or 2 whose solid content in an oil-in-water emulsion is 0.2-5 weight part with respect to 1 weight part of solid content in liquid food. 乳化剤が水溶性高分子化合物である、請求項1〜3の何れか1項に記載の食品粉末の製造方法。  The method for producing a food powder according to any one of claims 1 to 3, wherein the emulsifier is a water-soluble polymer compound. 液状食品が植物エキスである、請求項1〜4の何れか1項に記載の食品粉末の製造方法。  The method for producing a food powder according to any one of claims 1 to 4, wherein the liquid food is a plant extract. 請求項1〜5の何れか1項に記載の製造方法により得られる、食品粉末。  Food powder obtained by the production method according to any one of claims 1 to 5. 油脂と乳化剤溶液とを乳化処理してなる水中油型乳化物由来の固形分を乾燥助剤として含む、食品粉末。  A food powder comprising, as a drying aid, a solid content derived from an oil-in-water emulsion obtained by emulsifying an oil and fat and an emulsifier solution. 乳化剤1重量部に対し油脂0.2〜20重量部を含む、請求項7に記載の食品粉末。  The food powder according to claim 7, comprising 0.2 to 20 parts by weight of fat / oil with respect to 1 part by weight of the emulsifier. 食品粉末を100重量%とした場合に、水中油型乳化物の固形分を20〜80重量%含む、請求項7又は8に記載の食品粉末。  The food powder according to claim 7 or 8, comprising 20 to 80% by weight of a solid content of the oil-in-water emulsion when the food powder is 100% by weight. 乳化剤が水溶性高分子化合物である、請求項7〜9の何れか1項に記載の食品粉末。  The food powder according to any one of claims 7 to 9, wherein the emulsifier is a water-soluble polymer compound. 植物エキス由来の固形分を含む、請求項7〜10の何れか1項に記載の食品粉末。  The food powder according to any one of claims 7 to 10, comprising a solid content derived from a plant extract.
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JP2021052680A (en) * 2019-09-30 2021-04-08 ハウス食品株式会社 Powdery food raw material composition and method for producing the same
CN115444116A (en) * 2022-09-29 2022-12-09 海南科技职业大学 Pitaya powder rich in coconut oil and preparation method and application thereof

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JPH02242638A (en) * 1989-03-14 1990-09-27 Kanegafuchi Chem Ind Co Ltd Preparation of powdery fats and oils
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JPH02117361A (en) * 1988-10-25 1990-05-01 Kanegafuchi Chem Ind Co Ltd Fat-containing powdery spice seasoning composition and preparation thereof
JPH02207764A (en) * 1989-02-06 1990-08-17 Netsusuru Kk Preparation of powdery cream readily dispersible in cold water
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JP2021052680A (en) * 2019-09-30 2021-04-08 ハウス食品株式会社 Powdery food raw material composition and method for producing the same
CN115444116A (en) * 2022-09-29 2022-12-09 海南科技职业大学 Pitaya powder rich in coconut oil and preparation method and application thereof
CN115444116B (en) * 2022-09-29 2023-10-27 海南科技职业大学 Dragon fruit powder rich in coconut oil and preparation method and application thereof

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