JP2009219393A - Luxury drink containing non-caffeine milk - Google Patents

Luxury drink containing non-caffeine milk Download PDF

Info

Publication number
JP2009219393A
JP2009219393A JP2008065968A JP2008065968A JP2009219393A JP 2009219393 A JP2009219393 A JP 2009219393A JP 2008065968 A JP2008065968 A JP 2008065968A JP 2008065968 A JP2008065968 A JP 2008065968A JP 2009219393 A JP2009219393 A JP 2009219393A
Authority
JP
Japan
Prior art keywords
milk
caffeine
beverage
sugar
weight
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
JP2008065968A
Other languages
Japanese (ja)
Other versions
JP4642090B2 (en
Inventor
Yukiko Nakajima
有樹子 中島
Yuko Yotsumoto
祐子 四元
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Kirin Beverage Corp
Kirin Brewery Co Ltd
Original Assignee
Kirin Beverage Corp
Kirin Brewery Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Kirin Beverage Corp, Kirin Brewery Co Ltd filed Critical Kirin Beverage Corp
Priority to JP2008065968A priority Critical patent/JP4642090B2/en
Publication of JP2009219393A publication Critical patent/JP2009219393A/en
Application granted granted Critical
Publication of JP4642090B2 publication Critical patent/JP4642090B2/en
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Landscapes

  • Dairy Products (AREA)
  • Non-Alcoholic Beverages (AREA)

Abstract

<P>PROBLEM TO BE SOLVED: To provide packaged a luxury drink containing non-caffeine milk having excellent flavor, and to provide a method for producing the favorite drink. <P>SOLUTION: This packaged luxury drink containing non-caffeine milk, which is given with caffeine-containing drink-like bitterness and body, is obtained by mixing with milk components, 1-10 wt.% of roast sugar which has an absorbance of 360 nm of 0.04-0.9 when in the form of an aqueous solution of a Brix degree of 0.1° Bx, and pH of 2.0-4.0 when in the form of an aqueous solution of 10° Bx, and 0.1-0.2 wt.% of common salt. The packaged luxury drink containing non-caffeine milk has bitterness and body like caffeine drink such as coffee and black tea, even without using a raw material to be used for a drink containing milk, such as coffee and black tea, and has no caffeine. <P>COPYRIGHT: (C)2010,JPO&INPIT

Description

本発明は、新規容器詰ノンカフェイン乳入り嗜好性飲料、及びその製造方法に関し、特に、通常乳入り飲料に用いられるコーヒーや紅茶などの原料を使用しなくても、該コーヒーや紅茶などのカフェイン飲料風の苦味やコクを有しており、しかも、ノンカフェインである新規容器詰乳入り嗜好性飲料及びその製造方法に関する。   The present invention relates to a novel container-packed non-caffeinated milk-containing palatability beverage and a method for producing the same, and in particular, without using raw materials such as coffee and tea usually used in milk-containing beverages, such as coffee and tea. The present invention relates to a beverage having a caffeine-like bitterness and richness, and a non-caffeine-containing new packaged milk-containing taste beverage and a method for producing the same.

近年、飲料製造技術の進展や冷蔵輸送網の発達などにともない、容器詰飲料の形態で、冷蔵状態で流通・保存されるチルド飲料のカテゴリーの商品が多く販売されるようになっている。チルド飲料は、冷蔵輸送すること、賞味期間を通常の容器詰め飲料に比べて短縮することにより、殺菌条件を緩和できるという特性を有する。それに伴い加熱殺菌による風味の低下が抑えられることもあって、従来の容器詰め飲料よりも優れた香味の製品が増えて人気を博している。そのなかでも乳成分を比較的多量に含んだ乳入り飲料は、従来の容器詰め飲料と比べた場合に香味の差別性が明確であることもあって、チルド飲料の中では重要な位置を占めている。   In recent years, with the progress of beverage production technology and the development of refrigerated transport networks, many products in the category of chilled beverages that are distributed and stored in a refrigerated state in the form of packaged beverages are being sold. Chilled beverages have the property that sterilization conditions can be relaxed by transporting them in a refrigerator and shortening the best-before period as compared to ordinary container-packed beverages. Along with this, a decrease in flavor due to heat sterilization is suppressed, and flavor products superior to conventional container-packed beverages are increasing in popularity. Among them, milk-containing beverages that contain a relatively large amount of milk components occupy an important position among chilled beverages, as the distinction of flavor is clear when compared to conventional container-packed beverages. ing.

この乳成分を多く含む乳入り飲料は、一般的にコーヒーや紅茶の抽出物と混合して販売されている。その理由の一つとしては、一定の乳成分量の下ではコーヒーや茶類の抽出液を配合しないと、飲料全体のコク味が充分感じられないという香味設計上の問題があげられる。もちろん、乳成分量を増加させればその問題の一部は解決できるが、その対応は飲料の原材料費の増加につながるので実用化という面では必ずしも容易ではないという事情がある。   Milk-containing beverages containing a large amount of milk components are generally sold in a mixture with coffee and tea extracts. One reason for this is the flavor design problem that the full taste of the beverage cannot be fully felt unless a coffee or tea extract is blended under a certain amount of milk components. Of course, if the amount of milk components is increased, a part of the problem can be solved, but since the response leads to an increase in the raw material cost of the beverage, there is a situation that it is not always easy in practical use.

また、近年の飲食品に対する健康志向に伴って、飲料の分野でも、ノンカフェイン飲料に対する消費者の要望がある。その場合には、乳入り飲料としての高い嗜好性があったとしても、前述のようにコーヒーや紅茶を使用するとその消費者の要望には応えられないことになる。そこで、かかる消費者の要望に応えるために、コーヒー豆や紅茶葉、更にはそれらの抽出液から、超臨界ガス抽出処理や活性炭などの吸着剤処理によってカフェインを除く技術も提案されているので(特開2006−174746号公報、特開平7−313062号公報、特開平5−219889号公報)、乳入り飲料の調製に際して、それらの脱カフェインされた原料を使用することでこの問題を解決することも考えられる。しかし、それらのいくつかは実用化されているものの、まだコストが高く、更に、脱カフェイン処理をしているために、カフェイン自体の持つ苦味やコクが失われ、得られる製品の香味も充分でないという問題も残っており、一般の商品に汎用的に使用できるという段階には至っていない。   In addition, with the recent health consciousness of food and drink, there is a consumer demand for non-caffeinated drinks in the field of beverages. In that case, even if there is a high palatability as a milk-containing beverage, if the coffee or tea is used as described above, the demand of the consumer cannot be met. Therefore, in order to meet the demands of such consumers, a technology has also been proposed in which caffeine is removed from coffee beans, tea leaves, and their extracts by supercritical gas extraction treatment or adsorbent treatment such as activated carbon. (Japanese Patent Laid-Open No. 2006-174746, Japanese Patent Laid-Open No. 7-313062, Japanese Patent Laid-Open No. 5-219889), in the preparation of milk-containing beverages, this problem is solved by using these decaffeinated ingredients. It is also possible to do. However, although some of them have been put to practical use, they are still expensive, and because they are decaffeinated, the bitterness and richness of caffeine itself are lost, and the flavor of the product obtained is also The problem that it is not enough remains, and it has not reached the stage where it can be used for general products for general purposes.

そこで、コーヒーや茶類等のようなカフェイン含有飲料成分以外の成分を添加することによって、乳入り飲料のコク味をあげる技術も提案されている。例えば、特開平8−23878号公報には、ミルク入り飲料に、カルシウム塩を添加することで、及び、特開2007−215451号公報には、乳製品を含有する飲料に、ナトリウム塩、カリウム塩、カルシウム塩、マグネシウム塩のような塩類を0.0005〜0.1質量%を添加することでコク味と旨味を強化した飲料が開示されている。しかし、これは実施例からも明らかなようにあくまでも乳入りコーヒーなどの飲料に隠し味的に少量配合することを想定しており、カフェイン含有飲料成分を含有しない新たな嗜好性飲料を作ろうとするものではない。因みに、乳入りの容器詰め飲料に対して味覚調整のために極少量の食塩を配合するという技術は従来より一般的に使用されていた技術にとどまるものである。   Then, the technique which raises the richness of a milk-containing drink by adding components other than caffeine-containing beverage components such as coffee and tea has been proposed. For example, JP-A-8-23878 discloses adding a calcium salt to a beverage containing milk, and JP-A-2007-215451 discloses a sodium salt and potassium salt in beverages containing dairy products. In addition, beverages with enhanced richness and umami taste by adding 0.0005 to 0.1 mass% of salts such as calcium salt and magnesium salt are disclosed. However, as is apparent from the examples, it is assumed that a small amount is hidden in a beverage such as coffee with milk, and a new palatability beverage that does not contain caffeine-containing beverage ingredients is prepared. Not what you want. Incidentally, the technique of blending an extremely small amount of salt for taste adjustment in a container-packed beverage containing milk is a technique that has been generally used conventionally.

カフェイン含有飲料成分以外の成分を添加することによって、乳入り飲料のコク味をあげる他の方法として、食物繊維やデキストリンなどを使ったり(特開2004−41118号公報)、適当な香料を添加したりすることにより、ボディ感、コク味を出すことが知られている。しかし、これらもあくまでもそれだけで成立する技術ではなく、乳入りコーヒー飲料や、乳入り紅茶飲料の味覚の調整といった範囲に留まるものである。したがって、これまでに、乳入り飲料において、その苦味やコク味を付与するために、従来行なわれているコーヒーや茶類等のようなカフェイン含有飲料成分の添加に代替えできる嗜好性の高い飲料の調製法は提案されていない。   By adding ingredients other than caffeine-containing beverage ingredients, dietary fiber, dextrin, etc. can be used as another method for increasing the richness of beverages containing milk (Japanese Patent Application Laid-Open No. 2004-41118), or appropriate flavors are added. It is known to give a feeling of body and richness by doing. However, these are not techniques that are established by itself, and are limited to the range of adjustment of the taste of coffee coffee with milk and tea drink with milk. Therefore, to date, beverages with high palatability that can replace the conventional addition of caffeine-containing beverage ingredients such as coffee and tea to impart the bitterness and richness in milk-containing beverages. No preparation method has been proposed.

一方で、従来より、カスタードプリンのようなゲル化食品の調製に際して、ゲル化食品の着色或いは味付けの目的から、砂糖を焙煎(ロースト)し、カラメル化したカラメルソースが用いられている。カラメルソースは、通常、砂糖類を水と併せて火にかけ、180℃位で、混ぜないで煮詰め、砂糖が煮詰まってチョコレート色になった(カラメル化した)時点で、熱湯を注いで、かき混ぜ溶解し調製される。カラメルソースは、特に、着色或いは味付けの目的から、容器詰めカスタードプリンのような多層プディングの上層等に用いられている(特開平8−154611号公報、特開平10−313799号公報、特開平11−243892号公報)。   On the other hand, conventionally, when preparing a gelled food product such as custard pudding, a caramel sauce obtained by roasting sugar and caramelizing it has been used for the purpose of coloring or seasoning the gelled food product. Caramel sauce is usually cooked with water and sugar at 180 ° C, boiled without mixing, and when the sugar is boiled and becomes chocolate-colored (caramelized), pour hot water and stir to dissolve. Prepared. Caramel sauce is used for the upper layer of a multilayer pudding such as a custard pudding packed in a container for the purpose of coloring or seasoning (Japanese Patent Laid-Open Nos. 8-154611, 10-313799, and 11). -243892).

また、焙煎(ロースト)した砂糖を食品の調製に用いる例として、砂糖類を乾熱下、140℃〜150℃に到達するまで加熱・焙煎することにより製造した、2.5重量%濃度水溶液の波長280nmにおける吸光度が0.15〜0.95の焙煎糖を、高級アイスクリームやチョコレート利用食品に添加したものが開示されている(特開平10−33126号公報)。この開示のものは、従来のカラメルや、カラメルソースに用いられる焙煎糖に比較して、140℃〜150℃という比較的低温で焙煎し、特定の吸光度のものに調整することによって、香気成分を調整した焙煎糖を、高級アイスクリームに配合して、該アイスクリームの風味レベルを変えないで、該アイスクリームに配合するバニラ香料を半減したり、或いは、チョコレート利用食品に配合して、その雑味、苦味及び渋味を軽減することを狙ったものである。しかし、該公報に記載のものにおいては、かかる焙煎糖とコーヒーや紅茶のようなカフェイン含有飲料の香味・風味の関係については、何も記載されていない。   In addition, as an example of using roasted (roasted) sugar for the preparation of food, 2.5% by weight concentration produced by heating and roasting sugar under dry heat until reaching 140 ° C to 150 ° C. A solution in which roasting sugar having an absorbance of 0.15 to 0.95 at a wavelength of 280 nm of an aqueous solution is added to high-grade ice cream or chocolate-based food is disclosed (Japanese Patent Laid-Open No. 10-33126). Compared with conventional caramel and roasted sugar used in caramel sauce, the disclosure disclosed herein is roasted at a relatively low temperature of 140 ° C. to 150 ° C. and adjusted to have a specific absorbance. Mixing roasted sugar with adjusted ingredients in high-grade ice cream, without changing the flavor level of the ice cream, halving the vanilla flavor added to the ice cream, or blending it into chocolate-based foods It aims to reduce its miscellaneous taste, bitterness and astringency. However, in the publication described in the publication, nothing is described about the relationship between the roasted sugar and the flavor and flavor of caffeine-containing beverages such as coffee and tea.

特開平5−219889号公報。Japanese Patent Laid-Open No. 5-219898. 特開平7−313062号公報。JP-A-7-313062. 特開平8−23878号公報。JP-A-8-23878. 特開平8−154611号公報。JP-A-8-154611. 特開平10−33126号公報。JP-A-10-33126. 特開平10−313799号公報。Japanese Patent Application Laid-Open No. 10-313799. 特開平11−243892号公報。Japanese Patent Application Laid-Open No. 11-243892. 特開2004−41118号公報。Japanese Patent Application Laid-Open No. 2004-41118. 特開2006−174746号公報。JP 2006-174746 A. 特開2007−215451号公報。JP 2007-215451 A.

本発明の課題は、優れた香味の新規容器詰ノンカフェイン乳入り嗜好性飲料、及びその製造方法を提供すること、特に、通常乳入り飲料に用いられるコーヒーや紅茶などの原料を使用しなくても、該コーヒーや紅茶などのカフェイン飲料風の苦味やコクを有しており、しかも、ノンカフェインである新規容器詰乳入り嗜好性飲料及びその製造方法を提供することにある。   It is an object of the present invention to provide a novel container-packed non-caffeinated milk-flavored beverage with excellent flavor and a method for producing the same, and in particular, without using raw materials such as coffee and tea normally used in milk-containing beverages. However, it is to provide a palatable beverage with a caffeine-like bitterness and richness such as the coffee and tea, and a non-caffeine-filled palatable milk-like taste beverage and a method for producing the same.

本発明者は、上記課題を達成するために乳入り嗜好性飲料の調製に際して配合するノンカフェイン配合原料について鋭意検討を行なう中で、乳成分を含む飲料に対して、特定の焙煎条件において焙煎し、特定のブリックス度における水溶液が特定の吸光度及びpHを有するローストシュガー(焙煎糖)を特定量配合し、更に、特定量の食塩を配合することにより、従来のように、乳入り飲料に用いられるコーヒーや紅茶などのカフェイン飲料原料を使用しなくても、該コーヒーや紅茶などのカフェイン飲料風の苦味やコクを有しており、しかも、ノンカフェインである新規な容器詰乳入り嗜好性飲料を提供することができることを見い出し、本発明を完成するに至った。   In order to achieve the above-mentioned problems, the present inventor has been diligently studying the non-caffeine blending raw material blended in the preparation of a palatable beverage containing milk, and in a specific roasting condition for a beverage containing a milk component. By roasting and mixing a specific amount of roasted sugar (roasted sugar) whose aqueous solution at a specific Brix degree has a specific absorbance and pH, and then adding a specific amount of salt, it contains milk as before. A novel container that has a bitter taste and richness of caffeine beverages such as coffee and tea without using caffeine beverage ingredients such as coffee and tea used for beverages, and is non-caffeine The present inventors have found that a palatable beverage containing packed milk can be provided, and have completed the present invention.

すなわち、本発明は、乳成分を含む飲料であって、乳成分に、ブリックス度0.1°Bxの水溶液にした場合に360nmの吸光度が0.04以上0.9以下であり、10°Bxの水溶液にした場合にpHが2.0以上、4.0以下であるローストシュガーを1〜10重量%と、食塩を0.1〜0.2重量%配合することにより、カフェイン含有飲料風苦味とコクを付与した新規容器詰ノンカフェイン乳入り嗜好性飲料を提供することからなる。本発明においては、ローストシュガーが、ブリックス度0.1°Bxの水溶液にした場合に360nmの吸光度が0.1〜0.8の範囲であるものが特に好ましい。該ローストシュガーの360nmの吸光度において、0.04より小さい(淡色)の場合、苦味が足りず、飲料配合時に十分なコク感を与えることができない。また、0.9より大きい(濃色)の場合、雑味(酸味、えぐみ、不快な苦味など)が生じ、また、配合した飲料の液色がカラメル色素の影響で濃くなり、商品として良好な香味・外観のバランスに調製することが難しいなど、商品の官能(香味・外観)に望ましくない影響を与える。   That is, the present invention is a beverage containing a milk component, and when the milk component is made into an aqueous solution having a Brix degree of 0.1 ° Bx, the absorbance at 360 nm is 0.04 or more and 0.9 or less, and 10 ° Bx Caffeine-containing beverage style by blending 1 to 10% by weight of roasted sugar having a pH of 2.0 or more and 4.0 or less and 0.1 to 0.2% by weight of sodium chloride. It consists in providing a new container-packed non-caffeinated milk-flavored beverage with a bitterness and richness. In the present invention, it is particularly preferable that the roasted sugar has an absorbance at 360 nm in the range of 0.1 to 0.8 when the aqueous solution has a Brix degree of 0.1 ° Bx. When the absorbance at 360 nm of the roasted sugar is less than 0.04 (light color), the bitterness is insufficient, and a sufficient rich feeling cannot be given when blending beverages. In addition, when it is greater than 0.9 (dark color), a miscellaneous taste (acidity, sardine, unpleasant bitterness, etc.) occurs, and the liquid color of the blended beverage becomes dark due to the effect of caramel color, which is good as a product. It has an undesirable effect on the sensation (flavor / appearance) of the product, for example, it is difficult to adjust to a balanced flavor / appearance.

本発明において用いられるローストシュガーは、糖類を170℃になるまで緩やかに焙煎・加熱し、加熱停止後余熱で180℃になることを確認した後、反応を終了させることにより調製することができる。本発明において、ローストシュガー調製に用いられる糖類としては、砂糖が特に好ましい。また、本発明において、容器詰ノンカフェイン乳入り嗜好性飲料の配合成分の特に好ましい割合としては、乳成分の量が、乳固形分として1〜11重量%、ローストシュガー量が2〜5重量%、食塩が0.1〜0.2重量%の配合割合を挙げることができる。   The roasted sugar used in the present invention can be prepared by slowly roasting and heating the saccharide until it reaches 170 ° C., and after confirming that the residual heat reaches 180 ° C. after stopping the heating. . In the present invention, sugar is particularly preferable as the saccharide used for the roasted sugar preparation. Moreover, in this invention, as a particularly preferable ratio of the compounding component of the non-caffeinated milk-containing palatable beverage, the amount of the milk component is 1 to 11% by weight as the milk solid content, and the roasted sugar amount is 2 to 5%. %, And a salt content of 0.1 to 0.2% by weight.

本発明の容器詰ノンカフェイン乳入り嗜好性飲料は、冷蔵状態で流通・保存されるチルド飲料として、流通・保存に供することができる。   The packaged non-caffeinated milk-containing palatable beverage of the present invention can be used for distribution and storage as a chilled beverage distributed and stored in a refrigerated state.

すなわち具体的には本発明は、(1)乳成分を含む飲料であって、乳成分に、ブリックス度0.1°Bxの水溶液にした場合に360nmの吸光度が0.04以上0.9以下であり、10°Bxの水溶液にした場合にpHが2.0以上、4.0以下であるローストシュガーを1〜10重量%と、食塩を0.1〜0.2重量%配合したことを特徴とするカフェイン含有飲料風苦味とコクを付与した容器詰ノンカフェイン乳入り嗜好性飲料や、(2)ローストシュガーが、砂糖を原料として調製したものであることを特徴とする上記(1)記載のカフェイン含有飲料風苦味とコクを付与した容器詰ノンカフェイン乳入り嗜好性飲料からなる。   That is, the present invention specifically relates to (1) a beverage containing a milk component, and when the milk component is an aqueous solution having a Brix degree of 0.1 ° Bx, the absorbance at 360 nm is 0.04 or more and 0.9 or less. 1 to 10% by weight of roasted sugar having a pH of 2.0 or more and 4.0 or less and 0.1 to 0.2% by weight of sodium chloride in a 10 ° Bx aqueous solution. The above-mentioned (1), characterized in that the caffeine-containing beverage-like bitterness and richness of the caffeine-containing non-caffeine milk-flavored beverage, and (2) roasted sugar prepared from sugar as a raw material (1) ) A caffeine-containing beverage-like bitter taste and richness as described above.

また本発明は、(3)乳成分の量が、乳固形分として1〜11重量%であって、ローストシュガー量が2〜5重量%、食塩が0.1〜0.2重量%であるであることを特徴とする上記(1)又は(2)記載のカフェイン含有飲料風苦味とコクを付与した容器詰ノンカフェイン乳入り嗜好性飲料や、(4)糖類を170℃になるまで緩やかに焙煎・加熱し、加熱停止後余熱で180℃になることを確認した後、反応を終了させることにより、ブリックス度0.1°Bxの水溶液にした場合に360nmの吸光度が0.04以上0.9以下であり、10°Bxの水溶液にした場合にpHが2.0以上、4.0以下であるローストシュガーを調製し、該ローストシュガーを乳成分に1〜10重量%、更に、食塩を0.1〜0.2重量%配合し、常法により容器に充填したことを特徴とするカフェイン含有飲料風苦味とコクを付与した容器詰ノンカフェイン乳入り嗜好性飲料の製造方法からなる。   In the present invention, (3) the amount of the milk component is 1 to 11% by weight as the milk solid content, the amount of roasted sugar is 2 to 5% by weight, and the salt is 0.1 to 0.2% by weight. The above-mentioned (1) or (2) caffeine-containing beverage-like bitterness and richness-contained non-caffeine milk-containing palatability beverage, or (4) sugar until 170 ° C. After slowly roasting and heating, after confirming that the residual heat reaches 180 ° C. after stopping the heating, the reaction is terminated, whereby the absorbance at 360 nm is 0.04 when the aqueous solution has a Brix degree of 0.1 ° Bx. The roast sugar having a pH of 2.0 or more and 4.0 or less when the aqueous solution is 10 ° Bx or more is 0.9 or less, and the roast sugar is added to the milk component in an amount of 1 to 10% by weight. , 0.1 to 0.2% by weight of salt, It consists of a method for producing a non-caffeinated milk-containing palatable beverage with a caffeine-containing beverage-like bitterness and richness that is characterized by being filled in a container.

本発明により提供される容器詰ノンカフェイン乳入り嗜好性飲料は、コーヒーや紅茶などカフェインを含む原料を用いなくても、カフェイン含有飲料が本来持つような、深いコクと若干の苦味が付与され、更には甘味の強いベースにおいても後切れが良く甘さが口に残らない優れた香味を有する。また、本発明の容器詰ノンカフェイン乳入り嗜好性飲料は、液色についてもコーヒーや紅茶のような茶色い液色をしており、濃い味をイメージすることができる非常に嗜好性が高い新規飲料を提供する。   The non-caffeinated milk-flavored beverage provided by the present invention has a deep body and a slight bitterness that caffeine-containing beverages originally have, without using caffeine-containing ingredients such as coffee and tea. Furthermore, even in a base having a strong sweetness, it has an excellent flavor with a good finish and a sweetness that does not remain in the mouth. In addition, the non-caffeinated milk-flavored beverage of the present invention has a brown liquid color such as coffee and tea with respect to the liquid color, and has a very high palatability that can image a deep taste. Provide beverages.

本発明は、糖類を170℃になるまで緩やかに焙煎・加熱し、加熱停止後余熱で180℃になることを確認した後、反応を終了させることにより、ブリックス度0.1°Bxの水溶液にした場合に360nmの吸光度が0.04以上であり、10°Bxの水溶液にした場合にpHが3.6以下であるローストシュガーを調製し、該ローストシュガーを乳成分に1〜10重量%、更に、食塩を0.1〜0.2重量%配合し、常法により容器に充填することにより、カフェイン含有飲料風苦味とコクを付与した新規容器詰ノンカフェイン乳入り嗜好性飲料を提供することからなる。   In the present invention, the sugar is slowly roasted and heated to 170 ° C. After confirming that the residual heat reaches 180 ° C. after the heating is stopped, the reaction is terminated, whereby an aqueous solution having a Brix degree of 0.1 ° Bx is obtained. When prepared, a roasted sugar having an absorbance at 360 nm of 0.04 or more and a pH of 3.6 or less when prepared as a 10 ° Bx aqueous solution is prepared, and the roasted sugar is added to the milk component in an amount of 1 to 10% by weight. Furthermore, a novel non-caffeinated milk-containing palatable beverage containing caffeine-containing beverage-like bitterness and richness by adding 0.1 to 0.2% by weight of sodium chloride and filling the container in a conventional manner Consist of providing.

<乳入り飲料>
本発明で対象とする乳成分を含む乳入り飲料とは、乳成分を乳固形分として0.1重量%以上含むものが該当する。ただし、本発明の効果が顕著に得られるという意味では乳固形分1〜9重量%(牛乳を用いた場合、牛乳の量:約10〜70重量%)含むものが好ましい。本発明でいう乳とは、牛由来の牛乳を前提としているが、そのほかの動物、例えばヤギ由来のものであっても構わない。また、牛乳をそのまま乾燥粉末化した全脂粉乳や、それから脂肪分を抜いた脱脂粉乳も牛乳の代替として用いられる。
<Milk drink>
The milk-containing beverage containing a milk component as a target in the present invention corresponds to a beverage containing 0.1% by weight or more of a milk component as a milk solid content. However, in the sense that the effects of the present invention are remarkably obtained, those containing 1 to 9% by weight of milk solid content (when milk is used, the amount of milk: about 10 to 70% by weight) are preferable. The milk referred to in the present invention is premised on cow-derived milk, but may be derived from other animals such as goats. In addition, whole milk powder milk obtained by directly converting milk into dry powder and skim milk powder from which fat has been removed are also used as an alternative to milk.

<ローストシュガー>
本発明で使用するローストシュガーとは、0.1°Bxの水溶液にした場合360nmの吸光度が0.04以上0.9以下、好ましくは0.1以上0.8以下であって、10°Bxの水溶液にした場合に、pHが2.0以上4.0以下、好ましくは2.5以上3.6以下であるローストシュガーとして定義される。この数値範囲以外のものは、苦味を中心とした香味、外観或いは品質の安定性などの点で本発明に使用するには適さない。本発明のローストシュガーを調製するための糖類としては、通常、例えば、砂糖・果糖・はちみつ・メープルシロップなどの糖類甘味料を用いることができるが、特に、該糖類に限定されない。また、該ローストシュガーとして、池田糖化工業株式会社や昭和化学工業株式会社などから販売されている市販品の「ローストシュガー」から適宜選択することで入手することができる。
<Roasted sugar>
The roasted sugar used in the present invention has an absorbance at 360 nm of 0.04 or more and 0.9 or less, preferably 0.1 or more and 0.8 or less when an aqueous solution of 0.1 ° Bx is used. Is defined as roasted sugar having a pH of 2.0 or more and 4.0 or less, preferably 2.5 or more and 3.6 or less. Those outside this numerical range are not suitable for use in the present invention in terms of flavor, appearance, and quality stability centered on bitterness. As the saccharide for preparing the roasted sugar of the present invention, saccharide sweeteners such as sugar, fructose, honey, and maple syrup can be usually used, but are not particularly limited to the saccharide. In addition, the roasted sugar can be obtained by appropriately selecting from commercially available “roasted sugar” sold by Ikeda Sakuka K.K.

本発明において、ローストシュガーを調製するには、糖類を、例えば、約1〜3時間かけて、略170℃(170〜175℃程度)になるまで加熱(融解)する。加熱に際して、一定の攪拌を行なうことにより、加熱加温反応の進行を調整することができる。所定温度(略170℃)に達したら加熱処理を終了し、引き続き、余熱で180℃程度に達温させる。この間に、加熱(融解)したローストシュガーの外観(着色)及び香味の変化の進行・調整を行うことができる。余熱加温反応の進行は、一定の攪拌を行なうことにより調整することができる。余熱加温反応の終了後、必要量の湯又は水の添加、及び攪拌の強度調整(強く)により、更に冷却すると共に、調製したローストシュガーを所定の物性値(吸光度、pH)に調整する。これらの工程により、所望の官能(色、外観、香味)及び物性に調整されたローストシュガーを得ることができる。本発明において、ローストシュガーは、飲料に対して、1−10重量%、好ましくは2−5重量%の範囲で添加する。それよりも少ないと本発明の効果が得られにくく、多いと苦くなりすぎて飲料の嗜好性が低下してしまう。   In the present invention, to prepare roasted sugar, the saccharide is heated (melted) to about 170 ° C. (about 170 to 175 ° C.), for example, over about 1 to 3 hours. During the heating, the progress of the heating and warming reaction can be adjusted by performing constant stirring. When the temperature reaches a predetermined temperature (approximately 170 ° C.), the heat treatment is terminated, and subsequently the temperature is increased to about 180 ° C. with residual heat. During this time, the appearance (coloring) and flavor change of the heated (melted) roasted sugar can be progressed and adjusted. The progress of the preheating heating reaction can be adjusted by carrying out constant stirring. After the preheating warming reaction is completed, the required amount of hot water or water is added and the strength of stirring is further adjusted (strongly), and the prepared roast sugar is adjusted to predetermined physical properties (absorbance, pH). By these steps, roasted sugar adjusted to the desired functionality (color, appearance, flavor) and physical properties can be obtained. In the present invention, roasted sugar is added in a range of 1 to 10% by weight, preferably 2 to 5% by weight, based on the beverage. If it is less than that, it is difficult to obtain the effect of the present invention.

<食塩>
本発明で使用する食塩は、通常の食用の塩化ナトリウムでよい。配合量は0.1重量%以上、0.2重量%以下とする。好ましくは0.15重量%である。これ以下だと、本発明効果が得られにくく、多いと塩味が強くなりすぎて嗜好性が損なわれる。
<Salt>
The salt used in the present invention may be normal edible sodium chloride. The blending amount is 0.1% by weight or more and 0.2% by weight or less. Preferably it is 0.15 weight%. If it is less than this, the effect of the present invention is difficult to obtain, and if it is too much, the salty taste becomes too strong and the palatability is impaired.

<飲料の製造法>
本発明の容器詰め飲料は通常の乳性飲料の製造法に従って製造すればよい(「最新ソフトドリンクス 光淋」参照)。なお、本発明の飲料に使用する原料としては、乳原料、ローストシュガー・食塩以外に、・糖類・乳化剤・安定剤・香料などが挙げられるが、これに限られない。飲料に使用できる原料であって本発明の作用効果を阻害しないものであればいずれも使用できる。
<Beverage production method>
What is necessary is just to manufacture the container-packed drink of this invention in accordance with the manufacturing method of a normal dairy drink (refer to "the latest soft drinks Korin"). In addition to milk raw materials and roasted sugar / salt, the raw materials used in the beverage of the present invention include, but are not limited to, sugars, emulsifiers, stabilizers, fragrances, and the like. Any raw material that can be used in beverages and does not impair the effects of the present invention can be used.

<製品、流通形態>
本発明の嗜好性飲料の製品形態としては、容器詰飲料として調製され、該容器形態としては、PETボトル、缶、壜、紙容器、チルドカップなどを想定することができる。流通形態としては、常温流通、チルド流通のどちら向けの製品にでも対応可能であるが、香味の点で殺菌強度の低いチルド流通向けの飲料、チルド飲料が望ましい。又、ドライ流通品として製造を行う際は、容器がPETボトルの際はアセプティック充填を行い、缶及び壜容器の際はレトルト殺菌を行うことが望ましい。
<Product, distribution form>
The product form of the palatable beverage of the present invention is prepared as a container-packed drink, and as the container form, PET bottles, cans, bottles, paper containers, chilled cups, and the like can be assumed. As a distribution form, it is possible to deal with products for both normal temperature distribution and chilled distribution, but a drink for chilled distribution and a chilled drink with low bactericidal strength are desirable in terms of flavor. Moreover, when manufacturing as a dry distribution product, it is desirable to perform aseptic filling when the container is a PET bottle, and to perform retort sterilization when the container is a can and bottle container.

以下、実施例により本発明をより具体的に説明するが、本発明の技術的範囲はこれらの例示に限定されるものではない。   EXAMPLES Hereinafter, although an Example demonstrates this invention more concretely, the technical scope of this invention is not limited to these illustrations.

[ローストシュガーの調製例]
砂糖を直火がまを用いて、攪拌しながら約3時間かけてゆっくり加熱した。170℃を超えた時点で加熱を止めた。余熱で180℃になることを確認したのちに反応を終了させた。このローストシュガーは0.1°Bxの水溶液にした場合360nmの吸光度は0.21であり、10°Bxの水溶液のpHは3.2であった。
[Preparation example of roasted sugar]
The sugar was slowly heated using an open flame with stirring for about 3 hours. Heating was stopped when the temperature exceeded 170 ° C. After confirming that the remaining heat reached 180 ° C., the reaction was terminated. When this roasted sugar was converted to an aqueous solution of 0.1 ° Bx, the absorbance at 360 nm was 0.21, and the pH of the aqueous solution of 10 ° Bx was 3.2.

[飲料の調製:乳固形分量5重量%(牛乳量40重量%)の場合]
牛乳400gに対して、グラニュー糖75gを調合し、更に、表1のローストシュガー(実施例1の調製例により調製したもの)、及び、食塩を配合した。最終的に脱イオン水を用いて1000gにフィルアップした後、殺菌して180gのガラス瓶につめ、本発明実施例或いは比較例の飲料を調製した。
[Beverage preparation: Milk solid content 5% by weight (milk 40% by weight)]
With respect to 400 g of milk, 75 g of granulated sugar was prepared, and roasted sugar (prepared according to the preparation example of Example 1) in Table 1 and sodium chloride were further added. Finally, it was filled up to 1000 g with deionized water, then sterilized and filled into a 180 g glass bottle to prepare a beverage of the present invention example or a comparative example.

(評価)
官能評価は熟練した5名のパネリストによっておこなった。評価は、コク味、苦味、キレ味、総合評価を5点満点で評価した。横軸:ローストシュガー量(重量%)、縦軸:食塩量(重量%)、評価点:表1中、左より「コク味」、「苦味」、「キレ味」、「総合評価」をそれぞれ表す。結果を表1に示す。なお、表1中、ローストシュガー量(重量%)0.5、15%のもの、及びNaCl(重量%)0.05、0.3%のものは比較例を、それ以外のものは、本発明の実施例を示す。
(Evaluation)
The sensory evaluation was conducted by five skilled panelists. Evaluation evaluated the full-bodied taste, bitterness, sharpness, and comprehensive evaluation on a 5-point scale. Horizontal axis: Roasted sugar amount (% by weight), Vertical axis: Salt amount (% by weight), Evaluation points: From Table 1, “Body taste”, “Bitter taste”, “Kire taste”, “Comprehensive evaluation” are shown from the left To express. The results are shown in Table 1. In Table 1, those with roasted sugar amount (% by weight) 0.5 and 15% and those with NaCl (% by weight) 0.05 and 0.3% are comparative examples, and those other than that are Examples of the invention are shown.

Figure 2009219393
Figure 2009219393

[牛乳量の変動による影響]
ローストシュガーを3%・15%、食塩を0.15%・0.3%に固定して、牛乳量を表2のように変動させる以外は、実施例2と同様にしてサンプルを調製した。それらの官能評価結果を実施例2の表1にならい記載した。結果を表2に示す。なお、表2中、ローストシュガー量(重量%)3%のものは本発明の実施例を、15%のものは比較例を示す。
[Effects of changes in milk volume]
Samples were prepared in the same manner as in Example 2 except that roast sugar was fixed at 3%, 15%, and salt was fixed at 0.15%, 0.3%, and the amount of milk was varied as shown in Table 2. The sensory evaluation results are shown in Table 1 of Example 2. The results are shown in Table 2. In Table 2, a roasted sugar amount (% by weight) of 3% indicates an example of the present invention, and a 15% value indicates a comparative example.

Figure 2009219393
Figure 2009219393

[飲料製品調製例]
ローストシュガー(池田糖化工業社製「ニガミシラップ」;0.1°Bx水溶液の360nm吸光度が0.37、10°Bxの水溶液のpHは3.0)120kg、乳化剤4kg、炭酸水素ナトリウム2kgを温水で溶解した後、クッションタンクへ投入した。更に、溶解したグラニュー糖300kg、食塩6kgをクッションタンクへ投入した。この溶解液についてホモジナイズ処理した後、牛乳1600kgを入れた調合タンクへ投入し、最終的に総量4000kgの調合液に仕上げた(乳成分量:40重量%、ローストシュガー:3重量%、食塩:0.15重量%)。出来上がった調合液を、更に、ストレーナーを通した後、チューブラー殺菌機で殺菌後、速やかに冷却を行い、別途用意した洗浄済みのチルドカップに充填し、アルミ蓋を取り付け、本発明の飲料を製造した。
[Beverage product preparation example]
Roasted sugar ("Nigami syrup" manufactured by Ikeda Sakka Kogyo Co., Ltd .; 360 ° absorbance of 0.1 ° Bx aqueous solution is 0.37, pH of aqueous solution of 10 ° Bx is 3.0) 120kg, emulsifier 4kg, sodium bicarbonate 2kg with warm water After dissolution, it was put into a cushion tank. Furthermore, 300 kg of dissolved granulated sugar and 6 kg of sodium chloride were put into a cushion tank. After homogenizing the solution, it was put into a preparation tank containing 1600 kg of milk and finally finished into a preparation liquid of a total amount of 4000 kg (milk component amount: 40% by weight, roasted sugar: 3% by weight, salt: 0 .15% by weight). The prepared liquid is further passed through a strainer, sterilized with a tubular sterilizer, quickly cooled, filled into a separately prepared chilled cup, an aluminum lid attached, and the beverage of the present invention. Manufactured.

(評価)
本飲料は、従来のカフェイン含有飲料を添加した場合に劣らぬ、深いコクと若干の苦味を有し、更には、後切れが良く甘さが口に残らず、非常に嗜好性が高い飲料であった。
(Evaluation)
This beverage has a deep richness and slight bitterness that is not inferior when a conventional caffeine-containing beverage is added. Met.

Claims (4)

乳成分を含む飲料であって、乳成分に、ブリックス度0.1°Bxの水溶液にした場合に360nmの吸光度が0.04以上0.9以下であり、10°Bxの水溶液にした場合にpHが2.0以上、4.0以下であるローストシュガーを1〜10重量%と、食塩を0.1〜0.2重量%配合したことを特徴とするカフェイン含有飲料風苦味とコクを付与した容器詰ノンカフェイン乳入り嗜好性飲料。   A beverage containing a milk component, and when the milk component is made into an aqueous solution having a Brix degree of 0.1 ° Bx, the absorbance at 360 nm is 0.04 or more and 0.9 or less, and when the aqueous solution is made into a 10 ° Bx aqueous solution. Caffeine-containing beverage-like bitterness and richness, characterized by blending 1 to 10% by weight of roasted sugar having a pH of 2.0 or more and 4.0 or less and 0.1 to 0.2% by weight of salt. A non-caffeinated milk-flavored beverage that has been added. ローストシュガーが、砂糖を原料として調製したものであることを特徴とする請求項1記載のカフェイン含有飲料風苦味とコクを付与した容器詰ノンカフェイン乳入り嗜好性飲料。   The roasted sugar is prepared from sugar as a raw material, and the caffeine-containing beverage-like bitterness and richness of a non-caffeinated milk-filled container-filled beverage according to claim 1 characterized by the above-mentioned. 乳成分の量が、乳固形分として1〜11重量%であって、ローストシュガー量が2〜5重量%、食塩が0.1〜0.2重量%であるであることを特徴とする請求項1又は2記載のカフェイン含有飲料風苦味とコクを付与した容器詰ノンカフェイン乳入り嗜好性飲料。   The amount of the milk component is 1 to 11% by weight as a milk solid content, the amount of roasted sugar is 2 to 5% by weight, and the salt is 0.1 to 0.2% by weight. Item 3. A containerized non-caffeine milk-flavored beverage with a caffeine-containing beverage-like bitterness and richness according to item 1 or 2. 糖類を170℃になるまで緩やかに焙煎・加熱し、加熱停止後余熱で180℃になることを確認した後、反応を終了させることにより、ブリックス度0.1°Bxの水溶液にした場合に360nmの吸光度が0.04以上0.9以下であり、10°Bxの水溶液にした場合にpHが2.0以上、4.0以下であるローストシュガーを調製し、該ローストシュガーを乳成分に1〜10重量%、更に、食塩を0.1〜0.2重量%配合し、常法により容器に充填したことを特徴とするカフェイン含有飲料風苦味とコクを付与した容器詰ノンカフェイン乳入り嗜好性飲料の製造方法。
When the sugar is slowly roasted and heated to 170 ° C., and after confirming that the residual heat reaches 180 ° C. after stopping the heating, the reaction is terminated to obtain an aqueous solution having a Brix degree of 0.1 ° Bx. A roast sugar having an absorbance at 360 nm of 0.04 or more and 0.9 or less and a pH of 2.0 or more and 4.0 or less when an aqueous solution of 10 ° Bx is prepared is prepared. 1 to 10% by weight, further 0.1 to 0.2% by weight of sodium chloride, and filled into a container according to a conventional method A method for producing a palatability drink containing milk.
JP2008065968A 2008-03-14 2008-03-14 Non-caffeinated milk-flavored beverage Expired - Fee Related JP4642090B2 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP2008065968A JP4642090B2 (en) 2008-03-14 2008-03-14 Non-caffeinated milk-flavored beverage

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP2008065968A JP4642090B2 (en) 2008-03-14 2008-03-14 Non-caffeinated milk-flavored beverage

Publications (2)

Publication Number Publication Date
JP2009219393A true JP2009219393A (en) 2009-10-01
JP4642090B2 JP4642090B2 (en) 2011-03-02

Family

ID=41236877

Family Applications (1)

Application Number Title Priority Date Filing Date
JP2008065968A Expired - Fee Related JP4642090B2 (en) 2008-03-14 2008-03-14 Non-caffeinated milk-flavored beverage

Country Status (1)

Country Link
JP (1) JP4642090B2 (en)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2013100118A1 (en) * 2011-12-28 2013-07-04 昭和産業株式会社 Composition for improving taste of microwave oven-cooked chicken and method for improving taste of microwave oven-cooked chicken
JP2018023306A (en) * 2016-08-09 2018-02-15 アサヒ飲料株式会社 Tea beverage and method for reinforcing the flavor of fruit juice

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS52110873A (en) * 1976-03-11 1977-09-17 Hasegawa Co Ltd Coffee taste substance having coffee like flavor
JPH1033126A (en) * 1996-07-26 1998-02-10 Ezaki Glico Co Ltd Roast sugar and food blended with the same
WO2001025262A1 (en) * 1999-10-04 2001-04-12 Ajinomoto Co., Inc. Sweetener compositions with high degree of sweetness having improved sweetness, corrigents and utilization thereof
JP2002536957A (en) * 1998-06-03 2002-11-05 ソシエテ デ プロデユイ ネツスル ソシエテ アノニム How to make coffee substitutes
JP2009060881A (en) * 2007-09-10 2009-03-26 Ikeda Shokken Kk Method for producing roast food, roast food obtained by the same method and food containing the same

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS52110873A (en) * 1976-03-11 1977-09-17 Hasegawa Co Ltd Coffee taste substance having coffee like flavor
JPH1033126A (en) * 1996-07-26 1998-02-10 Ezaki Glico Co Ltd Roast sugar and food blended with the same
JP2002536957A (en) * 1998-06-03 2002-11-05 ソシエテ デ プロデユイ ネツスル ソシエテ アノニム How to make coffee substitutes
WO2001025262A1 (en) * 1999-10-04 2001-04-12 Ajinomoto Co., Inc. Sweetener compositions with high degree of sweetness having improved sweetness, corrigents and utilization thereof
JP2009060881A (en) * 2007-09-10 2009-03-26 Ikeda Shokken Kk Method for producing roast food, roast food obtained by the same method and food containing the same

Non-Patent Citations (2)

* Cited by examiner, † Cited by third party
Title
JPN6010062451, Z. PAZOLA, et al., "Changes in Carbohydrates during the Production of Coffee Substitute Extracts, especially in the Roas", Food Chem., 1979, Vol.4, No.1, Pages 41−52, GB *
JPN6010062457, A. BERGER, et al., "Detection of Adulteration in Pure Soluble Coffee by Enzymatic Suger Determination", Lebensm. Wiss. Technol., 1991, Vol.24, No.1, Pages 59−62, CH *

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2013100118A1 (en) * 2011-12-28 2013-07-04 昭和産業株式会社 Composition for improving taste of microwave oven-cooked chicken and method for improving taste of microwave oven-cooked chicken
JP2013138630A (en) * 2011-12-28 2013-07-18 Showa Sangyo Co Ltd Composition for improving taste of microwave oven-cooked chicken and method for improving taste of microwave oven-cooked chicken
JP2018023306A (en) * 2016-08-09 2018-02-15 アサヒ飲料株式会社 Tea beverage and method for reinforcing the flavor of fruit juice

Also Published As

Publication number Publication date
JP4642090B2 (en) 2011-03-02

Similar Documents

Publication Publication Date Title
US20110281009A1 (en) Milk-flavored beverage
HU228828B1 (en) Coffee concentrate system and process for its production
TWI762723B (en) Colorless and transparent beverage containing potassium and its manufacturing method
JP5547965B2 (en) Container stuffed coffee drinks
WO2017021428A1 (en) Ready-to-drink beverages with improved texture by controlled protein aggregation
JP5208326B2 (en) Coffee beverage and method for producing the same
CA2970068C (en) Ready-to-drink milk beverages with improved texture/mouthfeel by controlled protein aggregation, and method of making thereof
JP6868086B1 (en) Flavor expression enhancer containing rotundone as an active ingredient
JP2024024078A (en) CONTAINER-PACKAGED COFFEE BEVERAGE CONTAINING γ-AMINOBUTYRIC ACID
JP4642090B2 (en) Non-caffeinated milk-flavored beverage
TWI759546B (en) Colorless and transparent beverages containing calcium
JP5881301B2 (en) Bottled milk coffee drink
JP2009268397A (en) Bottled coffee drink containing sodium hydroxide
JP2015500654A (en) Liquid creamer and method for producing the same
TWI770270B (en) Colorless and transparent beverage containing sodium and its manufacturing method
JP6918260B1 (en) Coffee beverage in a transparent container containing milk solids
JP2020103059A (en) Beverage and method of producing the same
JP2019013216A (en) Foamable beverage
JP7432221B2 (en) Method for producing acidic milk beverage
JP6045547B2 (en) Containerized coffee drink containing sodium hydroxide
JP2009142206A (en) Packed coffee drink controlled in formation of precipitates
JP2021103944A (en) Packaged coffee beverage and method for improving flavor of packaged coffee beverage
WO2020099232A1 (en) Liquid creamer
JP2002095416A (en) Milk constituent phase-separation-type ice coffee in transparent bottle
JP2023164260A (en) Cocoa concentrate for preparing cocoa beverage

Legal Events

Date Code Title Description
A977 Report on retrieval

Free format text: JAPANESE INTERMEDIATE CODE: A971007

Effective date: 20101025

A131 Notification of reasons for refusal

Free format text: JAPANESE INTERMEDIATE CODE: A131

Effective date: 20101028

A521 Written amendment

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20101110

TRDD Decision of grant or rejection written
A01 Written decision to grant a patent or to grant a registration (utility model)

Free format text: JAPANESE INTERMEDIATE CODE: A01

Effective date: 20101129

A01 Written decision to grant a patent or to grant a registration (utility model)

Free format text: JAPANESE INTERMEDIATE CODE: A01

A61 First payment of annual fees (during grant procedure)

Free format text: JAPANESE INTERMEDIATE CODE: A61

Effective date: 20101130

R150 Certificate of patent or registration of utility model

Free format text: JAPANESE INTERMEDIATE CODE: R150

FPAY Renewal fee payment (event date is renewal date of database)

Free format text: PAYMENT UNTIL: 20131210

Year of fee payment: 3

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

LAPS Cancellation because of no payment of annual fees