JP2010285408A5 - - Google Patents
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- JP2010285408A5 JP2010285408A5 JP2009142149A JP2009142149A JP2010285408A5 JP 2010285408 A5 JP2010285408 A5 JP 2010285408A5 JP 2009142149 A JP2009142149 A JP 2009142149A JP 2009142149 A JP2009142149 A JP 2009142149A JP 2010285408 A5 JP2010285408 A5 JP 2010285408A5
- Authority
- JP
- Japan
- Prior art keywords
- mmol
- same method
- production example
- sulfide obtained
- tetramethylpyrroline
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
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Description
［実施例２］
実施例１において、製造例２と同様の方法にて得たドデシルメチルスルフィド６．２ｇ（２８．９ミリモル）に代えて、製造例３と同様の方法にて得たノニルメチルスルフィド５．０ｇ（２８．９ミリモル）を用いた以外は、実施例１と同様にして、３−オキシラニル−２，２，５，５−テトラメチルピロリン−１−オキシル２．５ｇ（１３．７ミリモル、反応率４８％）を得た。
[Example 2]
In Example 1, 5.0 g of nonylmethyl sulfide obtained by the same method as in Production Example 3 was used instead of 6.2 g (28.9 mmol) of dodecylmethyl sulfide obtained by the same method as in Production Example 2. 2 -oxiranyl-2,2,5,5-tetramethylpyrroline-1-oxyl 2 .2 except that 28.9 mmol) was used. 5 g (13.7 mmol, 48% conversion) was obtained.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2009142149A JP2010285408A (en) | 2009-06-15 | 2009-06-15 | Method for producing 3-oxiranyl-2,2,5,5-tetramethylpyrrolin-1-oxyl |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2009142149A JP2010285408A (en) | 2009-06-15 | 2009-06-15 | Method for producing 3-oxiranyl-2,2,5,5-tetramethylpyrrolin-1-oxyl |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JP2010285408A JP2010285408A (en) | 2010-12-24 |
| JP2010285408A5 true JP2010285408A5 (en) | 2012-06-07 |
Family
ID=43541391
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2009142149A Pending JP2010285408A (en) | 2009-06-15 | 2009-06-15 | Method for producing 3-oxiranyl-2,2,5,5-tetramethylpyrrolin-1-oxyl |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JP2010285408A (en) |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP5969981B2 (en) * | 2011-03-31 | 2016-08-17 | 住友精化株式会社 | Radical composition and battery using the same |
| WO2012133204A1 (en) * | 2011-03-31 | 2012-10-04 | 学校法人早稲田大学 | Battery |
| CN114728895A (en) | 2019-11-28 | 2022-07-08 | 赛拓有限责任公司 | Improved process for the preparation of asymmetric dialkyl sulfides |
Family Cites Families (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS61282371A (en) * | 1985-06-03 | 1986-12-12 | チバ−ガイギ− アクチエンゲゼルシヤフト | Manufacture of alkyloxysilane |
| JP5424402B2 (en) * | 2007-09-21 | 2014-02-26 | 学校法人早稲田大学 | Pyrroline-based nitroxide polymer and battery using the same |
-
2009
- 2009-06-15 JP JP2009142149A patent/JP2010285408A/en active Pending
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