JP2012082107A - Plate glass forming apparatus and method of forming glass sheet - Google Patents
Plate glass forming apparatus and method of forming glass sheet Download PDFInfo
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03B—MANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
- C03B17/00—Forming molten glass by flowing-out, pushing-out, extruding or drawing downwardly or laterally from forming slits or by overflowing over lips
- C03B17/06—Forming glass sheets
- C03B17/064—Forming glass sheets by the overflow downdraw fusion process; Isopipes therefor
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Abstract
Description
本発明は溶融ガラスを板状に成形するための板ガラス成形装置及びそれを用いた板ガラスの成形方法に関する。 The present invention relates to a sheet glass forming apparatus for forming molten glass into a plate shape and a method for forming a sheet glass using the same.
一般に、薄い板ガラスを製造する場合、断面が略くさび形の成形体の上部に形成されたオーバーフロー溝に溶融ガラスを供給し、溶融ガラスをオーバーフロー溝の両側から溢れさせて成形体の両側の側壁面を流下させた後、各々の溶融ガラスを成形体の下頂部で融合させて板状に成形し、切断して板ガラスを得る方法が知られている。この成形方法は一般にオーバーフローダウンドロー法と呼ばれている。 In general, when manufacturing thin plate glass, molten glass is supplied to an overflow groove formed on the upper part of a substantially wedge-shaped molded body, and the molten glass is overflowed from both sides of the overflow groove to form side wall surfaces on both sides of the molded body. After flowing down, a method is known in which each molten glass is fused at the lower top of the molded body, formed into a plate shape, and cut to obtain a plate glass. This forming method is generally called an overflow down draw method.
上記の成形方法に用いられる成形装置は、図3に示すように、保温壁1により形成される成形室1a内に、断面が略くさび形であり頂部にオーバーフロー溝2aを有する成形体2を配置し、成形体2のオーバーフロー溝2aに溶融ガラスGを供給し、溢れさせて成形体2の両側の側壁面2bを流下させ、成形体2の下頂部2cで融合させることにより板状ガラスSGを成形し、開口部1bを通して引き出されるようになっており、成形体2の両側に発熱体3を配置した構造になっている。 As shown in FIG. 3, the molding apparatus used in the above molding method arranges a molded body 2 having a substantially wedge-shaped cross section and an overflow groove 2a at the top in a molding chamber 1a formed by a heat insulating wall 1. Then, the molten glass G is supplied to the overflow groove 2a of the molded body 2, overflowed, the side wall surfaces 2b on both sides of the molded body 2 are caused to flow down, and fused at the lower top portion 2c of the molded body 2, whereby the sheet glass SG is obtained. The molded body is drawn out through the opening 1b, and has a structure in which the heating element 3 is disposed on both sides of the molded body 2.
この方法及び装置は、液晶ディスプレイ用ガラス基板、有機ELディスプレイ用ガラス基板、太陽電池用カバーガラス、タッチパネル用カバーガラス等、薄肉の板ガラスの製造に適している。 This method and apparatus are suitable for the production of thin plate glasses such as glass substrates for liquid crystal displays, glass substrates for organic EL displays, cover glasses for solar cells, cover glasses for touch panels, and the like.
オーバーフローダウンドロー法で板ガラスを成形する場合、成形体下頂部付近でガラスの温度が低下して失透が発生するという問題がある。この問題を解決する方法として、成形体、特に成形体下頂部を加熱する方法を採用することが有効である。特許文献1〜5には成形体を加熱する方法が開示されている。 In the case of forming a sheet glass by the overflow down draw method, there is a problem in that devitrification occurs due to the temperature of the glass being lowered near the lower top of the formed body. As a method for solving this problem, it is effective to employ a method of heating the molded body, particularly the lower top portion of the molded body. Patent Documents 1 to 5 disclose methods for heating a molded body.
特許文献1には、流体制御体(本発明の成形体に相当)内に発熱体を設け、その発熱によって流体制御体表面を間接加熱する構成が開示されている。ところがこの構成では、発熱体の両側に電流供給用のターミナルを設置する必要があり、設備的な制約がある。また発熱体が流体制御体中心部に埋め込まれた状態にあることから、流体制御部の下頂部を所望の温度に調節することが困難である。 Patent Document 1 discloses a configuration in which a heating element is provided in a fluid control body (corresponding to the molded body of the present invention), and the surface of the fluid control body is indirectly heated by the heat generation. However, in this configuration, it is necessary to install terminals for supplying current on both sides of the heating element, and there are equipment limitations. Further, since the heating element is embedded in the central portion of the fluid control body, it is difficult to adjust the lower top portion of the fluid control section to a desired temperature.
特許文献2には、成形体の下端縁部(本発明の成形体下頂部に相当)に白金等からなる加熱源を配置し、通電することによって下端縁部を直接加熱する構成が開示されている。ところがこの加熱源は電源に接続される必要があり、設備的な制約があるだけでなく、ターミナルからの放熱があるため幅方向で均一に加熱することが困難である。 Patent Document 2 discloses a configuration in which a heating source made of platinum or the like is disposed at the lower edge of the molded body (corresponding to the lower top of the molded body of the present invention), and the lower edge is directly heated by energization. Yes. However, this heating source needs to be connected to a power source, which is not only limited in terms of equipment but also difficult to heat uniformly in the width direction due to heat radiation from the terminal.
特許文献3には、フュージョンセル(本発明の成形体に相当)表面に形成された白金被膜に通電加熱してフュージョンセルを直接加熱する構成が開示されている。ところがこの構成では、加熱エリアを細分化し、必要な部分のみを加熱することが困難である。 Patent Document 3 discloses a configuration in which a fusion cell is directly heated by energizing and heating a platinum coating formed on the surface of a fusion cell (corresponding to the molded body of the present invention). However, with this configuration, it is difficult to subdivide the heating area and heat only necessary portions.
特許文献4には、成形用楔状体(本発明の成形体に相当)の先端近傍(本発明の成形体下頂部に相当)内部に白金等からなる導電性部材を組み込み、或いは楔状体先端部を導電性部材で形成し、これらを通電することによって先端部を加熱する構成が開示されている。ところがこの導電性部材は電源に接続される必要があり、設備的な制約があるだけでなく、ターミナルからの放熱があるため幅方向で均一に加熱することが困難である。 In Patent Document 4, a conductive member made of platinum or the like is incorporated in the vicinity of the tip of the wedge-shaped body for molding (corresponding to the molded body of the present invention) (corresponding to the lower top of the molded body of the present invention), or the tip of the wedge-shaped body The structure which heats a front-end | tip part by forming these with an electroconductive member and energizing these is disclosed. However, this conductive member needs to be connected to a power source, and is not only limited in terms of equipment, but is also difficult to heat uniformly in the width direction due to heat radiation from the terminal.
特許文献5には、成形体先端部を、成形体の耐火物が吸収する周波数のエネルギーを照射して加熱する構成が記載されている。ところがこの構成では、特定の部分のみを加熱することが困難である。また、その周波数を高出力で出力するのは非常に困難で設備も高価になり大型化にも対応できない。 Patent Document 5 describes a configuration in which the tip of the molded body is heated by irradiation with energy having a frequency absorbed by the refractory of the molded body. However, in this configuration, it is difficult to heat only a specific part. In addition, it is very difficult to output the frequency at a high output, the equipment is expensive, and the size cannot be increased.
本発明の目的は、成形体下頂部での失透を防止することが可能な新規な板ガラス成形装置及びこれを用いた板ガラスの成形方法を提供することである。 An object of the present invention is to provide a novel sheet glass forming apparatus capable of preventing devitrification at the lower top portion of a formed body and a method for forming a sheet glass using the same.
本発明の板ガラス成形装置は、頂部に供給された溶融ガラスを両側壁面に溢流させるオーバーフロー溝と、該オーバーフロー溝の両側に溢れる溶融ガラスを流下させるための側壁面と、両側壁面を流下した溶融ガラスを融合させる下頂部とを有する断面略くさび状の成形体を備えた板ガラス成形装置において、少なくとも前記下頂部の表面が白金又は白金合金からなるとともに、下頂部表面を加熱する高周波誘導加熱手段が設けられてなることを特徴とする。 The sheet glass forming apparatus of the present invention includes an overflow groove for overflowing the molten glass supplied to the top to both side wall surfaces, a side wall surface for flowing the molten glass overflowing on both sides of the overflow groove, and a melt flowing down the both side wall surfaces. In a sheet glass forming apparatus having a substantially wedge-shaped molded body having a lower apex portion for fusing glass, at least the surface of the lower apex portion is made of platinum or a platinum alloy, and high-frequency induction heating means for heating the lower apex surface is provided. It is characterized by being provided.
本発明においては、高周波誘導加熱手段が高周波加熱コイルを含み、前記高周波加熱コイルが成形体の下頂部近傍に、下頂部と離間して設けられていることが好ましい。 In the present invention, it is preferable that the high-frequency induction heating means includes a high-frequency heating coil, and the high-frequency heating coil is provided in the vicinity of the lower top portion of the molded body and separated from the lower top portion.
本発明においては、高周波加熱コイルが略U字型であって、成形体の幅方向に設けられていることが好ましい。 In the present invention, the high-frequency heating coil is preferably substantially U-shaped and provided in the width direction of the molded body.
本発明においては、高周波加熱コイルが成形体両側に対称に配置されていることが好ましい。 In the present invention, it is preferable that the high-frequency heating coils are arranged symmetrically on both sides of the molded body.
本発明においては、下頂部近傍に配置してある高周波加熱コイルの給電方向が成形体両側で同じ方向である事が好ましい。 In the present invention, it is preferable that the feeding direction of the high-frequency heating coil arranged in the vicinity of the lower top is the same direction on both sides of the molded body.
本発明においては、下頂部近傍に配置してある高周波加熱コイルの配置位置が成形体下頂部先端と実質的に同じ高さである事が好ましい。 In the present invention, it is preferable that the arrangement position of the high-frequency heating coil arranged in the vicinity of the lower top portion is substantially the same height as the tip of the lower top portion of the molded body.
本発明においては、高周波加熱コイルが、耐火物内に固定されてなることが好ましい。 In the present invention, the high-frequency heating coil is preferably fixed in the refractory.
本発明の板ガラスの成形方法は、上記した板ガラス成形装置を用いてガラスを板状に成形することを特徴とする。 The glass sheet forming method of the present invention is characterized in that glass is formed into a plate shape using the above glass sheet forming apparatus.
本発明は、成形体下頂部を高周波誘導加熱することが可能であるため、成形体下頂部におけるガラスの温度低下を防止し、温度低下によって生じるガラスの失透を効果的に抑制することができる。 In the present invention, since the lower top portion of the molded body can be subjected to high-frequency induction heating, it is possible to prevent the glass from lowering the temperature at the lower top portion of the molded body and effectively suppress the devitrification of the glass caused by the temperature decrease. .
しかも成形体表面や内部に、外部の電源と接続される発熱体や導電体を形成する必要がない。 In addition, there is no need to form a heating element or a conductor connected to an external power source on or inside the molded body.
以下、実施例に基づいて本発明を説明する。図1は本発明の装置の好適な実施態様を示しており、図1(a)は装置断面を示す概略説明図、図1(b)は装置正面を示す概略説明図である。なお本発明の板ガラス成形装置はこれに限定されるものではない。 Hereinafter, the present invention will be described based on examples. FIG. 1 shows a preferred embodiment of the apparatus of the present invention. FIG. 1 (a) is a schematic explanatory view showing a cross section of the apparatus, and FIG. 1 (b) is a schematic explanatory view showing the front of the apparatus. The plate glass forming apparatus of the present invention is not limited to this.
本発明の板ガラス成形装置は、保温壁1により形成される成形室1a内に、断面が略くさび形であり、頂部にオーバーフロー溝2aと、該オーバーフロー溝の両側に溢れる溶融ガラスGを流下させるための側壁面2bと、両側壁面を流下した溶融ガラスGを融合させる下頂部2cとを有する成形体2が配置されている。 The sheet glass forming apparatus of the present invention has a substantially wedge-shaped cross section in a forming chamber 1a formed by a heat insulating wall 1, and allows an overflow groove 2a to flow down at the top and molten glass G overflowing on both sides of the overflow groove. The molded body 2 having the side wall surface 2b and the lower top portion 2c for fusing the molten glass G flowing down the both side wall surfaces is disposed.
成形体2の下頂部2cは、白金からなる被膜で覆われた構造となっている。本実施例では、この白金被膜は、下頂部2cのみに形成される構成となっているが、これに代えて成形体2全体を覆う構成を採用しても差し支えない。また白金に代えて白金−ロジウム等の白金合金で被膜2cを形成してもよい。 The lower top portion 2c of the molded body 2 has a structure covered with a coating made of platinum. In the present embodiment, the platinum coating is configured to be formed only on the lower top portion 2c, but a configuration covering the entire molded body 2 may be employed instead. The coating 2c may be formed of a platinum alloy such as platinum-rhodium instead of platinum.
成形室1a内には、成形体2の両側壁面と対抗するようにして発熱体3が配置されており、成形室内を所望の温度に保持している。 A heating element 3 is arranged in the molding chamber 1a so as to oppose both side wall surfaces of the molding 2, and the molding chamber is maintained at a desired temperature.
さらに成形室1a内には、白金被膜を高周波誘導加熱することが可能な高周波誘導加熱手段が設けられている。 Furthermore, high-frequency induction heating means capable of high-frequency induction heating of the platinum coating is provided in the molding chamber 1a.
高周波誘導加熱手段は、図示せぬ高周波電源と、高周波電源に接続された高周波加熱コイル4とを含む。高周波加熱コイル4に高周波電流を流すと、電磁誘導作用によって成形体下頂部2c付近に高密度の渦電流が発生し、そのジュール熱で白金被膜が発熱する。この発熱を利用して成形体下頂部2cを加熱し、成形体下頂部2cと接するガラス、或いは下頂部2cから離れつつあるガラスの失透を防止することができる。 The high frequency induction heating means includes a high frequency power source (not shown) and a high frequency heating coil 4 connected to the high frequency power source. When a high-frequency current is passed through the high-frequency heating coil 4, a high-density eddy current is generated near the lower top 2c of the molded body due to electromagnetic induction, and the platinum film generates heat due to the Joule heat. By utilizing this heat generation, the molded body lower top portion 2c can be heated to prevent devitrification of the glass in contact with the molded body lower top portion 2c or the glass that is coming away from the lower top portion 2c.
高周波加熱コイル4の形状は特に制限はないが、本実施例では、成形体2の幅方向に延びる略U字型であって、その直線部分が成形体2の全幅に亘って延びている。このようなコイル形状を採用すれば、シンプルな構成でありながら、成形体2の全幅に亘って均一に加熱することが容易になる。 The shape of the high-frequency heating coil 4 is not particularly limited, but in this embodiment, it is a substantially U-shape that extends in the width direction of the molded body 2, and the straight portion extends over the entire width of the molded body 2. By adopting such a coil shape, it becomes easy to uniformly heat the entire width of the molded body 2 with a simple configuration.
また高周波加熱コイル4は、成形体2から離間させて設置する。高周波加熱コイル4は成形体2の両側に対称に配置することが好ましい。対称に配置しておけば両側の加熱条件を同じにすることができる。また成形体下頂部2c近傍に配置してある両側のコイルの給電方向を同じ方向にすることが好ましい。同じ方向であれば成形体下頂部2cの先端付近両側に流れる電流方向が同じ方向になり、お互い影響しあうことなく効率よく先端を加熱できる。給電方向を同じ方向にするために、2本のU字型コイルを、成形体を挟んで対称に配置しても良いし、図2のように1本のコイルでつなげてもよい。また成形体下頂部2c近傍に配置してある高周波加熱コイル4の配置位置が成形体下頂部先端と実質的に同じ高さに配置することが好ましい。同じ高さに配置されると成形体下頂部2c先端が加熱され失透発生抑制に効果的である。また高周波加熱コイル4は、保温壁1を構成する耐火物内に設置することが好ましい。耐火物内に高周波加熱コイル4を設置しておけば、高周波加熱コイル4と成形体2とを確実に電気的に絶縁することができる。しかも高周波加熱コイル4と成形体2との距離を常に一定に維持することが可能となり、成形体下頂部2cを安定して加熱することができる。 Further, the high frequency heating coil 4 is set apart from the molded body 2. The high-frequency heating coil 4 is preferably disposed symmetrically on both sides of the molded body 2. If it arrange | positions symmetrically, the heating conditions of both sides can be made the same. Moreover, it is preferable that the feeding direction of the coils on both sides arranged in the vicinity of the molded product lower top portion 2c is the same direction. If they are in the same direction, the directions of current flowing on both sides near the tip of the molded product lower top 2c are the same, and the tip can be efficiently heated without affecting each other. In order to make the feeding direction the same direction, two U-shaped coils may be arranged symmetrically with the molded body interposed therebetween, or may be connected by a single coil as shown in FIG. Moreover, it is preferable that the arrangement position of the high-frequency heating coil 4 arranged in the vicinity of the molded product lower top portion 2c is arranged at substantially the same height as the tip of the molded product lower top portion. If it arrange | positions at the same height, the molded object lower top part 2c front-end | tip will be heated and it is effective in suppressing devitrification generation | occurrence | production. The high-frequency heating coil 4 is preferably installed in a refractory that constitutes the heat insulating wall 1. If the high frequency heating coil 4 is installed in the refractory, the high frequency heating coil 4 and the molded body 2 can be reliably electrically insulated. In addition, the distance between the high-frequency heating coil 4 and the molded body 2 can always be kept constant, and the molded body lower top 2c can be stably heated.
次に上記した板ガラス成形装置を用いて板ガラスを成形する方法を説明する。なお本発明の方法は、必ずしも下記の方法に制約されるものではない。 Next, a method for forming a sheet glass using the above-described sheet glass forming apparatus will be described. The method of the present invention is not necessarily limited to the following method.
まず図示しないガラス溶融装置にて、ガラス原料をガラス化し、均質化する。このようにして得られた溶融ガラスGを、図示しない溶融ガラス供給管にて成形体2のオーバーフロー溝2aに連続的に供給する。オーバーフロー溝2aに供給された溶融ガラスGは、オーバーフロー溝2aの両側から溢れ、成形体両側壁面2bに沿って流下する。側壁面2bに沿って成形体表面を流下した溶融ガラスGは、やがて成形体下頂部2cで融合し板状ガラスSGとなる。ここで成形体下頂部2cを、予め高周波誘導加熱手段によって高周波誘導加熱しておくことにより、ガラスの温度低下を防止する。 First, a glass raw material is vitrified and homogenized by a glass melting apparatus (not shown). The molten glass G thus obtained is continuously supplied to the overflow groove 2a of the molded body 2 through a molten glass supply pipe (not shown). The molten glass G supplied to the overflow groove 2a overflows from both sides of the overflow groove 2a and flows down along the both side walls 2b of the molded body. The molten glass G flowing down the surface of the molded body along the side wall surface 2b is eventually fused at the molded body lower top portion 2c to become a sheet glass SG. Here, the lower temperature of the glass is prevented by preliminarily heating the molded body lower top 2c by high-frequency induction heating means using high-frequency induction heating means.
さらに成形体下頂部2cを離れた板状ガラスSGの両端を、図示しない冷却ローラーで把持し、板幅方向の収縮を抑制する。さらに引っ張りローラーで板状ガラスSGを下方へ延伸し、所望の板厚になるように成形する。さらに必要に応じてロール成形し、さらに徐冷炉に投入する。アニール後、所定のサイズに切断することによって板ガラスを得ることができる。 Furthermore, the both ends of the sheet glass SG which has left the compact lower top 2c are gripped by a cooling roller (not shown) to suppress contraction in the sheet width direction. Further, the sheet glass SG is stretched downward by a pulling roller and formed to have a desired plate thickness. Further, roll forming is performed as necessary, and the resultant is further put into a slow cooling furnace. After annealing, a plate glass can be obtained by cutting into a predetermined size.
本発明の方法及び装置は、液晶ディスプレイ用ガラス基板、有機ELディスプレイ用ガラス基板、太陽電池用カバーガラス、タッチパネル用カバーガラス等の作製に好適である。またこれら以外にもCCD、CMOS等のイメージセンサ用カバーガラス、半導体レーザー用ガラス、マイクロレンズアレイ用基板ガラス、ディスプレイ保護用ガラス等の作製にも好適に使用できる。 The method and apparatus of the present invention are suitable for producing a glass substrate for liquid crystal display, a glass substrate for organic EL display, a cover glass for solar cell, a cover glass for touch panel, and the like. In addition to these, it can also be suitably used for producing cover glass for image sensors such as CCD and CMOS, glass for semiconductor laser, substrate glass for microlens array, display protection glass and the like.
1 保温壁
2 成形体
2a オーバーフロー溝
2b 側壁面
2c 下頂部
3 発熱体
4 高周波加熱コイル
G 溶融ガラス
SG 板状ガラス
DESCRIPTION OF SYMBOLS 1 Heat insulating wall 2 Molded body 2a Overflow groove 2b Side wall surface 2c Lower top part 3 Heat generating body 4 High frequency heating coil G Molten glass SG Sheet glass
Claims (8)
A plate glass forming method comprising forming glass into a plate shape using the plate glass forming apparatus according to claim 1.
Priority Applications (1)
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Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2015026615A1 (en) * | 2013-08-20 | 2015-02-26 | Corning Incorporated | Method and apparatus for glass sheet manufacturing including an induction heated enclosure |
JP2019026489A (en) * | 2017-07-26 | 2019-02-21 | 日本電気硝子株式会社 | Method and apparatus for manufacturing glass article |
WO2021256176A1 (en) * | 2020-06-18 | 2021-12-23 | 日本電気硝子株式会社 | Device for manufacturing glass article and method for manufacturing same |
Citations (2)
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JP2006143563A (en) * | 2004-11-24 | 2006-06-08 | Hoya Corp | Glass molding, optical element, their production method, fused glass outflow device and device for producing glass molding |
JP2009518275A (en) * | 2005-12-08 | 2009-05-07 | コーニング インコーポレイテッド | Method and apparatus for pulling low liquidus viscosity glass |
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Patent Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
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JP2006143563A (en) * | 2004-11-24 | 2006-06-08 | Hoya Corp | Glass molding, optical element, their production method, fused glass outflow device and device for producing glass molding |
JP2009518275A (en) * | 2005-12-08 | 2009-05-07 | コーニング インコーポレイテッド | Method and apparatus for pulling low liquidus viscosity glass |
Cited By (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2015026615A1 (en) * | 2013-08-20 | 2015-02-26 | Corning Incorporated | Method and apparatus for glass sheet manufacturing including an induction heated enclosure |
CN105658587A (en) * | 2013-08-20 | 2016-06-08 | 康宁股份有限公司 | Method and apparatus for glass sheet manufacturing including an induction heated enclosure |
JP2019026489A (en) * | 2017-07-26 | 2019-02-21 | 日本電気硝子株式会社 | Method and apparatus for manufacturing glass article |
WO2021256176A1 (en) * | 2020-06-18 | 2021-12-23 | 日本電気硝子株式会社 | Device for manufacturing glass article and method for manufacturing same |
JP7488509B2 (en) | 2020-06-18 | 2024-05-22 | 日本電気硝子株式会社 | Glass article manufacturing apparatus and manufacturing method thereof |
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