JP2010168308A5 - - Google Patents
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- Publication number
- JP2010168308A5 JP2010168308A5 JP2009012345A JP2009012345A JP2010168308A5 JP 2010168308 A5 JP2010168308 A5 JP 2010168308A5 JP 2009012345 A JP2009012345 A JP 2009012345A JP 2009012345 A JP2009012345 A JP 2009012345A JP 2010168308 A5 JP2010168308 A5 JP 2010168308A5
- Authority
- JP
- Japan
- Prior art keywords
- general formula
- compound represented
- salt
- producing
- onium
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
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- 239000011780 sodium chloride Substances 0.000 claims 9
- 150000003839 salts Chemical class 0.000 claims 8
- 150000001875 compounds Chemical class 0.000 claims 6
- 238000004519 manufacturing process Methods 0.000 claims 6
- 125000000217 alkyl group Chemical group 0.000 claims 3
- 125000004432 carbon atoms Chemical group C* 0.000 claims 3
- 229910052731 fluorine Inorganic materials 0.000 claims 3
- 239000011737 fluorine Substances 0.000 claims 3
- YCKRFDGAMUMZLT-UHFFFAOYSA-N fluorine atom Chemical compound [F] YCKRFDGAMUMZLT-UHFFFAOYSA-N 0.000 claims 3
- 229910052783 alkali metal Inorganic materials 0.000 claims 2
- 150000001768 cations Chemical class 0.000 claims 2
- KRHYYFGTRYWZRS-UHFFFAOYSA-M fluoride anion Chemical compound [F-] KRHYYFGTRYWZRS-UHFFFAOYSA-M 0.000 claims 2
- 239000007858 starting material Substances 0.000 claims 2
- QPJDMGCKMHUXFD-UHFFFAOYSA-N Cyanogen chloride Chemical compound ClC#N QPJDMGCKMHUXFD-UHFFFAOYSA-N 0.000 claims 1
- IIACRCGMVDHOTQ-UHFFFAOYSA-N Sulfamic acid Chemical compound NS(O)(=O)=O IIACRCGMVDHOTQ-UHFFFAOYSA-N 0.000 claims 1
- -1 alkali metal salt Chemical class 0.000 claims 1
- 150000001340 alkali metals Chemical class 0.000 claims 1
- WATWJIUSRGPENY-UHFFFAOYSA-N antimony Chemical compound [Sb] WATWJIUSRGPENY-UHFFFAOYSA-N 0.000 claims 1
- 229910052787 antimony Inorganic materials 0.000 claims 1
- RQNWIZPPADIBDY-UHFFFAOYSA-N arsenic Chemical compound [As] RQNWIZPPADIBDY-UHFFFAOYSA-N 0.000 claims 1
- 229910052785 arsenic Inorganic materials 0.000 claims 1
- 229910052797 bismuth Inorganic materials 0.000 claims 1
- 229910052801 chlorine Inorganic materials 0.000 claims 1
- 239000000460 chlorine Substances 0.000 claims 1
- ZAMOUSCENKQFHK-UHFFFAOYSA-N chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 claims 1
- 229910052802 copper Inorganic materials 0.000 claims 1
- 238000000034 method Methods 0.000 claims 1
- 229910052725 zinc Inorganic materials 0.000 claims 1
Claims (5)
下記スキーム中一般式（I）で表される化合物とオニウム塩とを反応させて一般式（II）で表されるクロロスルホニルイミドのオニウム塩を得る工程、
上記クロロスルホニルイミドのオニウム塩と、第１１族〜第１５族、第４周期〜第６周期の元素（但し、砒素およびアンチモンは除く）よりなる群から選ばれる少なくとも１種の元素を含むフッ化物とを反応させて一般式（III）で表される化合物を得る工程、
をこの順で含むことを特徴とするフルオロスルホニルイミド塩の製造方法。
A step of obtaining a chlorosulfonylimide onium salt represented by the general formula (II) by reacting a compound represented by the general formula (I) with an onium salt in the following scheme;
A fluoride containing at least one element selected from the group consisting of onium salts of chlorosulfonylimide and elements of Groups 11 to 15 and Groups 4 to 6 (excluding arsenic and antimony) And a step of obtaining a compound represented by the general formula (III),
In this order, a method for producing a fluorosulfonylimide salt.
式（VII）中、Ｒ2はアルカリ金属、Ｒ4は、フッ素又は炭素数１〜６のフッ化アルキル基を示し、ｌは１である。 A compound represented by the following general formula (VII) obtained by further reacting the compound represented by the general formula (III) obtained by the method according to any one of claims 1 to 4 with an alkali metal salt. The manufacturing method of the fluoro sulfonylimide salt in any one of Claims 1-4 including the process of obtaining.
In the formula (VII), R 2 represents an alkali metal, R 4 represents fluorine or a fluorinated alkyl group having 1 to 6 carbon atoms, and 1 is 1.
Priority Applications (5)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2009012345A JP5208782B2 (en) | 2009-01-22 | 2009-01-22 | Fluorosulfonylimides and process for producing the same |
| EP09727567.1A EP2257495B1 (en) | 2008-03-31 | 2009-03-30 | Sulfonylimide salt and method for producing the same |
| PCT/JP2009/057010 WO2009123328A1 (en) | 2008-03-31 | 2009-03-30 | Sulfonylimide salt and method for producing the same |
| US12/935,410 US8134027B2 (en) | 2008-03-31 | 2009-03-30 | Sulfonylimide salt and method for producing the same |
| CN200980111233.6A CN101980955B (en) | 2008-03-31 | 2009-03-30 | Sulfonylimide salt and method for producing the same |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2009012345A JP5208782B2 (en) | 2009-01-22 | 2009-01-22 | Fluorosulfonylimides and process for producing the same |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2010168308A JP2010168308A (en) | 2010-08-05 |
| JP2010168308A5 true JP2010168308A5 (en) | 2011-08-04 |
| JP5208782B2 JP5208782B2 (en) | 2013-06-12 |
Family
ID=42700796
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2009012345A Active JP5208782B2 (en) | 2008-03-31 | 2009-01-22 | Fluorosulfonylimides and process for producing the same |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JP5208782B2 (en) |
Families Citing this family (18)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP5653130B2 (en) * | 2010-08-24 | 2015-01-14 | 三菱マテリアル株式会社 | Method for producing bis (fluorosulfonyl) imide |
| WO2012108284A1 (en) | 2011-02-10 | 2012-08-16 | 日本曹達株式会社 | Process for production of fluorosulfonylimide ammonium salt |
| SG192235A1 (en) | 2011-03-03 | 2013-09-30 | Nippon Soda Co | Process for producing fluorine-containing sulfonylimide salt |
| JP5740466B2 (en) * | 2011-03-03 | 2015-06-24 | 日本曹達株式会社 | Method for producing fluorosulfonylimide salt |
| JP2014105115A (en) * | 2012-11-22 | 2014-06-09 | Mitsubishi Materials Corp | High-purity bis(fluorosulfonyl)imide, and production method thereof |
| JP6147523B2 (en) * | 2013-02-25 | 2017-06-14 | 株式会社日本触媒 | Method for producing fluorosulfonylimide salt |
| JP6577317B2 (en) * | 2014-09-30 | 2019-09-18 | 株式会社日本触媒 | Method for producing fluorosulfonylimide compound |
| JP6361486B2 (en) * | 2014-12-01 | 2018-07-25 | セントラル硝子株式会社 | Non-aqueous electrolyte battery electrolyte and non-aqueous electrolyte battery using the same |
| JP6645855B2 (en) * | 2015-02-03 | 2020-02-14 | 株式会社日本触媒 | Method for producing fluorosulfonylimide compound |
| JP7128422B2 (en) | 2017-04-10 | 2022-08-31 | セントラル硝子株式会社 | Method for producing phosphorylimide salt, method for producing non-aqueous electrolyte containing said salt, and method for producing non-aqueous secondary battery |
| KR101955096B1 (en) * | 2017-06-26 | 2019-03-06 | 임광민 | Novel preparing method of very efficient and simple lithium bis(fluorosulfonyl)imide |
| PL3750848T3 (en) * | 2018-04-10 | 2024-05-20 | Lg Energy Solution, Ltd. | Method for preparing lithium bis(fluorosulfonyl)imide salt |
| WO2021171948A1 (en) * | 2020-02-27 | 2021-09-02 | 株式会社日本触媒 | Composition, electrolytic solution material, and electrolytic solution |
| US20240079643A1 (en) | 2021-03-01 | 2024-03-07 | Nippon Shokubai Co., Ltd. | Electrolyte compact production method and electrolyte compact |
| JPWO2023276568A1 (en) | 2021-06-30 | 2023-01-05 | ||
| EP4343915A1 (en) | 2021-06-30 | 2024-03-27 | Nippon Shokubai Co., Ltd. | Composition production method and non-aqueous electrolyte solution |
| CN117480658A (en) | 2021-06-30 | 2024-01-30 | 株式会社日本触媒 | Method for producing nonaqueous electrolyte |
| WO2023025776A1 (en) | 2021-08-27 | 2023-03-02 | Solvay Sa | Reactive distillation process for preparing fluorosulfonylimide salts |
Family Cites Families (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO1995026056A1 (en) * | 1994-03-21 | 1995-09-28 | Centre National De La Recherche Scientifique | Ionic conducting material having good anticorrosive properties |
-
2009
- 2009-01-22 JP JP2009012345A patent/JP5208782B2/en active Active
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