JP2013066838A - Multieffect evaporator-type distilled water manufacturing apparatus - Google Patents

Multieffect evaporator-type distilled water manufacturing apparatus Download PDF

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JP2013066838A
JP2013066838A JP2011206946A JP2011206946A JP2013066838A JP 2013066838 A JP2013066838 A JP 2013066838A JP 2011206946 A JP2011206946 A JP 2011206946A JP 2011206946 A JP2011206946 A JP 2011206946A JP 2013066838 A JP2013066838 A JP 2013066838A
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Haruo Nishi
治男 西
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ISHIN GIKEN KK
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Abstract

PROBLEM TO BE SOLVED: To provide a multieffect evaporator-type distilled water manufacturing apparatus capable of efficiently separating pure steam from steam-water mixed solution by arranging a steam-water separation mechanism for applying centrifugal force to the steam-water mixed solution generated in a heating chamber of each evaporator in a lower chamber of each evaporator.SOLUTION: The multieffect evaporator-type distilled water manufacturing apparatus includes: a preheating means for supply water; a plurality of evaporators for successively generating steam-water mixed solution from the preheated supply water; a steam-water separation means for separating the generated steam-water mixed solution into steam and water; a condenser for cooling the steam/water separated pure steam with the supply water and cooling water to generate distilled water; and an outer air introducing means connected to the condenser. In the manufacturing apparatus, the steam-water separation mechanism is arranged in the lower chamber of each evaporator, the steam-water separation mechanism includes a spiral fin arranged between an outer cylinder of the lower chamber and an inner cylinder inserted into the center part of the lower chamber, and the steam-water separation mechanism separates pure stem from the steam-water mixed solution by applying centrifugal force to the steam-water mixed solution.

Description

本発明は多重効用缶式蒸留水製造装置に関し、更に詳しくは複数の竪形蒸発缶とその付属機器等から構成される多重効用缶式蒸留水製造装置の改良に関する。例えば各種医薬品の製造工場や医療現場では、GMP(医薬品及び医薬部外品の製造管理及び品質管理の基準)や日本薬局方に適合した蒸留水が求められる。本発明はかかる蒸留水を製造するための多重効用缶式蒸留水製造装置の改良に関する。   The present invention relates to a multi-effect can-type distilled water production apparatus, and more particularly to an improvement of a multi-effect can-type distilled water production apparatus composed of a plurality of vertical evaporators and their attached devices. For example, various pharmaceutical manufacturing factories and medical sites require distilled water suitable for GMP (standards for manufacturing and quality control of pharmaceuticals and quasi-drugs) and the Japanese Pharmacopoeia. The present invention relates to an improvement of a multi-effect can-type distilled water production apparatus for producing such distilled water.

従来、前記のような多重効用缶式蒸留水製造装置として、供給水の予熱手段と、予熱した供給水から気水混合液を順次発生させる複数の蒸発缶と、発生させた気水混合液の気水分離手段と、気水分離した純蒸気を供給水及び冷却水で冷却して蒸留水とするコンデンサと、コンデンサに接続された外気導入手段とを備えるものが知られている(例えば特許文献1及び2参照)。   Conventionally, as a multi-effect can-type distilled water production apparatus as described above, supply water preheating means, a plurality of evaporators for sequentially generating a mixture of air and water from the preheated supply water, and the generated mixture of air and water An apparatus is known that includes an air / water separation means, a condenser that cools the pure steam separated from the air / water with supply water and cooling water to form distilled water, and an outside air introduction means that is connected to the condenser (for example, Patent Documents). 1 and 2).

ところが、かかる従来の多重効用缶式蒸留水製造装置には、蒸発缶の加熱室で発生させた気水混合液を、蒸発缶の下部室にて、純蒸気は上方へ、また蒸発しなかった供給水(以下、単に飽和水ともいう)は下方へと単に比重分離するだけであるため、気水混合液の気水分離効率が悪く、純蒸気と共に飽和水の一部が持ち込まれてしまうという問題がある。   However, in such a conventional multi-effect can-type distilled water production apparatus, the pure water does not evaporate upward in the lower chamber of the evaporator by using the gas-water mixture generated in the heating chamber of the evaporator. Since the feed water (hereinafter also simply referred to as saturated water) is simply separated by specific gravity downward, the steam-water mixture efficiency is poor, and some saturated water is brought in along with pure steam. There's a problem.

特開昭60−051588号公報Japanese Patent Laid-Open No. 60-051588 特開平10−296236号公報JP-A-10-296236

本発明が解決しようとする課題は、各蒸発缶の下部室に、各蒸発缶の加熱室で発生させた気水混合液の下方向流れに直接遠心力を加える気水分離機構を設けて、該気水混合液から純蒸気を効率的に分離することができるようにした多重効用缶式蒸留水製造装置を提供することにある。   The problem to be solved by the present invention is to provide a steam separation mechanism that applies a centrifugal force directly to the downward flow of the steam-water mixture generated in the heating chamber of each evaporator in the lower chamber of each evaporator. An object of the present invention is to provide a multi-effect can-type distilled water production apparatus capable of efficiently separating pure steam from the gas-water mixture.

前記の課題を解決する本発明は、供給水の予熱手段と、予熱した供給水から気水混合液を順次発生させる複数の蒸発缶と、発生させた気水混合液の気水分離手段と、気水分離した純蒸気を供給水及び冷却水で冷却して蒸留水とするコンデンサと、コンデンサに接続された外気導入手段とを備える多重効用缶式蒸留水製造装置において、各蒸発缶の下部室に気水分離機構が設けられており、該気水分離機構は、下部室の外筒と下部室の中央部に挿入された内筒との間に設けられた螺旋状フィンを備えていて、かかる気水分離機構により気水混合液に遠心力を加えて該気水混合液から純蒸気を分離するようにして成ることを特徴とする多重効用缶式蒸留水製造装置に係る。   The present invention that solves the above-mentioned problems is a feed water preheating means, a plurality of evaporators that sequentially generate a steam-water mixture from the preheated feed water, a steam-water separation means for the generated steam-water mixture, In a multi-effect can-type distilled water production apparatus comprising a condenser that cools pure steam separated by steam with supply water and cooling water to form distilled water, and an outside air introducing means connected to the condenser, a lower chamber of each evaporator The air / water separation mechanism is provided with a helical fin provided between the outer cylinder of the lower chamber and the inner cylinder inserted in the center of the lower chamber, A multi-effect can-type distilled water producing apparatus is characterized in that a pure steam is separated from the air / water mixture by applying a centrifugal force to the air / water mixture by the air / water separation mechanism.

本発明に係る多重効用缶式蒸留水製造装置(以下、単に本発明の装置という)も、従来の多重効用缶式蒸留水製造装置と同様、供給水の予熱手段と、予熱した供給水から気水混合液を順次発生させる複数の蒸発缶と、発生させた気水混合液の気水分離手段と、気水分離した純蒸気を供給水及び冷却水で冷却して蒸留水とするコンデンサと、コンデンサに接続された外気導入手段とを備えている。   The multi-effect can-type distilled water production apparatus (hereinafter simply referred to as the apparatus of the present invention) according to the present invention is similar to the conventional multi-effect can-type distilled water production apparatus. A plurality of evaporators that sequentially generate a water mixture, a steam separator for the generated steam / water mixture, a condenser that cools the pure steam separated by steam with supply water and cooling water to form distilled water, And an outside air introducing means connected to the capacitor.

本発明の装置では、気水分離手段として、複数の蒸発缶の各下部室に気水分離機構が設けられている。各蒸発缶は、供給水や飽和水を加熱室の伝熱管へと送入する上部室と、伝熱管へと送入した供給水や飽和水を加熱蒸気で間接加熱する加熱室と、加熱により発生した気水混合液を純蒸気と飽和水とに分離する下部室とに大別されるが、本発明の装置ではかかる蒸発缶の各下部室に気水分離機構が設けられているのである。   In the apparatus of the present invention, a steam / water separation mechanism is provided in each lower chamber of the plurality of evaporators as the steam / water separation means. Each evaporator has an upper chamber that feeds supply water and saturated water to the heat transfer tube of the heating chamber, a heating chamber that indirectly heats the supply water and saturated water sent to the heat transfer tube with heating steam, The generated gas / water mixture is roughly divided into lower chambers for separating pure steam and saturated water. In the apparatus of the present invention, each of the lower chambers of the evaporator is provided with an air / water separation mechanism. .

本発明の装置において、各蒸発缶の下部室に設けられた気水分離機構は、下部室の外筒と下部室の中央部に挿入された内筒との間に設けられた螺旋状フィンを備えている。本発明の装置は、下部室に落下してくる気水混合液に、螺旋状フィンで旋回させることにより遠心力を加え、かかる遠心力により該気水混合液から純蒸気を分離するようになっている。各下部室には、螺旋状フィンの上方に、螺旋状フィンと同じ方向へ旋回する螺旋状羽根を設けるのが好ましく、また螺旋状フィンの下方に、螺旋状フィンで回転しながら分離されてくる飽和水を中央部に集めて下部室から排出し易くするための集液部材を設けるのが好ましい。かかる集液部材としては、詳しくは後述するように、下部室の底面から離間して水平方向に支持された円板上部材と、該円板上部材の周縁部から所定間隔で垂設された複数の横断面くの字状部材とを備え、これらのくの字状部材によって、螺旋状フィンにより回転しながら分離されてくる飽和水を中央部に集めるようにしたものが好ましい。   In the apparatus of the present invention, the steam-water separation mechanism provided in the lower chamber of each evaporator has a helical fin provided between the outer cylinder of the lower chamber and the inner cylinder inserted in the center of the lower chamber. I have. The apparatus of the present invention applies centrifugal force to the air / water mixture falling into the lower chamber by swirling with a spiral fin, and separates pure vapor from the air / water mixture by the centrifugal force. ing. Each lower chamber is preferably provided with a spiral blade swirling in the same direction as the spiral fin above the spiral fin, and is separated while rotating with the spiral fin below the spiral fin. It is preferable to provide a liquid collecting member for collecting saturated water in the central part and facilitating discharge from the lower chamber. As the liquid collecting member, as will be described in detail later, a disc upper member that is spaced apart from the bottom surface of the lower chamber and supported in the horizontal direction, and is suspended from the peripheral portion of the disc upper member at a predetermined interval. It is preferable to provide a plurality of cross-sectionally U-shaped members and collect saturated water separated in the central portion while being rotated by the helical fins by these U-shaped members.

また本発明の装置において、各蒸発缶の下流側には気水分離器を接続することもできるが、該気水分離器には気水分離機構を設けるのが好ましい。かかる気水分離機構としては、気水分離器の外筒と気水分離器の中央部に挿入された先端閉鎖の内筒との間に設けられた螺旋状フィンを備えていて、かかる気水分離機構により微細水滴を含んだ純蒸気に遠心力を加えて該純蒸気から微細水滴を分離するようにしたものが好ましい。   In the apparatus of the present invention, a steam / water separator can be connected to the downstream side of each evaporator, but the steam / water separator is preferably provided with a steam / water separation mechanism. Such a steam-water separation mechanism includes a spiral fin provided between an outer cylinder of the steam-water separator and a closed inner cylinder inserted in the center of the steam-water separator. It is preferable to apply a centrifugal force to pure steam containing fine water droplets by a separation mechanism to separate the fine water droplets from the pure vapor.

更に本発明の装置において、発生する純蒸気や製造する蒸留水の非凝縮性気体の含有量を減らすため、第1蒸発缶の上部室には脱気機構を設けるのが好ましい。脱気機構としては、全体として偏平な円錐状部材を上段に備え且つ中央部に向かい降下する傾斜面を有する全体としてリング状部材を下段に備えていて、かかる脱気機構により供給水を上段の円錐状部材及び下段のリング状部材の各表面に沿って薄膜状で流しつつ脱気するようにしたものが好ましい。かかる脱気機構は、場合によっては2番目以降の蒸発缶の上部室にも設けることができる。   Furthermore, in the apparatus of the present invention, it is preferable to provide a degassing mechanism in the upper chamber of the first evaporator in order to reduce the content of the generated pure steam and the non-condensable gas of distilled water to be produced. As the deaeration mechanism, a flat conical member as a whole is provided in the upper stage, and an overall ring-shaped member having an inclined surface that descends toward the center part is provided in the lower stage. It is preferable to deaerate while flowing in a thin film along each surface of the conical member and the lower ring member. In some cases, such a deaeration mechanism can be provided in the upper chamber of the second and subsequent evaporators.

本発明によると、各蒸発缶の下部室に、各蒸発缶の加熱室で発生させた気水混合液に遠心力を加える気水分離機構を設けたため、これにより気水混合液から純蒸気を効率的に分離することができるという効果がある。   According to the present invention, since the steam / water separation mechanism is provided in the lower chamber of each evaporator, the centrifugal force is applied to the steam / water mixture generated in the heating chamber of each evaporator. There is an effect that it can be separated efficiently.

本発明の装置を例示する全体図。1 is an overall view illustrating an apparatus of the present invention. 図1の本発明の装置における第1蒸発缶の下部室とその気水分離機構を示す拡大縦断面図。The expanded longitudinal cross-sectional view which shows the lower chamber of the 1st evaporator in the apparatus of this invention of FIG. 1, and its steam-water separation mechanism. 図2の気水分離機構における螺旋状フィンを示す側面図。The side view which shows the helical fin in the steam-water separation mechanism of FIG. 図2の気水分離機構における螺旋状羽根を示す平面図。The top view which shows the spiral blade in the steam-water separation mechanism of FIG. 図1の本発明の装置における第1蒸発缶の下部室とその集液部材を示す拡大横断面図。FIG. 2 is an enlarged cross-sectional view showing a lower chamber of a first evaporator and a liquid collecting member thereof in the apparatus of the present invention shown in FIG. 1. 図1の本発明の装置における気水分離器とその気水分離機構を示す拡大縦断面図。FIG. 2 is an enlarged longitudinal sectional view showing a steam / water separator and a steam / water separation mechanism in the apparatus of the present invention of FIG. 1. 図1の本発明の装置における第1蒸発缶の上部室とその脱気機構を示す拡大縦断面図。FIG. 2 is an enlarged longitudinal sectional view showing an upper chamber of a first evaporator and a deaeration mechanism thereof in the apparatus of the present invention shown in FIG. 1.

図1にしたがって、本発明の装置を説明する。図1に例示した本発明の装置では、合計3本の第1蒸発缶70、第2蒸発缶80及び第3蒸発缶90を備えている。第1蒸発缶70、第2蒸発缶80及び第3蒸発缶90の各下流側には気水分離器75,85,95が接続されており、気水分離器95の下流側にコンデンサが接続されている。コンデンサは第1コンデンサ30と第2コンデンサ40とからなり、気水分離器95は第1コンデンサ30に接続され、第1コンデンサ30に第2コンデンサ40が接続されていて、第2コンデンサ40には蒸留水出口配管4が接続されている。   The apparatus of the present invention will be described with reference to FIG. The apparatus of the present invention illustrated in FIG. 1 includes a total of three first evaporators 70, second evaporators 80, and third evaporators 90. The steam separators 75, 85, and 95 are connected to the downstream sides of the first evaporator 70, the second evaporator 80, and the third evaporator 90, and the condenser is connected to the downstream side of the steam separator 95. Has been. The capacitor is composed of the first capacitor 30 and the second capacitor 40, the steam separator 95 is connected to the first capacitor 30, the second capacitor 40 is connected to the first capacitor 30, and the second capacitor 40 has A distilled water outlet pipe 4 is connected.

第1蒸発缶70、第2蒸発缶80及び第3蒸発缶90は、上部室70A,80A,90A、加熱室70B,80B,90B及び下部室70C,80C,90Cの大きく3室に区分されており、加熱室70B,80B,90Bには、上部室70A,80A,90Aから下部室70C,80C,90Cに渡る複数の伝熱管70D,80D,90Dが通されている。   The first evaporator 70, the second evaporator 80, and the third evaporator 90 are roughly divided into three chambers: an upper chamber 70A, 80A, 90A, a heating chamber 70B, 80B, 90B, and a lower chamber 70C, 80C, 90C. A plurality of heat transfer tubes 70D, 80D, 90D extending from the upper chambers 70A, 80A, 90A to the lower chambers 70C, 80C, 90C are passed through the heating chambers 70B, 80B, 90B.

各蒸発缶の下部室70C,80C,90Cには気水分離機構が設けられている。下部室80C,90Cの気水分離機構は下部室70Cの気水分離機構と同じになっているので、以下、下部室70Cの気水分離機構について説明する。図2及び図3に示すように、第1蒸発缶70の下部室70Cの気水分離機構は、下部室70Cの外筒70Lと下部室70Cの中央部に挿入された内筒70Mとの間に設けられた螺旋状フィン70Nを備えていて、かかる気水分離機構により気水混合液に遠心力を加えて該気水混合液から純蒸気を分離するようになっている。図1に例示した本発明の装置では、図3〜図5に示すように、下部室70Cには、螺旋状フィン70Nの上方に、螺旋状フィン70Nと同じ方向へ旋回する螺旋状羽根70Kが設けられており、また螺旋状フィン70Nの下方に、螺旋状フィン70Nで回転しながら分離されてくる飽和水を中央部に集めて下部室70Cから排出し易くするための集液部材70Pが設けられている。図示した本発明の装置の場合、集液部材70Pは、下部室70Cを形成する底面から離間して水平方向に支持された円板上部材70Qと、円板上部材70Qの下面周縁部から突出して垂設された合計4本の横断面くの字状部材70Rとを備え、かかるくの字状部材70Rにより、回転しながら分離されてくる飽和水を中央部に集めるようになっている。   A steam / water separation mechanism is provided in the lower chambers 70C, 80C, and 90C of each evaporator. Since the air / water separation mechanism of the lower chambers 80C and 90C is the same as the air / water separation mechanism of the lower chamber 70C, the air / water separation mechanism of the lower chamber 70C will be described below. As shown in FIGS. 2 and 3, the air / water separation mechanism of the lower chamber 70C of the first evaporator 70 is formed between an outer cylinder 70L of the lower chamber 70C and an inner cylinder 70M inserted in the center of the lower chamber 70C. A spiral fin 70N provided on the air-water mixture is provided, and the air-water mixture is subjected to centrifugal force by the air-water separation mechanism to separate pure steam from the air-water mixture. In the apparatus of the present invention illustrated in FIG. 1, as shown in FIGS. 3 to 5, in the lower chamber 70 </ b> C, a spiral blade 70 </ b> K swirling in the same direction as the spiral fin 70 </ b> N is disposed above the spiral fin 70 </ b> N. Also provided below the spiral fin 70N is a liquid collection member 70P for collecting saturated water separated while rotating by the spiral fin 70N in the central portion and facilitating discharge from the lower chamber 70C. It has been. In the case of the illustrated apparatus of the present invention, the liquid collection member 70P protrudes from a disk upper member 70Q supported in a horizontal direction spaced apart from the bottom surface forming the lower chamber 70C, and a lower surface peripheral portion of the disk upper member 70Q. A total of four U-shaped members 70R having a transverse cross section are provided, and by these U-shaped members 70R, saturated water separated while rotating is collected in the central portion.

また各蒸発缶の下流側に接続された気水分離器75,85,95にも気水分離機構が設けられている。気水分離器85,95の気水分離機構は気水分離器75の気水分離機構と同じになっているので、以下、気水分離器75の気水分離機構について説明する。図5に示すように、気水分離器75の気水分離機構は、気水分離器75の外筒75Jと気水分離器75の中央部に挿入された先端閉鎖の内筒75Kとの間に設けられた螺旋状フィン75Lを備えており、この螺旋状フィン75Lは前記の螺旋状フィン70Nと同様の構成になっていて、かかる気水分離機構により微細水滴を含んだ純蒸気に遠心力を加えて純蒸気から微細水滴を分離するようになっている。   The steam separators 75, 85, and 95 connected to the downstream side of each evaporator also have a steam / water separation mechanism. Since the steam-water separation mechanism of the steam-water separators 85 and 95 is the same as the steam-water separation mechanism of the steam-water separator 75, the steam-water separation mechanism of the steam-water separator 75 will be described below. As shown in FIG. 5, the steam / water separation mechanism of the steam / water separator 75 is formed between an outer cylinder 75 </ b> J of the steam / water separator 75 and an inner cylinder 75 </ b> K with a closed tip inserted in the center of the steam / water separator 75. The spiral fin 75L has the same configuration as that of the spiral fin 70N, and a centrifugal force is applied to pure steam containing fine water droplets by the air-water separation mechanism. Is added to separate fine water droplets from pure steam.

更に第1蒸発缶70の上部室70Aには脱気機構が設けられている。この脱気機構は、上蓋70Uに合計3本の平板状の支持部材70Vで支持された全体として円錐状部材70Sを上段に備え且つ上部室70Aの外筒70Wに支持された中央部に向かい降下する傾斜面を有する全体としてリング状部材70Tを下段に備えていて、かかる脱気機構により供給水を薄膜状に落下させて脱気するようになっている。   Further, a deaeration mechanism is provided in the upper chamber 70 </ b> A of the first evaporator 70. This deaeration mechanism includes a conical member 70S as a whole supported by a total of three flat plate-like support members 70V on the upper lid 70U, and descends toward the center supported by the outer cylinder 70W of the upper chamber 70A. A ring-shaped member 70T as a whole having an inclined surface is provided in the lower stage, and the degassing mechanism causes the supply water to fall into a thin film shape for deaeration.

図1に基づいて本発明の装置を更に詳細に説明する。図1において、1は供給水入口配管であり、第1コンデンサ30の供給水入口ノズルに接続されている。供給水入口配管1には、供給水ポンプ1B、圧力センサ1C、流量計1D、自動式開閉弁1E及び手動式の水量調整弁1Fが介装されている。   The device of the present invention will be described in more detail with reference to FIG. In FIG. 1, reference numeral 1 denotes a supply water inlet pipe, which is connected to a supply water inlet nozzle of the first condenser 30. The supply water inlet pipe 1 is provided with a supply water pump 1B, a pressure sensor 1C, a flow meter 1D, an automatic on-off valve 1E, and a manual water amount adjustment valve 1F.

第1コンデンサ30は、第2コンデンサ40と共に、蒸留水製造運転中に蒸留水となる純蒸気を冷却及び凝縮するものであり、共に二重管板式多管円筒型熱交換器である。第1コンデンサ30において、供給水入口配管1の供給水は第1コンデンサ30の伝熱管を通過する際は冷却用として用いられ、自らは加熱される。また第2コンデンサ40において、冷却水入口配管8より送られる冷却水は、第2コンデンサ40の伝熱管を経て内部を冷却し、自らは加熱されて冷却水出口配管9より排出される。8Cは第2コンデンサ40から出る製造した蒸留水の温度を後述の温度センサ4Bにて設定温度(例えば95〜105℃)に保持するように冷却水量を調節するための比例式制御弁である。   The 1st capacitor | condenser 30 cools and condenses the pure vapor | steam used as distilled water during the distilled water manufacture driving | operation with the 2nd capacitor | condenser 40, Both are double tube plate type multi-tube cylindrical heat exchangers. In the first condenser 30, the supply water of the supply water inlet pipe 1 is used for cooling when passing through the heat transfer pipe of the first condenser 30 and is heated by itself. In the second condenser 40, the cooling water sent from the cooling water inlet pipe 8 cools the inside through the heat transfer pipe of the second condenser 40, and is heated and discharged from the cooling water outlet pipe 9. 8C is a proportional control valve for adjusting the amount of cooling water so that the temperature of distilled water produced from the second condenser 40 is maintained at a set temperature (for example, 95 to 105 ° C.) by a temperature sensor 4B described later.

第1コンデンサ30には気水分離器95から送られてくる純蒸気の入口が設けられており、また第3蒸発缶90の加熱室90Bで製造された凝縮水の入口が設けられている。第1コンデンサ30の内部に導入された純蒸気及び凝縮水は第1コンデンサ30の伝熱管により凝縮及び冷却されて蒸留水となり、第1コンデンサ30下部の蒸留水出口より排出され、下段に設けられた第2コンデンサ40に入る。   The first condenser 30 is provided with an inlet for pure steam sent from the steam separator 95 and an inlet for condensed water produced in the heating chamber 90 </ b> B of the third evaporator 90. Pure steam and condensed water introduced into the first condenser 30 are condensed and cooled by the heat transfer tube of the first condenser 30 to be distilled water, discharged from the distilled water outlet at the lower part of the first condenser 30, and provided in the lower stage. The second capacitor 40 is entered.

第1コンデンサ30上部には、蒸留水製造運転中、第1コンデンサ30内に蓄積した非凝縮性気体を抜くための非凝縮性気体抜き口が設けられており、非凝縮性気体抜き口には非凝縮性気体出口配管6が接続されている。非凝縮性気体出口配管6には、非凝縮性気体を抜く方向に作用する逆止弁6C及び手動弁6Dが介装されている。蒸留水製造を休止する場合、第2コンデンサ40の伝熱管に冷却水を供給して装置内部に残留する純蒸気を凝縮させると、内部が負圧になる傾向になる。かかる負圧を防ぐために、外気吸込配管15から外気を吸込み、ベントフィルタ6Fで外気に含まれた微生物や微粒子を取り除いた後、逆止弁6Bを介して装置内部に外気を入れ、内部が負圧になるのを防ぐ。逆止弁6Bは外気の導入のみを許す逆止弁である。ベントフィルタ6Fは、気水分離器75と第2蒸発缶80とを接続する蒸気配管76から分岐した配管77を介して導入される純蒸気にて蒸気滅菌することができる。このときの純蒸気は、第1蒸発缶70の上部室70Aに設けた前記の脱気機構により非凝縮性気体を除去して非凝縮性気体の含有量を少なくしたもので、蒸気滅菌に用いるのに適している。   The upper part of the first condenser 30 is provided with a non-condensable gas vent for removing the non-condensable gas accumulated in the first condenser 30 during the distilled water production operation. A non-condensable gas outlet pipe 6 is connected. The non-condensable gas outlet pipe 6 is provided with a check valve 6C and a manual valve 6D that act in the direction of extracting the non-condensable gas. When the production of distilled water is suspended, if the cooling water is supplied to the heat transfer tube of the second condenser 40 to condense the pure steam remaining inside the apparatus, the inside tends to become negative pressure. In order to prevent such negative pressure, outside air is sucked in from the outside air suction pipe 15 and microorganisms and fine particles contained in the outside air are removed by the vent filter 6F, and then outside air is introduced into the apparatus through the check valve 6B. Prevent pressure. The check valve 6B is a check valve that allows only the introduction of outside air. The vent filter 6 </ b> F can be steam sterilized with pure steam introduced through a pipe 77 branched from the steam pipe 76 connecting the steam separator 75 and the second evaporator 80. The pure steam at this time is obtained by removing the non-condensable gas by the deaeration mechanism provided in the upper chamber 70A of the first evaporator 70 to reduce the content of the non-condensable gas, and is used for steam sterilization. Suitable for

第1コンデンサ30下部には排出口が設けられており、第1コンデンサ30内部で凝縮されなかった純蒸気及び凝縮水を第2コンデンサ40に排出する。第2コンデンサ40上部には受け口が設けられており、この受け口から第1コンデンサ30内部で凝縮されなかった純蒸気及び凝縮水が流入する。流入した純蒸気は第2コンデンサ40の伝熱管にて残らず凝縮され、第1コンデンサ30から流入した凝縮水と共に蒸留水出口配管4から排出される。このとき、温度センサ4Bの設定温度(通常は95〜105℃)を保持するように、冷却水量が調節される。   A discharge port is provided at the lower portion of the first capacitor 30, and pure steam and condensed water that have not been condensed inside the first capacitor 30 are discharged to the second capacitor 40. A receiving port is provided in the upper part of the second capacitor 40, and pure steam and condensed water that have not been condensed inside the first capacitor 30 flow from the receiving port. The pure steam that has flowed in is condensed in the heat transfer tube of the second condenser 40 and is discharged from the distilled water outlet pipe 4 together with the condensed water that has flowed in from the first condenser 30. At this time, the cooling water amount is adjusted so as to maintain the set temperature of the temperature sensor 4B (usually 95 to 105 ° C.).

第1コンデンサ30は、排熱回収器50及び予熱器60を介して第1蒸発缶70に接続され、供給水を第1蒸発缶に供給する。排熱回収器50及び予熱器60は共に二重管板式多管円筒型熱交換器である。排熱回収器50には、予熱器60及び第1蒸発缶70の蒸気ドレンを受ける口が設けられており、供給水はかかる排熱回収器50及び予熱器60にて予熱された後、予熱された高温の供給水となって第1蒸発缶70に供給される。一方、熱回収済みの蒸気ドレンは温度が下がり、逆止弁3Bを介して蒸気ドレン出口配管3から流出する。図1において、2は予熱器60及び第1蒸発缶70の加熱室70Bに蒸気を供給する蒸気入口配管であり、2Bは手動開閉弁である。また71は加熱室70Bの蒸気ドレンを排出する蒸気ドレン排出配管であり、71Aは蒸気トラップ、71Bは逆止弁である。   The first condenser 30 is connected to the first evaporator 70 via the exhaust heat recovery device 50 and the preheater 60, and supplies supply water to the first evaporator. Both the exhaust heat recovery device 50 and the preheater 60 are double tube plate type multi-tube cylindrical heat exchangers. The exhaust heat recovery device 50 is provided with a port for receiving the steam drain of the preheater 60 and the first evaporator 70, and the supplied water is preheated by the exhaust heat recovery device 50 and the preheater 60 and then preheated. The high temperature supplied water is supplied to the first evaporator 70. On the other hand, the temperature of the steam drain that has been heat-recovered decreases, and flows out of the steam drain outlet pipe 3 via the check valve 3B. In FIG. 1, 2 is a steam inlet pipe for supplying steam to the preheater 60 and the heating chamber 70B of the first evaporator 70, and 2B is a manual on-off valve. 71 is a steam drain discharge pipe for discharging the steam drain of the heating chamber 70B, 71A is a steam trap, and 71B is a check valve.

第1蒸発缶70は、供給された供給水の一部を加熱蒸気との熱交換により効率よく蒸発させて純蒸気とする二重管板式多管円筒型熱交換器であり、予熱供給水が導入される上部室70Aと、加熱蒸気が導入される加熱室70Bと、純蒸気と飽和水との気水混合液が導入される下部室70Cとに区分されていて、加熱室70Bには上部室70Aの予熱供給水を下部室70Cに導く複数の伝熱管70Dが挿設されている。加熱室70B上部には加熱蒸気の供給口が設けられており、また加熱室70B下部には加熱蒸気のドレンを缶外に導く蒸気ドレン排出配管71が接続されている。蒸気ドレン排出配管71の排出側端部は排熱回収器50に接続されている。そして、下部室70C上部には純蒸気排出口が設けられており、また底部には蒸発しなかつた飽和水の飽和水排出口が設けられている。   The first evaporator 70 is a double tube plate type multi-tube cylindrical heat exchanger that efficiently evaporates a part of the supplied water by heat exchange with heating steam to obtain pure steam. It is divided into an upper chamber 70A to be introduced, a heating chamber 70B into which heated steam is introduced, and a lower chamber 70C into which a gas / water mixture of pure steam and saturated water is introduced. A plurality of heat transfer tubes 70D for guiding the preheated water supplied from the chamber 70A to the lower chamber 70C are inserted. A heating steam supply port is provided in the upper part of the heating chamber 70B, and a steam drain discharge pipe 71 that guides the drain of the heating steam to the outside of the can is connected to the lower part of the heating chamber 70B. The discharge side end of the steam drain discharge pipe 71 is connected to the exhaust heat recovery unit 50. The upper portion of the lower chamber 70C is provided with a pure steam discharge port, and the bottom portion is provided with a saturated water discharge port that has not evaporated.

第1蒸発缶70の上部室70Aに入った予熱供給水は、ここで図7について前記した脱気機構により脱気された後、伝熱管70Dを経て下部室70Cに至る間に加熱室70Bの加熱蒸気により加熱されて気液混合状態となり、下部室70Cに落下し、ここで図2〜図5について前記した気水分離機構により純蒸気と飽和水とに分離され、純蒸気は上昇して上部の蒸気排出口に至り、飽和水は下降して下部の飽和水排出口より排出される。72は飽和水配管であって、一端が第1蒸発缶70底部の飽和水排出口に接続され、また他端が第2蒸発缶80の上部室80A上部の接続口に接続されていて、飽和水が第2蒸発缶80の上部室80Aに供給されるようになっている。72Aは飽和水配管72に設けられたオリフイスであって、飽和水配管72のパッキンを介して所定孔径のオリフイス孔を有するオリフイス板が介装されたものからなっている。後述する各オリフイスも同様の構造となっているが、それぞれのオリフイスによって所定の孔径ものが選定される。   The preheated water that has entered the upper chamber 70A of the first evaporator 70 is degassed by the degassing mechanism described above with reference to FIG. 7, and then passes through the heat transfer tube 70D to reach the lower chamber 70C. It is heated by the heated steam to be in a gas-liquid mixed state and falls into the lower chamber 70C where it is separated into pure steam and saturated water by the steam-water separation mechanism described above with reference to FIGS. It reaches the upper steam outlet and the saturated water descends and is discharged from the lower saturated water outlet. 72 is a saturated water pipe, one end of which is connected to the saturated water discharge port at the bottom of the first evaporator 70 and the other end is connected to the connection port of the upper chamber 80A of the second evaporator 80, Water is supplied to the upper chamber 80 </ b> A of the second evaporator 80. Reference numeral 72A denotes an orifice provided in the saturated water pipe 72, and an orifice plate having an orifice hole with a predetermined hole diameter is interposed through a packing of the saturated water pipe 72. Each of the orifices to be described later has the same structure, but each orifice has a predetermined hole diameter.

第1蒸発缶70の純蒸気排出口と第2蒸発缶80の加熱室80Bの蒸気供給口との間には、気水分離器75を介して第2蒸発缶の加熱源となる純蒸気を送る蒸気配管73が接続されている。気水分離器75に送られた純蒸気は、ここで図6について前記した気水分離機構により微細水滴が除去され、除去された微細水滴はオリフイス75Dを介して第2蒸発缶80の下部室80Cに入る。   Between the pure steam discharge port of the first evaporator 70 and the steam supply port of the heating chamber 80B of the second evaporator 80, pure steam serving as a heating source of the second evaporator is passed through the steam / water separator 75. A steam pipe 73 to be sent is connected. From the pure steam sent to the steam separator 75, fine water droplets are removed by the steam / water separation mechanism described above with reference to FIG. 6, and the removed fine water droplets are placed in the lower chamber of the second evaporator 80 via the orifice 75D. Enter 80C.

第2蒸発缶80は、第1蒸発缶70と異なり、二重管板を持たない多管円筒型熱交換器である、上部室80Aに入った前記の飽和水は伝熱管80Dを経て下部室80Cに至る間に、加熱室80Bの純蒸気により加熱され、気液混合状態となって下部室80Cに落下し、気液混合液は下部室60Cにて第1蒸発缶70の下部室70Cと同じ気水分離機構にて純蒸気と飽和水とに分離され、純蒸気は上昇して上部の蒸気排出口に至り、飽和水は下降して下部の飽和水排出口より排出される。82は飽和水配管であって、一端が第2蒸発缶80底部の飽和水排出口に接続され、また他端が第3蒸発缶90の上部室90Aの接続口に接続されていて、飽和水が第3蒸発缶90の上部室90Aに供給されるようになっている。82Aは飽和水配管82に設けられたオリフイスである。   Unlike the first evaporator 70, the second evaporator 80 is a multi-tube cylindrical heat exchanger that does not have a double tube plate, and the saturated water that has entered the upper chamber 80A passes through the heat transfer tube 80D to the lower chamber. While reaching 80C, it is heated by pure steam in the heating chamber 80B, becomes a gas-liquid mixed state and falls into the lower chamber 80C, and the gas-liquid mixed solution is separated from the lower chamber 70C of the first evaporator 70 in the lower chamber 60C. It is separated into pure steam and saturated water by the same steam separation mechanism, and the pure steam rises to reach the upper steam discharge port, and the saturated water descends and is discharged from the lower saturated water discharge port. 82 is a saturated water pipe, one end of which is connected to the saturated water discharge port at the bottom of the second evaporator 80 and the other end is connected to the connection port of the upper chamber 90 </ b> A of the third evaporator 90. Is supplied to the upper chamber 90 </ b> A of the third evaporator 90. 82 A is an orifice provided in the saturated water pipe 82.

81は凝縮水配管であって、第2蒸発缶80の加熱室80Bでの熱交換により生成した凝縮水を第3蒸発缶90の加熱室90Bの下部に導くものであり、81Aは凝縮水配管81に介装されたオリフイスである。第2蒸発缶80の蒸気排出口と第3蒸発缶90の加熱室90Bの蒸気供給口とは蒸気配管83で接続されており、蒸気配管83には気水分離器75と同様の構造の気水分離器85が介装されていて、気水分離器85で除去された微細水滴はオリフイス86Aを介して第3蒸発缶の下部室90Cに入るようになっている。   81 is a condensate water pipe that guides the condensed water generated by heat exchange in the heating chamber 80B of the second evaporator 80 to the lower part of the heating chamber 90B of the third evaporator 90, and 81A is a condensate water pipe. This is an orifice installed in 81. The steam outlet of the second evaporator 80 and the steam supply port of the heating chamber 90 </ b> B of the third evaporator 90 are connected by a steam pipe 83, and the steam pipe 83 has the same structure as the steam separator 75. A water separator 85 is interposed, and fine water droplets removed by the steam separator 85 enter the lower chamber 90C of the third evaporator through the orifice 86A.

第3蒸発缶90の構造は第2蒸発缶80と同様になっており、飽和水配管82にて供給される飽和水を蒸気との熱交換により一部蒸発させ、更に純蒸気と飽和水との気水混合液とする蒸発缶である。第3蒸発缶90は、飽和水が導入される上部室90Aと、蒸気が導入される加熱室90Bと、気水混合液が導入される下部室90Cとに区分されている。加熱室90Bには上部室90Aの飽和水を下部室90Cに導く伝熱管90Dが挿設されており、また加熱室90Bには純蒸気を導入する供給口と、熱交換により凝縮された純蒸気の凝縮水を底部より缶外に排出する凝縮水排出配管91が設けられている。下部室90C上部には蒸気排出口が設けられており、また下部室90Cの底部には飽和水排出口が設けられている。第3蒸発缶90では、上部室90Aに入った飽和水は伝熱管90Dを経て下部室90Eに至る間に、加熱室90Bの純蒸気により加熱され、気水混合液となって、下部室90Cに落下し、ここで第1蒸発缶70の下部室70Cと同じ気水分離機構にて純蒸気と飽和水に分けられ、蒸気は下部室90Cの上部の蒸気排出口に至る。   The structure of the third evaporator 90 is the same as that of the second evaporator 80. The saturated water supplied by the saturated water pipe 82 is partially evaporated by heat exchange with the steam, and further, pure steam and saturated water It is an evaporator used as an air-water mixture. The third evaporator 90 is divided into an upper chamber 90A into which saturated water is introduced, a heating chamber 90B into which steam is introduced, and a lower chamber 90C into which an air / water mixture is introduced. The heating chamber 90B is provided with a heat transfer tube 90D for introducing saturated water from the upper chamber 90A to the lower chamber 90C. The heating chamber 90B has a supply port for introducing pure steam and pure steam condensed by heat exchange. A condensed water discharge pipe 91 for discharging the condensed water from the bottom to the outside of the can is provided. A steam discharge port is provided at the upper part of the lower chamber 90C, and a saturated water discharge port is provided at the bottom of the lower chamber 90C. In the third evaporator 90, the saturated water that has entered the upper chamber 90A passes through the heat transfer tube 90D and reaches the lower chamber 90E, and is heated by the pure steam in the heating chamber 90B to become a gas-water mixture, thereby forming the lower chamber 90C. Here, the steam is separated into pure steam and saturated water by the same steam separation mechanism as the lower chamber 70C of the first evaporator 70, and the steam reaches the steam outlet at the upper part of the lower chamber 90C.

7は飽和水出口配管であり、7Bは自動式開閉弁、7Cはオリフイスである。91は凝縮水配管であり、熱交換による凝縮水を第1コンデンサ30の凝縮水入口に送るものであって、91Aはオリフイスである。93は気水分離器95を介して純蒸気を第1コンデンサ30に送る蒸気配管である。気水分離器95で除去された微細水滴は蒸気トラップ96A及び逆止弁96Bを介して飽和水出口配管7に合流している。第3蒸発缶90で発生した蒸気は気水分離器95を介して第1コンデンサ30に流入する。   7 is a saturated water outlet pipe, 7B is an automatic on-off valve, and 7C is an orifice. 91 is a condensate water pipe, which sends condensate by heat exchange to the condensate inlet of the first condenser 30, and 91A is an orifice. A steam pipe 93 sends pure steam to the first condenser 30 through the steam separator 95. The fine water droplets removed by the steam separator 95 merge into the saturated water outlet pipe 7 via the steam trap 96A and the check valve 96B. The steam generated in the third evaporator 90 flows into the first condenser 30 via the steam separator 95.

4は第2コンデンサ40下部の蒸留水出口に接続され、蒸留水を外部に導くための蒸留水出口配管である。蒸留水出口配管4は一部U字形状に配設されている。4Cは蒸留水出口配管4に介装された水質センサであって、蒸留水の導電率が計測可能となっている。4Bは蒸留水出口配管4に取付けられた温度調節計と電気的に繋がっている温度センサであり、例えば95〜105℃の設定温度に設定され、第2コンデンサ40に接続された冷却水入口配管8の比例制御弁8Cに電気的に連係されていて、蒸留水出口配管4の蒸留水の温度が所定温度を越えた場合に作動して冷却水の流入水量を制御するようになっている。4Dは蒸留水出口配管4に介装された自動式開閉弁であり、5は蒸留水出口配管4の自動式開閉弁4Dの上流位置で分岐された廃蒸留水出口配管であって、水質センサ4Cの測定結果が設定の水質値以上の場合は蒸留水出口配管4の自動式開閉弁4Dが開、廃蒸留水出口配管5の自動式開閉弁5Bが閉にされ、蒸留水が蒸留水出口配管4より排出される。そして水質センサ4Cの測定結果が設定の水質値以下の場合は蒸留水出口配管4の開閉弁4Dが閉、廃蒸留水出口配管5の開閉弁5Bが開にされ、水質基準に合わない蒸留水は廃蒸留水出口配管5より排出される。   Reference numeral 4 denotes a distilled water outlet pipe connected to the distilled water outlet at the lower part of the second condenser 40 to guide distilled water to the outside. The distilled water outlet pipe 4 is partially U-shaped. 4C is a water quality sensor interposed in the distilled water outlet pipe 4, and the conductivity of distilled water can be measured. 4B is a temperature sensor that is electrically connected to a temperature controller attached to the distilled water outlet pipe 4, and is set to a set temperature of 95 to 105 ° C., for example, and is connected to the second condenser 40. Eight proportional control valves 8C are electrically linked to operate when the temperature of distilled water in the distilled water outlet pipe 4 exceeds a predetermined temperature to control the inflow amount of cooling water. 4D is an automatic opening / closing valve interposed in the distilled water outlet pipe 4, 5 is a waste distilled water outlet pipe branched at an upstream position of the automatic opening / closing valve 4D of the distilled water outlet pipe 4, and is a water quality sensor. When the measurement result of 4C is equal to or higher than the set water quality value, the automatic opening / closing valve 4D of the distilled water outlet pipe 4 is opened, the automatic opening / closing valve 5B of the waste distilled water outlet pipe 5 is closed, and the distilled water is discharged from the distilled water outlet. It is discharged from the pipe 4. If the measurement result of the water quality sensor 4C is below the set water quality value, the on-off valve 4D of the distilled water outlet pipe 4 is closed, the on-off valve 5B of the waste distilled water outlet pipe 5 is opened, and distilled water that does not meet the water quality standard Is discharged from the waste distilled water outlet pipe 5.

以上、蒸発缶と気水分離器を各3本備える場合について図面に基づき本発明の装置を説明したが、蒸発缶と気水分離器がそれ以上に多い例えば4〜7本の場合でも同様である。   As mentioned above, although the apparatus of this invention was demonstrated based on drawing about the case where each is equipped with three evaporators and a steam-water separator, it is the same also in the case where there are more evaporators and steam-water separators, for example, 4-7. is there.

1 供給水入口配管
2 加熱用の蒸気入口配管
3 蒸気ドレン出口配管
4 蒸留水出口配管
5 廃蒸留水出口配管
6 非凝縮性気体出口配管
7 飽和水出口配管
8 冷却水入口配管
9 冷却水出口配管
15 外気入口配管
30 第1コンデンサ
40 第2コンデンサ
50 排熱回収器
60 予熱器
70 第1蒸発缶
80 第2蒸発缶
90 第3蒸発缶
70K 螺旋状羽根
70N,75L 螺旋状フィン
70P 集液部材
70Q 円板状部材
70R くの字状部材
70S 円錐状部材
70T リング状部材
75,85,95 気水分離器
1 Supply water inlet piping 2 Heating steam inlet piping 3 Steam drain outlet piping 4 Distilled water outlet piping 5 Waste distilled water outlet piping 6 Non-condensable gas outlet piping 7 Saturated water outlet piping 8 Cooling water inlet piping 9 Cooling water outlet piping 15 External air inlet pipe 30 1st capacitor 40 2nd capacitor 50 Waste heat recovery device 60 Preheater 70 1st evaporation can 80 2nd evaporation can 90 3rd evaporation can 70K Spiral blade 70N, 75L Spiral fin 70P Liquid collection member 70Q Disc-shaped member 70R U-shaped member 70S Conical member 70T Ring-shaped member 75, 85, 95 Air-water separator

Claims (3)

供給水の予熱手段と、予熱した供給水から気水混合液を順次発生させる複数の蒸発缶と、発生させた気水混合液の気水分離手段と、気水分離した純蒸気を供給水及び冷却水で冷却して蒸留水とするコンデンサと、コンデンサに接続された外気導入手段とを備える多重効用缶式蒸留水製造装置において、各蒸発缶の下部室に気水分離機構が設けられており、該気水分離機構は、下部室の外筒と下部室の中央部に挿入された内筒との間に設けられた螺旋状フィンを備えていて、かかる気水分離機構により気水混合液に遠心力を加えて該気水混合液から純蒸気を分離するようにして成ることを特徴とする多重効用缶式蒸留水製造装置。   Supply water preheating means, a plurality of evaporators that sequentially generate an air / water mixture from the preheated supply water, an air / water separation means for the generated air / water mixture, and air / water separated pure steam as supply water and In a multi-effect can-type distilled water production apparatus comprising a condenser that is cooled with cooling water to form distilled water, and an outside air introduction means connected to the condenser, a steam-water separation mechanism is provided in the lower chamber of each evaporator. The air / water separation mechanism includes a spiral fin provided between the outer cylinder of the lower chamber and the inner cylinder inserted in the central portion of the lower chamber, and the air / water mixture is provided by the air / water separation mechanism. A multi-effect can-type distilled water production apparatus characterized in that a pure steam is separated from the gas-water mixture by applying a centrifugal force. 各蒸発缶の下流側に気水分離器が接続され、該気水分離器には気水分離機構が設けられており、該気水分離機構は、気水分離器の外筒と気水分離器の中央部に挿入された先端閉鎖の内筒との間に設けられた螺旋状フィンを備えていて、かかる気水分離機構により微細水滴を含んだ純蒸気に遠心力を加えて該純蒸気から該微細水滴を分離するようにした請求項1記載の多重効用缶式蒸留水製造装置。   A steam separator is connected to the downstream side of each evaporator, and the steam separator is provided with a steam separator. The steam separator is separated from the outer cylinder of the steam separator. A spiral fin provided between the inner cylinder of the closed end inserted in the center of the vessel, and the pure steam containing fine water droplets is subjected to centrifugal force by such a steam-water separation mechanism. The multi-effect can type distilled water producing apparatus according to claim 1, wherein the fine water droplets are separated from the water. 第1蒸発缶の上部室に脱気機構が設けられており、該脱気機構は、全体として偏平な円錐状部材を上段に備え且つ中央部に向かい降下する傾斜面を有する全体としてリング状部材を下段に備えていて、かかる脱気機構により供給水を脱気するようにした請求項1又は2記載の多重効用缶式蒸留水製造装置。   A deaeration mechanism is provided in the upper chamber of the first evaporator, and the deaeration mechanism as a whole has a generally flat conical member in the upper stage and has an inclined surface that descends toward the center as a whole. The multi-effect can type distilled water production apparatus according to claim 1, wherein the feed water is degassed by the degassing mechanism.
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CN107537168A (en) * 2017-10-19 2018-01-05 榆林学院 A kind of regulation and control fixed gas scapus dynamic characteristic promotes the device of steam condensation

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