JP2017000125A - Milk flavor improver - Google Patents
Milk flavor improver Download PDFInfo
- Publication number
- JP2017000125A JP2017000125A JP2015120912A JP2015120912A JP2017000125A JP 2017000125 A JP2017000125 A JP 2017000125A JP 2015120912 A JP2015120912 A JP 2015120912A JP 2015120912 A JP2015120912 A JP 2015120912A JP 2017000125 A JP2017000125 A JP 2017000125A
- Authority
- JP
- Japan
- Prior art keywords
- milk
- flavor
- milk flavor
- flavor improving
- product
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
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Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23C—DAIRY PRODUCTS, e.g. MILK, BUTTER OR CHEESE; MILK OR CHEESE SUBSTITUTES; MAKING THEREOF
- A23C9/00—Milk preparations; Milk powder or milk powder preparations
- A23C9/152—Milk preparations; Milk powder or milk powder preparations containing additives
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/38—Other non-alcoholic beverages
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L27/00—Spices; Flavouring agents or condiments; Artificial sweetening agents; Table salts; Dietetic salt substitutes; Preparation or treatment thereof
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L27/00—Spices; Flavouring agents or condiments; Artificial sweetening agents; Table salts; Dietetic salt substitutes; Preparation or treatment thereof
- A23L27/20—Synthetic spices, flavouring agents or condiments
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L9/00—Puddings; Cream substitutes; Preparation or treatment thereof
- A23L9/10—Puddings; Dry powder puddings
Abstract
Description
本発明は、含硫アミノ酸、または含硫アミノ酸を含有する組成物を有効成分とする乳風味改善剤、特に、乳性飲食品に牛乳様のフレッシュな風味を付与する、含硫アミノ酸を有効成分とする乳風味改善剤に関する。 The present invention relates to a milk flavor improving agent comprising a sulfur-containing amino acid or a composition containing a sulfur-containing amino acid as an active ingredient, particularly a sulfur-containing amino acid that imparts a milk-like fresh flavor to a milky food or drink. It relates to a milk flavor improving agent.
近年、消費者の食生活の多様化にともない飲食品についても多様性が求められており、多くの商品群が開発されている。その中でも、牛乳、加工乳、乳飲料、乳酸菌飲料、乳配合飲料、バター、チーズ、ヨーグルト、アイスクリームなどの乳性飲食品は、元来牛乳等が有する種々の栄養素の観点から、健康志向の飲食品として有望視されており、現在、数多くの品目が上市されている。 In recent years, with the diversification of consumer eating habits, diversity has also been demanded for food and drink products, and many product groups have been developed. Among them, dairy foods and beverages such as milk, processed milk, milk beverages, lactic acid bacteria beverages, milk blended beverages, butter, cheese, yogurt, and ice cream are health-oriented from the viewpoint of the various nutrients that milk originally has. It is considered promising as a food and drink, and many items are currently on the market.
しかしながら、牛乳や乳製品の価格高騰や需給逼迫に加え、消費者の健康志向による低脂肪タイプのニーズ拡大により、乳性飲食品に使用する牛乳や乳製品の使用量を減らすことが多くなっている。 However, in addition to rising prices of milk and dairy products and tight supply and demand, the use of low-fat types due to consumer health has led to a reduction in the amount of milk and dairy products used in dairy foods and drinks. Yes.
牛乳や乳製品の使用量を減らすことにより、それらの乳性飲食品では乳脂感やコク味等の牛乳の風味が不足することとなる。従来、この風味不足を補うため、乳製品の酵素処理、微生物発酵した脂肪酸、アミノ酸、ペプチドを有効成分とする呈味素材、およびアミノ酸、ペプチド、核酸を有効成分とする酵母エキスが使用されていた。 By reducing the amount of milk and dairy products used, those milk-based foods and drinks lack milk flavor and a rich flavor of milk. Conventionally, in order to make up for this lack of flavor, dairy enzyme treatment, microbial fermented fatty acids, amino acids, and taste ingredients containing peptides as active ingredients, and yeast extracts containing amino acids, peptides and nucleic acids as active ingredients have been used. .
例えば、乳脂肪含有食品材料をペニシリウム・クリソゲヌムに属する微生物の産生するリパーゼの存在下に、酵素反応させることにより、持続性乳製品フレ−バ−を製造する方法(特許文献1)、乳または乳加工品をリパーゼの存在下に酵素反応させて得られる酵素分解物および乳または乳加工品を香気回収手段に供して得られる回収香から乳製品フレーバーを製造する方法(特許文献2)、原料ミックスに、アミノ酸及び酸を添加することにより発酵乳と同様の風味を有する無発酵食品が得られる方法(特許文献3)、食用植物油脂と酵母エキス粉末の混合物を粉末状態で加熱して調製されるミート様フレーバーを有する粉末調味料と酵母エキスを配合したことによる、チーズ風味及び/又は乳感を増強する方法(特許文献4)、5’−グアニル酸ナトリウムを3重量%以上、酵母エキス中の全アミノ酸に対するペプチドの割合が90重量%以上含有する酵母エキスと脱脂粉乳及び/又は脱脂乳を水に溶解後、乾燥して得られる低脂肪又は無脂肪の乳製品用調味料(特許文献5)などが挙げられる。 For example, a method for producing a sustained dairy flavor by reacting a milk fat-containing food material with an enzyme reaction in the presence of a lipase produced by a microorganism belonging to Penicillium chrysogenum (Patent Document 1), milk or milk A method for producing a dairy flavor from an enzyme degradation product obtained by subjecting a processed product to an enzyme reaction in the presence of lipase and a recovered flavor obtained by subjecting milk or a processed milk product to aroma recovery means (Patent Document 2), a raw material mix In addition, an amino acid and an acid are added to obtain a non-fermented food having the same flavor as fermented milk (Patent Document 3), and a mixture of edible vegetable oil and yeast extract powder is heated in a powder state. Method of enhancing cheese flavor and / or milky feeling by blending powdery seasoning having meat-like flavor and yeast extract (Patent Document 4), 5'-g Low fat obtained by dissolving 3% by weight or more of sodium nilate and 90% by weight or more of the peptide with respect to all amino acids in the yeast extract and skim milk powder and / or skim milk dissolved in water and drying Non-fat dairy seasonings (Patent Document 5) and the like.
しなしながら、それらの提案は不足する乳脂感やコク味等の呈味の風味増強に関するものである。一方で、日本で広く普及した超高温加熱処理法(以下UHTと記す)殺菌牛乳が消費者に牛乳として認知されているが、製造直後のUHT殺菌牛乳の持つ特有の牛乳感を連想させるフレッシュな風味を再現させる提案はこれまでされていない。 However, these proposals are related to a flavor enhancement such as lack of milk fat feeling and rich taste. On the other hand, ultra-high temperature heat treatment method (hereinafter referred to as UHT) pasteurized milk widely used in Japan is recognized as milk by consumers, but it is a fresh reminiscent of the unique milk feeling of UHT pasteurized milk immediately after manufacture. No proposal has been made to reproduce the flavor.
本発明の目的は、乳性飲食品に添加することにより、牛乳をUHT殺菌することで生成する、牛乳様のフレッシュな風味を想起させる乳性飲食品を得ることができる乳風味改善剤を提供することにある。 The object of the present invention is to provide a milk flavor improving agent capable of obtaining a milk-like food and drink reminiscent of a milk-like fresh flavor, which is produced by UHT sterilization of milk by being added to the milk-related food and drink. There is to do.
本発明者らは、前述の課題を解決するために鋭意検討した結果、乳性飲食品に含硫アミノ酸、または含硫アミノ酸を含有する組成物を添加することにより、牛乳をUHT殺菌することで生成する、牛乳様のフレッシュな風味を想起させ、乳風味を改善させることを見出し本発明の完成に至った。 As a result of intensive studies to solve the above-mentioned problems, the present inventors have made UHT pasteurization of milk by adding a sulfur-containing amino acid or a composition containing a sulfur-containing amino acid to a milky food or drink. The present inventors have found a milk-like fresh flavor to be produced and found that the milk flavor is improved, and the present invention has been completed.
本発明は、以下の乳風味改善剤および乳風味改善組成物を提供することができる。
(1)含硫アミノ酸を有効成分とする乳性飲食品の乳風味改善剤。
(2)含硫アミノ酸がメチオニン、システイン、シスチンまたはグルタチオンからなる群から選択される1種または2種以上である、(1)の乳風味改善剤。
(3)(1)または(2)の含硫アミノ酸を0.01質量%〜30質量%含有する、乳風味改善剤。
(4)(3)の乳風味改善剤が酵母エキスである、乳風味改善剤。
(5)(3)または(4)の乳風味改善剤を含有する乳風味改善組成物。
(6)さらに乳風味フレーバーを含有する(5)の乳風味改善組成物。
(7)加熱されたものである、(5)または(6)の乳風味改善組成物。
(8)(5)〜(7)いずれかの乳風味改善組成物を含有する乳性飲食品。
(9)(5)〜(7)いずれかの乳風味改善組成物を、乳性飲食品に対して0.1ppm〜2.0質量%添加する、乳性飲食品の乳風味改善方法。
(10)(3)または(4)の乳風味改善剤を乳風味フレーバーに添加後、加熱する乳風味改善組成物の製造方法。
(11)(5)〜(7)いずれかの乳風味改善組成物を乳性飲食品に添加後、加熱する乳性飲食品の製造方法。
The present invention can provide the following milk flavor improving agent and milk flavor improving composition.
(1) A milk flavor improving agent for dairy foods and drinks containing a sulfur-containing amino acid as an active ingredient.
(2) The milk flavor improving agent according to (1), wherein the sulfur-containing amino acid is one or more selected from the group consisting of methionine, cysteine, cystine or glutathione.
(3) A milk flavor improving agent containing 0.01% by mass to 30% by mass of the sulfur-containing amino acid of (1) or (2).
(4) The milk flavor improving agent whose milk flavor improving agent of (3) is a yeast extract.
(5) A milk flavor improving composition containing the milk flavor improving agent of (3) or (4).
(6) The milk flavor improving composition according to (5), further comprising a milk flavor flavor.
(7) The milk flavor improving composition according to (5) or (6), which is heated.
(8) A milky food or drink containing the milk flavor improving composition according to any one of (5) to (7).
(9) The milk flavor improvement method of milky food / beverage products which adds the milk flavor improvement composition in any one of (5)-(7) 0.1 ppm-2.0 mass% with respect to milky food / beverage products.
(10) A method for producing a milk flavor improving composition, wherein the milk flavor improving agent according to (3) or (4) is added to a milk flavor flavor and then heated.
(11) A method for producing a milky food or drink, wherein the milk flavor improving composition according to any one of (5) to (7) is added to the milky food or drink and then heated.
本発明の含硫アミノ酸を有効成分とする乳風味改善剤は、それ自体またはそれを含有する組成物を乳性飲食品に添加することにより、牛乳をUHT殺菌することで生成する、牛乳様のフレッシュな風味を想起させ、乳風味を改善することができる。 The milk flavor improving agent containing the sulfur-containing amino acid of the present invention as an active ingredient is produced by adding UHT sterilization of milk by adding the composition containing the same to the milky food or drink. Reminiscent of a fresh flavor and can improve milk flavor.
以下、本発明の牛乳様のフレッシュな風味を想起させ、乳風味を改善させる効果を有する乳風味改善剤についてさらに詳細に説明する。 Hereinafter, the milk flavor improving agent having the effect of improving the milk flavor will be described in more detail by recalling the milk-like fresh flavor of the present invention.
本発明で使用される含硫アミノ酸とは、含硫化合物であって、アミノ基とカルボキシル基の両方の官能基を有し、アミノ基がカルボキシル基のα位に結合している化合物であれば、特に限定されず、ジペプチド、トリペプチド等のペプチド化合物であっても良い。例えば、メチオニン、システイン、シスチンまたはグルタチオンを挙げることができる。 The sulfur-containing amino acid used in the present invention is a sulfur-containing compound, as long as it has a functional group of both an amino group and a carboxyl group, and the amino group is bonded to the α-position of the carboxyl group. However, it is not particularly limited, and peptide compounds such as dipeptides and tripeptides may be used. For example, methionine, cysteine, cystine or glutathione can be mentioned.
本発明で使用される酵母エキスとは、前記含硫アミノ酸を含有する酵母エキスであれば特に限定されず、前記含硫アミノ酸が高含有である酵母エキスであることが好ましい。例えば、システインペプチド含有酵母エキスなどが挙げられ、ハイチオンエキス(登録商標)YH、アロマイルド(登録商標)U(以上興人ライフサイエンス社製)、グルタイーストエキスN、グルタイーストエキスDN(以上協和発酵バイオ社製)、イーストパウダーHG(オリエンタル酵母工業社製)、スプリンガー4101/0−PW−L(バイオスプリンガー社製)などを挙げることができる。 The yeast extract used in the present invention is not particularly limited as long as it is a yeast extract containing the sulfur-containing amino acid, and is preferably a yeast extract containing a high content of the sulfur-containing amino acid. Examples include cysteine peptide-containing yeast extract, and the like. Hythion extract (registered trademark) YH, Alomiled (registered trademark) U (manufactured by Kojin Life Science Co., Ltd.), Gluta yeast extract N, Gluta yeast extract DN (Kyowa) Fermentation Bio), yeast powder HG (Oriental Yeast Co., Ltd.), Springer 4101 / 0-PW-L (BioSpringer) and the like.
本発明で使用される含硫アミノ酸の酵母エキスなどに含有される量は0.01質量%〜30質量%、好ましくは0.1質量%〜25質量%、より好ましくは1質量%〜20質量%を挙げることができる。含硫アミノ酸の含有量はなるべく高含量であることが好ましい。 The amount contained in the yeast extract of sulfur-containing amino acids used in the present invention is 0.01% by mass to 30% by mass, preferably 0.1% by mass to 25% by mass, more preferably 1% by mass to 20% by mass. %. The sulfur-containing amino acid content is preferably as high as possible.
本発明の乳性飲食品とは、牛乳、乳、加工乳、乳飲料、乳酸菌飲料、乳配合飲料などの飲食品であり、乳が配合された飲食品を示す。乳性飲食品の例としては、牛乳、山羊乳などの生乳、脱脂粉乳、全脂粉乳、調整粉乳、濃縮乳などの加工乳、生クリーム、アイスクリーム、バター、チーズ、ヨーグルト、クリームパウダー、粉末たんぱく飲料、発酵乳、乳酸菌飲料などの乳由来製品、ホワイトソース、ミルクプリン、クリームスープ、粉末たんぱく食品などの食品を挙げることができる。 The dairy food / beverage products of the present invention are food / beverage products such as cow's milk, milk, processed milk, milk beverages, lactic acid bacteria beverages and milk-containing beverages, and refer to foods / beverage products containing milk. Examples of dairy foods and drinks include raw milk such as cow's milk and goat milk, skim milk powder, whole milk powder, modified milk powder, processed milk such as concentrated milk, fresh cream, ice cream, butter, cheese, yogurt, cream powder, powder Examples include milk-derived products such as protein beverages, fermented milk, and lactic acid bacteria beverages, and foods such as white sauce, milk pudding, cream soup, and powdered protein foods.
本発明の乳風味改善剤を乳性飲食品に添加し、その後加熱することにより、乳性飲食品の乳風味を改善することができる。特に、乳性飲食品に、牛乳をUHT殺菌することで生成する、牛乳様のフレッシュな風味を想起させることができる。 By adding the milk flavor improving agent of this invention to milky food / beverage products, and heating after that, the milk flavor of milky food / beverage products can be improved. In particular, milk-like food and drink can be recalled with a milk-like fresh flavor produced by UHT sterilization of milk.
本発明の乳風味改善剤の乳性飲食品に対する添加量は、0.1ppm〜2.0質量%、好ましくは1ppm〜0.5質量%、さらに好ましくは10ppm〜0.1質量%を挙げることができる。添加量が0.1ppmより少ないと、乳性飲食品の乳風味が改善されず、また、添加量が2.0質量%より多いと、乳風味改善剤を乳性飲食品に添加後加熱した際に、不快な硫黄臭を生じさせることになってしまう。 The addition amount of the milk flavor improving agent of the present invention to the dairy food or drink is 0.1 ppm to 2.0% by mass, preferably 1 ppm to 0.5% by mass, and more preferably 10 ppm to 0.1% by mass. Can do. When the addition amount is less than 0.1 ppm, the milk flavor of the milky food or drink is not improved. When the addition amount is more than 2.0% by mass, the milk flavor improving agent is added to the milky food or drink and then heated. In that case, an unpleasant sulfur odor will be generated.
前記に示すように、本発明の乳風味改善剤をそのまま乳性飲食品に添加することも可能であるが、乳風味改善剤を乳風味フレーバーに添加した乳風味改善組成物を乳性飲食品に添加することもできるし、乳風味改善剤と乳風味フレーバーを乳性飲食品に別々に添加することもできる。本発明の乳風味改善組成物の乳性飲食品に対する添加量は、0.1ppm〜2.0質量%、好ましくは1ppm〜1.0質量%、さらに好ましくは5ppm〜0.2質量%、より好ましくは10ppm〜0.1質量%を挙げることができる。 As described above, it is possible to add the milk flavor improving agent of the present invention to the milky food or drink as it is, but the milk flavor improving composition obtained by adding the milk flavor improving agent to the milk flavor flavor is used as the milky food or drink. The milk flavor improving agent and the milk flavor flavor can be added separately to the dairy food or drink. The added amount of the milk flavor improving composition of the present invention to the dairy food or drink is 0.1 ppm to 2.0 mass%, preferably 1 ppm to 1.0 mass%, more preferably 5 ppm to 0.2 mass%, and more. Preferably 10 ppm-0.1 mass% can be mentioned.
本発明の乳風味改善組成物は、乳性飲食品に、ミルク感、脂肪感、クリーム感などの風味を付与または増強するとともに、牛乳様のフレッシュな風味を想起させることができる。さらに乳風味改善剤を乳風味フレーバーに添加した後に加熱することにより、さらに牛乳様のフレッシュな風味を想起させる乳風味改善組成物を得ることができる。 The milk flavor improving composition of the present invention can give or enhance flavors such as milk, fat, and cream to milky foods and drinks, and can remind a fresh milk-like flavor. Further, by adding a milk flavor improving agent to the milk flavor flavor and then heating, a milk flavor improving composition reminiscent of a fresh milk-like flavor can be obtained.
また、前記に示すように、本発明の乳風味改善剤もしくは乳風味改善組成物を加熱することにより、または乳風味改善剤もしくは乳風味改善組成物を添加した乳性飲食品を加熱することにより、牛乳様のフレッシュな風味を想起させることができる。加熱温度は、通常60〜160℃、好ましくは70〜150℃であることが望ましい。また加熱時間は2秒〜30分、好ましくは2秒〜20分であることが望ましい。 Moreover, as shown above, by heating the milk flavor improving agent or milk flavor improving composition of the present invention, or by heating a milky food or drink to which the milk flavor improving agent or milk flavor improving composition is added. You can recall the fresh flavor of milk. The heating temperature is usually 60 to 160 ° C, preferably 70 to 150 ° C. The heating time is 2 seconds to 30 minutes, preferably 2 seconds to 20 minutes.
本発明の乳風味改善剤もしくは乳風味改善組成物を加熱することにより、または乳風味改善剤もしくは乳風味改善組成物を添加した乳性飲食品を加熱することにより、含硫アミノ酸を前駆体として、硫化水素やジメチルスルフィドなどの含硫化合物が生成し、この含硫化合物が乳性飲食品に牛乳様のフレッシュな風味を付与する効果を有する。 By heating the milk flavor improving agent or milk flavor improving composition of the present invention, or by heating a milky food or drink to which the milk flavor improving agent or milk flavor improving composition is added, a sulfur-containing amino acid is used as a precursor. Then, sulfur-containing compounds such as hydrogen sulfide and dimethyl sulfide are produced, and this sulfur-containing compound has an effect of imparting a milk-like fresh flavor to milky foods and drinks.
本発明で使用する乳風味フレーバーは、ラクトン類、脂肪酸類、アルデヒド類、エステル類、アルコール類、ケトン類、含窒素化合物類、含硫化合物類など公知の香料化合物;乳脂のリパーゼ分解物;乳タンパク質のプロテアーゼ分解物;乳、濃縮乳、粉乳、ミルクホエー、バター、チーズ、ヨーグルトもしくはこれらの混合物からの乳または乳加工品の分画物などを挙げることができる。 Milk flavor flavors used in the present invention are known perfume compounds such as lactones, fatty acids, aldehydes, esters, alcohols, ketones, nitrogen-containing compounds, sulfur-containing compounds; lipase degradation products of milk fat; milk Protein protease degradation products; milk, concentrated milk, milk powder, milk whey, butter, cheese, yoghurt or a mixture of milk or a processed product thereof.
香料化合物としては、例えば、「特許庁、周知慣用技術集(香料)第II部食品香料、P88−131、平成12年1月14日発行」に記載されている天然精油、天然香料、合成香料を挙げることができる。 Examples of the fragrance compound include natural essential oils, natural fragrances, and synthetic fragrances described in “Patent Office, Well-known Technique Collection (Fragrance) Part II Food Fragrance, P88-131, Issued on Jan. 14, 2000”. Can be mentioned.
例えば、γ−カプロラクトン、γ−ヘプタラクトン、γ−オクタラクトン、γ−ノナラクトン、γ−デカラクトン、7−デセン−4−オリド、3−メチル−4−デセン−4−オリド、3−メチル−5−デセン−4−オリド、γ−ウンデカラクトン、γ−ドデカラクトン、γ−トリデカラクトン、γ−テトラデカラクトン、δ−カプロラクトン、2−ヘキセン−5−オリド、2−ヘプテン−5−オリド、δ−オクタラクトン、2−オクテン−5−オリド、4−メチル−5−オクタノリド、δ−ノナラクトン、2−ノネン−5−オリド、4−メチル−5−ノナノリド、δ−デカラクトン、2−デセン−5−オリド、4−メチル−5−デカノリド、δ−ウンデカラクトン、2−ウンデセン−5−オリド、4−メチル−5−ウンデカノリド、δ−ドデカラクトン、2−ドデセン−5−オリド、4−メチル−5−ドデカノリド、δ−トリデカラクトン、2−トリデセン−5−オリド、4−メチル−5−トリデカノリド、δ−テトラデカラクトン、2−テトラデセン−5−オリド、2−ペンタデセン−5−オリド、2−ヘキサデセン−5−オリド、2−ヘプタデセン−5−オリド、2−オクタデセン−5−オリド、2−ノナデセン−5−オリド、2−エイコセン−5−オリド、ε−デカラクトンなどのラクトン類;プロピオン酸、酪酸、吉草酸、イソ吉草酸、カプロン酸、トランス−2−ヘキセン酸、ヘプタン酸、カプリル酸、ノナン酸、5−ヒドロキシノナン酸、カプリン酸、2−デセン酸、4−デセン酸、5−デセン酸、6−デセン酸、9−デセン酸、5−ヒドロキシデセン酸、5−ヒドロキシウンデカン酸、ラウリン酸、5−ヒドロキシドデカン酸、ミリスチン酸、ペンタデカン酸、イソペンタデカン酸、パルミチン酸、ヘプタデカン酸、ステアリン酸、オレイン酸、リノール酸、リノレン酸などの脂肪酸類;アセトアルデヒド、プロパナール、ブタナール、2−ブテナール、ヘキサナール、オクタナール、4−ヘプテナール、2,4−オクタジエナール、ノナナール、2−ノネナール、2,4−ノナジエナール、2,6−ノナジエナール、デカナール、2,4−デカジエナール、ウンデカナール、2,4−ウンデカジエナール、ドデカナール、ベンズアルデヒド、バニリン、エチルバニリン、フルフラール、ヘリオトロピンジエチルアセタールなどのアルデヒド類;蟻酸エチル、酢酸エチル、酢酸ブチル、酢酸イソアミル、酢酸デシル、酢酸ドデシル、酢酸フェネチル、乳酸エチル、酪酸エチル、2−メチル酪酸エチル、3−エチル酪酸エチル、吉草酸メチル、カプロン酸メチル、カプロン酸エチル、ヘプタン酸メチル、ヘプタン酸エチル、カプリル酸エチル、カプリル酸イソアミル、カプリル酸ヘプチル、ノナン酸メチル、ノナン酸エチル、カプリン酸メチル、カプリン酸エチル、ウンデカン酸エチル、ラウリン酸メチル、ラウリン酸エチル、ミリスチン酸エチル、パルミチン酸エチル、サリチル酸メチル、コハク酸ジエチル、セバシン酸ジエチル、5−ヒドロキシヘキサン酸エチル、5−ヒドロキシデカン酸エチル、5−ヒドロキシウンデカン酸エチル、5−ヒドロキシデカン酸プロピル、5−ヒドロキシデカン酸イソプロピル、5−ヒドロキシオクタン酸2−メチルプロピル、5−ヒドロキシ−9−メチルデカン酸エチル、5−アセトキシデカン酸メチル、5−アセトキシデカン酸エチルなどのエステル類;エタノール、プロパノール、ブタノール、ペンタノール、ヘキサノール、ヘプタノール、オクタノール、ノナノール、デカノール、ベンジルアルコール、フェニルエチルアルコール、フルフリルアルコールなどのアルコール類;2−ヘプタノン、2−オクタノン、3−オクタノン、1−オクテン−3−オン、2−ノナノン、3−ノナノン、8−ノネン−2−オン、2−ウンデカノン、2−トリデカノン、アセトイン、5−ヒドロキシ−4−オクタノン、ジアセチル、2,3−ペンタジオン、2,3−ヘキサジオン、2,3−ヘプタジオン、アセチルイソバレリル、p−メトキシアセトフェノン、ベンゾフェノン、マルトールなどのケトン類;フェニルエチルアントラニレート、トリメチルアミン、インドール、スカトール、ピリジン、イソキノリン、ピラジン、メチルピラジンなどの含窒素化合物類;メタンチオール、イソブチルメルカプタン、2,4−ジチアペンタン、ジメチルスルフィド、ジメチルジスルフィド、ジメチルトリスルフィド、ジメチルスルフォキシド、ジメチルスルフォン、メチルスルフォニルメタン、メチルイソチオシアネート、エチルイソチオシアネート、アリルイソチオシアネート、2−メチル−3−ブタンチオール、メチオナール、チオ酢酸エチル、チオ酪酸メチル、3−ブテニルイソチオシアネート、2−メチルチオフェン、ベンゾチアゾール、スルフロール、アセチル乳酸チオメチルエステル、プロピオニル乳酸チオメチルエステル、ブチリル乳酸チオメチルエステル、バレリル乳酸チオメチルエステル、2−メチルブチリル乳酸チオメチルエステル、デシリル乳酸チオメチルエステル、アセチル乳酸チオエチルエステル、プロピオニル乳酸チオエチルエステル、ブチリル乳酸チオエチルエステル、バレリル乳酸チオエチルエステル、イソカプロイル乳酸チオプロピルエステルなどの含硫化合物類などの公知の香料化合物を挙げることができる。 For example, γ-caprolactone, γ-heptalactone, γ-octalactone, γ-nonalactone, γ-decalactone, 7-decen-4-olide, 3-methyl-4-decen-4-olide, 3-methyl-5- Decene-4-olide, γ-undecalactone, γ-dodecalactone, γ-tridecalactone, γ-tetradecalactone, δ-caprolactone, 2-hexene-5-olide, 2-heptene-5-olide, δ -Octalactone, 2-octene-5-olide, 4-methyl-5-octanolide, δ-nonalactone, 2-nonene-5-olide, 4-methyl-5-nonanolide, δ-decalactone, 2-decene-5 Orido, 4-methyl-5-decanolide, δ-undecalactone, 2-undecen-5-olide, 4-methyl-5-undecanolide, δ-dodecalactone 2-dodecene-5-olide, 4-methyl-5-dodecanolide, δ-tridecalactone, 2-tridecen-5-olide, 4-methyl-5-tridecanolide, δ-tetradecalactone, 2-tetradecene-5 Orido, 2-Pentadecene-5-Olide, 2-Hexadecene-5-Olide, 2-Heptadecene-5-Olide, 2-Octadecene-5-Olide, 2-Nonadecene-5-Olide, 2-Eicosene-5-Olide, Lactones such as ε-decalactone; propionic acid, butyric acid, valeric acid, isovaleric acid, caproic acid, trans-2-hexenoic acid, heptanoic acid, caprylic acid, nonanoic acid, 5-hydroxynonanoic acid, capric acid, 2- Decenoic acid, 4-decenoic acid, 5-decenoic acid, 6-decenoic acid, 9-decenoic acid, 5-hydroxydecenoic acid, 5-hydroxyundeca Fatty acids such as acid, lauric acid, 5-hydroxydodecanoic acid, myristic acid, pentadecanoic acid, isopentadecanoic acid, palmitic acid, heptadecanoic acid, stearic acid, oleic acid, linoleic acid, linolenic acid; acetaldehyde, propanal, butanal, 2-butenal, hexanal, octanal, 4-heptenal, 2,4-octadienal, nonanal, 2-nonenal, 2,4-nonadienal, 2,6-nonadienal, decanal, 2,4-decadienal, undecanal, 2 , 4-Undecadienal, dodecanal, benzaldehyde, vanillin, ethyl vanillin, furfural, heliotropin diethyl acetal and other aldehydes; ethyl formate, ethyl acetate, butyl acetate, isoamyl acetate, decyl acetate, acetic acid Dodecyl, phenethyl acetate, ethyl lactate, ethyl butyrate, ethyl 2-methylbutyrate, ethyl 3-ethylbutyrate, methyl valerate, methyl caproate, ethyl caproate, methyl heptanoate, ethyl heptanoate, ethyl caprylate, isoamyl caprylate , Heptyl caprylate, methyl nonanoate, ethyl nonanoate, methyl caprate, ethyl caprate, ethyl undecanoate, methyl laurate, ethyl laurate, ethyl myristate, ethyl palmitate, methyl salicylate, diethyl succinate, sebacic acid Diethyl, ethyl 5-hydroxyhexanoate, ethyl 5-hydroxydecanoate, ethyl 5-hydroxyundecanoate, propyl 5-hydroxydecanoate, isopropyl 5-hydroxydecanoate, 2-methylpropyl 5-hydroxyoctanoate Esters such as ethyl 5-hydroxy-9-methyldecanoate, methyl 5-acetoxydecanoate, ethyl 5-acetoxydecanoate; ethanol, propanol, butanol, pentanol, hexanol, heptanol, octanol, nonanol, decanol, benzyl alcohol, Alcohols such as phenylethyl alcohol and furfuryl alcohol; 2-heptanone, 2-octanone, 3-octanone, 1-octen-3-one, 2-nonanone, 3-nonanone, 8-nonen-2-one, 2- Undecanone, 2-tridecanone, acetoin, 5-hydroxy-4-octanone, diacetyl, 2,3-pentadione, 2,3-hexadione, 2,3-heptadione, acetylisovaleryl, p-methoxyacetophenone, benzopheno , Ketones such as maltol; nitrogen-containing compounds such as phenylethyl anthranilate, trimethylamine, indole, skatole, pyridine, isoquinoline, pyrazine, methylpyrazine; methanethiol, isobutyl mercaptan, 2,4-dithiapentane, dimethyl sulfide, dimethyl Disulfide, dimethyl trisulfide, dimethyl sulfoxide, dimethyl sulfone, methyl sulfonyl methane, methyl isothiocyanate, ethyl isothiocyanate, allyl isothiocyanate, 2-methyl-3-butanethiol, methional, ethyl thioacetate, methyl thiobutyrate, 3 -Butenyl isothiocyanate, 2-methylthiophene, benzothiazole, sulfuryl, acetyl lactate thiomethyl ester, propionyl lactate thiol Methyl ester, butyryl lactate thiomethyl ester, valeryl lactate thiomethyl ester, 2-methylbutyryl lactate thiomethyl ester, desilyl lactate thiomethyl ester, acetyl lactate thioethyl ester, propionyl lactate thioethyl ester, butyryl lactate thioethyl ester, valeryl lactate thiol Known perfume compounds such as sulfur-containing compounds such as ethyl ester and isocaproyl lactate thiopropyl ester can be mentioned.
本発明の乳脂のリパーゼ分解物に用いられる乳脂は具体的にはバター、クリームが挙げられる。また、乳脂のリパーゼ分解に用いられるリパーゼは、動物由来リパーゼ、微生物由来リパーゼのいずれのものも使用することができる。リパーゼ分解の方法は特に限定されないが、使用する酵素の至適pH、至適温度に近い条件で行うことが好ましい。 Specific examples of the milk fat used in the lipase degradation product of milk fat of the present invention include butter and cream. As the lipase used for lipase degradation of milk fat, any of animal-derived lipases and microorganism-derived lipases can be used. The method for lipase degradation is not particularly limited, but it is preferably performed under conditions close to the optimum pH and temperature of the enzyme used.
本発明で用いられるリパーゼとして具体的には、アスペルギルス属、ムコール属、ペニシリウム属、リゾープス属、カンディダ属、シュードモナス属、アルカリゲネス属、リゾムコール属、バキルス属、アクロモバクター属などの微生物由来リパーゼや、豚膵臓などの動物由来リパーゼを使用することができ、また、これらを任意に組み合わせて使用することもできる。さらには、リパーゼ以外の酵素を併用することもできる。 Specific examples of the lipase used in the present invention include lipases derived from microorganisms such as Aspergillus, Mucor, Penicillium, Rhizopus, Candida, Pseudomonas, Alkaligenes, Rhizomucor, Bacillus, and Achromobacter, Animal-derived lipases such as porcine pancreas can be used, and any combination thereof can be used. Furthermore, an enzyme other than lipase can be used in combination.
また、市販品としては、リパーゼL、リパーゼM、リパーゼAP、リパーゼAY、リパーゼP、リパーゼAK、リパーゼCES、リパーゼM−AP、リパーゼD、リパーゼN、リパーゼCT、リパーゼR、リパーゼMER(以上、天野エンザイム(株)製)、スミチーム(登録商標)NLS、スミチーム(登録商標)RLS、スミチーム(登録商標)ALS(以上、新日本化学工業(株)製)、リパーゼMY、リパーゼPL、リパーゼQLM(以上、名糖産業(株)製)、リパーゼP、PLA2、リパーゼ−サイケン(登録商標)、リリパーゼ(登録商標)A−10D(以上、ナガセケムテックス(株)製)、豚膵臓リパーゼ(シグマアルドリッチジャパン(株)製)、レシターゼ(登録商標)、パラターゼ、パラダーゼM(以上、ノボザイムズ(株)製)、タリパーゼ(田辺製薬(株)製)等を例示することができる。これらのリパーゼは単独又は数種組み合わせて利用することもできる。 As commercially available products, lipase L, lipase M, lipase AP, lipase AY, lipase P, lipase AK, lipase CES, lipase M-AP, lipase D, lipase N, lipase CT, lipase R, lipase MER (or more, Amano Enzyme), Sumiteam (registered trademark) NLS, Sumiteam (registered trademark) RLS, Sumiteam (registered trademark) ALS (manufactured by Shin Nippon Chemical Industry Co., Ltd.), lipase MY, lipase PL, lipase QLM ( As described above, manufactured by Meito Sangyo Co., Ltd.), lipase P, PLA2, lipase-psychene (registered trademark), lipase (registered trademark) A-10D (manufactured by Nagase ChemteX Corporation), porcine pancreatic lipase (Sigma Aldrich) Japan Co., Ltd.), lecitase (registered trademark), paratase, paradase M (above, Novozyi) Manufactured's Corporation), manufactured by Talipase (Tanabe Seiyaku Co.), etc. can be exemplified. These lipases can be used singly or in combination.
本発明における乳タンパク質のプロテアーゼ分解物は、脱脂粉乳、チーズ、ホエイタンパクなどの乳タンパクを原料とすることが好ましい。本発明の乳タンパク質のプロテアーゼ分解に使用される酵素としては、動物由来プロテアーゼ、微生物由来プロテアーゼのいずれのものも使用することができる。また、プロテアーゼ活性はエンド型、エキソ型のいずれのものも使用することができるが、エンド型のプロテアーゼ活性を有する酵素を使用することが好ましく、エンド型とエキソ型の混合物であることがより好ましい。プロテアーゼ分解の方法は特に限定されないが、使用する酵素の至適pH、至適温度に近い条件で行うことが好ましい。 The protease degradation product of milk protein in the present invention is preferably made from milk protein such as skim milk powder, cheese, whey protein and the like. As an enzyme used for protease degradation of the milk protein of the present invention, any of animal-derived protease and microorganism-derived protease can be used. In addition, the protease activity can be either endo-type or exo-type, but it is preferable to use an enzyme having endo-type protease activity, more preferably a mixture of endo-type and exo-type. . The method for protease degradation is not particularly limited, but it is preferably performed under conditions close to the optimum pH and temperature of the enzyme used.
本発明で用いられるプロテアーゼとして具体的には、アスペルギルス属、ペニシリウム属、リゾープス属、ペニシリウム属など微生物由来の酸性プロテアーゼ、アスペルギルス属、ストレプトマイセズ属、バキルス属など微生物由来の中性プロテアーゼ、アスペルギルス属、バキルス属など微生物由来のアルカリ性プロテアーゼ、パパインなどの植物由来プロテアーゼ、豚膵臓など動物由来のプロテアーゼを使用することができ、また、これらを任意に組み合わせて使用することもできる。 Specific examples of proteases used in the present invention include acidic proteases derived from microorganisms such as Aspergillus, Penicillium, Rhizopus, Penicillium, neutral proteases derived from microorganisms such as Aspergillus, Streptomyces, and Bacillus, Aspergillus In addition, alkaline proteases derived from microorganisms such as Bacillus, plant-derived proteases such as papain, and animal-derived proteases such as porcine pancreas can be used, and these can be used in any combination.
また、市販品としては、プロテアーゼA、プロテアーゼM、プロテアーゼP、プロテアーゼM−SD、プロテアーゼN、プロテアーゼNL、プロテアーゼS、ウマミザイム、ペプチダーゼR、ニューラーゼ(登録商標)A、ニューラーゼ(登録商標)F(以上、天野エンザイム(株)製)、スミチーム(登録商標)AP、スミチーム(登録商標)LP、スミチーム(登録商標)MP、スミチーム(登録商標)FP、スミチーム(登録商標)LPL(以上、新日本化学工業(株)製)、デナプシン2P、デナチーム(登録商標)AP、XP−415、ビオプラーゼ(登録商標)XL−416F、ビオプラーゼ(登録商標)SP−4FG、ビオプラーゼ(登録商標)SP−15FG(以上、ナガセケムテックス(株)製)、モルシン(登録商標)F、PD酵素、IP酵素、AO−プロテアーゼ(以上、キッコーマン(株)製)、パンチダーゼ(登録商標)YP−SS、パンチダーゼ(登録商標)NP−2、パンチダーゼ(登録商標)P(以上、ヤクルト薬品工業(株)製)、フレーバザイム(登録商標)、アロアーゼ(登録商標)、プロタメックス(登録商標)、ニュートラーゼ(登録商標)、アルカラーゼ(登録商標)(ノボザイムズ(株)製)、コクラーゼ(登録商標)SS、コクラーゼ(登録商標)P(以上、三共ライフテック(株)製)等を例示することができる。これらのプロテアーゼは単独又は数種組み合わせて利用することもできる。さらに、前記リパーゼと前記プロテアーゼを組み合わせて利用することもできる。 Commercially available products include Protease A, Protease M, Protease P, Protease M-SD, Protease N, Protease NL, Protease S, Umamizyme, Peptidase R, Neurase (registered trademark) A, Neurase (registered trademark) F (Above, Amano Enzyme Co., Ltd.), Sumiteam (registered trademark) AP, Sumiteam (registered trademark) LP, Sumiteam (registered trademark) MP, Sumiteam (registered trademark) FP, Sumiteam (registered trademark) LPL (above, New Japan) Chemical Industry Co., Ltd.), Denapsin 2P, Denateam (registered trademark) AP, XP-415, Bioplase (registered trademark) XL-416F, Biolase (registered trademark) SP-4FG, Biolase (registered trademark) SP-15FG (or more) , Manufactured by Nagase ChemteX Corporation), Morcin (registered trademark) , PD enzyme, IP enzyme, AO-protease (above, manufactured by Kikkoman Corporation), punchase (registered trademark) YP-SS, punchase (registered trademark) NP-2, punchase (registered trademark) P (above, Yakult Pharmaceutical Co., Ltd.) Co., Ltd.), Flazyzyme (registered trademark), Aroase (registered trademark), Protamex (registered trademark), Neutrase (registered trademark), Alcalase (registered trademark) (manufactured by Novozymes), Cochlase (registered trademark) (Trademark) SS, cochlase (registered trademark) P (manufactured by Sankyo Lifetech Co., Ltd.) and the like. These proteases can be used alone or in combination of several kinds. Further, the lipase and the protease can be used in combination.
本発明における乳または乳加工品の分画方法としては、蒸留、溶剤抽出、膜分離、樹脂吸着などが挙げられ、また、必要に応じて、水、アルコール類などの溶剤を加えた後、これらの方法により分画することができる。これらの方法は、任意に組み合わせて用いることができる。具体的には、たとえば蒸留法の場合、水蒸気蒸留液または濃縮回収液を疎水性有機溶媒で抽出した後、溶剤を回収する方法や、水蒸気蒸留液または濃縮回収液を多孔性樹脂、化学修飾型シリカゲル、カチオン交換樹脂、アニオン交換樹脂などの樹脂に吸着させ、吸着成分をエチルアルコール等で脱着する方法などが挙げられる。また、溶剤抽出の場合は、疎水性有機溶剤で抽出後、溶剤を回収する方法や、液体、亜臨界または超臨界状態の二酸化炭素で抽出し、二酸化炭素を分離する方法などが挙げられる。また、膜分離の場合は、目的に応じて分画分子量などにより任意の膜を選択することができ、限外濾過法、逆浸透法など任意の方法を用いることができる。また、樹脂吸着の場合は、多孔性樹脂、化学修飾型シリカゲル、カチオン交換樹脂、アニオン交換樹脂などのイオン交換樹脂などを任意に選択することができる。またこれらの方法を使用するに当たって、原料をリパーゼやプロテアーゼなどの酵素で前処理することもでき、分画物をあるいは分画物に糖やアミノ酸などを加えて加熱するなどの後処理を加えてもよい。 Examples of the fractionation method of milk or dairy products in the present invention include distillation, solvent extraction, membrane separation, resin adsorption, etc., and if necessary, after adding a solvent such as water or alcohols, It can be fractionated by the method of. These methods can be used in any combination. Specifically, for example, in the case of a distillation method, a steam distilled liquid or concentrated recovery liquid is extracted with a hydrophobic organic solvent, and then the solvent is recovered. Examples include a method of adsorbing on a resin such as silica gel, a cation exchange resin, and an anion exchange resin, and desorbing the adsorbed component with ethyl alcohol or the like. In the case of solvent extraction, a method of recovering the solvent after extraction with a hydrophobic organic solvent, a method of extracting with carbon dioxide in a liquid, subcritical or supercritical state, and separating carbon dioxide can be used. In the case of membrane separation, any membrane can be selected according to the molecular weight cut off according to the purpose, and any method such as ultrafiltration or reverse osmosis can be used. In the case of resin adsorption, an ion exchange resin such as a porous resin, chemically modified silica gel, a cation exchange resin, and an anion exchange resin can be arbitrarily selected. In addition, when using these methods, the raw material can be pretreated with an enzyme such as lipase or protease, and post-treatment such as heating the fraction or adding the sugar or amino acid to the fraction is added. Also good.
以下、本発明を実施例によりさらに具体的に説明する。なお、本発明はこれらに限定されるものではない。 Hereinafter, the present invention will be described more specifically with reference to examples. The present invention is not limited to these.
実施例1:乳飲料にシスチンを添加した効果
市販の乳飲料(乳脂肪分1.8%、無脂乳固形分8.0%、生乳50%未満)100gにシスチン0.1gを添加し、シスチンを添加後110℃にて1分間加熱し、冷却後冷蔵庫にて冷蔵保存した。これを本発明品1とする。市販の乳飲料を110℃にて1分間加熱し、冷却後冷蔵庫にて冷蔵保存したものを比較品1として、よく訓練されたパネラー10名により官能評価を行った。
Example 1: Effect of adding cystine to a milk beverage 0.1 g of cystine was added to 100 g of a commercially available milk beverage (milk fat content 1.8%, nonfat milk solid content 8.0%, raw milk less than 50%), After adding cystine, the mixture was heated at 110 ° C. for 1 minute, cooled, and stored in a refrigerator. This is product 1 of the present invention. A commercially available milk drink was heated at 110 ° C. for 1 minute, cooled, and then refrigerated and stored in a refrigerator. As a comparative product 1, sensory evaluation was performed by 10 well-trained panelists.
官能評価の方法は、冷蔵保存した本発明品1および比較品1を冷蔵庫より取り出し、プラスチックの試飲容器に少量注ぎ込み、試飲することにより行った。評価方法は試飲することにより、本発明品1および比較品1のどちらがより牛乳らしいと感じるかを評価した。ここで、本官能検査において牛乳らしいとは、牛乳様のフレッシュな風味を想起されることを示す。 The sensory evaluation method was performed by taking out the refrigerated product 1 of the present invention and the comparative product 1 from the refrigerator, pouring a small amount into a plastic tasting container, and tasting. By evaluating the evaluation method, it was evaluated which of the product 1 of the present invention and the comparative product 1 felt more like milk. Here, milk-like in this sensory test means that a milk-like fresh flavor is recalled.
官能評価の結果、パネラー10名中6名が本発明品1の方が牛乳らしいと評価した。よって、乳飲料にシスチンを添加することにより、乳飲料に牛乳様のフレッシュな風味を想起させる効果が示された。 As a result of sensory evaluation, 6 out of 10 panelists evaluated the product 1 of the present invention as being milk. Thus, the addition of cystine to a milk beverage showed an effect of recalling a milk-like fresh flavor in the milk beverage.
実施例2:乳飲料に酵母エキスを添加した効果
実施例1で用いた市販の乳飲料100gに酵母エキス「グルタイーストエキスN」(協和発酵バイオ社製、グルタチオン含有量8%)0.01gを添加し、110℃にて1分間加熱し、冷却後冷蔵庫にて冷蔵保存した。これを本発明品2とする。本発明品2および比較品1を実施例1と同様の方法でよく訓練されたパネラー10名により官能評価を行い、本発明品2および比較品1のどちらがより牛乳らしいと感じるかを評価した。
Example 2: Effect of adding yeast extract to milk beverage 0.01 g of yeast extract “Gluta yeast extract N” (Kyowa Hakko Bio Inc., glutathione content 8%) was added to 100 g of the commercial milk beverage used in Example 1. The mixture was added, heated at 110 ° C. for 1 minute, cooled and stored in a refrigerator after cooling. This is designated as Product 2 of the present invention. Sensory evaluation was performed by 10 panelists who were well trained in the same manner as in Example 1 for the product 2 of the present invention and the comparative product 1 to evaluate which of the product 2 of the present invention and the comparative product 1 felt more like milk.
官能評価の結果、パネラー10名中8名が本発明品2の方が牛乳らしいと評価した。よって、乳飲料にグルタチオンを含有する酵母エキスを添加することにより、乳飲料に牛乳様のフレッシュな風味を想起させる効果が示された。 As a result of sensory evaluation, 8 out of 10 panelists evaluated that the product 2 of the present invention was more milky. Therefore, the effect which reminds milk-like fresh flavor to milk drink was shown by adding the yeast extract containing glutathione to milk drink.
参考例1:乳風味フレーバーの調製
乳脂肪分45%生クリーム850gを加温した後、脱脂粉乳100gを加え、40〜45℃で加温溶解し、これをTKホモミキサー(プライミクス株式会社製)にて10分間混合溶解した。溶解した後、約75℃で20分間殺菌し、40℃に冷却し乳混合物とした。これとは別に、水50gにリリパーゼ(登録商標)A−10D(ナガセケムテックス社製)2gを溶解し、この酵素溶解物を前記乳混合物に添加し、40℃〜45℃にて24時間酵素処理をした。酵素処理終了後、約85℃で15分間加熱して酵素失活した。冷却後、分解物をTKホモミキサーにて10分間均質化し、乳風味フレーバー(参考品1)を得た。
Reference Example 1 Preparation of Milk Flavor Flavor After heating 850 g of milk cream 45% fresh cream, 100 g of skim milk powder was added and heated to dissolve at 40 to 45 ° C., and this was added to TK Homomixer (manufactured by Primix Co., Ltd.) And mixed for 10 minutes. After dissolution, the mixture was sterilized at about 75 ° C. for 20 minutes, cooled to 40 ° C. to obtain a milk mixture. Separately, 2 g of lipase (registered trademark) A-10D (manufactured by Nagase ChemteX) was dissolved in 50 g of water, and the enzyme lysate was added to the milk mixture and the enzyme was incubated at 40 ° C. to 45 ° C. for 24 hours. Processed. After completion of the enzyme treatment, the enzyme was inactivated by heating at about 85 ° C. for 15 minutes. After cooling, the decomposition product was homogenized with a TK homomixer for 10 minutes to obtain a milk flavor flavor (reference product 1).
実施例3:乳飲料に酵母エキスおよび乳風味フレーバーを添加した効果
実施例1で用いた市販の乳飲料100gに酵母エキス「グルタイーストエキスN」を5mg添加し、110℃にて1分間加熱し、冷却後冷蔵庫にて冷蔵保存した。これを本発明品3とする。また、実施例1で用いた市販の乳飲料100gに参考品1を0.05g添加し、110℃にて1分間加熱し、冷却後冷蔵庫にて冷蔵保存した。これを比較品2とする。さらに、実施例1で用いた市販の乳飲料100gに酵母エキス「グルタイーストエキスN」5mgおよび参考品1を0.05g添加し、110℃にて1分間加熱し、冷却後冷蔵庫にて冷蔵保存した。これを本発明品4とする。
Example 3 Effect of Adding Yeast Extract and Milk Flavor Flavor to Milk Beverage 5 mg of yeast extract “Gluta Yeast Extract N” was added to 100 g of the commercially available milk drink used in Example 1, and heated at 110 ° C. for 1 minute. After cooling, it was refrigerated and stored in a refrigerator. This is product 3 of the present invention. Further, 0.05 g of the reference product 1 was added to 100 g of the commercially available milk drink used in Example 1, heated at 110 ° C. for 1 minute, and after refrigeration, stored in a refrigerator. This is referred to as comparative product 2. Furthermore, 5 g of yeast extract “Gluta yeast extract N” and 0.05 g of reference product 1 were added to 100 g of the commercially available milk drink used in Example 1, heated at 110 ° C. for 1 minute, cooled and then refrigerated in a refrigerator. did. This is designated as Product 4 of the present invention.
本発明品3、4および比較品1、2を訓練されたパネラー4名により、実施例1と同様の方法で官能評価し、牛乳らしい順に4点〜1点と点数をつけて評価を行った。その結果を表1に示す。 Sensory evaluation was performed in the same manner as in Example 1 by 4 trained panelists of the present invention products 3 and 4 and comparative products 1 and 2, and the evaluation was performed with 4 to 1 points in the order of milk. . The results are shown in Table 1.
表1の結果、比較品1、2と比較して本発明品3、4がより牛乳らしいと評価された。また、本発明品3と比較して本発明品4はさらに牛乳らしいと評価され、パネラー全員が最も牛乳らしいと評価した。このことから、本発明の乳風味増強剤に乳風味フレーバーを添加することにより、牛乳様のフレッシュな風味を想起させる効果が強くなることが見出された。 As a result of Table 1, it was evaluated that the products 3 and 4 of the present invention were more milky than the comparative products 1 and 2. Moreover, compared with the product 3 of the present invention, the product 4 of the present invention was further evaluated as milk-like, and all the panelists evaluated it as milk-like. From this, it was found that the effect of recalling a milk-like fresh flavor is enhanced by adding a milk flavor to the milk flavor enhancer of the present invention.
実施例4:酵母エキスを添加した乳風味改善組成物の調製
乳脂肪分45%生クリーム805gを加温した後、脱脂粉乳95gを加え、40〜45℃で加温溶解し、これをTKホモミキサーにて10分間混合溶解した。溶解した後、約75℃で20分間殺菌し、40℃に冷却し乳混合物とした。これとは別に、水48gにリリパーゼA−10Dを1.9g溶解し、この酵素溶解物を前記乳混合物に添加し、40℃〜45℃にて24時間酵素処理をした。酵素処理終了後、約85℃で15分間加熱して酵素失活した。冷却後、酵母エキス「グルタイーストエキスN」を50g添加し、75℃で20分間殺菌し、再び冷却しTKホモミキサーにて10分間均質化し、乳風味改善組成物(本発明品5)を得た。
Example 4: Preparation of a milk flavor improving composition to which a yeast extract was added After heating 805 g of milk fat 45% fresh cream, 95 g of skimmed milk powder was added and heated to dissolve at 40 to 45 ° C. Mix and dissolve for 10 minutes with a mixer. After dissolution, the mixture was sterilized at about 75 ° C. for 20 minutes, cooled to 40 ° C. to obtain a milk mixture. Separately, 1.9 g of lipase A-10D was dissolved in 48 g of water, and this enzyme solution was added to the milk mixture, followed by enzyme treatment at 40 ° C. to 45 ° C. for 24 hours. After completion of the enzyme treatment, the enzyme was inactivated by heating at about 85 ° C. for 15 minutes. After cooling, 50 g of yeast extract “Gluta yeast extract N” was added, sterilized at 75 ° C. for 20 minutes, cooled again, and homogenized with TK homomixer for 10 minutes to obtain a milk flavor improving composition (Product 5 of the present invention). It was.
実施例5:乳飲料に酵母エキスを添加した乳風味改善組成物を添加した効果
実施例1で用いた市販の乳飲料100gに本発明品5を1mg添加し、これを本発明品6とした。同様に、乳飲料100gに本発明品5を0.01g添加したものを本発明品7、乳飲料100gに本発明品6を0.1g添加したものを本発明品8とした。本発明品6〜8および比較品1を実施例1と同様の方法でよく訓練されたパネラー10名により官能評価を行い、本発明品6〜8それぞれを、比較品1を対象としてどちらがより牛乳らしいと感じるか評価した。その結果を表2に示す。
Example 5: Effect of adding a milk flavor improving composition obtained by adding yeast extract to a milk beverage 1 mg of the product 5 of the present invention was added to 100 g of the commercially available milk beverage used in Example 1, and this was designated as the product 6 of the present invention. . Similarly, a product obtained by adding 0.01 g of the product 5 of the present invention to 100 g of a milk beverage was designated as product 7 of the present invention, and a product obtained by adding 0.1 g of the product 6 of the present invention to 100 g of milk beverage was designated as product 8 of the present invention. Sensory evaluation was performed on the products 6 to 8 of the present invention and the comparative product 1 by 10 panelists who were well trained in the same manner as in Example 1, and each of the products 6 to 8 of the present invention was compared with the comparison product 1 which was more milk. It was evaluated whether it felt like it. The results are shown in Table 2.
表2の結果、本発明品6〜8は比較品1より牛乳らしいと評価された。このことから、グルタチオンを含有する酵母エキスを乳風味フレーバーに添加した乳風味改善組成物を乳飲料に添加することにより、乳飲料に牛乳様のフレッシュな風味を想起させる効果があることを示された。 As a result of Table 2, the products 6 to 8 of the present invention were evaluated to be milk-like than the comparative product 1. From this, it was shown that by adding a milk flavor improving composition in which a yeast extract containing glutathione is added to a milk flavor flavor to a milk beverage, the milk beverage has an effect of recalling a fresh milk-like flavor. It was.
比較例1:ミルクプリンの調製
牛乳20g、グラニュー糖12g、脱脂粉乳3.5g、精製ヤシ油3g、ゲル化剤0.5g、粉末卵黄0.3g、乳化剤0.1g、に水を加えて80℃まで加熱し加熱混合を行った。その後、80℃にて15分間混合した。熱水を加えて全体で100gに質量調整した後撹拌し、冷却した後冷蔵庫にて冷蔵保存し、ミルクプリン(比較品3)を得た。
Comparative Example 1: Preparation of milk pudding 20 g of milk, 12 g of granulated sugar, 3.5 g of skim milk powder, 3 g of refined coconut oil, 0.5 g of gelling agent, 0.3 g of powdered egg yolk, 0.1 g of emulsifier and 80% water. The mixture was heated to ℃ and mixed. Then, it mixed for 15 minutes at 80 degreeC. Hot water was added to adjust the mass to 100 g as a whole, followed by stirring, cooling, and refrigerated storage in a refrigerator to obtain a milk pudding (Comparative Product 3).
比較例2:ミルクプリンに乳風味フレーバーを添加
牛乳20g、グラニュー糖12g、脱脂粉乳3.5g、精製ヤシ油3g、ゲル化剤0.5g、粉末卵黄0.3g、乳化剤0.1g、に水を加えて80℃まで加熱し加熱混合を行った。その後、参考品1を0.05g添加し、80℃にて15分間混合した。熱水を加えて全体で100gに質量調整した後撹拌し、冷却した後に冷蔵庫にて冷蔵保存し、ミルクプリン(比較品4)を得た。
Comparative Example 2: Milk flavor added to milk pudding 20 g of milk, 12 g of granulated sugar, 3.5 g of skim milk powder, 3 g of refined coconut oil, 0.5 g of gelling agent, 0.3 g of powdered egg yolk, 0.1 g of emulsifier, and water The mixture was heated to 80 ° C. and mixed by heating. Thereafter, 0.05 g of Reference Product 1 was added and mixed at 80 ° C. for 15 minutes. After adding hot water to adjust the mass to 100 g as a whole, the mixture was stirred, cooled, and then refrigerated in a refrigerator to obtain a milk pudding (Comparative Product 4).
実施例6:ミルクプリンに酵母エキスを添加
比較例2において、参考品1を0.05g添加する代わりに酵母エキス「グルタイーストエキスN」を5mg添加すること以外は比較例2と同様な方法で、ミルクプリン(本発明品9)を得た。
Example 6: Adding yeast extract to milk pudding In Comparative Example 2, in the same manner as Comparative Example 2 except that 5 mg of yeast extract “Gluta yeast extract N” was added instead of adding 0.05 g of Reference product 1. A milk pudding (Product 9 of the present invention) was obtained.
実施例7:ミルクプリンに酵母エキスおよび乳風味フレーバーを添加
比較例2において、参考品1を0.05g添加することに加えてさらに酵母エキス「グルタイーストエキスN」を5mg添加すること以外は比較例2と同様な方法で、ミルクプリン(本発明品10)を得た。
Example 7: Addition of yeast extract and milk flavor to milk pudding In Comparative Example 2, in addition to adding 0.05 g of the reference product 1, a comparison was made except that 5 mg of yeast extract “Gluta yeast extract N” was further added. In the same manner as in Example 2, milk pudding (Invention product 10) was obtained.
実施例8:ミルクプリンに酵母エキスおよび乳風味フレーバーを添加した効果
本発明品9、10および比較品3、4を訓練されたパネラー4名により、実施例1と同様の方法で官能評価し、牛乳らしい順に4点〜1点と点数をつけて評価を行った。その結果を表3に示す。
Example 8: Effect of adding yeast extract and milk flavor flavor to milk pudding The inventive products 9, 10 and comparative products 3 and 4 were subjected to sensory evaluation in the same manner as in Example 1 by 4 trained panelists. Evaluation was performed by assigning a score of 4 to 1 in the order of milk. The results are shown in Table 3.
表3の結果、比較品3、4と比較して本発明品9、10がより牛乳らしいと評価された。また、本発明品9と比較して本発明品10はさらに牛乳らしいと評価され、パネラー全員が最も牛乳らしいと評価した。このことから、本発明の乳風味増強剤に乳風味フレーバーを添加することにより、牛乳様のフレッシュな風味を想起させる効果が強くなることが見出された。 As a result of Table 3, it was evaluated that the products 9 and 10 of the present invention were more milky than the comparative products 3 and 4. Moreover, compared with the product 9 of the present invention, the product 10 of the present invention was further evaluated as milk-like, and all the panelists evaluated it as milk-like. From this, it was found that the effect of recalling a milk-like fresh flavor is enhanced by adding a milk flavor to the milk flavor enhancer of the present invention.
実施例9:ミルクプリンに酵母エキスを添加した乳風味改善組成物を添加した効果
比較例2において、参考品1を0.05g添加する代わりに本発明品5を1mg添加すること以外は比較例2と同様な方法で、ミルクプリン(本発明品11)を得た。また、同様に参考品1を0.05g添加する代わりに本発明品5を0.01g添加すること以外は比較例2と同様な方法で、ミルクプリン(本発明品12)を得た。さらに、同様に参考品1を0.05g添加する代わりに本発明品5を0.1g添加すること以外は比較例2と同様な方法で、ミルクプリン(本発明品13)を得た。
Example 9: Effect of adding a milk flavor improving composition obtained by adding yeast extract to milk pudding In Comparative Example 2, except that 0.05 g of the reference product 1 was added, 1 mg of the product 5 of the present invention was added. In the same manner as in No. 2, milk pudding (present product 11) was obtained. Similarly, milk pudding (invention product 12) was obtained in the same manner as in Comparative Example 2, except that 0.05 g of the reference product 1 was added instead of 0.01 g of the invention product 5. Further, milk pudding (present product 13) was obtained in the same manner as in Comparative Example 2, except that 0.05 g of the reference product 1 was added in the same manner and 0.1 g of the present product 5 was added.
本発明品11〜13および比較品3を実施例1と同様の方法でよく訓練されたパネラー10名により官能評価を行い、本発明品11〜13それぞれを、比較品3を対象としてどちらがより牛乳らしいと感じるか評価した。その結果を表4に示す。 Sensory evaluation was performed by 10 panelists who were well trained in the same manner as in Example 1 for the products 11 to 13 of the present invention and the comparative product 3, and each of the products 11 to 13 of the present invention was compared with the comparison product 3 which was more milk. It was evaluated whether it felt like it. The results are shown in Table 4.
表4の結果、本発明品11〜13は比較品3より牛乳らしいと評価された。このことから、グルタチオンを含有する酵母エキスを乳風味フレーバーに添加した乳風味改善組成物を乳飲料に添加することにより、乳飲料に牛乳様のフレッシュな風味を想起させる効果があることが示された。 As a result of Table 4, the inventive products 11 to 13 were evaluated to be milk-like than the comparative product 3. From this, it is shown that adding a milk flavor improving composition in which a yeast extract containing glutathione is added to a milk flavor flavor has an effect of recalling a milk-like fresh flavor in the milk beverage. It was.
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JP6680937B1 (en) * | 2019-09-27 | 2020-04-15 | 小川香料株式会社 | Milk fat imparting agent |
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