JP2017070906A - Processing method of organic waste - Google Patents
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A40/00—Adaptation technologies in agriculture, forestry, livestock or agroalimentary production
- Y02A40/10—Adaptation technologies in agriculture, forestry, livestock or agroalimentary production in agriculture
- Y02A40/20—Fertilizers of biological origin, e.g. guano or fertilizers made from animal corpses
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/10—Process efficiency
- Y02P20/133—Renewable energy sources, e.g. sunlight
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02W—CLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
- Y02W30/00—Technologies for solid waste management
- Y02W30/40—Bio-organic fraction processing; Production of fertilisers from the organic fraction of waste or refuse
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02W—CLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
- Y02W30/00—Technologies for solid waste management
- Y02W30/50—Reuse, recycling or recovery technologies
- Y02W30/78—Recycling of wood or furniture waste
Abstract
Description
本発明は、例えば下水汚泥、動植物性残渣、グリストラップ等のような水分を多量に含んだ有機性廃棄物を処理するのに好適な有機性廃棄物の処理方法に関するものである。 The present invention relates to a method for treating organic waste suitable for treating organic waste containing a large amount of water, such as sewage sludge, animal and vegetable residues, grease traps, and the like.
現在、我々の社会では、例えば下水汚泥、動植物性残渣、グリストラップ等のような水分を多く含んだ有機性廃棄物が様々な場所から大量に排出されている。これらはかなりの悪臭を放つものなので、以前は防水シートで底面を遮水した貯留地に埋設して処理されていたが、防水シートの劣化・破損による地下水汚染等の危険性を考えると十分な処理方法とは言えなかった。 Currently, in our society, organic wastes containing a lot of water such as sewage sludge, animal and vegetable residues, grease traps, etc. are discharged in large quantities from various places. Since these have a rather bad odor, they were previously treated by embedding them in a storage area where the bottom surface was shielded with a waterproof sheet, but considering the dangers of groundwater contamination due to deterioration and damage of the waterproof sheet, it is sufficient. It was not a treatment method.
そこで、現在、これらの有機性廃棄物は、セメントキルンでセメントの原料とともに高熱で焼却したり、焼却炉を用いて高熱で焼却して処理されている。しかし、水分を大量に含んだ有機性廃棄物を高熱で焼却するためには大量の燃料が必要なので、燃料費が嵩み、廃棄物の処理に多大なコストがかかるという問題がある。 Therefore, at present, these organic wastes are incinerated with high temperature using a cement kiln together with raw materials of cement, or incinerated with high heat using an incinerator. However, in order to incinerate organic waste containing a large amount of water with high heat, a large amount of fuel is required, so that there is a problem that the fuel cost increases and the disposal of the waste is very expensive.
また、有機性廃棄物が発生する場所のすぐ近くに廃棄物を高熱で焼却することができるセメントキルンや焼却炉が設置されていない場合は、セメントキルンや焼却炉が設置されている場所まで廃棄物を運ばなければならず、廃棄物の輸送のために費用が更にかかるという問題がある。 If a cement kiln or incinerator that can incinerate waste with high heat is not installed in the immediate vicinity of the place where organic waste is generated, discard it to the place where the cement kiln or incinerator is installed. There is a problem that the goods must be transported and the cost of transporting the waste is higher.
そこで、本件発明者等は堆肥の中にこれらの有機性廃棄物を混合させ、廃棄物中の有機物を堆肥内の微生物に分解させて有機物を減少させ、更に、堆肥内の発酵熱で廃棄物中の水分を蒸発させることによって有機性廃棄物を減容化させる方法を考案した。この方法によれば、廃棄物の処理のために燃料費や輸送費がかからないという利点がある。 Therefore, the present inventors mixed these organic wastes in the compost, decompose the organic matter in the waste into microorganisms in the compost, reduce the organic matter, and further, waste by the fermentation heat in the compost We devised a method to reduce the volume of organic waste by evaporating the water inside. According to this method, there is an advantage that fuel costs and transportation costs are not required for the disposal of waste.
ただ、この方法を採用した場合、堆肥の中の発酵がうまく進まないと、堆肥から大量の悪臭が発生するという問題がある。しかも、堆肥は、多くの場合、周囲が開放された状態の場所に形成されているので、堆肥から発生した大量の悪臭が近隣に拡散し、近隣住民に多大な迷惑を与えるという問題がある。 However, when this method is adopted, there is a problem that a large amount of malodor is generated from the compost if the fermentation in the compost does not proceed well. In addition, since compost is often formed in a place where the surroundings are open, there is a problem in that a large amount of bad odor generated from compost diffuses in the vicinity and causes great inconvenience to neighboring residents.
本発明が解決しようとする課題は、水分を多量に含んだ有機性廃棄物を堆肥を用いて減容化させる方法において障害となる悪臭の発生を十分に防止できない点である。 The problem to be solved by the present invention is that it is not possible to sufficiently prevent the generation of malodor that becomes an obstacle in the method of reducing the volume of organic waste containing a large amount of water using compost.
本発明は、水分を多量に含んだ有機性廃棄物を減容化させるため、木質破砕物と畜糞と有機性廃棄物との組成範囲を、これらの組成を重量%で示す三角図における、該木質破砕物が30重量%、該畜糞が70重量%、該有機性廃棄物が0重量%の組成を示す第一の点Aと、該木質破砕物が55重量%、該畜糞が45重量%、該有機性廃棄物が0重量%の組成を示す第二の点Bと、該木質破砕物が50重量%、該畜糞が45重量%、該有機性廃棄物が5重量%の組成を示す第三の点Cと、該木質破砕物が40重量%、該畜糞が50重量%、該有機性廃棄物が10重量%の組成を示す第四の点Dと、該木質破砕物が25重量%、該畜糞が65重量%、該有機性廃棄物が10重量%の組成を示す第五の点Eと、該木質破砕物が25重量%、該畜糞が70重量%、該有機性廃棄物が5重量%の組成を示す第六の点Fとをこの順に結ぶ6本の直線で囲まれた範囲内にしたことを最も主要な特徴とする。 In order to reduce the volume of organic waste containing a large amount of water, the present invention shows the composition range of crushed wood, animal dung, and organic waste in the triangular diagram showing the composition in weight%. The first point A showing a composition of 30% by weight of crushed wood, 70% by weight of the animal waste, 0% by weight of organic waste, 55% by weight of the crushed wood and 45% by weight of the animal waste The second point B in which the organic waste has a composition of 0% by weight, the wooden crushed material has a composition of 50% by weight, the animal manure has a composition of 45% by weight, and the organic waste has a composition of 5% by weight. A third point C, a fourth point D having a composition of 40% by weight of the crushed wood, 50% by weight of the animal waste and 10% by weight of the organic waste, and 25% of the crushed wood %, The fifth point E showing a composition of 65% by weight of the animal waste and 10% by weight of the organic waste, 25% by weight of the crushed wood, 0 wt%, and most main feature that it has within a range surrounded with the F sixth point showing the composition organic waste is 5% by weight six straight lines connecting in this order.
ここで、木質破砕物と畜糞と有機性廃棄物との組成範囲は、これらの組成を重量%で示す三角図における、該木質破砕物が35重量%、該畜糞が65重量%、該有機性廃棄物が0重量%の組成を示す第七の点Gと、該木質破砕物が35重量%、該畜糞が60重量%、該有機性廃棄物が5重量%の組成を示す第八の点Hと、該木質破砕物が40重量%、該畜糞が55重量%、該有機性廃棄物が5重量%の組成を示す第九の点Iと、該木質破砕物が45重量%、該畜糞が55重量%、該有機性廃棄物が0重量%の組成を示す第十の点Jとをこの順に結ぶ4本の直線で囲まれた範囲内にあれば、更に好ましい。 Here, the composition range of the crushed wood, livestock excrement and organic waste is as follows: the crushed wood is 35% by weight, the livestock feces is 65% by weight, and the organic A seventh point G indicating that the waste has a composition of 0% by weight; an eighth point indicating that the crushed wood is 35% by weight; the animal manure is 60% by weight; and the organic waste is 5% by weight. A ninth point I having a composition of H, 40% by weight of the crushed wood, 55% by weight of the animal waste, and 5% by weight of the organic waste; 45% by weight of the crushed wood, Is more preferably within a range surrounded by four straight lines connecting the tenth point J having a composition of 55% by weight and the organic waste having a composition of 0% by weight in this order.
なお、前記堆肥中の水分は50〜60重量%の範囲が好ましい。該堆肥中の水分が40重量%未満の場合は発酵が進まず、該堆肥中の水分が65重量%を越えると悪臭を発生するようになるが、該堆肥中の水分が50〜60重量%の範囲の場合は発酵が進むとともに、悪臭の発生が無いからである。 The water content in the compost is preferably in the range of 50 to 60% by weight. When the water content in the compost is less than 40% by weight, the fermentation does not proceed, and when the water content in the compost exceeds 65% by weight, a bad odor is generated, but the water content in the compost is 50-60% by weight. In the case of this range, it is because fermentation progresses and no bad odor is generated.
また、前記堆肥を形成している木質破砕物とは、剪定枝、木材粉、その他樹木由来の木くずをいう。また、畜糞とは、牛糞、鶏糞、豚糞又はこれらの糞から選択された1種又は2種以上をいう。また、有機性廃棄物とは、下水処理場の有機汚泥、グリストラップ、レストラン等の排水溝の清掃汚泥、食品工場やレストラン等から排出される動植物性残渣、家庭から排出される厨芥(生ごみ)その他、有機物を主体とする廃棄物をいう。 Further, the crushed wood forming the compost means pruned branches, wood powder, and other wood waste derived from trees. Moreover, livestock dung means 1 type, or 2 or more types selected from cow dung, chicken dung, pig dung, or these dung. Organic waste includes organic sludge from sewage treatment plants, grease traps, cleaning sludge from drains in restaurants, etc., animal and vegetable residues discharged from food factories and restaurants, etc. ) Others are wastes mainly composed of organic matter.
また、堆肥には廃食用油を添加してもよい。廃食用油とは、主として業務用に使用された天ぷら油、フライ油、揚げ物油をいう。廃食用油の添加量は堆肥の重量の5〜10重量%の範囲が好ましい。また、前記堆肥には窒素、リン酸又はカリを含むものを添加してこれらの成分を増加させてもよい。 In addition, waste cooking oil may be added to the compost. Waste cooking oil means tempura oil, frying oil, and deep-fried oil used mainly for business purposes. The amount of waste cooking oil added is preferably in the range of 5 to 10% by weight of the compost. Moreover, you may increase those components by adding what contains nitrogen, phosphoric acid, or potash to the compost.
前記堆肥は所定の期間毎に切り返して該堆肥内に空気を入れ、該堆肥内の好気性細菌の増殖を良好ならしめてもよい。前記堆肥にはBacillus属、Streptomyces属、Thermus thermophilusなどの好熱菌、Aspergillosis属などの糸状菌から選択された1種又は2種以上の微生物を添加・増殖させてもよい。 The compost may be cut back at predetermined intervals and air may be introduced into the compost to improve the growth of aerobic bacteria in the compost. One or more microorganisms selected from thermophilic bacteria such as Bacillus genus, Streptomyces genus, Thermus thermophilus, and filamentous fungi such as Aspergillosis genus may be added to and grown in the compost.
本発明の有機性廃棄物の処理方法は、水分を多量に含んだ有機性廃棄物を混合させた堆肥を良好な条件で発酵させることができるので、堆肥からの悪臭の発生を抑制し、近隣に悪臭による迷惑をかけないで済むという利点がある。 Since the organic waste processing method of the present invention can ferment compost mixed with organic waste containing a large amount of moisture under good conditions, the generation of malodor from the compost is suppressed, and the neighborhood There is an advantage that it does not cause trouble due to bad smell.
また、本発明の有機性廃棄物の処理方法は、水分を多量に含んだ有機性廃棄物を混合させた堆肥を良好な条件で発酵させることができるので、水分を多量に含んだ有機性廃棄物を効率良く減容化させることができるという利点がある。 Further, the organic waste treatment method of the present invention can ferment compost mixed with organic waste containing a large amount of moisture under good conditions, so that organic waste containing a large amount of moisture There is an advantage that the volume can be reduced efficiently.
また、本発明の有機性廃棄物の処理方法は、前記堆肥中の水分を50〜60重量%の範囲とした場合、堆肥の発酵を更に促進させ、減水率を更に上昇させることができるので、水分を多量に含んだ有機性廃棄物を、悪臭を発生させることなく、更に効率良く減容化させることができるという利点がある。 In addition, the organic waste processing method of the present invention can further promote the fermentation of the compost and can further increase the water reduction rate when the water content in the compost is in the range of 50 to 60% by weight. There is an advantage that the organic waste containing a large amount of moisture can be more efficiently reduced in volume without generating malodor.
本発明の有機性廃棄物の処理方法は、堆肥に廃食用油を5〜10重量%の範囲で添加すると、堆肥の発酵を更に促進させ、減水率を更に上昇させることができるので、水分を多量に含んだ有機性廃棄物を、悪臭を発生させることなく、更に効率良く減容化させることができるという利点がある。 In the method for treating organic waste according to the present invention, when waste edible oil is added to the compost in the range of 5 to 10% by weight, the fermentation of the compost can be further promoted and the water reduction rate can be further increased. There is an advantage that the organic waste containing a large amount can be more efficiently reduced in volume without generating a bad odor.
堆肥を使用した有機性廃棄物の処理方法において、有機性廃棄物中の有機物を速やかに分解・消化させ、有機性廃棄物中の水分を速やかに蒸発させ、かつ悪臭をできるだけ発生させないという目的を、簡単な方法で、有機性廃棄物の減容化の効率を低下させることなく実現した。 In the organic waste treatment method using compost, the purpose is to quickly decompose and digest the organic matter in the organic waste, to quickly evaporate the water in the organic waste, and to prevent the generation of malodors as much as possible. This was achieved in a simple way without reducing the efficiency of organic waste volume reduction.
図1は本発明の一実施例に係る有機性廃棄物の処理方法の基本的な工程を示す工程図である。以下、この工程図を参照しながら実施例1について説明する。 FIG. 1 is a process diagram showing basic steps of a method for treating organic waste according to an embodiment of the present invention. Hereinafter, Example 1 will be described with reference to this process chart.
防水処理を施したコンクリート舗装の上に木質破砕物と畜糞を交互に撒いて、木質破砕物と畜糞からなる、高さ1.8m、幅2.5m、長さ40mの堆積を形成した。ここで、木質破砕物としては剪定枝を使用し、畜糞としては牛糞を使用した。木質破砕物と畜糞の割合(wt%)は表1に示す通りとした。
次に、この堆積を、攪拌機械で時々切り返しながら、15日間発酵させた。堆積を形成してから15日後、堆積の中の温度を測定したところ、85℃であった。また、堆積を形成している木質破砕物と畜糞を観察してみたところ、木質破砕物と畜糞が減容し堆肥(コンポスト)の状態になっていた。 The deposit was then fermented for 15 days with occasional turning on a stirrer. 15 days after the formation of the deposit, the temperature in the deposit was measured and found to be 85 ° C. In addition, when observing the crushed wood and animal dung forming the sediment, the crushed wood and animal dung were reduced in volume and composted.
次に、この堆積の上に有機性廃棄物を撒き、この有機性廃棄物を撒いた堆積を攪拌機械で切り返して堆肥と有機性廃棄物を良く混合した。ここで、有機性廃棄物としては下水汚泥を使用した。また、この時の木質破砕物と畜糞と下水汚泥の割合は前記の表1に示す通りであり、堆積の水分含有率(wt%)を調べたところ、堆積の水分含有率(wt%)は表2に示す通りであった。
次に、この堆積を攪拌機械で切り返しながら24時間発酵させ、この堆積から出る臭いの状況について調べたところ前記の表1に示す通りであった。 Next, this deposit was fermented for 24 hours while turning back with a stirrer, and the state of odor coming out of this deposit was examined.
表1の結果を基に、悪臭が許容できる範囲と悪臭が許容できない範囲を、木質破砕物と畜糞と有機性廃棄物との組成を重量%で示す三角図(図2)に示したところ、該木質破砕物が30重量%、該畜糞が70重量%、該有機性廃棄物が0重量%の組成を示す第一の点Aと、該木質破砕物が55重量%、該畜糞が45重量%、該有機性廃棄物が0重量%の組成を示す第二の点Bと、該木質破砕物が50重量%、該畜糞が45重量%、該有機性廃棄物が5重量%の組成を示す第三の点Cと、該木質破砕物が40重量%、該畜糞が50重量%、該有機性廃棄物が10重量%の組成を示す第四の点Dと、該木質破砕物が25重量%、該畜糞が65重量%、該有機性廃棄物が10重量%の組成を示す第五の点Eと、該木質破砕物が25重量%、該畜糞が70重量%、該有機性廃棄物が5重量%の組成を示す第六の点Fとをこの順に結ぶ6本の直線で囲まれた範囲内の臭気は許容できる程度であったが、この範囲外の臭気は許容できない程度であった。
Based on the results of Table 1, the range in which malodors can be tolerated and the range in which malodors are unacceptable is shown in a triangular diagram (FIG. 2) showing the composition of crushed wood, animal manure and organic waste in weight%. The first point A showing a composition of 30% by weight of the crushed wood, 70% by weight of the animal waste and 0% by weight of the organic waste, 55% by weight of the crushed wood and 45% of the animal waste The second point B, in which the organic waste has a composition of 0% by weight, the crushed wood, 50% by weight, the
また、表1の結果を基に、悪臭が気にならない範囲と悪臭が許容できる範囲を、木質破砕物と畜糞と有機性廃棄物との組成を重量%で示す三角図(図2)に示したところ、該木質破砕物が35重量%、該畜糞が65重量%、該有機性廃棄物が0重量%の組成を示す第七の点Gと、該木質破砕物が35重量%、該畜糞が60重量%、該有機性廃棄物が5重量%の組成を示す第八の点Hと、該木質破砕物が40重量%、該畜糞が55重量%、該有機性廃棄物が5重量%の組成を示す第九の点Iと、該木質破砕物が45重量%、該畜糞が55重量%、該有機性廃棄物が0重量%の組成を示す第十の点Jとをこの順に結ぶ4本の直線で囲まれた範囲内の臭気は気にならない程度であった。 Moreover, based on the results in Table 1, the range in which malodors are not worrisome and the range in which malodors are acceptable is shown in a triangular diagram (Fig. 2) showing the composition of crushed wood, animal manure and organic waste in weight percent. As a result, a seventh point G having a composition of 35% by weight of the crushed wood, 65% by weight of the animal waste and 0% by weight of the organic waste, 35% by weight of the crushed wood, 8th point H showing a composition of 60% by weight of the organic waste and 5% by weight of the organic waste, 40% by weight of the crushed wood, 55% by weight of the animal waste, and 5% by weight of the organic waste Ninth point I indicating the composition of the above and the tenth point J indicating the composition of 45% by weight of the crushed wood, 55% by weight of the animal manure, and 0% by weight of the organic waste are connected in this order. The odor within the range surrounded by the four straight lines was of no concern.
実施例1の試料番号19の条件で、堆肥中の水分を30〜80重量%の範囲で変化させて含まれている水分の減少率、すなわち減水率(wt%/day)を求めたところ、表3に示す通りの結果が得られた。
表3をグラフにしたところ図3に示す通りとなった。表3及び図3に示す通り、堆肥中の水分が40重量%未満の場合は減水率が低くて、発酵が進まず、該堆肥中の水分が65重量%を越えた場合は減水率が低くて、悪臭を発生していたが、該堆肥中の水分が50〜60重量%の範囲の場合は減水率が高くて、発酵が良好に進み、悪臭の発生も無かった。 When Table 3 was graphed, it was as shown in FIG. As shown in Table 3 and FIG. 3, when the water content in the compost is less than 40% by weight, the water reduction rate is low, the fermentation does not proceed, and when the water content in the compost exceeds 65% by weight, the water reduction rate is low. Although malodor was generated, when the water content in the compost was in the range of 50 to 60% by weight, the water reduction rate was high, the fermentation proceeded well, and no malodor was generated.
実施例1の試料番号17の条件で、廃食油を1〜50重量%の範囲で添加させて発酵の状況と減水率(wt%/day)を観察したところ、表4に示す通りの結果が得られた。
表4をグラフにしたところ図4に示す通りとなった。表4及び図4に示す通り、堆肥中に廃食油を添加すると発酵が進み、減水率が上昇し出し、堆肥中の廃食油が5〜10重量%の範囲では発酵が著しくなり、減水率が高くなるが、堆肥中の廃食油が40重量%を越えると発酵が進まなくなり、減水率が低下することがわかる。 When Table 4 was graphed, it was as shown in FIG. As shown in Table 4 and FIG. 4, when waste edible oil is added to compost, fermentation proceeds, the water reduction rate starts to increase, and in the range of 5 to 10% by weight of waste edible oil in compost, fermentation becomes significant and the water reduction rate is low. Although it becomes high, when waste cooking oil in compost exceeds 40 weight%, it turns out that fermentation stops and water reduction rate falls.
実施例1の試料番号19の堆肥、すなわち、悪臭の発生がなく、極めて良好に発酵している堆肥を採取し、堆肥中の微生物を、定法を用いて分離・培養し、微生物を同定したところ、Thermus thermophilus、Bacillus subtilis、Bacillus thermoamylovorans、Bacillus licheniformisが見出された。 Composting sample No. 19 of Example 1, ie, compost fertilizing without any foul odor and being excellently fermented, microorganisms in the compost were separated and cultured using a conventional method, and the microorganisms were identified Thermus thermophilus, Bacillus subtilis, Bacillus thermoamylovorans, Bacillus licheniformis were found.
畜糞として鶏糞、豚糞、牛糞+鶏糞、牛糞+豚糞、鶏糞+豚糞、牛糞+鶏糞+豚糞を使用し、実施例1と同様の条件で実験をしたところ、臭い、減容化について、実施例1と同様の結果が得られた。 Using chicken feces, pig feces, cow feces + chicken feces, cow feces + pig feces, chicken feces + pig feces, cattle feces + chicken feces + pig feces as animal feces, the experiment was conducted under the same conditions as in Example 1. The same results as in Example 1 were obtained.
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