JP2011038709A - Exhaust method and exhaust device for refining apparatus - Google Patents

Exhaust method and exhaust device for refining apparatus Download PDF

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JP2011038709A
JP2011038709A JP2009186937A JP2009186937A JP2011038709A JP 2011038709 A JP2011038709 A JP 2011038709A JP 2009186937 A JP2009186937 A JP 2009186937A JP 2009186937 A JP2009186937 A JP 2009186937A JP 2011038709 A JP2011038709 A JP 2011038709A
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exhaust
dust collector
refining
upstream
dry dust
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JP5483317B2 (en
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Yoshinobu Masutani
佳宣 増谷
Tsunetoshi Iwamoto
常寿 岩本
Nobutoshi Yoshimoto
信寿 吉本
Hidekazu Todoroki
秀和 轟
Hiroshi Komatsubara
広志 小松原
Satoshi Niizaki
諭 新崎
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Daido Steel Co Ltd
Nippon Yakin Kogyo Co Ltd
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Daido Steel Co Ltd
Nippon Yakin Kogyo Co Ltd
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Abstract

<P>PROBLEM TO BE SOLVED: To effectively prevent damage of a dry type dust collector without causing enlargement of a facility or increase of operation costs. <P>SOLUTION: In the exhaust method, a vacuum lid 2 covered on a refining container 1, an exhaust duct 3 connected to the vacuum lid 2 and provided with the dry type dust collector 5 in the middle, and a bypass duct 36 communicating an upstream side and a downstream side of the dry type dust collector 5 are provided, the bypass duct 36 is opened at an initial stage of refining starting, exhaust is carried out by the bypass duct to replace air in the exhaust duct 31 of the upstream side of the dry type dust collector 5 with non-oxidizing gas from the refining container 1, and then, the bypass duct 36 is closed to carry out exhaust via the dry type dust collector 5. <P>COPYRIGHT: (C)2011,JPO&INPIT

Description

本発明は精錬装置の排気方法および排気装置に関し、特に排気路に乾式集塵機を備えた精錬装置の排気方法および排気装置に関する。   The present invention relates to an exhaust method and an exhaust device for a refining apparatus, and more particularly to an exhaust method and an exhaust apparatus for a refining apparatus having a dry dust collector in an exhaust path.

真空転炉や、VOD,RH−OB等の真空脱ガス装置、あるいは真空脱ガス装置を付設したAOD等における精錬容器から発生する排ガス中には多量のダストが含まれているため、真空ないし減圧用の排気路には上記ダストを捕集するために乾式集塵機を設置することが多い。ところで、上記ダストはマグネシウム等の金属微粉末を主とするものであり、金属微粉末は通常、非酸化状態のままで上記集塵装置に捕集される。そして、この捕集されたダストに、精錬開始に伴って吸引された空気中の酸素が触れるとダストが爆発的に燃焼して、上記集塵機を損傷し、ないしその機能低下を生じるおそれがある。   Exhaust gas generated from smelting vessels in vacuum converters, vacuum degassing equipment such as VOD and RH-OB, or AOD equipped with vacuum degassing equipment contains a large amount of dust, so vacuum or decompression In many cases, a dry dust collector is installed in the exhaust passage for collecting the dust. By the way, the dust is mainly composed of fine metal powder such as magnesium, and the fine metal powder is usually collected in the dust collector in a non-oxidized state. When the collected dust comes into contact with oxygen in the air sucked at the start of refining, the dust explosively burns, damaging the dust collector or reducing its function.

そこで、例えば特許文献1では、精錬開始時の集塵機内への大量の空気流入を防止するために、精錬開始に先立って集塵機から精錬容器までの上流側排気路を気密状態にし、さらに精錬開始時には上流側排気路に非酸化性ガスを注入することが提案されている。   Therefore, for example, in Patent Document 1, in order to prevent a large amount of air from flowing into the dust collector at the start of refining, the upstream exhaust passage from the dust collector to the refining vessel is made airtight prior to the start of refining, and further at the start of refining. It has been proposed to inject non-oxidizing gas into the upstream exhaust passage.

特開平10−183231JP-A-10-183231

しかし、上流側排気路を気密状態にしても当該排気路の容積が大きい場合には排気路中に残留する大量の空気が乾式集塵機内に侵入して捕集ダストの爆発的燃焼を誘起するおそれがあった。特に、上流側排気路にはサイクロンセパレータやガスクーラを設けることが多く、この場合には上記排気路の容積は実質的にかなり大きくなる。上流側排気路に非酸化性ガスを注入すれば捕集ダストの燃焼の危険は無くなるが、この場合には非酸化性ガスが大量に必要となるためガス貯留用タンクの設置による設備の大型化や運転コストの増大を招くという問題があった。   However, even if the upstream exhaust passage is airtight, if the volume of the exhaust passage is large, a large amount of air remaining in the exhaust passage may enter the dry dust collector and induce explosive combustion of the collected dust. was there. In particular, a cyclone separator or a gas cooler is often provided in the upstream exhaust passage, and in this case, the volume of the exhaust passage is substantially increased. If non-oxidizing gas is injected into the upstream exhaust passage, there is no danger of burning collected dust. However, in this case, a large amount of non-oxidizing gas is required. In addition, there is a problem that the operation cost increases.

そこで、本発明はこのような課題を解決するもので、設備の大型化や運転コストの増大を招くことなく乾式集塵機の損傷を効果的に防止できる精錬装置の排気方法および排気装置を提供することを目的とする。   Therefore, the present invention solves such problems, and provides an exhaust method and an exhaust apparatus for a refining apparatus that can effectively prevent damage to a dry dust collector without incurring an increase in equipment size or operating cost. With the goal.

上記目的を達成するために、本第1発明の精錬装置の排気方法は、精錬容器(1)の開口に覆着された真空蓋(2)と、当該真空蓋(2)に連結され、その途中に乾式集塵機(5)が少なくとも設けられた排気路(3)と、乾式集塵機(5)の上流側と下流側を連通させるバイパス路(36)とを設け、精錬開始初期にバイパス路(36)を開き当該バイパス路により排気を行って乾式集塵機(5)の上流側の排気路(31)内の空気を精錬容器(1)からの非酸化性ガスで置換し、その後、バイパス路(36)を閉じて乾式集塵機(5)を介して排気を行うことを特徴とする。   In order to achieve the above object, a method for exhausting a refining apparatus according to the first aspect of the present invention is connected to a vacuum lid (2) covered with an opening of a refining vessel (1) and the vacuum lid (2). An exhaust passage (3) provided with at least a dry dust collector (5) and a bypass passage (36) communicating the upstream side and the downstream side of the dry dust collector (5) are provided in the middle, and the bypass passage (36 ) Is opened and exhausted through the bypass passage to replace the air in the exhaust passage (31) on the upstream side of the dry dust collector (5) with the non-oxidizing gas from the refining vessel (1), and then the bypass passage (36 ) Is closed and exhausted through a dry dust collector (5).

本第1発明においては、精錬開始初期に乾式集塵機の上流側と下流側を連通させるバイパス路で排気を行って乾式集塵機の上流側の排気路内の空気を精錬容器からの非酸化性ガスで置換し、その後にバイパス路を閉じて乾式集塵機を介して排気を行うようにしている。これにより、乾式集塵機のフィルタに非酸化状態のマグネシウム等の金属微粉末を主とするダストが捕集されていても、非酸化性ガスの排ガスで置換された上流側の排気路内には酸素が殆ど存在しないから、これが乾式集塵機内に吸引されてもダストの爆発的燃焼が生じることは無く、集塵機の損傷や機能低下が回避される。本第1発明によれば、精錬容器で発生する非酸化性ガスで上流側の排気路内の空気を置換するようにしているから、非酸化性ガスの貯留用タンクを設ける必要はなく、設備の大型化や運転コストの増大を避けることができる。   In the first aspect of the invention, the exhaust gas is exhausted by a bypass passage that connects the upstream side and the downstream side of the dry dust collector at the beginning of the refining, and the air in the exhaust passage on the upstream side of the dry dust collector is converted into non-oxidizing gas from the refining vessel. After the replacement, the bypass is closed and exhausted through a dry dust collector. As a result, even when dust mainly containing non-oxidized magnesium fine powder such as magnesium is collected in the filter of the dry dust collector, oxygen in the upstream exhaust passage replaced with the exhaust gas of non-oxidizing gas is contained. Therefore, even if it is sucked into the dry dust collector, explosive combustion of dust does not occur, and damage and deterioration of the dust collector are avoided. According to the first invention, since the air in the upstream exhaust passage is replaced with the non-oxidizing gas generated in the refining vessel, there is no need to provide a storage tank for the non-oxidizing gas. Increase in size and increase in operating costs can be avoided.

本第2発明では、本第1発明において、前記上流側の排気路(31)の開口にはこれを真空蓋(2)の排気口(21)に連結する伸縮継手(33)が設けられており、精錬開始前の伸縮継手(33)の連結時に前記バイパス路(36)を開いて当該バイパス路により排気を行う。   In the second invention, in the first invention, the opening of the upstream exhaust passage (31) is provided with an expansion joint (33) for connecting it to the exhaust port (21) of the vacuum lid (2). When the expansion joint (33) is connected before the refining is started, the bypass passage (36) is opened and exhaust is performed through the bypass passage.

本第2発明においては、バイパス路による排気がなされて、伸縮継手の開口から空気が吸引されているから、精錬容器内の溶融金属からの火炎は、漏れることなく全て伸縮継手の内部に吸引される。これにより、真空蓋の排気口への連結面に設けたOリングの焼損が防止される。   In the second aspect of the invention, since the exhaust air is exhausted through the bypass passage and air is sucked from the opening of the expansion joint, all the flame from the molten metal in the refining vessel is sucked into the expansion joint without leaking. The This prevents burning of the O-ring provided on the connection surface to the exhaust port of the vacuum lid.

本第3発明では、本第1発明又は本第2発明において、前記上流側の排気路(31)に、サイクロンセパレータ(71)とこれに直列に連結されたガスクーラ(72)が設けられている。   In the third invention, in the first invention or the second invention, a cyclone separator (71) and a gas cooler (72) connected in series to the upstream exhaust passage (31) are provided. .

本第3発明においては、サイクロンセパレータとガスクーラを設けたことによって上流側排気路の実質的な容量が大きくなっており、ここに大量の空気が滞留している。したがって精錬開始初期にバイパス路により排気を行って上流側排気路内の空気を精錬容器からの非酸化性ガスで置換しておくことによって、乾式集塵機内でのダストの爆発的燃焼を確実に防止することができる。   In the third invention, the substantial capacity of the upstream exhaust passage is increased by providing the cyclone separator and the gas cooler, and a large amount of air stays there. Therefore, exhausting through the bypass passage at the beginning of refining and replacing the air in the upstream exhaust passage with non-oxidizing gas from the refining vessel ensures prevention of dust explosive combustion in the dry dust collector. can do.

本第4発明の精錬装置の排気装置では、精錬容器(1)の開口に覆着された真空蓋(2)と、当該真空蓋(2)に連結され、その途中に乾式集塵機(5)が少なくとも設けられた排気路(3)と、乾式集塵機(5)の上流側と下流側を連通させるバイパス路(36)と、乾式集塵機(5)の上流側でバイパス路(36)の連結部よりも下流側の排気路(31)に設けられた第1仕切弁(41)と、乾式集塵機(5)の下流側でバイパス路(36)の連結部よりも下流側の排気路(32)に設けられた第2仕切弁(42)と、前記バイパス路(45)に設けられた第3仕切弁(45)とを備える。   In the exhaust apparatus of the refining apparatus of the fourth aspect of the present invention, the vacuum lid (2) covered by the opening of the refining vessel (1) and the vacuum lid (2) are connected, and the dry dust collector (5) is in the middle. At least an exhaust passage (3) provided, a bypass passage (36) communicating the upstream side and the downstream side of the dry dust collector (5), and a connecting portion of the bypass passage (36) on the upstream side of the dry dust collector (5) The first gate valve (41) provided in the downstream exhaust passage (31) and the exhaust passage (32) downstream of the connecting portion of the bypass passage (36) on the downstream side of the dry dust collector (5). A second gate valve (42) provided and a third gate valve (45) provided in the bypass passage (45) are provided.

本第5発明では、本第4発明において、前記乾式集塵機(5)の上流側でバイパス路(36)の連結部よりも上流側の排気路(31)に、サイクロンセパレータ(71)とこれに直列に連結されたガスクーラ(72)が設けられている。   According to the fifth aspect of the present invention, in the fourth aspect of the present invention, the cyclone separator (71) and the cyclone separator (71) are connected to the exhaust path (31) upstream of the connecting portion of the bypass path (36) on the upstream side of the dry dust collector (5). A gas cooler (72) connected in series is provided.

上記カッコ内の符号は、後述する実施形態に記載の具体的手段との対応関係を示すものである。   The reference numerals in the parentheses indicate the correspondence with specific means described in the embodiments described later.

以上のように、本発明によれば、設備の大型化や運転コストの増大を招くことなく乾式集塵機の損傷を効果的に防止することができる。   As described above, according to the present invention, it is possible to effectively prevent the dry dust collector from being damaged without increasing the size of the facility and increasing the operating cost.

本発明の第1実施形態における、待機状態での精錬装置の排気装置の系統図である。It is a systematic diagram of the exhaust device of the refining device in the standby state in the first embodiment of the present invention. 本発明の第1実施形態における、精錬初期の精錬装置の排気装置の系統図である。It is a systematic diagram of the exhaust device of the refining apparatus in the first embodiment of the refining in the first embodiment of the present invention. 本発明の第1実施形態における、精錬主期の精錬装置の排気装置の系統図である。It is a systematic diagram of the exhaust apparatus of the refining apparatus in the refining main period in 1st Embodiment of this invention. 本発明の第2実施形態における、待機状態での精錬装置の排気装置の系統図である。It is a systematic diagram of the exhaust device of the refining device in the standby state in the second embodiment of the present invention. 本発明の第2実施形態における、精錬初期の精錬装置の排気装置の系統図である。It is a systematic diagram of the exhaust apparatus of the refining apparatus in the refining initial stage in 2nd Embodiment of this invention. 本発明の第2実施形態における、精錬主期の精錬装置の排気装置の系統図である。It is a systematic diagram of the exhaust apparatus of the refining apparatus of the refining main period in 2nd Embodiment of this invention.

(第1実施形態)
図1には精錬装置の排気装置の一例を示す。図1において、精錬装置を構成する精錬容器1には着脱可能に真空蓋2が覆着されている。真空蓋2はその排気口21が、排気路たる排気ダクト3に伸縮継手33によって連結可能であり、待機状態では伸縮継手33は図示するように短縮され切り離されていてその開口が大気に開放している。
(First embodiment)
FIG. 1 shows an example of an exhaust device of a refining device. In FIG. 1, a vacuum lid 2 is detachably attached to a refining vessel 1 constituting the refining apparatus. The vacuum lid 2 has an exhaust port 21 that can be connected to an exhaust duct 3 serving as an exhaust path by an expansion joint 33. In the standby state, the expansion joint 33 is shortened and disconnected as shown in the figure, and the opening is opened to the atmosphere. ing.

排気ダクト3は上流側ダクト31と下流側ダクト32で構成されており、伸縮継手33を設けた上流側ダクト31は仕切弁41を介して、フィルタ51を内設した乾式集塵機5の入口に連結されている。下流側ダクト32は乾式集塵機5の出口に連結され、仕切弁42を介して排気ポンプ装置6に至っている。排気ポンプ装置6は例えば3台の真空ポンプを並列に接続して構成されている。   The exhaust duct 3 is composed of an upstream duct 31 and a downstream duct 32, and the upstream duct 31 provided with the expansion joint 33 is connected to the inlet of the dry dust collector 5 provided with a filter 51 through a gate valve 41. Has been. The downstream duct 32 is connected to the outlet of the dry dust collector 5 and reaches the exhaust pump device 6 via a gate valve 42. The exhaust pump device 6 is configured, for example, by connecting three vacuum pumps in parallel.

上流側ダクト31には仕切弁41よりも上流位置に、開閉弁43を設けた大気復圧管34が連結されている。また、下流側ダクト32には仕切弁42よりも上流位置に、開閉弁44を設けた非酸化性ガス復圧管35が連結されている。そして、上流側ダクト31の、仕切弁41よりも上流位置と、下流側ダクト32の、仕切弁42よりも上流位置の間がバイパスダクト36で連結してあり、このバイパスダクト36には途中に仕切弁45が設けてある。待機状態では、仕切弁41,42,45および開閉弁43,44は全て閉じている。   An atmospheric return pressure pipe 34 provided with an on-off valve 43 is connected to the upstream duct 31 at a position upstream of the gate valve 41. In addition, a non-oxidizing gas return pressure pipe 35 provided with an opening / closing valve 44 is connected to the downstream duct 32 at a position upstream of the gate valve 42. A position upstream of the gate valve 41 in the upstream duct 31 and a position upstream of the gate valve 42 in the downstream duct 32 are connected by a bypass duct 36. A gate valve 45 is provided. In the standby state, the gate valves 41, 42, 45 and the on-off valves 43, 44 are all closed.

精錬を開始する場合には、伸縮継手33を伸張連結するのに先立って、仕切弁42,45が開放され、排気ポンプ装置6の真空ポンプのうちの一台が起動させられる。この状態で伸縮継手33を伸張させて、これを真空蓋2の排気口21に連結する。この際、伸縮継手33の開口から空気が吸引されていることにより、精錬容器1内の溶融金属からの火炎は、漏れることなく全て伸縮継手33の内部に吸引され、真空蓋2の排気口21への連結面に設けたOリングが焼損することが防止される。なお、この場合の真空ポンプによる排気は、火炎が漏れることなく全て伸縮継手33の内部に吸引されるために必要最小限のものであれば良い。   When refining is started, before the expansion joint 33 is extended and connected, the gate valves 42 and 45 are opened, and one of the vacuum pumps of the exhaust pump device 6 is activated. In this state, the expansion joint 33 is extended and connected to the exhaust port 21 of the vacuum lid 2. At this time, since air is sucked from the opening of the expansion joint 33, all the flame from the molten metal in the refining vessel 1 is sucked into the expansion joint 33 without leaking, and the exhaust port 21 of the vacuum lid 2. It is possible to prevent the O-ring provided on the connection surface to the burnout. Note that the exhaust by the vacuum pump in this case may be the minimum necessary for suctioning all of the flame into the expansion joint 33 without leaking.

伸縮継手33を排気口21に連結した後は、排気ポンプ装置6の真空ポンプを全て起動する。これにより、図2の矢印で示すように、精錬容器1から伸縮継手33、上流側ダクト31、バイパスダクト36、下流側ダクト32を経て排気ポンプ装置6に至る排気経路が形成され、上流側ダクト31内の空気が排気されて精錬容器1で発生したAr,CO,CO2等の非酸化性ガスを多量に含む排ガスで置換される。置換の終了は、伸縮継手33を連結してからの経過時間によって判断しても良いし、精錬容器1内の圧力によって判断しても良い。精錬容器1内の圧力によって判断する場合は、容器1内の圧力が40〜85KPa以下、好ましくは75KPa、さらに好ましくは68KPaになったことを検出して判断するのが好ましい。   After the expansion joint 33 is connected to the exhaust port 21, all the vacuum pumps of the exhaust pump device 6 are activated. As a result, an exhaust path is formed from the refining vessel 1 through the expansion joint 33, the upstream duct 31, the bypass duct 36, and the downstream duct 32 to the exhaust pump device 6 as shown by the arrows in FIG. The air in 31 is exhausted and replaced with exhaust gas containing a large amount of non-oxidizing gas such as Ar, CO, CO 2 generated in the refining vessel 1. The end of the replacement may be determined by the elapsed time after connecting the expansion joint 33 or may be determined by the pressure in the refining vessel 1. When judging based on the pressure in the refining container 1, it is preferable to judge by detecting that the pressure in the container 1 is 40 to 85 KPa or less, preferably 75 KPa, and more preferably 68 KPa.

この後、仕切弁41を開放するとともに仕切弁45を閉じて、図3の矢印で示すように、精錬容器1からの排ガスを乾式集塵機5に通して精錬容器1内の排気を行い、真空ないし減圧下での精錬を行う。この際、乾式集塵機5のフィルタ51には非酸化状態のマグネシウム等の金属微粉末を主とするダストが捕集されるが、非酸化性ガスの排ガスで置換された上流側ダクト31内には酸素が殆ど存在しないから、当該ダクト内の気体が乾式集塵機内に吸引されてもダストの爆発的燃焼を生じることはなく、フィルタ51の焼損が回避される。   Thereafter, the gate valve 41 is opened and the gate valve 45 is closed, and as shown by the arrow in FIG. 3, the exhaust gas from the smelting vessel 1 is exhausted through the dry dust collector 5 to evacuate the smelting vessel 1 Refining under reduced pressure. At this time, dust mainly containing fine metal powder such as magnesium in a non-oxidized state is collected in the filter 51 of the dry dust collector 5, but in the upstream duct 31 replaced with non-oxidizing gas exhaust gas. Since there is almost no oxygen, even if the gas in the duct is sucked into the dry dust collector, no explosive combustion of dust occurs, and burning of the filter 51 is avoided.

精錬が終了した場合には、仕切弁41,42を閉じ、開閉弁43,44を開いて上流側ダクト31を大気で復圧するとともに、乾式集塵機5内および下流側ダクト32内を非酸化性ガスで復圧する。その後、伸縮継手33を短縮させて切り離すとともに開閉弁43,44を閉じ、排気ポンプ装置6の真空ポンプを停止して、図1に示す待機状態に戻す。   When the refining is completed, the gate valves 41 and 42 are closed, the on-off valves 43 and 44 are opened to return the upstream duct 31 to atmospheric pressure, and the inside of the dry dust collector 5 and the downstream duct 32 is non-oxidizing gas. Restore pressure. Thereafter, the expansion joint 33 is shortened and disconnected, and the on-off valves 43 and 44 are closed, the vacuum pump of the exhaust pump device 6 is stopped, and the standby state shown in FIG. 1 is restored.

(第2実施形態)
図4には排気装置の他の例を示す。本実施形態における排気装置では排気ダクト3の上流側ダクト31に、比較的粒径の大きいダストを捕集するサイクロンセパレータ71と、これに直列に連結されて排ガスの温度を低下させるガスクーラ72が設けられている。サイクロンセパレータ71とガスクーラ72が設けられたことによって上流側ダクト31の実質的容量が非常に大きくなっており、図4に示す待機状態ではサイクロンセパレータ71等を含む上流側ダクト31に大量の空気が滞留している。なお、サイクロンセパレータ71とガスクーラ72を設けた以外の排気装置の構成は第1実施形態と同一である。
(Second Embodiment)
FIG. 4 shows another example of the exhaust device. In the exhaust system according to the present embodiment, a cyclone separator 71 that collects dust having a relatively large particle diameter and a gas cooler 72 that is connected in series to lower the temperature of exhaust gas are provided in the upstream duct 31 of the exhaust duct 3. It has been. Due to the provision of the cyclone separator 71 and the gas cooler 72, the substantial capacity of the upstream duct 31 is very large, and in the standby state shown in FIG. 4, a large amount of air flows into the upstream duct 31 including the cyclone separator 71 and the like. It stays. The configuration of the exhaust device other than the cyclone separator 71 and the gas cooler 72 is the same as that of the first embodiment.

仕切弁41,42,45および開閉弁43,44が全て閉じている待機状態から、操業を開始する場合には、伸縮継手33を伸張連結するのに先立って、仕切弁42,45が開放され、排気ポンプ装置6の真空ポンプのうちの一台が起動させられる。この状態で伸縮継手33を伸張させて真空蓋2の排気口21に連結する。この際、伸縮継手33の開口から空気が吸引されていることにより、精錬容器1内の溶融金属からの火炎は、漏れることなく全て伸縮継手33の内部に吸引され、真空蓋2の排気口21への連結面に設けたOリングが焼損することが防止される。なお、この場合の真空ポンプによる排気は、火炎が漏れることなく全て伸縮継手33の内部に吸引されるために必要最小限のものであれば良い。   When the operation is started from a standby state in which the gate valves 41, 42, 45 and the on-off valves 43, 44 are all closed, the gate valves 42, 45 are opened before the expansion joint 33 is extended and connected. One of the vacuum pumps of the exhaust pump device 6 is activated. In this state, the expansion joint 33 is extended and connected to the exhaust port 21 of the vacuum lid 2. At this time, since air is sucked from the opening of the expansion joint 33, all the flame from the molten metal in the refining vessel 1 is sucked into the expansion joint 33 without leaking, and the exhaust port 21 of the vacuum lid 2. It is possible to prevent the O-ring provided on the connection surface to the burnout. Note that the exhaust by the vacuum pump in this case may be the minimum necessary for suctioning all of the flame into the expansion joint 33 without leaking.

伸縮継手33を排気口21に連結した後は、排気ポンプ装置6の真空ポンプを全て起動する。これにより、図5の矢印で示すように、精錬容器1から伸縮継手33、上流側ダクト31、サイクロンセパレータ71、ガスクーラ72、バイパスダクト36、下流側ダクト32を経て排気ポンプ装置6に至る排気経路が形成され、上記各ダクト31や、サイクロンセパレータ71およびガスクーラ72内の空気が排気されて、精錬容器1で発生したAr,CO,CO2等の非酸化性ガスを多量に含む排ガスで置換される。置換の終了は、伸縮継手33を連結してからの経過時間によって判断しても良いし、精錬容器1内の圧力によって判断しても良い。精錬容器1内の圧力によって判断する場合は、容器1内の圧力が40〜85KPa以下、好ましくは75KPa、さらに好ましくは68KPaになったことを検出して判断するのが好ましい。   After the expansion joint 33 is connected to the exhaust port 21, all the vacuum pumps of the exhaust pump device 6 are activated. Thus, as shown by the arrows in FIG. 5, the exhaust path from the refining vessel 1 to the exhaust pump device 6 through the expansion joint 33, the upstream duct 31, the cyclone separator 71, the gas cooler 72, the bypass duct 36, and the downstream duct 32. And the air in each duct 31, cyclone separator 71 and gas cooler 72 is exhausted and replaced with exhaust gas containing a large amount of non-oxidizing gas such as Ar, CO, CO 2 generated in the refining vessel 1. . The end of the replacement may be determined by the elapsed time after connecting the expansion joint 33 or may be determined by the pressure in the refining vessel 1. When judging based on the pressure in the refining container 1, it is preferable to judge by detecting that the pressure in the container 1 is 40 to 85 KPa or less, preferably 75 KPa, and more preferably 68 KPa.

この後、仕切弁41を開放するとともに仕切弁45を閉じて、図6に示すように、精錬容器1からの排ガスを乾式集塵機5に通して精錬容器1内の排気を行い、真空ないし減圧下での精錬を行う。この際、乾式集塵機5のフィルタ51には非酸化状態のマグネシウム等の金属微粉末を主とするダストが捕集されるが、非酸化性ガスの排ガスで置換された上流側ダクト31内や、サイクロンセパレータ71およびガスクーラ72内には酸素が殆ど存在しないから、ダストの爆発的燃焼が生じることは無く、フィルタ51の焼損が回避される。   Thereafter, the gate valve 41 is opened and the gate valve 45 is closed, and as shown in FIG. 6, the exhaust gas from the smelting vessel 1 is exhausted through the dry dust collector 5 to evacuate the smelting vessel 1 under vacuum or reduced pressure. Refining at At this time, the filter 51 of the dry dust collector 5 collects dust mainly composed of fine metal powder such as magnesium in a non-oxidized state, but in the upstream duct 31 replaced with exhaust gas of non-oxidizing gas, Since there is almost no oxygen in the cyclone separator 71 and the gas cooler 72, explosive combustion of dust does not occur, and burning of the filter 51 is avoided.

精錬操業が終了した場合には、仕切弁41,42を閉じ、開閉弁43,44を開いて上流側ダクト31、サイクロンセパレータ71およびガスクーラ72を大気で復圧するとともに、乾式集塵機5内および下流側ダクト32内を非酸化性ガスで復圧する。その後、伸縮継手33を短縮させて切り離すとともに開閉弁43,44を閉じて、図4に示す待機状態に戻す。   When the refining operation is completed, the gate valves 41 and 42 are closed, the on-off valves 43 and 44 are opened, the upstream duct 31, the cyclone separator 71, and the gas cooler 72 are restored to the atmosphere, and the dry dust collector 5 and the downstream side thereof are restored. The inside of the duct 32 is decompressed with a non-oxidizing gas. Thereafter, the expansion joint 33 is shortened and disconnected, and the on-off valves 43 and 44 are closed to return to the standby state shown in FIG.

上記各実施形態において、乾式集塵機は必ずしもフィルタ式のものである必要はない。また、排気ポンプ装置の真空ポンプを一台とし、これに流量調節弁を付設して、伸縮継手連結時の排気量を調節するようにしても良い。なお、第2実施形態において、サイクロンセパレータおよびガスクーラはいずれか一方のみを設けるものであっても良い。   In each of the above embodiments, the dry dust collector is not necessarily a filter type. Further, the vacuum pump of the exhaust pump device may be a single unit, and a flow rate adjusting valve may be attached thereto to adjust the exhaust amount when the expansion joint is connected. In the second embodiment, only one of the cyclone separator and the gas cooler may be provided.

1…精錬容器、2…真空蓋、21…排気口、3…排気ダクト(排気路)、31…上流側ダクト(上流側排気路)、33…伸縮継手、36…バイパスダクト(バイパス路)、41…仕切弁(第1仕切弁)、42…仕切弁(第2仕切弁)、45…仕切弁(第3仕切弁)、5…乾式集塵機、71…サイクロンセパレータ、72…ガスクーラ。   DESCRIPTION OF SYMBOLS 1 ... Smelting container, 2 ... Vacuum lid, 21 ... Exhaust port, 3 ... Exhaust duct (exhaust path), 31 ... Upstream duct (upstream exhaust path), 33 ... Expansion joint, 36 ... Bypass duct (bypass path), 41 ... Gate valve (first gate valve), 42 ... Gate valve (second gate valve), 45 ... Gate valve (third gate valve), 5 ... Dry dust collector, 71 ... Cyclone separator, 72 ... Gas cooler.

Claims (5)

精錬容器の開口に覆着された真空蓋と、当該真空蓋に連結され、その途中に乾式集塵機が少なくとも設けられた排気路と、乾式集塵機の上流側と下流側を連通させるバイパス路を設け、精錬開始初期にバイパス路を開き当該バイパス路により排気を行って乾式集塵機の上流側の排気路内の空気を精錬容器からの非酸化性ガスで置換し、その後、バイパス路を閉じて乾式集塵機を介して排気を行うことを特徴とする精錬装置の排気方法。 A vacuum lid covered with the opening of the refining vessel, an exhaust passage connected to the vacuum lid and provided with at least a dry dust collector in the middle thereof, and a bypass passage communicating the upstream side and the downstream side of the dry dust collector, Open the bypass passage at the beginning of refining, exhaust through the bypass passage, replace the air in the exhaust passage upstream of the dry dust collector with non-oxidizing gas from the refining vessel, then close the bypass passage and install the dry dust collector The exhaust method of the refining apparatus, wherein exhaust is performed through the exhaust gas. 前記上流側の排気路の開口にはこれを真空蓋の排気口に連結する伸縮継手が設けられており、精錬開始前の伸縮継手の連結時に前記バイパス路を開いて当該バイパス路により排気を行う請求項1に記載の精錬装置の排気方法。 The opening of the upstream exhaust passage is provided with an expansion joint for connecting it to the exhaust port of the vacuum lid, and when the expansion joint is connected before refining is started, the bypass passage is opened and exhausted through the bypass passage. The exhaust method of the refining apparatus according to claim 1. 前記上流側の排気路に、サイクロンセパレータとこれに直列に連結されたガスクーラが設けられている請求項1又は2に記載の精錬装置の排気方法。 The exhaust method for a refining apparatus according to claim 1, wherein a cyclone separator and a gas cooler connected in series with the cyclone separator are provided in the upstream exhaust path. 精錬容器の開口に覆着された真空蓋と、当該真空蓋に連結され、その途中に乾式集塵機が少なくとも設けられた排気路と、乾式集塵機の上流側と下流側を連通させるバイパス路と、乾式集塵機の上流側でバイパス路の連結部よりも下流側の排気路に設けられた第1仕切弁と、乾式集塵機の下流側でバイパス路の連結部よりも下流側の排気路に設けられた第2仕切弁と、前記バイパス路に設けられた第3仕切弁とを備える精錬装置の排気装置。 A vacuum lid covered by the opening of the refining vessel, an exhaust passage connected to the vacuum lid and provided with at least a dry dust collector, a bypass passage communicating the upstream side and the downstream side of the dry dust collector, and a dry type A first gate valve provided in the exhaust passage downstream of the bypass passage connecting portion on the upstream side of the dust collector and a first gate valve provided in the exhaust passage downstream of the dry dust collector downstream of the bypass passage connecting portion. An exhaust device for a refining apparatus comprising a two-way valve and a third gate valve provided in the bypass passage. 乾式集塵機の上流側でバイパス路の連結部よりも上流側の排気路に、サイクロンセパレータとこれに直列に連結されたガスクーラが設けられている請求項4に記載の精錬装置の排気装置。 The exhaust apparatus for a refining apparatus according to claim 4, wherein a cyclone separator and a gas cooler connected in series with the cyclone separator are provided in an exhaust path upstream of the connecting part of the bypass path on the upstream side of the dry dust collector.
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