JP2010053082A - Solid powdery cosmetic and method for producing the same - Google Patents

Solid powdery cosmetic and method for producing the same Download PDF

Info

Publication number
JP2010053082A
JP2010053082A JP2008220361A JP2008220361A JP2010053082A JP 2010053082 A JP2010053082 A JP 2010053082A JP 2008220361 A JP2008220361 A JP 2008220361A JP 2008220361 A JP2008220361 A JP 2008220361A JP 2010053082 A JP2010053082 A JP 2010053082A
Authority
JP
Japan
Prior art keywords
raw material
cosmetic
material powder
solid
powder
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
JP2008220361A
Other languages
Japanese (ja)
Other versions
JP5469833B2 (en
Inventor
Ikuo Fukuda
郁夫 福田
Hisao Ishikawa
尚夫 石川
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Kao Corp
Original Assignee
Kao Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Kao Corp filed Critical Kao Corp
Priority to JP2008220361A priority Critical patent/JP5469833B2/en
Priority to CN200980131982.5A priority patent/CN102123854B/en
Priority to EP09810047A priority patent/EP2329945A4/en
Priority to PCT/JP2009/065095 priority patent/WO2010024399A1/en
Priority to US13/060,913 priority patent/US20120139164A1/en
Publication of JP2010053082A publication Critical patent/JP2010053082A/en
Application granted granted Critical
Publication of JP5469833B2 publication Critical patent/JP5469833B2/en
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Images

Landscapes

  • Cosmetics (AREA)

Abstract

<P>PROBLEM TO BE SOLVED: To provide a solid powdery cosmetic having a projecting part having high stereoscopicity, and uniform and high hardness as a whole, and being excellent in taking-up property of the powder during using. <P>SOLUTION: This solid powdery cosmetic is provided by compression-molding raw material powder containing ≤15 mass% liquid component, having an approximately flat form having an upper surface and a lower surface and also providing a projecting part at the upper surface. The ratio (H1/D1) of height H1 from the datum level of the upper surface to the highest position of the projecting part to a crossing length D1 in a straight line drawn as passing through the highest position so as to make the crossing length of the powdery cosmetic as a minimum by planar view is 0.05 to 0.4, and the difference of hardness of the powdery cosmetic in the height direction is within 20%. <P>COPYRIGHT: (C)2010,JPO&INPIT

Description

本発明は、固形粉末化粧料及びその製造方法に関する。   The present invention relates to a solid powder cosmetic and a method for producing the same.

固形粉末化粧料に意匠性を付与して高級感等を高める目的で、その表面を立体形状にする技術が知られている。例えば特許文献1には、固形粉末化粧料の表面をドーム状、半球状、円錐状、角錐状、ダイヤカット状等の多種多様な立体形状に成型するための方法が提案されている。また、表面に花弁状の凸部を有する固形粉末化粧料も提案されている(特許文献2参照)。   For the purpose of imparting a design property to a solid powder cosmetic and enhancing a high-class feeling or the like, a technique for making the surface into a three-dimensional shape is known. For example, Patent Document 1 proposes a method for molding the surface of a solid powder cosmetic into a variety of three-dimensional shapes such as a dome shape, a hemispherical shape, a conical shape, a pyramidal shape, and a diamond cut shape. Further, a solid powder cosmetic having a petal-like convex portion on the surface has also been proposed (see Patent Document 2).

上述した形状を有する固形粉末化粧料の製造において、立体性の高い凸部の形状を油圧や電動サーボプレスなどの高圧力で成形しようとすると、凸部内のエア抜けが悪いため凸部の密度が低くなって強度が不足する傾向にある。強度を上げようとしてプレス圧を高くすると、成形体のスプリングバック現象によって成形体にひびや割れが発生してしまう。これらの現象は凸型形状だけではなく、成形体の縦断面が三角形や半円形の場合でも同様である。このため、凸部の高さや形状を自由にデザインすることができず、意匠性の高い立体形状の固形粉末化粧料を製造することは容易ではなかった。   In the production of the solid powder cosmetic having the above-described shape, if the shape of the convex portion having high three-dimensionality is to be molded with high pressure such as hydraulic pressure or electric servo press, the air density in the convex portion is poor and the density of the convex portion is low. It tends to be low and the strength is insufficient. When the press pressure is increased to increase the strength, the molded body is cracked or cracked due to the springback phenomenon of the molded body. These phenomena are not limited to the convex shape, but are the same even when the longitudinal section of the molded body is triangular or semicircular. For this reason, the height and shape of a convex part cannot be designed freely, and it is not easy to manufacture a solid powder cosmetic material having a high design and a solid shape.

固形粉末化粧料の製造において、上述した油圧や電動サーボプレスの装置を用いる場合に、超音波を併用することが提案されている(特許文献3及び4参照)。特に、特許文献4に記載の方法では、粒径5〜500μmの熱可塑性材料を5〜80重量%含有する粉末混合物を、加圧室の底に置きピストンで加圧する際に、一方向から超音波力を加えている。これらの方法によれば、従来の高圧プレス成形に比べ、低圧での圧縮成型が可能になるとされている。また、断面が凸型の形状であってもよいとされているが、全体にわたって均一な硬度を有するとともに、使用時の粉の取れ性に優れたものを得ることは容易ではない。   In the production of solid powder cosmetics, it has been proposed to use ultrasonic waves when using the above-described hydraulic or electric servo press devices (see Patent Documents 3 and 4). In particular, in the method described in Patent Document 4, when a powder mixture containing 5 to 80% by weight of a thermoplastic material having a particle size of 5 to 500 μm is placed on the bottom of a pressurizing chamber and pressurized with a piston, Applying sonic power. According to these methods, it is said that compression molding at a low pressure is possible as compared with conventional high pressure press molding. Moreover, although it is said that a convex shape may be sufficient as a cross section, it is not easy to obtain the thing which has uniform hardness over the whole and was excellent in the powder taking-out property at the time of use.

特開平5−201829号公報Japanese Patent Laid-Open No. 5-201829 特開2001−213721号公報JP 2001-213721 A 特開昭63−275511号公報JP-A 63-275511 特開平5−70325号公報JP-A-5-70325

本発明の目的は、前述した従来技術が有する欠点を解消し得る固形粉末化粧料及びその製造方法を提供することにある。   An object of the present invention is to provide a solid powder cosmetic and a method for producing the same that can eliminate the disadvantages of the above-described conventional techniques.

本発明は、15質量%以下の液状成分を含む原料粉末を圧縮成型してなり、上面及び下面を有するとともに上面に凸状部を備えた略扁平な形状の固形粉末化粧料であって、
上面の基準面から凸状部の最高位置までの高さH1と、該最高位置を通り、かつ平面視において粉末化粧料の横断長が最小となるように引かれた直線における該横断長D1との比(H1/D1)が0.05〜0.4であり、粉末化粧料の高さ方向の硬度差が20%以内である固形粉末化粧料を提供するものである。
The present invention is a solid powder cosmetic material having a substantially flat shape formed by compression molding a raw material powder containing a liquid component of 15% by mass or less, having an upper surface and a lower surface and having a convex portion on the upper surface,
A height H1 from the reference surface of the upper surface to the highest position of the convex portion, and the transverse length D1 in a straight line that passes through the highest position and is minimized so that the transverse length of the powder cosmetic is minimized in plan view The ratio (H1 / D1) is 0.05 to 0.4, and a solid powder cosmetic in which the difference in hardness in the height direction of the powder cosmetic is within 20% is provided.

また本発明は、前記の固形粉末化粧料の好適な製造方法であって、15質量%以下の液状成分を含む原料粉末を金型内に充填し、該原料粉末を挟んで相対向してそれぞれ配された成型用杵の少なくとも一方によって該原料粉末に超音波振動を与えながら、両杵によって圧縮を加える圧縮成型を行い、上面及び下面を有するとともに上面に凸状部を備えた略扁平な形状の固形粉末化粧料を製造する方法であって、
原料粉末を圧縮成型する前に、該圧縮成型の圧力よりも低い圧力を加えた状態下に、原料粉末に超音波振動をパルス的に印加する予備成型を行う固形粉末化粧料の製造方法を提供するものである。
The present invention is also a preferred method for producing the above-described solid powder cosmetic, wherein a raw material powder containing a liquid component of 15% by mass or less is filled in a mold, and the raw material powders are opposed to each other. A substantially flat shape having a top surface and a bottom surface and having a convex portion on the top surface while performing compression molding to compress the raw material powder while applying ultrasonic vibration to the raw material powder with at least one of the molding rods arranged A method for producing a solid powder cosmetic comprising:
Provided a method for producing a solid powder cosmetic that performs pre-molding by applying ultrasonic vibration to the raw material powder in a pulsed manner under a state where a pressure lower than the pressure of the compression molding is applied before compressing the raw material powder. To do.

本発明によれば、立体性の高い凸部を有する固形粉末化粧料であって、全体にわたって均一でかつ高い硬度を有するとともに、使用時の粉の取れ性に優れた固形粉末化粧料を提供することができる。   According to the present invention, there is provided a solid powder cosmetic having convex portions with high three-dimensionality, having a uniform and high hardness throughout, and having excellent powder take-up properties during use. be able to.

以下本発明を、その好ましい実施形態に基づき図面を参照しながら説明する。図1には、本発明の固形粉末化粧料の一実施形態の斜視図が示されている。図2(a)は、図1に示す化粧料の平面図であり、図2(b)及び(c)は図2(a)におけるb−b線断面図及びc−c線断面図である。本実施形態の化粧料1は、立体性の高い凸部を有するにもかかわらず、全体にわたって均一でかつ高い硬度を有するとともに、使用時の粉の取れ性に優れた点に特徴を有するものである。   The present invention will be described below based on preferred embodiments with reference to the drawings. FIG. 1 shows a perspective view of an embodiment of the solid powder cosmetic of the present invention. Fig.2 (a) is a top view of the cosmetics shown in FIG. 1, FIG.2 (b) and (c) are the bb sectional view taken on the line in FIG.2 (a), and the cc sectional view. . The cosmetic 1 according to the present embodiment is characterized in that it has a uniform and high hardness throughout the whole despite having convex portions with a high degree of three-dimensionality, and also has an excellent powder take-out property during use. is there.

図1及び図2(a)に示すように、化粧料1は、平面視して、角が丸みを帯びた矩形状をしている。この矩形は、図2(a)に示すように長辺L1(図2に記載)と短辺L2とからなる。図2(b)及び図2(c)に示すように、化粧料1は、上面1aと、これに対向する下面1bとを有している。下面1bは平坦な水平面をなしている。一方、上面1aは、その周縁部に位置する平坦な水平面からなる基面部2と、基面部2と滑らかに連なる三次元状の立体面部3を有している。立体面部3は、斜面部3a及び下面1bと平行な天面部3bとを有している。そして、基面部2よりも上方の部位が立体形状の凸状部4となっている。   As shown in FIGS. 1 and 2 (a), the cosmetic 1 has a rectangular shape with rounded corners in plan view. As shown in FIG. 2A, this rectangle is composed of a long side L1 (described in FIG. 2) and a short side L2. As shown in FIG.2 (b) and FIG.2 (c), the cosmetics 1 have the upper surface 1a and the lower surface 1b facing this. The lower surface 1b has a flat horizontal surface. On the other hand, the upper surface 1 a has a base surface portion 2 made of a flat horizontal surface located at the peripheral edge portion thereof, and a three-dimensional solid surface portion 3 smoothly connected to the base surface portion 2. The three-dimensional surface portion 3 has a slope portion 3a and a top surface portion 3b parallel to the lower surface 1b. A portion above the base surface portion 2 is a three-dimensional convex portion 4.

凸状部4は、b−b線断面でみると台形をなしている。また、c−c線断面でみても台形をなしている。そして、このような形状の凸状部4を有する化粧料1は、その全体としてみると、略扁平な形状をしている。   The convex portion 4 has a trapezoidal shape when viewed along the line bb. Moreover, it is trapezoid even if it sees in the cc line cross section. And the cosmetic 1 which has the convex-shaped part 4 of such a shape is carrying out the substantially flat shape when it sees as the whole.

上述したとおり、本実施形態の化粧料1は、凸状部4の立体性が高いものである。凸状部4の立体性の尺度として、本実施形態においてはH1/D1を採用している。ここでH1は、上面1aの基準面である基面部2から凸状部4の最高位置までの高さで定義される。D1は、凸状部4の最高位置を通り、かつ化粧料1の平面視において化粧料1の横断長が最小となるように引かれた直線における該横断長で定義される。本実施形態においては、化粧料1は平面視において矩形をしているので、D1は矩形の短辺であるL2と一致する。   As described above, the cosmetic 1 of the present embodiment has a high three-dimensionality of the convex portion 4. In this embodiment, H1 / D1 is adopted as a measure of the three-dimensionality of the convex portion 4. Here, H1 is defined as the height from the base surface portion 2 which is the reference surface of the upper surface 1a to the highest position of the convex portion 4. D1 is defined by the crossing length in a straight line that passes through the highest position of the convex portion 4 and is drawn so that the crossing length of the cosmetic 1 is minimized in the plan view of the cosmetic 1. In the present embodiment, since the cosmetic 1 has a rectangular shape in plan view, D1 coincides with L2 that is the short side of the rectangle.

凸状部4に同じ高さの最高位置が2箇所以上存在するときは、D1の値が最も小さくなる位置を最高位置と定義する。また、凸状部4の形状によっては、図3に示すように化粧料1全体が凸状部4を構成し、水平な平坦部が存在しない場合がある。このような場合における基面部は凸状部4の最低位置と定義し、そこから最高位置までの高さをH1とする。   When two or more highest positions with the same height exist in the convex portion 4, the position where the value of D1 is the smallest is defined as the highest position. Moreover, depending on the shape of the convex part 4, as shown in FIG. 3, the cosmetic 1 whole may comprise the convex part 4, and a horizontal flat part may not exist. The base surface portion in such a case is defined as the lowest position of the convex portion 4, and the height from that position to the highest position is H1.

本実施形態においては、凸状部4の立体性の尺度である上述のH1/D1を0.05〜0.4の範囲、好ましくは0.1〜0.3の範囲に設定している。H1/D1の値をこの範囲に設定することで、化粧料1に十分な立体感を付与することができ、意匠性の高い化粧料となすことができる。   In the present embodiment, the above-mentioned H1 / D1, which is a measure of the three-dimensionality of the convex portion 4, is set in the range of 0.05 to 0.4, preferably in the range of 0.1 to 0.3. By setting the value of H1 / D1 within this range, a sufficient three-dimensional effect can be imparted to the cosmetic 1, and a cosmetic with high design properties can be obtained.

化粧料1のH1/D1の値は上述の範囲であるところ、H1及びD1それぞれの値それ自体は、化粧料1の具体的な用途に応じ、次のとおりであることが好ましい。化粧料1が例えばアイシャドウである場合、H1に関しては、この範囲を0.5〜5mm、特に1〜3mmとすることができる。D1に関しては、一般的に5〜30mmが用いられる。同様の観点から、化粧料1が例えばファンデーションである場合、H1に関しては、この範囲を1〜5mm、特に2〜5mmとすることでき、D1に関しては、一般的に30〜60mmが用いられる。なお、化粧料1の下面1bから基面部2までの高さH2は、本実施形態において臨界的でなく、化粧料1の具体的な用途等に応じ適切に設定できる。   Although the value of H1 / D1 of cosmetic 1 is in the above-described range, the values of H1 and D1 themselves are preferably as follows according to the specific use of cosmetic 1. When the cosmetic 1 is, for example, an eye shadow, this range can be set to 0.5 to 5 mm, particularly 1 to 3 mm for H1. About D1, 5-30 mm is generally used. From the same viewpoint, when the cosmetic 1 is, for example, a foundation, this range can be set to 1 to 5 mm, particularly 2 to 5 mm for H1, and 30 to 60 mm is generally used for D1. In addition, the height H2 from the lower surface 1b of the cosmetic 1 to the base surface portion 2 is not critical in the present embodiment, and can be appropriately set according to a specific application or the like of the cosmetic 1.

H1/D1の値が上述の範囲に設定されている化粧料は、これを圧縮成型によって製造する場合、その立体形状に起因して、一般に平面視における各部位の加圧力を均一にすることが容易でない。これに対して本実施形態の化粧料1は、その各部位における硬さが均一になっている点に特徴の一つを有する。硬さの均一性に関する尺度として、本実施形態においてはマイクロゴム硬度計MD−1(高分子計器(株)製、触針φ0.16mm、長さ0.5mm)で測定された硬度(以下、「アスカー硬度」と言う。)を採用している。そして、化粧料1の高さ方向の硬度差が20%以下、好ましくは15%以下となっている。化粧料1の高さ方向の硬度差は、図4に示すように、化粧料1の上面1aでの硬度A1、及び化粧料1をその上面1aから下面1b側に向けて最低3等分となるように簡易フライス盤等(例えばローランド製MDX−40)で、下層を破壊及び圧密しないように底面と平行に順次削り取っていったときの、各層でのアスカー硬度A2、A3、・・・、Anを測定し、測定されたアスカー硬度の最大値AMaxと最小値AMinとの差を、最小値AMinで除して100を乗じた値、すなわち〔(AMax−AMin)/AMin〕×100で定義される。なお、各層のアスカー硬度は数点測定してその平均値を用いても良い。 Cosmetics in which the value of H1 / D1 is set in the above-described range can generally be made uniform in the pressure applied to each part in plan view due to its three-dimensional shape when manufactured by compression molding. Not easy. On the other hand, the cosmetic 1 of this embodiment has one of the characteristics in that the hardness in each part is uniform. As a measure for hardness uniformity, in this embodiment, the hardness (hereinafter, referred to as a stylus φ0.16 mm, length 0.5 mm) measured by a micro rubber hardness meter MD-1 (manufactured by Kobunshi Keiki Co., Ltd., stylus φ0.16 mm, length 0.5 mm). "Asker hardness"). And the hardness difference of the height direction of the cosmetics 1 is 20% or less, Preferably it is 15% or less. As shown in FIG. 4, the hardness difference in the height direction of the cosmetic 1 is divided into at least three equal parts of the hardness A 1 on the upper surface 1a of the cosmetic 1 and the cosmetic 1 from the upper surface 1a toward the lower surface 1b. Asker hardness A 2 , A 3 in each layer when the lower layer is sequentially scraped in parallel with the bottom surface so as not to break and compact with a simple milling machine or the like (eg, MDX-40 manufactured by Roland)・ A n is measured, and the difference between the maximum value A Max and the minimum value A Min of the measured Asker hardness is divided by the minimum value A Min and multiplied by 100, that is, [(A Max −A Min ) / A Min ] × 100. In addition, the Asker hardness of each layer may measure several points and use the average value.

アスカー硬度の測定においては、各層において、同じ場所か又は互いに近接する場所(例えば2mm以内の距離)の測定を行う場合には、硬度計の針の進入量(0.5mm)を考慮すると、化粧料1を削り取る厚みを1mm以上とすることが好ましい。一方、各層において、硬度測定の部位を離れた場所にすることができる場合には、化粧料1を削り取る厚みに特に制限はない。尤も、削り取る厚みを過度に小さくすることには特段の技術的な意味はなく、一般に0.5〜2mm程度の厚みで以て削り取ればよい。   In the measurement of Asker hardness, when measuring the same place or a place close to each other (for example, a distance within 2 mm) in each layer, taking into account the amount of penetration of the hardness meter needle (0.5 mm), makeup The thickness of scraping off the material 1 is preferably 1 mm or more. On the other hand, in each layer, there is no particular limitation on the thickness at which the cosmetic material 1 is scraped when the hardness measurement site can be separated. However, there is no particular technical meaning in reducing the thickness to be scraped excessively, and it is generally sufficient to scrape with a thickness of about 0.5 to 2 mm.

化粧料1は、原料粉末を金型内に充填して直接成型してもよいし、原料粉末を容器内で圧縮成型して得たものであってもよい。容器は一般に、底面が平坦であり、かつ該底面上に、該底面と同形の開口部を有する浅底の皿状の形状を有している。かかる容器内で一体的に成型された化粧料1は、そのままファンデーション、アイシャドウ、チーク等の化粧品の製品形態に供することができる。   The cosmetic 1 may be directly molded by filling the raw material powder in a mold, or may be obtained by compression molding the raw material powder in a container. The container generally has a shallow dish-like shape having a flat bottom surface and an opening having the same shape as the bottom surface on the bottom surface. The cosmetic 1 integrally molded in such a container can be used as it is for cosmetic product forms such as foundations, eye shadows, and teaks.

化粧料1は、15質量%以下の液状成分を含む原料粉末を用いて製造されたものである。ここで言う液状成分には、例えば水、及び低級アルコール等の水溶性有機溶剤などの水性成分、並びに室温で液体である油性成分が包含される。液状成分が15質量%超である原料粉末を用いた場合には、液架橋力が高くなり、超音波による流動化の効果が得られにくくなってしまう。   Cosmetic 1 is manufactured using the raw material powder containing a liquid component of 15 mass% or less. The liquid component mentioned here includes, for example, water and an aqueous component such as a water-soluble organic solvent such as a lower alcohol, and an oily component that is liquid at room temperature. When the raw material powder having a liquid component of more than 15% by mass is used, the liquid crosslinking power becomes high, and it becomes difficult to obtain the effect of fluidization by ultrasonic waves.

原料粉末の構成成分は、化粧料1の具体的な用途に応じて適切なものが選択される。化粧料1が例えばファンデーションやチークである場合には、粉末成分が好ましくは85〜95質量%、更に好ましくは85〜90質量%含有される。この粉末成分は、例えばタルク、マイカ、セリサイト、カオリン等の体質顔料、ベンガラ、黄酸化鉄、黒酸化鉄等の着色顔料、パール顔料などの光輝顔料を包含する。粉末成分に加え、化粧料1は、界面活性剤、防腐剤、酸化防止剤、香料、紫外線吸収剤、保湿剤、殺菌剤などを適宜含有することができる。   As a constituent component of the raw material powder, an appropriate one is selected according to the specific use of the cosmetic 1. When the cosmetic 1 is a foundation or teak, for example, the powder component is preferably contained in an amount of 85 to 95% by mass, more preferably 85 to 90% by mass. Examples of the powder component include extender pigments such as talc, mica, sericite, and kaolin, colored pigments such as bengara, yellow iron oxide, and black iron oxide, and bright pigments such as pearl pigments. In addition to the powder component, the cosmetic 1 can appropriately contain a surfactant, an antiseptic, an antioxidant, a fragrance, an ultraviolet absorber, a moisturizer, a bactericide, and the like.

特に、化粧料1を、後述する方法で製造する場合には、原料粉末中に、融点が40〜150℃である固体の油性成分を好ましくは0.5〜10質量%、更に好ましくは1〜5質量%含有させる。これによって、全体にわたって均一でかつ高い硬度を有するとともに、使用時の取れ性に優れた化粧料を容易に得ることができる。この油性成分としては、例えばミツロウ、鯨ロウ等の動物性ワックス;カルナウバロウ、キャンデリラロウ、ライスワックス、木ロウ等の植物性ワックス;モンタンワックス、オゾケライト、セレシン、パラフィンワックス、マイクロクリスタリンワックス等の鉱物性ワックス;ポリエチレンワックス、硬化ひまし油、水素添加ホホバ油、ステアリン酸アミド、シリコンワックス等の合成ワックスを用いることができる。   In particular, when the cosmetic 1 is produced by the method described later, the solid oily component having a melting point of 40 to 150 ° C. is preferably 0.5 to 10% by mass, more preferably 1 to 1%, in the raw material powder. 5% by mass is contained. As a result, it is possible to easily obtain a cosmetic material that has a uniform and high hardness throughout and is excellent in the ability to be removed during use. Examples of the oil component include animal waxes such as beeswax and whale wax; plant waxes such as carnauba wax, candelilla wax, rice wax, and wood wax; minerals such as montan wax, ozokerite, ceresin, paraffin wax, and microcrystalline wax. Synthetic waxes such as polyethylene wax, hydrogenated castor oil, hydrogenated jojoba oil, stearamide, and silicon wax can be used.

図5には、本実施形態の化粧料1を製造するために用いられる好ましい装置の模式図が示されている。装置10は枠体11を備えている。枠体11の高さ方向の中央部には、成型テーブル12が水平方向に取り付けられている。成型テーブル12の中央部には貫通孔が設けられており、その貫通孔にタブレット成型用金型13が嵌合されている。金型13はその上下が開口した筒状の形状をしている。金型13はその上部に側方へ張り出すフランジ13aを有している。フランジ13aは成型テーブル12へボルト締め(図示せず)されている。   The schematic diagram of the preferable apparatus used in order to manufacture the cosmetics 1 of this embodiment is shown by FIG. The apparatus 10 includes a frame body 11. A molding table 12 is attached to the center of the frame 11 in the height direction in the horizontal direction. A through hole is provided in the center of the molding table 12, and a tablet molding die 13 is fitted in the through hole. The mold 13 has a cylindrical shape whose upper and lower sides are open. The mold 13 has a flange 13a projecting laterally at the top. The flange 13a is bolted (not shown) to the molding table 12.

金型13の筒状開口部の上下の位置には超音波振動素子14a,14bが配されている。各素子14a,14bはエアシリンダ15a,15bによって支持されている。上部エアシリンダ15aは、枠体11の天板11aに取り付けられ、それから垂下している。一方、下部エアシリンダ15bは、枠体11の底板11b上に取り付けられている。これによって、各超音波振動素子14a,14bはそれぞれ上下方向へ移動可能になっている。なお、超音波振動素子の移動手段はエアシリンダに限定されず、他に油圧シリンダや、電動モータを用いたボールネジプレス等の機器を用いても良い。   Ultrasonic vibrating elements 14 a and 14 b are arranged at positions above and below the cylindrical opening of the mold 13. Each element 14a, 14b is supported by air cylinders 15a, 15b. The upper air cylinder 15a is attached to the top plate 11a of the frame 11 and hangs from it. On the other hand, the lower air cylinder 15 b is mounted on the bottom plate 11 b of the frame body 11. Thereby, each ultrasonic vibration element 14a, 14b can be moved in the vertical direction. Note that the moving means of the ultrasonic vibration element is not limited to the air cylinder, and other devices such as a hydraulic cylinder or a ball screw press using an electric motor may be used.

各超音波振動素子14a,14bの先端にはホーン16a,16bが取り付けられている。各ホーン16a,16bの先端は成型用金型13の筒状開口部と同一形状をなしている。これら三者は同一軸線上に位置している。各ホーン16a,16bは、化粧料1の原料粉末を圧縮成型する際に、該原料粉末に超音波振動を与える役割、及び該原料粉末を圧縮するための成型用杵としての役割を有している。したがって以下の説明では、これらのホーンをそれぞれ上杵16a、下杵16bと呼ぶことにする。各杵16a,16bの先端形状は、金型13の筒状開口部と同形状になっている。   Horns 16a and 16b are attached to the tips of the ultrasonic vibration elements 14a and 14b. The tips of the horns 16a and 16b have the same shape as the cylindrical opening of the molding die 13. These three are located on the same axis. Each horn 16a, 16b has a role of giving ultrasonic vibration to the raw material powder when compressing the raw material powder of the cosmetic 1, and a role as a molding cage for compressing the raw material powder. Yes. Therefore, in the following description, these horns will be referred to as an upper rod 16a and a lower rod 16b, respectively. The tip shapes of the flanges 16 a and 16 b are the same as the cylindrical opening of the mold 13.

以上の構造を有する装置10を用いた化粧料1の製造方法を図6(a)ないし(c)を参照しながら説明すると、先ず図6(a)に示すように、下部エアシリンダ15bを動作させ、金型内に予め挿入されている下杵を、原料粉末を充填するために金型内で下降させる。また上部エアシリンダ15aを動作させ、上杵16aを上昇させて成型テーブル12上の空間に待避させる。これによって、金型13にはその筒状開口部と下杵16bとで画成される凹部が形成される。この凹部に、原料粉末20を充填する。   The manufacturing method of the cosmetic 1 using the apparatus 10 having the above structure will be described with reference to FIGS. 6A to 6C. First, as shown in FIG. 6A, the lower air cylinder 15b is operated. Then, the lower brace previously inserted in the mold is lowered in the mold in order to fill the raw material powder. Further, the upper air cylinder 15a is operated, and the upper rod 16a is raised and retracted in the space on the molding table 12. As a result, a concave portion defined by the cylindrical opening and the lower collar 16b is formed in the mold 13. The raw material powder 20 is filled in the recess.

次に、エアシリンダ15aを動作させて、上杵16aを降下させ、原料粉末20が充填されている前記の凹部内へ上杵16を挿入する。上杵16aの位置を固定し、次に下杵16bを上昇させ、図6(b)に示すように原料粉末20に圧縮力を加えて成型を行う。なお、容器(例えば浅底の皿状の容器)内に原料粉末を充填して成型する場合には、下杵16bを金型内で下降させる前に下杵16bの上に容器(図示せず)を載せ、その後下杵16bを降下させる。あるいは下杵16bを降下させた後に容器(図示せず)を金型内の下杵上に置く。その後、容器内に原料粉末を充填して圧縮成型する工程は、容器を用いない場合と同様である。   Next, the air cylinder 15a is operated to lower the upper rod 16a, and the upper rod 16 is inserted into the concave portion filled with the raw material powder 20. The position of the upper iron 16a is fixed, and then the lower iron 16b is raised, and the raw material powder 20 is molded by applying a compressive force as shown in FIG. 6 (b). In the case where the raw material powder is filled in a container (for example, a shallow dish-shaped container) and molded, a container (not shown) is placed on the lower iron 16b before the lower iron 16b is lowered in the mold. ) And then lower the lower arm 16b. Alternatively, after lowering the lower punch 16b, a container (not shown) is placed on the lower punch in the mold. Thereafter, the process of filling and compressing the raw material powder in the container is the same as when the container is not used.

また、得られる化粧料の高さ方向の硬度差をより小さくするために、本成型前に予備圧縮を実施することが好ましい。予備成型は、本成型を行う前に、本成型の圧力よりも低い圧力を加えた状態下に、原料粉末20に超音波振動をパルス的に印加することからなる。本成型に先立ちこの予備成型を行うことで、金型の凹部内で原料粉末20がより効果的に均質化し、かつ空気抜きが促進される。その結果、全体にわたって均一でかつ高い硬度を有するとともに、使用時の取れ性に優れた立体性の高い凸状部4を有する化粧料1を得ることができる。超音波振動の印加は、各杵16a,16bの振動条件を同じか、又は異ならせて、両杵16a,16bを用いて行ってもよく、あるいは一方の杵のみを振動させて行ってもよい。   In order to further reduce the hardness difference in the height direction of the cosmetic material to be obtained, it is preferable to perform preliminary compression before the main molding. Preliminary molding consists of applying ultrasonic vibration to the raw material powder 20 in a pulsed manner under a state where a pressure lower than the pressure of the main molding is applied before performing the main molding. By performing this preliminary molding prior to the main molding, the raw material powder 20 is more effectively homogenized in the concave portion of the mold, and air venting is promoted. As a result, it is possible to obtain a cosmetic 1 that has a uniform and high hardness throughout, and has a convex portion 4 with a high degree of stericity that is excellent in ease of use. The application of the ultrasonic vibration may be performed using both the scissors 16a and 16b with the vibration conditions of the scissors 16a and 16b being the same or different, or may be performed by vibrating only one of the scissors. .

図7には、予備成型及びそれに引き続く本成型の操作条件の一例が示されている。同図においては実線が原料粉末20に加わる圧力を示し、一点鎖線が下杵16bの位置(予備成型開始時からの上昇量)を示す。点線は超音波振動の印加のタイミングを示し、パルスが下がっている状態の時に超音波振動が印加されていること示す。   FIG. 7 shows an example of operating conditions for pre-molding and subsequent main molding. In the figure, the solid line indicates the pressure applied to the raw material powder 20, and the alternate long and short dash line indicates the position of the lower punch 16b (the amount of increase from the start of pre-forming). The dotted line indicates the timing of application of ultrasonic vibration, and indicates that ultrasonic vibration is being applied when the pulse is in a lowered state.

図7に示すように、予備成型においては、本成型よりも低い圧力を原料粉末20に加える。予備成型時の圧力は、本成型の圧力の10〜70%、特に20〜50%であることが、原料粉末20の均質化及び空気抜きの促進の点から好ましい。予備成型時に印加する超音波振動の印加時間は50〜300ミリ秒、特に100〜200ミリ秒であることが好ましい。印加時間が長いと、固体の油性成分が超音波振動による摩擦熱で溶融・固化して均質化・エア抜きを阻害することがあるので、固体の油性成分が摩擦熱で溶融してしまわない程度の印加時間を採用することが有利である。超音波の周波数は、10〜100kHz、特に15〜30kHzであることが好ましい。パルスの印加回数は1〜5回、特に2〜3回であることが好ましい。パルス印加のインターバルは、50〜300、特に100〜200ミリ秒であることが好ましい。各回の印加時間は上述の範囲であることを条件として同じにしてもよく、あるいは異ならせてもよい。印加のインターバルや周波数についても同様である。   As shown in FIG. 7, in the preliminary molding, a lower pressure than that in the main molding is applied to the raw material powder 20. The pressure at the time of the pre-molding is preferably 10 to 70%, particularly 20 to 50% of the pressure of the main molding from the viewpoint of homogenizing the raw material powder 20 and promoting air bleeding. The application time of ultrasonic vibration applied during the pre-molding is preferably 50 to 300 milliseconds, particularly 100 to 200 milliseconds. If the application time is long, the solid oil component may melt and solidify due to frictional heat generated by ultrasonic vibrations, which may hinder homogenization and air bleeding, so that the solid oil component does not melt due to frictional heat. It is advantageous to employ an application time of The frequency of the ultrasonic waves is preferably 10 to 100 kHz, particularly 15 to 30 kHz. The number of pulses applied is preferably 1 to 5 times, particularly preferably 2 to 3 times. The pulse application interval is preferably 50 to 300, particularly 100 to 200 milliseconds. The application time of each time may be the same on condition that it is in the above-mentioned range, or may be different. The same applies to the application interval and frequency.

予備成型が完了したら引き続き本成型を行う。本成型は、上杵16a及び下杵16bを解放することなく、予備成型時の圧力を更に増加させることで行う。具体的には、上杵16aの位置は予備成型時と同様とし、下杵16aを更に上昇させることで、原料粉末20に圧力を加える。下杵16bを上昇させている間、原料粉末20に超音波振動を印加してもよく、あるいは、下杵16bが所定の位置まで上昇するまでは超音波振動の印加は行わず、下杵16bが所定の位置に到達した時点で超音波振動の印加を行ってもよい。図7に示す操作条件においては、下杵16bが所定の位置に到達した時点で超音波振動の印加を開始している。   Once the preliminary molding is completed, the main molding is continued. The main molding is performed by further increasing the pressure at the time of preliminary molding without releasing the upper collar 16a and the lower collar 16b. Specifically, the position of the upper punch 16a is the same as that at the time of preforming, and the lower punch 16a is further raised to apply pressure to the raw material powder 20. While raising the lower eyelid 16b, ultrasonic vibration may be applied to the raw material powder 20, or no ultrasonic vibration is applied until the lower eyelid 16b rises to a predetermined position. Application of ultrasonic vibration may be performed at the time when reaches a predetermined position. Under the operating conditions shown in FIG. 7, the application of ultrasonic vibration is started when the lower eyelid 16b reaches a predetermined position.

本成型においては、原料粉末20を挟んで相対向してそれぞれ配された上下の杵16a,16bによって超音波振動を与えつつ圧縮成型を行う。原料粉末20の成分は超音波を受けることで振動し、それによって摩擦熱が発生する。この摩擦熱によって、原料粉末20中に含まれている融点が40〜150℃である固体の油性成分が溶融して粒子同士を結合する。原料粉末20を挟んで上下から超音波振動を与えることで粒子の振動が促進され、粉末の結合の強度が均一になる。これによって、一方の杵のみによって超音波振動を与えつつ圧縮成型を行ってきた特許文献4等に記載の方法に比較して、圧縮の圧力を低くしても圧縮成型物の強度を同程度に高くすることが可能になる。その結果、硬度が高いにもかかわらず、取れ性に優れた化粧料1を容易に得ることができる。各杵16a,16bの振動条件は同じでもよく、あるいは異なっていてもよいが、一般的には同条件としておく。   In the main molding, compression molding is performed while applying ultrasonic vibrations by the upper and lower ridges 16a and 16b arranged opposite to each other with the raw material powder 20 interposed therebetween. The components of the raw material powder 20 are vibrated by receiving ultrasonic waves, thereby generating frictional heat. Due to this frictional heat, the solid oil component having a melting point of 40 to 150 ° C. contained in the raw material powder 20 is melted to bond the particles together. By applying ultrasonic vibration from above and below the raw material powder 20, the vibration of the particles is promoted, and the strength of the bonding of the powder becomes uniform. As a result, compared with the method described in Patent Document 4 or the like in which compression molding is performed while applying ultrasonic vibration only by one of the scissors, the strength of the compression molded product is comparable even if the compression pressure is lowered. It becomes possible to make it higher. As a result, it is possible to easily obtain the cosmetic 1 having excellent take-off properties despite its high hardness. The vibration conditions of each of the flanges 16a and 16b may be the same or different, but generally the same conditions are set.

化粧料1の具体的な用途や組成にもよるが、本成型においては、上下の杵16a,16bによって加わる圧力を好ましくは0.1〜2.5MPa、更に好ましくは0.1〜1.0MPaという低圧に設定することができる。これに対して、一方の杵のみによって超音波振動を与えつつ圧縮成型を行ってきた特許文献4等に記載の方法では、本製造方法よりも一桁以上高い圧力で圧縮成型を行っていた。   Although depending on the specific application and composition of the cosmetic 1, in this molding, the pressure applied by the upper and lower ridges 16a and 16b is preferably 0.1 to 2.5 MPa, more preferably 0.1 to 1.0 MPa. Can be set to a low pressure. On the other hand, in the method described in Patent Document 4 and the like in which compression molding is performed while applying ultrasonic vibration only by one of the scissors, the compression molding is performed at a pressure higher by one digit or more than the present manufacturing method.

圧力を低い値に設定できることは、主剤である原料成分に対して、物理的なダメージが少なくなるという利点がある。また、本実施形態においては、原料粉末が液体成分を含有している場合があるが、そのような場合であっても、本成型の圧力が低いので、粉末成分が破壊されて液体成分が染み出して品質上問題となったり、これに起因して製造上のトラブルを発生したりすることもない。   The ability to set the pressure to a low value has an advantage that physical damage is reduced with respect to the raw material component as the main agent. In this embodiment, the raw material powder may contain a liquid component. Even in such a case, since the pressure of the main molding is low, the powder component is destroyed and the liquid component is stained. There is no problem with quality and no trouble in production due to this.

原料粉末20に加える超音波振動の条件は、原料粉末20の成分やその配合量、及び目的とする化粧料1の具体的な用途等に応じて適宜調整が可能である。化粧料1が例えばファンデーションやチークである場合には、超音波の周波数は10〜100kHz、特に15〜30kHzとすることが好ましい。この範囲の周波数とすることで、媒質である原料粉末20内での超音波の減衰の程度が小さくなり、原料粉末20の深部にまで振動が伝達される。   The conditions of the ultrasonic vibration applied to the raw material powder 20 can be appropriately adjusted according to the components of the raw material powder 20, the blending amount thereof, the specific use of the target cosmetic 1, and the like. When the cosmetic 1 is, for example, a foundation or a teak, the frequency of the ultrasonic wave is preferably 10 to 100 kHz, particularly 15 to 30 kHz. By setting the frequency within this range, the degree of attenuation of the ultrasonic wave in the raw material powder 20 that is a medium is reduced, and vibration is transmitted to the deep part of the raw material powder 20.

超音波の振幅は、化粧料1が例えばファンデーションやチークである場合には、5〜100μm、特に10〜50μmであることが好ましい。この範囲の振幅とすることで、粒子の振動が十分に大きくなり、それに起因して十分な摩擦熱が発生する。その結果、短時間での成型が可能になる。   When the cosmetic 1 is, for example, a foundation or a cheek, the ultrasonic amplitude is preferably 5 to 100 μm, particularly preferably 10 to 50 μm. By setting the amplitude within this range, the vibration of the particles becomes sufficiently large, and sufficient frictional heat is generated due to this. As a result, molding in a short time becomes possible.

超音波振動の印加時間は短時間でも十分であり、本実施形態において特に臨界的でない。この理由は、原料粉末20を挟んで上下から超音波振動を与えることに起因している。印加時間は、好ましくは0.1〜5秒、更に好ましくは0.2〜2.0秒である。油性成分の融点や配合量、原料粉末20の重量や厚みにもよるが、余りに長時間印加すると、表面が高温になり、原料の劣化、油性成分の溶融固化が進んで過剰硬度(化粧料1の使用時に粉が取りづらい)、杵への付着増加、色焼け等が発生する場合がある。   The application time of ultrasonic vibration is sufficient even for a short time, and is not particularly critical in the present embodiment. The reason for this is that ultrasonic vibration is applied from above and below across the raw material powder 20. The application time is preferably 0.1 to 5 seconds, more preferably 0.2 to 2.0 seconds. Depending on the melting point and blending amount of the oil component and the weight and thickness of the raw material powder 20, if it is applied for an excessively long time, the surface becomes high temperature, the deterioration of the raw material, the melt solidification of the oil component proceeds, and the excess hardness (cosmetics 1 It may be difficult to remove powder when using), increased adhesion to wrinkles, and color burn.

本成型が完了したら超音波振動を停止し、図6(c)に示すように上部エアシリンダ15aを動作させ、上杵16aを上昇させて成型テーブル12上の空間に待避させる。また下部エアシリンダ15bを動作させ、下杵16bも上昇させる。これによって金型13の筒状開口部から目的物である化粧料1を取り出す。   When the main molding is completed, the ultrasonic vibration is stopped, the upper air cylinder 15a is operated as shown in FIG. 6C, and the upper rod 16a is lifted and retracted in the space on the molding table 12. Further, the lower air cylinder 15b is operated and the lower rod 16b is also raised. As a result, the target cosmetic 1 is taken out from the cylindrical opening of the mold 13.

このようにして得られた化粧料1は、先に述べたとおり、ファンデーションやチーク、アイシャドウ等として用いられる。   The cosmetic 1 thus obtained is used as a foundation, teak, eye shadow or the like as described above.

以上、本発明をその好ましい実施形態に基づき説明したが、本発明は前記実施形態に制限されない。例えば前記の実施形態においては、上杵16a及び下杵16bの双方を振動させて超音波振動を印加したが、これに代えて上杵16a及び下杵16bのいずれか一方のみを用いて超音波振動を印加してもよい。   As mentioned above, although this invention was demonstrated based on the preferable embodiment, this invention is not restrict | limited to the said embodiment. For example, in the above-described embodiment, both the upper eyelid 16a and the lower eyelid 16b are vibrated and ultrasonic vibration is applied. Instead, only one of the upper eyelid 16a and the lower eyelid 16b is used for ultrasonic waves. Vibration may be applied.

また前記の実施形態においては、原料粉末20が上杵16aに付着することを防止する目的で、これらの間にポリ四フッ化エチレン製のシート等の付着防止用介在物を介在させてもよく、あるいは不織布及び/又は織布を介在させて、化粧料1の表面に網目模様を施し、化粧料1に一層の高級感を付与してもよい。   In the above-described embodiment, for the purpose of preventing the raw material powder 20 from adhering to the upper bowl 16a, an anti-adhesion inclusion such as a polytetrafluoroethylene sheet may be interposed therebetween. Alternatively, a mesh pattern may be applied to the surface of the cosmetic 1 by interposing a non-woven fabric and / or a woven fabric to give the cosmetic 1 a higher-class feeling.

以下、実施例により本発明を更に詳細に説明する。しかしながら本発明の範囲は、かかる実施例に制限されない。特に断らない限り、「%」は「質量%」を意味する。   Hereinafter, the present invention will be described in more detail with reference to examples. However, the scope of the present invention is not limited to such examples. Unless otherwise specified, “%” means “mass%”.

〔実施例1〕
図5に示す装置を用い、図6に示す方法でチークを製造した。装置10における超音波振動素子14a,14bとしては、精電舎電子工業製のランジュバン素子(発振周波数19kHz、最大出力1200W、最大振幅26μm)を用いた。粉末原料20としては、以下の表1に示す組成のものを混合して用いた。
[Example 1]
A cheek was produced by the method shown in FIG. 6 using the apparatus shown in FIG. As the ultrasonic vibration elements 14a and 14b in the apparatus 10, Langevin elements (oscillation frequency 19 kHz, maximum output 1200 W, maximum amplitude 26 μm) manufactured by Seidensha Electronics Co., Ltd. were used. As the powder raw material 20, the compositions shown in Table 1 below were mixed and used.

Figure 2010053082
Figure 2010053082

図5に示す装置を図6(a)に示す状態にして、金型の凹部に原料粉末を5g充填した。次に上杵16aを降下させて凹部内に挿入し、所定の位置で固定して図6(b)に示す状態とした。この状態下に予備成型を行った。予備成型の条件は以下の表2に示すとおりである。   The apparatus shown in FIG. 5 was changed to the state shown in FIG. 6A, and 5 g of raw material powder was filled in the concave portion of the mold. Next, the upper collar 16a was lowered and inserted into the recess, and fixed at a predetermined position, as shown in FIG. 6 (b). Pre-molding was performed under this condition. The conditions for the pre-molding are as shown in Table 2 below.

Figure 2010053082
Figure 2010053082

予備成型に引き続き、本成型を行った。本成型の条件は以下の表3に示すとおりである。   Subsequent to the preliminary molding, the main molding was performed. The conditions for the main molding are as shown in Table 3 below.

Figure 2010053082
Figure 2010053082

本成型の完了後、超音波振動を停止し、上杵を上昇・待避させ、また下杵も上昇させて、図6(c)に示すように目的物である固形粉末化粧料を金型内から取り出した。この固形粉末化粧料におけるH1は3mm、D1は24mm、H1/D1は0.125であった。   After completion of the main molding, the ultrasonic vibration is stopped, the upper eyelid is raised and retracted, and the lower eyelid is also raised, so that the solid powder cosmetic as the object is put into the mold as shown in FIG. It was taken out from. In this solid powder cosmetic, H1 was 3 mm, D1 was 24 mm, and H1 / D1 was 0.125.

〔実施例2〕
実施例1において、予備成型を行わない以外は実施例1と同様にして、同実施例と同形状で同寸の固形粉末化粧料(チーク)を製造した。
[Example 2]
In Example 1, a solid powder cosmetic (teak) having the same shape and the same size as that of Example 1 was produced in the same manner as Example 1 except that the preforming was not performed.

〔比較例1〕
前記の表1に示す原料粉末を用いて、実施例1と同形状で同寸の固形粉末化粧料の成型が可能な金型及び杵並びに加圧装置としての油圧シリンダを用いて圧力18MPaで圧縮成型した。充填量は実施例1と同じく5gであった。このようにして、固形粉末化粧料(チーク)を製造した。
[Comparative Example 1]
Using the raw material powder shown in Table 1 above, compression is performed at a pressure of 18 MPa using a mold and a punch that can form a solid powder cosmetic of the same shape and size as in Example 1 and a hydraulic cylinder as a pressurizing device. Molded. The filling amount was 5 g as in Example 1. In this way, a solid powder cosmetic (teak) was produced.

〔評価〕
実施例及び比較例で得られた固形粉末化粧料について、上述した方法で高さ方向の硬度差を測定した。また、外観の状態を目視評価した。更に、粉の取れ性を10人の専門パネラーにより官能評価し、下記基準により判定した。これらの結果を以下の表4に示す。
[Evaluation]
About the solid powder cosmetics obtained in Examples and Comparative Examples, the hardness difference in the height direction was measured by the method described above. In addition, the appearance was visually evaluated. Furthermore, sensory evaluation was performed on the powder take-off property by 10 expert panelists, and the determination was made according to the following criteria. These results are shown in Table 4 below.

〔粉の取れ性 評価〕
A:7人以上が良いと評価した。
B:4〜6人が良いと評価した。
C:2〜3人が良いと評価した。
D:1人以下が良いと評価した。
[Evaluation of powder removal]
A: Seven or more people evaluated it as good.
B: Four to six people evaluated it as good.
C: Two to three people evaluated it as good.
D: Rated less than 1 person as good.

Figure 2010053082
Figure 2010053082

表4に示す結果から明らかなように、実施例1の固形粉末化粧料(本発明品)は、比較例1の固形粉末化粧料に比べ、全体として均一な硬度を有していることが判る。また、硬度が高いにもかかわらず、粉の取れ性に優れており、また成型も首尾良く行えること判る。   As is apparent from the results shown in Table 4, it can be seen that the solid powder cosmetic of Example 1 (product of the present invention) has a uniform hardness as a whole as compared with the solid powder cosmetic of Comparative Example 1. . In addition, it can be seen that, despite its high hardness, it is excellent in powder picking and can be molded successfully.

図1は、本発明の固形粉末化粧料の一実施形態を示す斜視図である。FIG. 1 is a perspective view showing an embodiment of the solid powder cosmetic of the present invention. 図2(a)は、図1に示す化粧料の平面図であり、図2(b)及び(c)は図2(a)におけるb−b線断面図及びc−c線断面図である。Fig.2 (a) is a top view of the cosmetics shown in FIG. 1, FIG.2 (b) and (c) are the bb sectional view taken on the line in FIG.2 (a), and the cc sectional view. . 図3は、本発明に係る化粧料の別の実施形態を示す縦断面図である。FIG. 3 is a longitudinal sectional view showing another embodiment of the cosmetic according to the present invention. 図4は、化粧料の硬度を測定する部位を示す説明図である。FIG. 4 is an explanatory view showing a part for measuring the hardness of the cosmetic. 図5は、図1に示す固形粉末化粧料を製造するために用いられる好ましい装置を示す模式図である。FIG. 5 is a schematic view showing a preferred apparatus used for producing the solid powder cosmetic shown in FIG. 図6は、図5示す装置を用いた固形粉末化粧料の製造工程を示す図である。FIG. 6 is a diagram showing a manufacturing process of a solid powder cosmetic using the apparatus shown in FIG. 図7は、予備成型及び本成型の操作条件を示すグラフである。FIG. 7 is a graph showing operating conditions for pre-molding and main molding.

符号の説明Explanation of symbols

1 固形粉末化粧料
1a 上面
1b 下面
2 基面部
3 立体面部
4 凸状部
DESCRIPTION OF SYMBOLS 1 Solid powder cosmetics 1a Upper surface 1b Lower surface 2 Base surface part 3 Solid surface part 4 Convex part

Claims (8)

15質量%以下の液状成分を含む原料粉末を圧縮成型してなり、上面及び下面を有するとともに上面に凸状部を備えた略扁平な形状の固形粉末化粧料であって、
上面の基準面から凸状部の最高位置までの高さH1と、該最高位置を通り、かつ平面視において粉末化粧料の横断長が最小となるように引かれた直線における該横断長D1との比(H1/D1)が0.05〜0.4であり、粉末化粧料の高さ方向の硬度差が20%以内である固形粉末化粧料。
A solid powder cosmetic having a substantially flat shape, which is formed by compression molding a raw material powder containing a liquid component of 15% by mass or less, has an upper surface and a lower surface, and has a convex portion on the upper surface,
A height H1 from the reference surface of the upper surface to the highest position of the convex portion, and the transverse length D1 in a straight line that passes through the highest position and is minimized so that the transverse length of the powder cosmetic is minimized in plan view The ratio (H1 / D1) is 0.05 to 0.4, and the hardness difference in the height direction of the powder cosmetic is within 20%.
原料粉末を容器内で圧縮成型して得られたものである請求項1記載の固形粉末化粧料。   The solid powder cosmetic according to claim 1, wherein the raw powder is obtained by compression molding in a container. 融点が40〜150℃である固体の油性成分を0.5〜10質量%含有する原料粉末を、超音波振動を与えながら圧縮成型して得られたものである請求項1又は2記載の固形粉末化粧料。   The solid according to claim 1 or 2, which is obtained by compression molding a raw material powder containing 0.5 to 10% by mass of a solid oily component having a melting point of 40 to 150 ° C while applying ultrasonic vibration. Powder cosmetic. 圧縮成型する前に、該圧縮成型の圧力よりも低い圧力を加えた状態下に超音波振動をパルス的に印加する予備成型に付されて得られたものである請求項1ないし3のいずれかに記載の固形粉末化粧料。   The compression molding according to any one of claims 1 to 3, which is obtained by being subjected to a preliminary molding in which ultrasonic vibration is applied in a pulsed manner under a state where a pressure lower than the compression molding pressure is applied before the compression molding. The solid powder cosmetic described in 1. 縦断面における上面の形状が台形状又は上に凸のドーム状である請求項1ないし4のいずれかに記載の固形粉末化粧料。   The solid powder cosmetic according to any one of claims 1 to 4, wherein the shape of the upper surface in the longitudinal section is a trapezoidal shape or a convex dome shape. 15質量%以下の液状成分を含む原料粉末を金型内に充填し、該原料粉末を挟んで相対向してそれぞれ配された成型用杵の少なくとも一方によって該原料粉末に超音波振動を与えながら、両杵によって圧縮を加える圧縮成型を行い、上面及び下面を有するとともに上面に凸状部を備えた略扁平な形状の固形粉末化粧料を製造する方法であって、
原料粉末を圧縮成型する前に、該圧縮成型の圧力よりも低い圧力を加えた状態下に、原料粉末に超音波振動をパルス的に印加する予備成型を行う固形粉末化粧料の製造方法。
A raw material powder containing a liquid component of 15% by mass or less is filled in a mold, and ultrasonic vibration is applied to the raw material powder by at least one of molding molds arranged opposite to each other with the raw material powder sandwiched therebetween. A method for producing a solid powder cosmetic material having a substantially flat shape having a top surface and a bottom surface and having a convex portion on the top surface, by performing compression molding by applying compression with both sides,
A method for producing a solid powder cosmetic comprising performing pre-molding by applying ultrasonic vibration to a raw material powder in a pulsed manner under a state in which a pressure lower than the pressure of the compression molding is applied before compressing the raw material powder.
原料粉末を容器内で圧縮成型する請求項6記載の固形粉末化粧料の製造方法。 The method for producing a solid powder cosmetic according to claim 6, wherein the raw material powder is compression molded in a container. 原料粉末として、融点が40〜150℃である固体の油性成分を0.5〜10質量%含有するものを用いる請求項6又は7記載の製造方法。   The manufacturing method of Claim 6 or 7 which uses what contains 0.5-10 mass% of solid oily components whose melting | fusing point is 40-150 degreeC as raw material powder.
JP2008220361A 2008-08-28 2008-08-28 Solid powder cosmetic and method for producing the same Expired - Fee Related JP5469833B2 (en)

Priority Applications (5)

Application Number Priority Date Filing Date Title
JP2008220361A JP5469833B2 (en) 2008-08-28 2008-08-28 Solid powder cosmetic and method for producing the same
CN200980131982.5A CN102123854B (en) 2008-08-28 2009-08-28 Powder compacting device and method for manufacturing solid powder compact
EP09810047A EP2329945A4 (en) 2008-08-28 2009-08-28 Powder compacting device and method for manufacturing solid powder compact
PCT/JP2009/065095 WO2010024399A1 (en) 2008-08-28 2009-08-28 Powder compacting device and method for manufacturing solid powder compact
US13/060,913 US20120139164A1 (en) 2008-08-28 2009-08-28 Powder compacting device and method for manufacturing solid powder compact

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP2008220361A JP5469833B2 (en) 2008-08-28 2008-08-28 Solid powder cosmetic and method for producing the same

Publications (2)

Publication Number Publication Date
JP2010053082A true JP2010053082A (en) 2010-03-11
JP5469833B2 JP5469833B2 (en) 2014-04-16

Family

ID=42069372

Family Applications (1)

Application Number Title Priority Date Filing Date
JP2008220361A Expired - Fee Related JP5469833B2 (en) 2008-08-28 2008-08-28 Solid powder cosmetic and method for producing the same

Country Status (1)

Country Link
JP (1) JP5469833B2 (en)

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2010052003A (en) * 2008-08-28 2010-03-11 Kao Corp Powder compression molding device
JP2011011224A (en) * 2009-06-30 2011-01-20 Kao Corp Method for producing solid powder molding
JP2012229171A (en) * 2011-04-25 2012-11-22 Kao Corp Method for producing solid powdered cosmetic

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS63275511A (en) * 1987-05-07 1988-11-14 Kobayashi Kooc:Kk Molding of powder cosmetic
JP2001213721A (en) * 2000-01-31 2001-08-07 Kao Corp Solid powder cosmetic

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS63275511A (en) * 1987-05-07 1988-11-14 Kobayashi Kooc:Kk Molding of powder cosmetic
JP2001213721A (en) * 2000-01-31 2001-08-07 Kao Corp Solid powder cosmetic

Non-Patent Citations (2)

* Cited by examiner, † Cited by third party
Title
JPN7013002765; 新化粧品学 第2版, 20010118, 408頁, 南山堂 *
JPN7013002766; 香粧品製造学 技術と実際 第1版第1刷, 20010825, 164〜165頁, フレグランスジャーナル社 *

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2010052003A (en) * 2008-08-28 2010-03-11 Kao Corp Powder compression molding device
JP2011011224A (en) * 2009-06-30 2011-01-20 Kao Corp Method for producing solid powder molding
JP2012229171A (en) * 2011-04-25 2012-11-22 Kao Corp Method for producing solid powdered cosmetic

Also Published As

Publication number Publication date
JP5469833B2 (en) 2014-04-16

Similar Documents

Publication Publication Date Title
JP5379579B2 (en) Manufacturing method of solid powder molding
JP5469833B2 (en) Solid powder cosmetic and method for producing the same
TWI438008B (en) Cosmetic manufacturing method
CN106572946A (en) Multi-composition cosmetic products and method for manufacturing same
JP2001213721A (en) Solid powder cosmetic
JPH01106807A (en) Method of squeezing powdery cosmetic blend
JP2520638B2 (en) Molding method for powder cosmetics
JP2010285409A (en) Method for producing solid powder cosmetic product
JPH08154732A (en) Production of cosmetic products
JP2001354519A (en) Solid powder cosmetic packed in container
JP4963466B2 (en) Solid cosmetic and method for producing the same
JP2891731B2 (en) Manufacturing method of pressed cosmetics
JP4592613B2 (en) Disintegrating tablet and method for producing the same
JP2671242B2 (en) Method for producing convex solid powder cosmetic
JP2003334699A (en) Pressure molding machine for solid powder
JP4454351B2 (en) Method for producing compression molded body
JP4454409B2 (en) Method for producing compression molded body
JP2010120082A (en) Powder compression molding apparatus and powder compression molding method
JPS624218A (en) Production of solid powder cosmetic having convex form
WO2023074412A1 (en) Press head production method, press head production system, and press head
JP5295885B2 (en) Manufacturing method of solid powder molding
JP5785766B2 (en) Method for producing solid powder cosmetic
JP6075874B2 (en) Powder compression molding equipment
JP2020132582A (en) Cosmetic manufacturing method and cosmetics
JP2018140973A (en) Bath agent

Legal Events

Date Code Title Description
A621 Written request for application examination

Free format text: JAPANESE INTERMEDIATE CODE: A621

Effective date: 20110610

A131 Notification of reasons for refusal

Free format text: JAPANESE INTERMEDIATE CODE: A131

Effective date: 20130618

A521 Written amendment

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20130808

TRDD Decision of grant or rejection written
A01 Written decision to grant a patent or to grant a registration (utility model)

Free format text: JAPANESE INTERMEDIATE CODE: A01

Effective date: 20140107

A61 First payment of annual fees (during grant procedure)

Free format text: JAPANESE INTERMEDIATE CODE: A61

Effective date: 20140203

R151 Written notification of patent or utility model registration

Ref document number: 5469833

Country of ref document: JP

Free format text: JAPANESE INTERMEDIATE CODE: R151

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

LAPS Cancellation because of no payment of annual fees