JP2009124999A - Whipped cream - Google Patents
Whipped cream Download PDFInfo
- Publication number
- JP2009124999A JP2009124999A JP2007303580A JP2007303580A JP2009124999A JP 2009124999 A JP2009124999 A JP 2009124999A JP 2007303580 A JP2007303580 A JP 2007303580A JP 2007303580 A JP2007303580 A JP 2007303580A JP 2009124999 A JP2009124999 A JP 2009124999A
- Authority
- JP
- Japan
- Prior art keywords
- whipped cream
- milk
- cellooligosaccharide
- mass
- acid
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
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Landscapes
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- Confectionery (AREA)
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Abstract
Description
本発明は、セロオリゴ糖と乳成分を含有し、低カロリーで安定性が高く、且つ、保形性に優れたホイップドクリーム、およびそれを配合した食品組成物または医薬品組成物に関する。 The present invention relates to a whipped cream containing cellooligosaccharide and a milk component, having low calories, high stability, and excellent shape retention, and a food composition or pharmaceutical composition containing the whipped cream.
オリゴ糖は、腸内細菌叢改善などの様々な生理活性効果を有し、その用途展開が望まれている食品素材である。中でもセロオリゴ糖をはじめとする難消化性オリゴ糖は、低カロリーであるため、特に望ましいとされている。
本発明で述べる、乳脂肪分を含有する組成物を泡立てて製造するホイップドクリームは、ケーキ類や菓子類などの製造に用いられる場合が多いが、泡立てた後の安定性に問題があり、その改善が求められている。また冷凍流通される商品も多く、冷解凍後の保形性の維持も重要な課題である。
Oligosaccharide is a food material that has various physiological activity effects such as improvement of intestinal microflora and is expected to be expanded in its use. Of these, indigestible oligosaccharides such as cellooligosaccharides are particularly desirable because of their low calories.
The whipped cream produced by whipping the composition containing milk fat described in the present invention is often used for the production of cakes, confectionery, etc., but there is a problem in stability after whipping, There is a need for improvement. In addition, there are many products that are distributed in freezing, and maintaining shape retention after cold thawing is also an important issue.
上記問題を解決する手段として、乳化剤や増粘多糖類などの食品添加物を配合する方法が知られているが、昨今の消費者の健康志向に反するものであり好ましくない。また増粘多糖類の配合により、増粘やマスキングが発生し、食感を損なうという問題がある。
あるいは、ショ糖やトレハロースのような消化性糖質を大量に添加する方法も提案されているが、高カロリーの消化性糖質を物性改良目的に大量に配合することは、消費者の健康を損ねる結果となり、好ましくない。
As a means for solving the above problems, a method of blending food additives such as emulsifiers and thickening polysaccharides is known. However, it is contrary to the health-consciousness of consumers today and is not preferable. Moreover, there exists a problem that thickening and masking generate | occur | produce by the mixing | blending of thickening polysaccharide, and food texture is impaired.
Alternatively, a method of adding a large amount of digestible carbohydrates such as sucrose and trehalose has also been proposed, but adding a large amount of high-calorie digestible carbohydrates for the purpose of improving physical properties improves the health of consumers. As a result, it is not preferable.
特許文献1には、β−グルコオリゴ糖と乳が配合された飲食物の開示があるが、β−グルコオリゴ糖の実態は、ゲンチオオリゴ糖であり、本発明のセロオリゴ糖とは化学構造を異にし、ホイップドクリームについては記載が無い。
特許文献2〜5には、糖アルコールや糖類が配合された、ホイップドクリームについての記載があるが、セロオリゴ糖については何ら言及されていない。
Patent Document 1 discloses a food and drink in which β-glucooligosaccharide and milk are blended, but the actual state of β-glucooligosaccharide is a gentiooligosaccharide, which has a different chemical structure from the cellooligosaccharide of the present invention, There is no description about whipped cream.
Patent Documents 2 to 5 have a description of whipped cream in which sugar alcohol or saccharide is blended, but nothing is mentioned about cellooligosaccharide.
特許文献6には、ある特定の水不溶性天然セルロース系物質を、セルラーゼの存在下で酵素分解して得られた、セロオリゴ糖を含むことを特徴とする食品組成物や医薬品組成物の記載がある。しかしながら、具体的にセロオリゴ糖を含有する食品組成物や医薬品組成物の例は示されておらず、その効果の実態は不明である。
特許文献7には、セロオリゴ糖を含有する食品組成物についての記載があるが、ホイップドクリームについては何ら言及されておらず、本発明とは内容を異にする。
Patent Document 6 describes a food composition and a pharmaceutical composition characterized by containing cellooligosaccharide obtained by enzymatic degradation of a specific water-insoluble natural cellulosic substance in the presence of cellulase. . However, specific examples of food compositions and pharmaceutical compositions containing cellooligosaccharides are not shown, and the actual effects are unknown.
Patent Document 7 describes a food composition containing cellooligosaccharide, but does not mention anything about whipped cream, which is different from the present invention.
本発明は、セロオリゴ糖と乳成分を含有し、低カロリーで安定性が高く、且つ、保形性に優れたホイップドクリーム、およびそれを配合した食品組成物または医薬品組成物を提供することを課題とする。 The present invention provides a whipped cream containing cellooligosaccharide and a milk component, having low calories, high stability, and excellent shape retention, and a food composition or pharmaceutical composition containing the same. Let it be an issue.
本発明者は、難消化性であるセロオリゴ糖を乳成分に配合することで、低カロリーで安定性が高く、且つ、保形性に優れたホイップドクリーム、およびそれを配合した食品組成物または医薬品組成物を提供できることを見出し、本発明をなすに至った。 The present inventor has incorporated low-digestible cellooligosaccharides into milk components, so that it is low in calories, high in stability, and excellent in shape retention, and a food composition containing the whipped cream or It has been found that a pharmaceutical composition can be provided, and has led to the present invention.
すなわち本発明は、以下の通りである。
(1) セロオリゴ糖と乳成分を含有し、乳脂肪分の含有量が5〜80質量%であることを特徴とする、ホイップドクリーム。
(2) 乳脂肪分の含有量が20〜60質量%である、(1)に記載のホイップドクリーム。
(3) セロオリゴ糖の配合量が0.001〜60質量%である、(1)または(2)に記載のホイップドクリーム。
(4) さらに1ppm〜10質量%の高甘味度甘味料を含有する、(1)から(3)の何れかに記載のホイップドクリーム。
(5) (1)から(4)のいずれかに記載のホイップドクリームを含有する、食品組成物または医薬品組成物。
That is, the present invention is as follows.
(1) A whipped cream comprising cellooligosaccharides and milk components, wherein the milk fat content is 5 to 80% by mass.
(2) The whipped cream according to (1), wherein the milk fat content is 20 to 60% by mass.
(3) The whipped cream according to (1) or (2), wherein the amount of cellooligosaccharide is 0.001 to 60% by mass.
(4) The whipped cream according to any one of (1) to (3), further containing 1 ppm to 10% by mass of a high-potency sweetener.
(5) A food composition or a pharmaceutical composition containing the whipped cream according to any one of (1) to (4).
本発明は、セロオリゴ糖と乳成分を含有し、低カロリーで安定性が高く、且つ、保形性に優れたホイップドクリーム、およびそれを配合した食品組成物または医薬品組成物を提供することを可能とする。 The present invention provides a whipped cream containing cellooligosaccharide and a milk component, having low calories, high stability, and excellent shape retention, and a food composition or pharmaceutical composition containing the same. Make it possible.
本発明者は、難消化性であるセロオリゴ糖を配合することで、低カロリーで安定性が高く、且つ、保形性に優れたホイップドクリーム、およびそれを配合した食品または医薬品組成物を提供できることを見出し、本発明をなすに至った。
以下、本発明について具体的に説明する。
The present inventor provides a whipped cream having low calorie, high stability and excellent shape retention, and a food or pharmaceutical composition containing the same by blending cellooligosaccharide which is indigestible The present inventors have found out that it is possible to achieve the present invention.
Hereinafter, the present invention will be specifically described.
本発明のセロオリゴ糖とは、グルコピラノース単位が2〜6個程度、β−1,4結合した構造を持つオリゴ糖であり、セロビオース、セロトリオース、セロテトラオース、セロペンタオースおよびセロヘキサオースからなる群より選択される主成分を、50質量%以上含有する。この主成分とその含有量としては、セロビオースを70質量%以上含有することが好ましく、90質量%以上であれば、さらに好ましい。これは上述のセロオリゴ糖主成分の中で、水に対する溶解度はセロビオースが最も高いことから、本発明のホイップドクリームに最も適しているからである。
また上述のセロオリゴ糖は、副成分としてグルコースを含有しても構わないが、吸湿性やカロリーの問題から、含有量は10質量%以下であることが好ましい。
The cellooligosaccharide of the present invention is an oligosaccharide having a structure in which about 2 to 6 glucopyranose units are linked by β-1,4, and consists of cellobiose, cellotriose, cellotetraose, cellopentaose and cellohexaose. 50 mass% or more of the main components selected from the group are contained. As this main component and its content, it is preferable to contain 70 mass% or more of cellobiose, and more preferably 90 mass% or more. This is because among the above-mentioned cellooligosaccharide main components, cellobiose has the highest solubility in water, and is therefore most suitable for the whipped cream of the present invention.
Moreover, although the above-mentioned cellooligosaccharide may contain glucose as a subcomponent, it is preferable that content is 10 mass% or less from the problem of hygroscopicity or a calorie.
本発明のセロオリゴ糖の製造方法としては、特に規定するものではないが、安全性の点からは、パルプをはじめとするセルロース系物質を、セルラーゼで酵素分解して得られるものを使用するのが好ましい。
本発明におけるセロオリゴ糖の、主たる成分であるセロビオースのエネルギー換算係数は、2kcal/gであり、難消化性糖質である。昨今の消費者の健康志向からみて、品質改良を目的に、高カロリーの消化性糖質を使用することは問題がある。
The method for producing the cellooligosaccharide of the present invention is not particularly specified, but from the viewpoint of safety, a cellulosic material such as pulp can be obtained by enzymatic decomposition with cellulase. preferable.
The energy conversion coefficient of cellobiose, which is the main component of the cellooligosaccharide in the present invention, is 2 kcal / g, which is an indigestible carbohydrate. From the viewpoint of consumers' recent health consciousness, there is a problem in using high-calorie digestible carbohydrates for the purpose of quality improvement.
ここで言う消化性糖質とは、健康増進法に基づく、健康表示基準対応のエネルギー換算係数が、4kcal/gの糖質であり、トレハロースなどがこれに含まれる。
ここで言うセルラーゼとは、セルラーゼを分解する酵素の総称であり、セルロースの分解活性を有する酵素が全て含まれる。セルラーゼ酵素源は、特に限定されるものではないが、例えばセルラーゼ産生菌体、菌体の産生する酵素を精製したもの、精製酵素を添加剤等とともに製剤化したものなどがあげられる。またその剤形も、特に限定されるものではないが、例えば液体、粉末、顆粒などがある。
The digestible saccharide referred to herein is a saccharide having an energy conversion coefficient corresponding to the health indication standard based on the health promotion method and having 4 kcal / g, and includes trehalose and the like.
Cellulase as used herein is a generic term for enzymes that degrade cellulase, and includes all enzymes having cellulose-degrading activity. The cellulase enzyme source is not particularly limited, and examples thereof include cellulase-producing bacterial cells, purified cellulase enzymes, and formulated purified enzymes with additives. The dosage form is not particularly limited, and examples thereof include liquids, powders and granules.
さらに、本発明のセロオリゴ糖の甘味度は、30程度であり、高甘味度甘味料とは異なり、自然な甘みを有する。
セルラーゼの起源についても、特に限定されるものではなく、公知のセルラーゼ産生微生物としては、Tricoderma属、Acremonium属、Aspergillus属、Bacillus属、Pseudomonas属、Penicillium属、Aeromonus属、Irpex属、Sporotrichum属、Humicola属、Cellovibrio属などがあるが、セルロースを分解する酵素であれば、上記公知の菌由来の酵素に限らず、新規の菌由来の酵素も、本発明でいうセルラーゼに含まれる。
Furthermore, the sweetness degree of the cellooligosaccharide of the present invention is about 30, and unlike natural sweeteners, it has a natural sweetness.
The origin of the cellulase is not particularly limited, and known cellulase-producing microorganisms include Tricoderma, Acremonium, Aspergillus, Bacillus, Pseudomonas, Penicillium, Aeromonus, Irpex, Sporotrum, Although there are genera, Cellobibrio genus, etc., as long as it is an enzyme that degrades cellulose, not only the above-mentioned known bacterially-derived enzymes but also novel bacterial-derived enzymes are included in the cellulase referred to in the present invention.
本発明におけるセロオリゴ糖の配合量は、特に限定されるものではないが、好ましくは0.001〜60質量%、さらに好ましくは0.1〜40質量%である。0.001質量%未満であると効果が見えにくい場合があり、60質量%を超えると口当たりに悪影響を及ぼす場合がある。 Although the compounding quantity of the cellooligosaccharide in this invention is not specifically limited, Preferably it is 0.001-60 mass%, More preferably, it is 0.1-40 mass%. If it is less than 0.001% by mass, the effect may be difficult to see, and if it exceeds 60% by mass, the mouthfeel may be adversely affected.
本発明における乳成分とは、後述の乳等の成分をさす。ここで言う乳は、その由来や加工の有無を特に限定するものではないが、例えば、牛乳、「山羊、羊、馬、ラクダなどの動物から得られる乳」、人乳、「豆乳などの植物から得られる乳」などがあげられる。
ここで言う乳等とは、その由来や加工の有無を特に限定するものではないが、上記の乳に加え、脱脂乳、加工乳、乳飲料、乳製品(クリーム、チーズ、濃縮ホエイ、濃縮乳、煉乳、全脂粉乳、脱脂粉乳、クリームパウダー、ホエイパウダー、たんぱく質濃縮ホエイパウダー、バターミルクパウダー、加糖粉乳、調製粉乳など)、調整豆乳、豆乳飲料、大豆飲料、植物性粉末(大豆全粒粉など)、植物性たんぱく(大豆たんぱく、小麦たんぱくなど)などが含まれる。
The milk component in the present invention refers to components such as milk described later. The milk mentioned here is not particularly limited in its origin and presence or absence of processing. For example, milk, “milk obtained from animals such as goats, sheep, horses, camels”, human milk, “plants such as soy milk” Milk obtained from ".
The term “milk” as used herein does not specifically limit the origin or presence of processing, but in addition to the above milk, skim milk, processed milk, milk drinks, dairy products (cream, cheese, concentrated whey, concentrated milk) Milk powder, whole milk powder, skim milk powder, cream powder, whey powder, protein concentrated whey powder, buttermilk powder, sweetened powdered milk, prepared powdered milk, etc.) , Vegetable protein (soy protein, wheat protein, etc.).
本発明の乳脂肪分とは、乳等に含まれる脂肪分をさす。
本発明のホイップドクリームにおける乳脂肪分の含有量は、5〜80質量%以上であり、好ましくは20〜60質量%、さらに好ましくは30〜50質量%である。5質量%以下であるとホイップすることが困難となり、80質量%を超えると食品組成物または医薬品組成物としての処方が限定されるからである。
The milk fat content of the present invention refers to a fat content contained in milk or the like.
The milk fat content in the whipped cream of the present invention is 5 to 80% by mass or more, preferably 20 to 60% by mass, and more preferably 30 to 50% by mass. This is because whipping is difficult when the amount is 5% by mass or less, and prescription as a food composition or pharmaceutical composition is limited when the amount exceeds 80% by mass.
本発明のホイップドクリームとは、後述する乳等を泡立てて起泡したクリームのことであり、その保存・流通形態は、常温・冷蔵・冷凍など、特に限定されるものではない。 The whipped cream of the present invention is a cream obtained by foaming milk or the like to be described later, and its storage / distribution form is not particularly limited, such as room temperature, refrigeration, and freezing.
また本発明のホイップドクリームには、必要に応じて、1ppm〜10質量%の高甘味度甘味料を含有させることができる。本発明の高甘味度甘味料とは、砂糖と比較して、数倍〜数万倍程度の甘味度を持ち、例えば、サッカリン、サッカリンNa、アスパルテーム、アセスルファムK、スクラロース、甘草抽出物、ステビア、ソーマチン、グリチルリチン、ネオテームなどがあげられる。 Moreover, the whipped cream of this invention can contain 1 ppm-10 mass% high sweetness degree sweetener as needed. The high-intensity sweetener of the present invention has a sweetness of several times to several tens of thousands of times as compared with sugar. For example, saccharin, saccharin Na, aspartame, acesulfame K, sucralose, licorice extract, stevia, Examples include thaumatin, glycyrrhizin and neotame.
本発明におけるホイップドクリームの安定性は、次式により算出される安定率をもとに表される。この安定率が3%以上の場合に、安定性改善効果があると判断される。
安定率(%)={(β−α)/α}×100
ここで、α:セロオリゴ糖を配合しないホイップドクリームの離水率(%)、β:セロオリゴ糖を配合したホイップドクリームの離水率(%)である。
The stability of the whipped cream in the present invention is expressed based on the stability rate calculated by the following equation. When this stability rate is 3% or more, it is determined that there is an effect of improving stability.
Stability rate (%) = {(β−α) / α} × 100
Here, α: water separation rate (%) of whipped cream not containing cellooligosaccharide, β: water separation rate (%) of whipped cream containing cellooligosaccharide.
本発明におけるホイップドクリームの保形性は、次式により算出される保形率をもとに表され、冷解凍時の保形性の指標である。この保形率が3%以上の場合に、保形性改善効果があると判断される。
保形率(%)={(δ−γ)/γ}×100
ここで、γ:セロオリゴ糖を配合しないホイップドクリームの強度(mN)、δ:セロオリゴ糖を配合したホイップドクリームの強度(mN)である。
The shape retention of the whipped cream in the present invention is expressed based on the shape retention rate calculated by the following formula, and is an index of shape retention during cold thawing. When this shape retention rate is 3% or more, it is judged that there is an effect of improving shape retention.
Shape retention rate (%) = {(δ−γ) / γ} × 100
Here, γ: strength (mN) of whipped cream not containing cellooligosaccharide, and δ: strength (mN) of whipped cream containing cellooligosaccharide.
本発明の食品組成物とは、一般に食品として供される組成物のことであり、例えば、「ゼリー、プリン、植物性発酵食品などのゲル状食品」、「アイスクリーム、アイスミルク、ラクトアイス、シャーベット、フローズンヨーグルトなどの冷菓」、「キャンディー、グミキャンディー、トローチ、錠菓、チョコレート、ビスケット、クッキー、米菓、餡製品、和洋菓子、洋生菓子、スナック菓子、砂糖菓子、プリンなどの菓子類」、「マヨネーズ、ドレッシング、ソース類、たれ類などの調味料」、「フライ類、コロッケ、餃子、中華饅頭などの調理加工品」、「カレー、ハヤシ、ミートソース、シチュー、スープなどのレトルト食品」、「麺類、スープ、野菜加工品などのチルド食品や冷凍食品」、「ハンバーグ、ベーコン、ソーセージ、サラミソーセージ、ハム類などの畜産加工品」、「蒲鉾、ちくわ、魚肉ハム・ソーセージ、揚げ蒲鉾などの水練製品」、「パン類、ケーキ類、生麺、乾麺、マカロニ、スパゲッティ、中華饅頭の皮、ケーキミックス、プレミックス、ホワイトソース、餃子・春巻等の皮類などの小麦加工食品」、「カレー、ソース、スープ、佃煮、ジャムなどの缶詰類や瓶詰類」、「野菜ペースト、肉のミンチ、果実ペースト、魚介類のペースト等のペースト類」、「果汁・果肉飲料、野菜飲料、酸性乳飲料、乳飲料、殺菌乳酸菌飲料、コーヒー飲料、紅茶飲料、緑茶、抹茶、ココア飲料、ウーロン茶、煎茶、フルーツ牛乳、炭酸飲料、アルコール飲料などの嗜好飲料」、「豆乳、調製豆乳、豆乳飲料、発酵豆乳、大豆飲料などの豆乳類」、「牛乳、加工乳、低脂肪乳などの牛乳類」、「クリーム、練乳、バター、ヨーグルト、チーズなどの乳製品」、「マーガリン、ファットスプレッド、ショートニングなどの油脂加工品」などがある。 The food composition of the present invention is a composition generally provided as a food, for example, “gel foods such as jelly, pudding, plant fermented food”, “ice cream, ice milk, lacto ice, sherbet” , Frozen yogurt and other frozen desserts ”,“ candy, gummy candy, troche, tablet confectionery, chocolate, biscuits, cookies, rice confectionery, rice cake products, Japanese and Western confectionery, Western confectionery, snack confectionery, sugar confectionery, pudding, etc. ”,“ Seasonings such as mayonnaise, dressings, sauces, sauces, etc., “Fried foods such as croquettes, dumplings, Chinese buns”, “Retort foods such as curry, hayashi, meat sauce, stew, soup”, “noodles , Chilled foods such as soups and processed vegetables and frozen foods "," hamburgers, bacon, sausages, Processed livestock products such as ramie sausages and hams ”,“ Boiled products such as salmon, chikuwa, fish ham / sausage, fried rice cakes ”,“ Breads, cakes, raw noodles, dried noodles, macaroni, spaghetti, Chinese bun skin , Cake mixes, premixes, white processed foods such as white sauce, dumplings and spring rolls, etc. "," Canned and bottling such as curry, sauce, soup, boiled, jam "," vegetable paste, meat Mince, fruit paste, paste of seafood paste, "fruit juice, pulp drink, vegetable drink, acid milk drink, milk drink, sterilized lactic acid bacteria drink, coffee drink, tea drink, green tea, matcha tea, cocoa drink, oolong tea, Sencha, fruit milk, carbonated beverages, alcoholic beverages, etc. ”,“ soy milk, prepared soy milk, soy milk beverages, fermented soy milk, soybean beverages such as soy beverages ”,“ milk, processed milk, Milk such as fat milk ", there is such as" cream, condensed milk, butter, yogurt, dairy products such as cheese, "" margarine, fat spreads, oils and fats processing products such as shortening ".
本発明の医薬品組成物とは、薬事法に規定される医薬品または医薬部外品の組成物であり、例えば、錠剤、散剤、細粒剤、顆粒剤、エキス剤、丸剤の固形製剤が挙げられ、上記の固形製剤以外でも、菓子、健康食品、食感改良剤、食物繊維強化剤等の食品、固形ファンデーション、浴用剤、動物薬、診断薬、農薬、肥料、セラミックス触媒などに利用されるものも本発明に含まれる。 The pharmaceutical composition of the present invention is a pharmaceutical or quasi-drug composition defined by the Pharmaceutical Affairs Law, and examples thereof include solid preparations such as tablets, powders, fine granules, granules, extracts, and pills. In addition to the above solid preparations, they are used for foods such as confectionery, health foods, texture improvers, dietary fiber reinforcing agents, solid foundations, bath preparations, animal drugs, diagnostic agents, agricultural chemicals, fertilizers, ceramics catalysts, etc. Are also included in the present invention.
また医薬部外品組成物の剤形としては、例えば、「セットローション、ヘアスティック、ヘアクリーム、ヘアスプレー、ヘアリキッドなどの整髪料」、「ヘアトニック、ヘアトリートメント、ヘアローションなどの養毛料」、「頭皮料、髪洗粉、シャンプーなどの洗髪料」、「ヘアリンス、オイルリンス、クリームリンス、ボディリンス、フェイシャルリンスなどのリンス類」、「クレンジングクリーム、洗顔クリーム、クレンジングミルク、クレンジングローション、洗粉などの洗顔料」、「パック、油性クリーム、中性クリーム、弱酸性クリーム等のクリーム、ミルクローション、スキンミルクなどの乳液」、「乾性肌用化粧水、普通肌用化粧水、脂肌用化粧水、男性用化粧水、男性ローション、アフターシェーブローションなどの化粧水」、「口紅、リップグロス、リップクリームなどの口紅類」、「バスソルト、バスオイルなどの浴用化粧品」、「オリーブ油、ベビーオイルなどを配合した化粧油」、「日焼け用化粧品」、「日焼け止め化粧品」、「歯磨き粉、歯磨きペースト、口腔用スプレーなどの口腔用組成物」などであっても良い。 Examples of the dosage form of the quasi-drug composition include, for example, “hair-setting agents such as set lotions, hair sticks, hair creams, hair sprays, hair liquids” and “hair-care agents such as hair tonics, hair treatments, and hair lotions”. , "Hair-washing agents such as scalp, hair-washing powder, shampoo", "Hair rinses, oil-rinsing, cream-rinsing, body-rinsing, facial-rinsing, etc.", "Cleansing cream, facial cleansing cream, cleansing milk, cleansing lotion, powder-washing etc. Face wash "," packs, oily creams, neutral creams, weakly acidic creams, milk lotions, skin milks "," dry skin lotions, skin lotions for normal skin, skin lotions for oily skin , Makeup for men, lotion, men lotion, after shave lotion "Lipsticks such as lipstick, lip gloss, lip balm", "Bath salts and bath oils such as bath oil", "Cosmetic oils containing olive oil, baby oil", "Sunscreen cosmetics", "Sunscreen" “Cosmetics”, “oral compositions such as toothpaste, toothpaste, and oral spray” may be used.
本発明のホイップドクリームと、それを含有する食品組成物または医薬品組成物には、本発明の効果を妨げない限りにおいて、上記の成分以外に、後述の食品素材、食品添加物、医薬品、医薬品添加物などを適宜配合しても良い。 The whipped cream of the present invention and the food composition or pharmaceutical composition containing it, as long as the effects of the present invention are not hindered, in addition to the above ingredients, food ingredients, food additives, pharmaceuticals, and pharmaceuticals described below You may mix | blend an additive etc. suitably.
ここで言う食品素材とは、一般に食品の原材料として使用される素材のことであり、薬事法で規定される医薬品および医薬部外品と、食品衛生法で規定される食品添加物を除き、飲食に供される全てのものが含まれる。
ここで言う食品添加物とは、食品の加工もしくは保存の目的で添加される物質のことである。
The food material referred to here is a material that is generally used as a raw material of food. Except for pharmaceuticals and quasi-drugs specified by the Pharmaceutical Affairs Law and food additives specified by the Food Sanitation Law, All that is provided to is included.
The food additive referred to here is a substance added for the purpose of processing or storing food.
食品添加物の例としては、厚生労働省の「指定添加物リスト」、「既存添加物名簿収載品目リスト」、「天然香料基原物質リスト」、「一般に食品として飲食に供させている物であって添加物として使用される品目リスト」などに収載される食品添加物や、JECFAなどの国際機関で安全性が確認されたもの、米国・欧州などの諸外国で使用が認可されている食品添加物などがあげられ、保存料・日持向上剤、酸化防止剤、甘味料、着色料・色素、乳化剤、増粘ゲル化剤、品質改良剤、調味料、酸味料、強化剤、香料、酵素などに分類される。 Examples of food additives are those specified by the Ministry of Health, Labor and Welfare's “designated additive list”, “existing additive list item list”, “natural fragrance-based raw material list”, and “food that is generally used for food and drink. Food additives listed in the “List of Items Used as Additives”, those that have been confirmed to be safe by international organizations such as JECFA, and food additives that are approved for use in other countries such as the United States and Europe Products, preservatives, shelf-life improvers, antioxidants, sweeteners, colorants / pigments, emulsifiers, thickening gelling agents, quality improvers, seasonings, acidulants, fortifiers, fragrances, enzymes And so on.
食品素材や食品添加物の例としては、以下のようなものがあげられる。
ここで言う食品素材としては、例えば、果実・野菜およびそのエキス類、果実・野菜加工品(フルーツプレパレーション、フルーツソース、ジャム等)、乾燥果実(干しぶどう、干しパイナップル等)、ナッツ・種子類(くるみ、ピーナッツ、アーモンド、マカデミアナッツ、ピーカンナッツ、大豆、ゴマ、芥子等)、牛乳、加工乳、豆乳、果汁、野菜汁、卵類(液卵、卵黄粉末等)、ココア末、糖や糖アルコール類、肉や魚のエキス類、タンパク質、ペプチド、アミノ酸類、食物繊維、天然由来高分子(コラーゲン、ヒアルロン酸、天然繊維等)、ビタミン類、生理活性物質(コエンザイムQ10、α−リポ酸、β−グルカン、セラミド等)、澱粉類、デキストリン、油脂類(サラダ油、ゴマ油、ラード、菜種油、ショートニング等)、アルコール類、塩類(食塩、Caなどのミネラル類等)、調味料(醤油、味噌、酢、みりん、砂糖、マヨネーズ、ドレッシング、タレ、豆板醤、ソース類等)、香辛料(シナモン、コショウ、唐辛子等)などがあげられる。
Examples of food materials and food additives include the following.
Examples of food materials mentioned here include fruits and vegetables and extracts thereof, processed fruits and vegetables (fruit preparations, fruit sauces, jams, etc.), dried fruits (raisins, dried pineapples, etc.), nuts and seeds (Walnuts, peanuts, almonds, macadamia nuts, pecan nuts, soybeans, sesame seeds, eggplants, etc.), milk, processed milk, soy milk, fruit juice, vegetable juice, eggs (liquid egg, egg yolk powder, etc.), cocoa powder, sugar and sugar alcohol , Meat and fish extracts, proteins, peptides, amino acids, dietary fiber, naturally derived polymers (collagen, hyaluronic acid, natural fiber, etc.), vitamins, physiologically active substances (coenzyme Q10, α-lipoic acid, β- Glucan, ceramide, etc.), starches, dextrin, fats and oils (salad oil, sesame oil, lard, rapeseed oil, shortening, etc.), al Cole, salt (minerals such as salt and Ca), seasoning (soy sauce, miso, vinegar, mirin, sugar, mayonnaise, dressing, sauce, soy sauce, sauces, etc.), spice (cinnamon, pepper, chili, etc.) ) Etc.
保存料・日持向上剤としては、例えば、例えば、過酸化水素、ソルビン酸およびソルビン酸K、デヒドロ酢酸Na、パラオキシ安息香酸エステル類、安息香酸および安息香酸Na、プロピオン酸およびその塩類、次亜塩素酸Na、酢酸、酢酸ナトリウム、グリシン、エチルアルコール、ポリリジンおよびその製剤、プロタミンおよびその製剤、リゾチームおよびその製剤、ペクチン分解物、アラニン、チアミンラウリル硫酸塩、ユッカフォーム抽出物、キトサンおよびその製剤、プロピレングリコールなどがあげられる。
酸化防止剤としては、例えば、ブチルヒドロキシアニソール、ブチルヒドロキシトルエン、L−アスコルビン酸およびアスコルビン酸Na、エリソルビン酸およびエリソルビン酸Na、ミックストコフェノールなどがあげられる。
Examples of preservatives and shelf-life improvers include, for example, hydrogen peroxide, sorbic acid and sorbic acid K, dehydroacetic acid Na, p-hydroxybenzoates, benzoic acid and sodium benzoate, propionic acid and salts thereof, hypochlorous acid, and the like. Na chlorate, acetic acid, sodium acetate, glycine, ethyl alcohol, polylysine and its preparation, protamine and its preparation, lysozyme and its preparation, pectin degradation product, alanine, thiamine lauryl sulfate, yuccaform extract, chitosan and its preparation, And propylene glycol.
Examples of the antioxidant include butylhydroxyanisole, butylhydroxytoluene, L-ascorbic acid and sodium ascorbate, erythorbic acid and sodium erythorbate, mixed cophenol and the like.
甘味料としては、例えば、上述の高甘味度甘味料、単糖類(アロース、タロース、グロース、グルコース、アルトロース、マンノース、ガラクトース、イドース、フルクトース、リボース、リキソース、キシロース、アラビノース、アピオース、エリトロース、トレオース、グリセルアルデヒド、セドヘプツロース、コリオース、プシコース、ソルボース、タガトース、リブロース、キシルロース、エリトルロース、ジヒドロキシアセトン等)、二糖類やオリゴ糖類(トレハロース、コージビオース、ニゲロース、マルトース、イソマルトース、イソトレハロース、ソホロース、ラミナリビオース、ゲンチオビオース、ラクトース、スクロース、パラチノース、トレハルオース、フラクトオリゴ糖、パラチノースオリゴ糖、グリコシルスクロース、ラクトスクロース、テアンデロース、ガラクトシルラクトース、ラクチュロース、α−結合ガラクトオリゴ糖、マルトオリゴ糖、イソマルトオリゴ糖、パノース、ニゲロオリゴ糖、トレハロース、デキストリン、サイクロデキストリン、分岐サイクロデキストリン、ゲンチオオリゴ糖、キシロオリゴ糖、キチンオリゴ糖、キトサンオリゴ糖、大豆オリゴ糖、ラフィノース、ビートオリゴ等)、糖アルコール類(グリセロール、エリスリトール、キシリトール、リビトール、アラビトール、ガラクチトール、ソルビトール、マンニトール、還元パラチノース、マルオトリイトール、イソマルトトリイトール、マルトテトライトール、イソマルトテトライトール等)、水飴、還元水飴、糖含有シロップ、液糖、糖蜜、蜂蜜などがあげられ、その化学構造や性状(固体、液体、顆粒など)は特に限定されない。 Examples of the sweetener include the above-described high-intensity sweetener, monosaccharide (allose, talose, growth, glucose, altrose, mannose, galactose, idose, fructose, ribose, lyxose, xylose, arabinose, apiose, erythrose, threose Glyceraldehyde, sedoheptulose, coliose, psicose, sorbose, tagatose, ribulose, xylulose, erythrulose, dihydroxyacetone, etc., disaccharides and oligosaccharides (trehalose, cordobiose, nigerose, maltose, isomaltose, isotrehalose, sophorose, laminaribio) , Gentiobiose, lactose, sucrose, palatinose, trehalose, fructooligosaccharide, palatinose oligosaccharide, glycosyl sucrose , Lactosucrose, theandelose, galactosyl lactose, lactulose, α-linked galactooligosaccharide, malto-oligosaccharide, isomalto-oligosaccharide, panose, nigerooligosaccharide, trehalose, dextrin, cyclodextrin, branched cyclodextrin, gentiooligosaccharide, xylooligosaccharide, chitin oligosaccharide , Chitosan oligosaccharide, soybean oligosaccharide, raffinose, beet oligo, etc.), sugar alcohols (glycerol, erythritol, xylitol, ribitol, arabitol, galactitol, sorbitol, mannitol, reduced palatinose, malotriitol, isomaltoliitol, malto Tetriitol, isomaltotetriitol, etc.), syrup, reduced syrup, sugar-containing syrup, liquid sugar, molasses, honey, etc. The chemical structure and properties (solid, liquid, granules, etc.) are not particularly limited.
着色料としては、β−カロチン色素、抽出カロチン色素、ビタミンB2、銅クロロフィルおよび銅クロロフィルNa、アナトー、アカキャベツ、アカダイコン、イカスミ、植物炭末、ウコン、エルダーベリー、カカオ、カロブ、クロロフィル、クチナシ黄、クチナシ青、クチナシ赤、グレープスキン、コチニール、コーリャン、シソ、シアナット、スピルリナ、タマリンド、タマネギ、トマト、パプリカ、ビートレッド、ブドウ果汁、ベニコウジ、ベニバナ黄、ベニバナ赤、マリーゴールド、ムラサキイモ、ムラサキコーン、ラック、カラメルなどがあげられる。
色素としては、例えば、赤色2号、赤色3号、赤色40号、赤色102号、赤色105号、赤色106号、黄色4号、黄色5号、青色1号、青色2号、赤色3号レーキ、赤色40号レーキ、黄色4号レーキ、黄色5号レーキ、青色1号レーキ、青色2号レーキなどがあげられる。
Coloring agents include β-carotene pigment, extracted carotene pigment, vitamin B2, copper chlorophyll and copper chlorophyll Na, anato, red cabbage, red radish, squid misty, plant charcoal powder, turmeric, elderberry, cacao, carob, chlorophyll, gardenia Yellow, gardenia blue, gardenia red, grapeskin, cochineal, gorilla, perilla, shea nut, spirulina, tamarind, onion, tomato, paprika, beet red, grape juice, red beetle, safflower yellow, safflower red, marigold, purple potato, purple Examples include corn, rack and caramel.
Examples of the dye include Red No. 2, Red No. 3, Red No. 40, Red No. 102, Red No. 105, Red No. 106, Yellow No. 4, Yellow No. 5, Blue No. 1, Blue No. 2, Red No. 3 Lake. Red No. 40 rake, Yellow No. 4 rake, Yellow No. 5 rake, Blue No. 1 rake, Blue No. 2 rake and the like.
乳化剤としては、例えば、グリセリン脂肪酸エステル、ソルビタン脂肪酸エステル、PGエステル、ショ糖脂肪酸エステル、有機酸モノグリセリド、ポリグリセリン脂肪酸エステル、ポリグリセリン縮合リシノレイン酸エステル、プロピレングリコール脂肪酸エステル、レシチン類(レシチン、酵素分解レシチン、酵素処理レシチン等)、植物ステロールなどがあげられる。 Examples of the emulsifier include glycerin fatty acid ester, sorbitan fatty acid ester, PG ester, sucrose fatty acid ester, organic acid monoglyceride, polyglycerin fatty acid ester, polyglycerin condensed ricinoleic acid ester, propylene glycol fatty acid ester, lecithin (lecithin, enzymatic degradation) Lecithin, enzyme-treated lecithin, etc.) and plant sterols.
増粘ゲル化剤としては、例えば、アルギン酸およびその塩(例えば、アルギン酸ナトリウムなど)、アルギン酸プロピレングリコールエステル、カルボキシメチルセルロースカルシウム、カルボキシメチルセルロースナトリウム、ヒドロキシプロピルメチルセルロース、デンプングリコール酸ナトリウム、デンプンリン酸エステルナトリウム、メチルセルロース、ポリアクリル酸ナトリウム、アーモンドガム、アラビアガム、キサンタンガム、アラビノガラクタン、エレミ樹脂、カラヤガム、ガッディガム、ダンマル樹脂、トラガントガム、モモ樹脂、アマシードガム、カシアガム、グアーガム、グアーガム分解物、ローカストビーンガム、タラガム、サイリウムシードガム、サバクヨモギシードガム、セスバニアガム、タマリンドシードガム、ジェランガム、トリアカンソスガム、アルギン酸およびその塩、カラギーナン、フクロノリ抽出物、ファーセルラン、アロエベラ抽出物、オクラ抽出物、キダチアロエ抽出物、トロロアオイ、ペクチン、アエロモナスガム、アウレオバシジウム培養液、アゾトバクター・ビネランジーガム、ウェランガム、エルウィニア・ミツエンシスガム、エンテロバクター・シマナスガム、エンテロバクターガム、カードラン、ジェランガム、スクレロガム、デキストラン、納豆菌ガム、プルラン、大豆多糖類、水溶性ヘミセルロース、カラギーナン、マクロホモプシスガム、ラムザンガム、レバン、酵母細胞壁、微小繊維状セルロースおよびその製剤、バクテリアセルロースおよびその製剤、結晶セルロースおよびその製剤、粉末セルロースおよびその製剤、キチン、キトサン、グルコサミン、オリゴグルコサミン、グルコマンナン、こんにゃく粉、寒天、デキストリン、分岐デキストリン、難消化性デキストリン、PGA、ポルフィラン、ファーセルラン、フコイダン、ゼラチンなどがあげられる。 Examples of the thickening gelling agent include alginic acid and a salt thereof (for example, sodium alginate), propylene glycol alginate, carboxymethylcellulose calcium, carboxymethylcellulose sodium, hydroxypropylmethylcellulose, sodium starch glycolate, sodium starch phosphate, Methyl cellulose, sodium polyacrylate, almond gum, gum arabic, xanthan gum, arabinogalactan, elemi resin, karaya gum, gaddy gum, dammar resin, tragacanth gum, peach resin, peach seed gum, cassia gum, guar gum, guar gum decomposition product, locust bean gum, tara gum, Psyllium seed gum, mackerel mugwort seed gum, sesbania gum, tamarind seed gum , Gellan gum, triacanthosum, alginic acid and its salts, carrageenan, fukuronori extract, fercellan, aloe vera extract, okra extract, trochia aloe extract, trooaoi, pectin, aeromonas gum, aureobasidium broth, azotobacter Vinelandie gum, Welan gum, Erwinia mitsuensis gum, Enterobacter shimanas gum, Enterobacter gum, curdlan, gellan gum, sclerogum, dextran, natto gum, pullulan, soybean polysaccharide, water-soluble hemicellulose, carrageenan, macrohomopsis gum, ramzan gum, Levan, yeast cell wall, microfibrous cellulose and formulations thereof, bacterial cellulose and formulations thereof, crystalline cellulose and formulations thereof, powdered cellulose and Formulation, chitin, chitosan, glucosamine, Oligoglucosamine, glucomannan, konjac flour, agar, dextrin, branched dextrin, indigestible dextrin, PGA, porphyran, furcellaran, fucoidan, and gelatin.
品質改良剤としては、ステアロイル乳酸Ca、フィチン酸、プロピレングリコール、リン酸Ca、リン酸Na、ピロリン酸Na、ポリリン酸Na、メタ・ヘキサリン酸Na、リン酸K、リン酸アンモニウム、リン酸、焼みょうばん、生みょうばん、ホエーたん白、カゼイン、カゼイネート、プラズマパウダー、粉末状大豆たん白、粉末状小麦たん白、ペースト状小麦たん白、EDTA塩類などがあげられる。
調味料としては、例えば、グルタミン酸Na、核酸系調味料、アミノ酸系調味料、エキス系調味料、酵母エキス、グリシン、アラニンなどがあげられる。
As quality improvers, stearoyl lactate Ca, phytic acid, propylene glycol, phosphate phosphate, Na phosphate, Na pyrophosphate, polyphosphate Na, meta-hexaphosphate Na, phosphate K, ammonium phosphate, phosphoric acid, baked Examples include alum, raw alum, whey protein, casein, caseinate, plasma powder, powdered soy protein, powdered wheat protein, pasty wheat protein, EDTA salts and the like.
Examples of the seasoning include sodium glutamate, nucleic acid seasoning, amino acid seasoning, extract seasoning, yeast extract, glycine, and alanine.
酸味料としては、例えば、クエン酸およびその塩、乳酸、リンゴ酸、酒石酸、コハク酸、フマル酸、アジピン酸、グルコン酸液、グルコノデルタラクトンなどがあげられる。
強化剤としては、例えば、ビタミンA、ビタミンB1、ビタミンB2、ビタミンB6、ビタミンB12、ビタミンC、ビタミンD、ビタミンE、ニコチン酸およびニコチン酸アミド、葉酸、パトテン酸Ca、グルコン酸Ca、乳酸Ca、天然Ca、ミルクCaなどがあげられる。
Examples of the acidulant include citric acid and salts thereof, lactic acid, malic acid, tartaric acid, succinic acid, fumaric acid, adipic acid, gluconic acid solution, glucono delta lactone and the like.
Examples of the fortifier include vitamin A, vitamin B1, vitamin B2, vitamin B6, vitamin B12, vitamin C, vitamin D, vitamin E, nicotinic acid and nicotinamide, folic acid, patenoic acid Ca, gluconic acid Ca, and lactate Ca , Natural Ca, milk Ca and the like.
香料としては、例えば、ピーチフレーバー、オレンジフレーバー、レモンフレーバー等のフルーツフレーバー類、アロマフレーバー類、マルトール、フラネオール等のシュガーフレーバー類、ソトロン等のフレーバーエンハンサー類、フラボノイド類、カカオマス等のポリフェノール類、プリカーサーフレーバー類、ミートフレーバー類、コーヒーフレーバー類、ミルクフレーバー、メントール類、デカラクトン類などがあげられる。
酵素としては、例えば、αアミラーゼ、βアミラーゼ、グルコアミラーゼ、プルラナーゼ、グルコースイソメラーゼ、プロテアーゼ、レンネット、パンクレアチン、パパインなどがあげられる。
Examples of the fragrance include fruit flavors such as peach flavor, orange flavor and lemon flavor, aroma flavors, sugar flavors such as maltol and furaneol, flavor enhancers such as sotron, polyphenols such as flavonoids and cacao mass, and precursors. Examples include flavors, meat flavors, coffee flavors, milk flavors, menthols, and decalactones.
Examples of the enzyme include α-amylase, β-amylase, glucoamylase, pullulanase, glucose isomerase, protease, rennet, pancreatin, and papain.
ここで言う医薬品とは、薬事法に規定される医薬品をさす。つまり以下の(1)〜(3)に該当するものであり、医薬品薬効成分の多くがこれに含まれる。
(1)日本薬局方に収められている物
(2)人又は動物の疾病の診断、治療又は予防に使用されることが目的とされている物であって、機械器具、歯科材料、医療用品及び衛生用品(以下「機械器具等」という。)でないもの(医薬部外品を除く。)
(3)人又は動物の身体の構造又は機能に影響を及ぼすことが目的とされている物であって、機械器具等でないもの(医薬部外品及び化粧品を除く。)
The term “medicine” as used herein refers to a drug prescribed by the Pharmaceutical Affairs Law. That is, it corresponds to the following (1) to (3), and many of medicinal medicinal ingredients are included in this.
(1) Items stored in the Japanese Pharmacopoeia (2) Items intended to be used for diagnosis, treatment or prevention of human or animal diseases, machinery, dental materials, medical supplies Non-sanitary products (hereinafter referred to as “machinery equipment”) (excluding quasi-drugs)
(3) Products that are intended to affect the structure or function of the human or animal body, and are not machinery or equipment (excluding quasi-drugs and cosmetics).
ここで言う医薬品添加物とは、薬事法上の医薬品や医薬部外品に該当しない、医薬品製剤に含まれる有効成分以外の物質であり、「製剤化を容易にする」、「品質の安定化を図る」、「有用性を高める」などを目的として、医薬品や医薬部外品などに添加される物質の総称である。用途により、賦形剤、崩壊剤、結合剤、流動化剤、矯味剤、香料、着色剤、甘味剤、溶剤、油脂、増粘剤、界面活性剤、ゲル化剤、安定剤、保存剤、緩衝剤、懸濁化剤、粘稠剤などに分類される。代表的な医薬品添加物は、「医薬品添加剤事典」(株式会社薬事日報社)、「医薬品添加物ハンドブック」(株式会社薬事日報社)などに収載されている。 Pharmaceutical additives mentioned here are substances other than active ingredients contained in pharmaceutical preparations that do not fall under the Pharmaceutical Affairs Law or quasi-drugs. It is a general term for substances added to pharmaceuticals and quasi-drugs for the purpose of “improving usefulness” and “increasing usability”. Depending on the application, excipients, disintegrants, binders, fluidizers, flavoring agents, fragrances, colorants, sweeteners, solvents, fats and oils, thickeners, surfactants, gelling agents, stabilizers, preservatives, It is classified into buffer, suspending agent, thickener and the like. Representative pharmaceutical additives are listed in “Pharmaceutical Additives Encyclopedia” (Pharmaceutical Daily Inc.), “Pharmaceutical Additives Handbook” (Pharmaceutical Daily Inc.), and the like.
次に実施例によって本発明をさらに詳細に説明する。なお本願発明にかかる物質の諸物性の評価は以下の手法に拠った。
<糖組成>
以下の条件で、糖組成分析を行った。
装置:高速液体クロマトグラフ「LC−20A型」(株式会社島津製作所製)
検出器:示差屈折率検出器(RI検出器)
カラム:「Asahipak NH2P−50」(昭和電工株式会社製)
カラム温度:40℃
移動相:アセトニトリル/水=75/25(容積比)
流量:1mL/min
Next, the present invention will be described in more detail with reference to examples. The evaluation of various physical properties of the substance according to the present invention was based on the following method.
<Sugar composition>
The sugar composition analysis was performed under the following conditions.
Apparatus: High-performance liquid chromatograph “LC-20A type” (manufactured by Shimadzu Corporation)
Detector: Differential refractive index detector (RI detector)
Column: “Asahipak NH2P-50” (manufactured by Showa Denko KK)
Column temperature: 40 ° C
Mobile phase: acetonitrile / water = 75/25 (volume ratio)
Flow rate: 1 mL / min
<離水率>
製造後、あらかじめ質量測定し、40℃で1時間保存したホイップドクリームを、「JIS Z 8801−1:2006 試験用ふるい−第1部:金属製網ふるい」に規定される、公称目開き355μmの試験用ふるいの上に静かに載せ、ふるいを通過した液体の質量をはかりとる。さらに次式に従って、離水率を算出する。
離水率(%)=(ホイップドクリームの質量)/(ふるいを通過した液体の質量)×100
<Water separation rate>
After the production, the whipped cream previously mass-measured and stored at 40 ° C. for 1 hour is defined as “JIS Z 8801-1: 2006 Test Sieve—Part 1: Metal Net Sieve”, nominal opening 355 μm Gently place it on the test sieve, and weigh the liquid that has passed through the sieve. Furthermore, the water separation rate is calculated according to the following formula.
Water separation rate (%) = (mass of whipped cream) / (mass of liquid passed through the sieve) × 100
<安定率と安定性改善効果>
安定性は、次式により算出される安定率をもとに表される。この安定率が3%以上の場合に、安定性改善効果があると判断される。
安定率(%)={(β−α)/α}×100
ここで、α:セロオリゴ糖を配合しないホイップドクリームの離水率(%)、β:セロオリゴ糖を配合したホイップドクリームの離水率(%)である。
<Stability rate and stability improvement effect>
Stability is expressed based on the stability rate calculated by the following equation. When this stability rate is 3% or more, it is determined that there is an effect of improving stability.
Stability rate (%) = {(β−α) / α} × 100
Here, α: water separation rate (%) of whipped cream not containing cellooligosaccharide, β: water separation rate (%) of whipped cream containing cellooligosaccharide.
<強度>
製造後、−20℃で12時間、さらに10℃の雰囲気下で1時間保存したホイップドクリームについて、以下の条件で押し込んだ時の、深度10mmにおける押し込み強度を求めた。
装置:RHEO METER「NRM−2002J型」(不動工業株式会社製)
押し込み治具:10mmφ球状治具
押し込み速度:60mm/min
測定温度:10℃
<Strength>
For the whipped cream stored at −20 ° C. for 12 hours and further under an atmosphere of 10 ° C. for 1 hour after the production, the indentation strength at a depth of 10 mm was obtained when the whipped cream was indented under the following conditions.
Apparatus: RHEO METER “NRM-2002J type” (manufactured by Fudo Kogyo Co., Ltd.)
Pushing jig: 10mmφ spherical jig Pushing speed: 60mm / min
Measurement temperature: 10 ° C
<保形率と保形改善効果>
保形性は、次式により算出される保形率をもとに表され、冷解凍時の保形性の指標である。この保形率が3%以上の場合に、保形性改善効果があると判断される。
保形率(%)={(δ−γ)/γ}×100
ここで、γ:セロオリゴ糖を配合しないホイップドクリームの強度(mN)、δ:セロオリゴ糖を配合したホイップドクリームの強度(mN)である。
<Shape retention rate and shape retention improvement effect>
The shape retention property is expressed based on the shape retention rate calculated by the following equation, and is an index of shape retention property during cold thawing. When this shape retention rate is 3% or more, it is judged that there is an effect of improving shape retention.
Shape retention rate (%) = {(δ−γ) / γ} × 100
Here, γ: strength (mN) of whipped cream not containing cellooligosaccharide, and δ: strength (mN) of whipped cream containing cellooligosaccharide.
以下、本発明を実施例と比較例を示して、具体的に説明するが、本発明はこれらに何ら限定されるものではない。
実施例で使用する原材料について、次の(1)〜(5)に示す。
EXAMPLES Hereinafter, although an Example and a comparative example are shown and this invention is demonstrated concretely, this invention is not limited to these at all.
The raw materials used in the examples are shown in the following (1) to (5).
(1)セロオリゴ糖の製造:普通寒天培地にTricoderma reesei、GL−1株(独立行政法人産業技術総合研究所 特許生物寄託センター、受領番号FERM BP−10323)を接種し、37℃で7日間培養後、その培地表面から胞子を1白金耳取り、ポリペプトン1g、酵母エキス0.5g、リン酸1カリウム2g、硫酸アンモニウム1.5g、硫酸マグネシウム0.3g、塩化カルシウム0.3g、トレースエレメント1mL(硼酸6mg、モリブデン酸アンモニウム4水和物26mg、塩化鉄(3)6水和物100mg、硫酸銅5水和物40mg、硫酸マンガン4水和物8mg、硫酸亜鉛7水和物200mgを全量100mLの精製水に溶解させたもの)、アデカノール1mL、結晶セルロース(旭化成ケミカルズ株式会社製「セオラスPH−101」)10gを全量1Lの精製水に懸濁および溶解させた培地に植菌し、28℃で5日間通気攪拌培養した。
培養中は、水酸化ナトリウム水溶液を用いて、培地のpHを2.8〜4.7となるように調節した。培養後の液を遠心分離し、上清を目開き0.46μmの精密ろ過膜で除菌し、ろ液を分画分子量13000の限外ろ過膜(旭化成ケミカルズ株式会社製 「マイクローザペンシル型モジュール ACP−0013」)を使用して、容積比で10倍濃縮し粗酵素を得た。
(1) Production of cellooligosaccharide: Trichoderma reesei, GL-1 strain (Incorporated Administrative Agency, National Institute of Advanced Industrial Science and Technology, Patent Biodeposition Center, receipt number FERM BP-10323) is inoculated on a normal agar medium and cultured at 37 ° C. for 7 days Thereafter, 1 platinum spore was removed from the surface of the medium, 1 g of polypeptone, 0.5 g of yeast extract, 2 g of potassium phosphate, 1.5 g of ammonium sulfate, 0.3 g of magnesium sulfate, 0.3 g of calcium chloride, 1 mL of trace element (boric acid) Purification of 6 mg, ammonium molybdate tetrahydrate 26 mg, iron (3) hexahydrate 100 mg, copper sulfate pentahydrate 40 mg, manganese sulfate tetrahydrate 8 mg, zinc sulfate heptahydrate 200 mg in a total volume of 100 mL Water dissolved), adecanol 1mL, crystalline cellulose (Asahi Kasei Chemicals Co., Ltd.) Was inoculated into Company Ltd. "Ceolus PH-101") medium were suspended and dissolved in 10g of purified water total amount 1L, for 5 days under aeration-agitation culture at 28 ° C..
During the culture, the pH of the medium was adjusted to 2.8 to 4.7 using an aqueous sodium hydroxide solution. The cultured liquid is centrifuged, the supernatant is sterilized with a microfiltration membrane having an opening of 0.46 μm, and the filtrate is ultrafiltered with a molecular weight cut off of 13,000 (“Microza Pencil Type Module” manufactured by Asahi Kasei Chemicals Corporation). ACP-0013 ") was used to obtain a crude enzyme by concentration 10 times by volume.
次に、市販針葉樹由来の溶解パルプを使用し、加水分解条件を塩酸濃度0.4%塩酸水溶液、120℃、1時間として、加水分解し、酸不溶性残渣を洗浄、ろ過し、ウェットケークを得た。このウェットケークをセルロース10%濃度の水分散体とし、超高性能分散機・湿式微粉砕機(アシザワ株式会社製、「パールミルRL」、φ1mmジルコニアビーズ使用 充填率80%)を使用し、圧密・磨砕処理を施し、セルロース微粒子分散体を得た。
この磨砕セルロースが2質量%、粗酵素をタンパク質濃度0.25%になるように50mM酢酸−酢酸ナトリウム緩衝液(pH4.5)に懸濁溶解させ、全量1000mLとし、ガラス製フラスコに仕込んだ。
Next, use a commercially available softwood-derived dissolving pulp, and hydrolyze it with a hydrochloric acid concentration of 0.4% aqueous hydrochloric acid at 120 ° C. for 1 hour to wash the acid-insoluble residue and filter to obtain a wet cake. It was. Using this wet cake as an aqueous dispersion with a concentration of 10% cellulose, using an ultra-high performance disperser / wet pulverizer (Ashizawa Co., Ltd., “Pearl Mill RL”, φ1 mm zirconia bead filling rate 80%) A grinding treatment was performed to obtain a cellulose fine particle dispersion.
The ground cellulose was suspended and dissolved in a 50 mM acetic acid-sodium acetate buffer solution (pH 4.5) so that the protein concentration was 2% by mass and the protein concentration was 0.25%, and the total volume was 1000 mL. .
このガラス製フラスコを、55℃の水槽に仕込み、内部を攪拌しながら4時間反応させた。反応終了後、反応液を懸濁状態で300μL分注し、限外ろ過モジュール(分画分子量10000)を使用し、酵素、未分解セルロースを取り除いた後、高速液体クロマトグラフィーで糖濃度を分析した。該反応液の糖濃度は、グルコース0.3質量%、セロビオース1.5質量%であった。
該反応液を、分画分子量13000の限外ろ過膜(旭化成ケミカルズ株式会社製、「マイクローザペンシル型モジュール ACP−0013」)でろ過し、得られたろ液を陽・陰イオン交換樹脂で脱イオン処理し、70℃、減圧下で蒸留し、20倍の糖濃度の水溶液を得た。
The glass flask was placed in a 55 ° C. water bath and reacted for 4 hours while stirring the interior. After completion of the reaction, 300 μL of the reaction solution was dispensed in a suspended state, the enzyme and undegraded cellulose were removed using an ultrafiltration module (fractional molecular weight 10,000), and then the sugar concentration was analyzed by high performance liquid chromatography. . The sugar concentration of the reaction solution was 0.3% by mass of glucose and 1.5% by mass of cellobiose.
The reaction solution is filtered through an ultrafiltration membrane having a molecular weight cut off of 13,000 (“Asahi Kasei Chemicals Co., Ltd.,“ Micro-the Pencil type module ACP-0013 ”), and the resulting filtrate is deionized with a cation / anion exchange resin. Treatment and distillation under reduced pressure at 70 ° C. gave an aqueous solution with a 20-fold sugar concentration.
上記で得られたセロオリゴ糖水溶液100mLを、200mLのガラス製フラスコに導入し、攪拌しながら、毎時10℃の速度で、70℃から5℃まで冷却した後、エタノールを水に加え晶析した。水溶液中に晶出したセロオリゴ糖を、減圧ろ過、乾燥、粉砕、篩下し、セロオリゴ糖粉末を得た。得たれたセロオリゴ糖粉末の糖組成は、グルコース0.9質量%、セロビオース98.2質量%、セロトリオース0.4質量%、セロテトラオース0.2質量%であった。 100 mL of the cellooligosaccharide aqueous solution obtained above was introduced into a 200 mL glass flask, cooled to 70 ° C. to 5 ° C. at a rate of 10 ° C. per hour while stirring, and then ethanol was added to water for crystallization. The cellooligosaccharide crystallized in the aqueous solution was filtered under reduced pressure, dried, pulverized, and sieved to obtain cellooligosaccharide powder. The sugar composition of the obtained cellooligosaccharide powder was 0.9 mass% glucose, 98.2 mass% cellobiose, 0.4 mass% cellotriose, and 0.2 mass% cellotetraose.
(2)グラニュー糖(第一糖業株式会社製)
(3)アスパルテーム(味の素株式会社製)
(4)クリーム(日本ミルクコミュニティ株式会社製、「生クリーム」、乳脂肪分48%、原材料名:生乳)
(5)ココア粉末(バンホーテン株式会社製)
(2) Granulated sugar (Daiichi Sugar Industry Co., Ltd.)
(3) Aspartame (Ajinomoto Co., Inc.)
(4) Cream (produced by Nippon Milk Community Co., Ltd., “Raw cream”, 48% milk fat, raw material name: raw milk)
(5) Cocoa powder (manufactured by Van Hoten Co., Ltd.)
[実施例1]
87.5質量%のクリームに、12.5質量%のセロオリゴ糖を添加し、回転型ホモジナイザー(プライミクス株式会社製、「T.K.ホモミクサー」)を使用して、5℃に保ちながら、6000rpmで2分間攪拌し、ホイップドクリームAを製造し、円筒型のサンプル瓶に充填した。乳脂肪分は42%であった。
製造後、40℃で1時間保存した後に求めた、ホイップドクリームAの離水率は8.8%であった。ホイップドクリームAの離水率と、比較例1のホイップドクリームXの離水率12.5%から、次式に従って安定率Aを求めたところ29.6%であり、安定性改善効果があることがわかった。
安定率A(%)={(β1−α1)/α1}×100
ここで、α1:セロオリゴ糖を配合しないホイップドクリームXの離水率(%)、β1:セロオリゴ糖を配合したホイップドクリームAの離水率(%)である。
[Example 1]
12.5% by mass of cellooligosaccharide was added to 87.5% by mass of cream, and 6000 rpm while maintaining at 5 ° C. using a rotary homogenizer (“TK homomixer” manufactured by Primix Co., Ltd.). Was stirred for 2 minutes to produce whipped cream A and filled into a cylindrical sample bottle. The milk fat content was 42%.
After the production, the water separation rate of whipped cream A obtained after storage at 40 ° C. for 1 hour was 8.8%. From the water separation rate of the whipped cream A and the water separation rate of 12.5% of the whipped cream X of Comparative Example 1, the stability factor A was obtained according to the following formula and found to be 29.6%, indicating that there was an effect of improving stability. I understood.
Stability rate A (%) = {(β1-α1) / α1} × 100
Here, α1: water separation rate (%) of whipped cream X not containing cellooligosaccharide, and β1: water separation rate (%) of whipped cream A containing cellooligosaccharide.
また製造後、−20℃で12時間、さらに10℃の雰囲気下で1時間保存したホイップドクリームAの強度は、325mNであった。ホイップドクリームAの強度と、比較例1のホイップドクリームXの強度163mNから、次式に従って保形率Aを求めたところ99.3%であり、保形性改善効果が認められた。
保形率A(%)={(δ1−γ1)/γ1}×100
ここで、γ1:セロオリゴ糖を配合しないホイップドクリームXの強度(mN)、δ1:セロオリゴ糖を配合したホイップドクリームAの強度(mN)である。
Moreover, the intensity | strength of the whipped cream A preserve | saved for 12 hours at -20 degreeC after manufacture and also 1 hour in the atmosphere of 10 degreeC was 325 mN. From the strength of whipped cream A and the strength of 163 mN of whipped cream X of Comparative Example 1, the shape retention ratio A was found to be 99.3% according to the following formula, and an effect of improving shape retention was recognized.
Shape retention ratio A (%) = {(δ1-γ1) / γ1} × 100
Here, γ1: strength (mN) of whipped cream X not containing cellooligosaccharide, δ1: strength (mN) of whipped cream A containing cellooligosaccharide.
[実施例2]
実施例1の12.5質量%のセロオリゴ糖の代わりに、8質量%のセロオリゴ糖、4.498質量%のグラニュー糖、0.002質量%のアスパルテームを添加して、実施例1と同様の方法で、ホイップドクリームBを製造し、円筒型のサンプル瓶に充填した。乳脂肪分は42%であった。
製造後、40℃で1時間保存した後に求めた、ホイップドクリームBの離水率は10.2%であった。ホイップドクリームBの離水率と、比較例1のホイップドクリームXの離水率12.5%から、次式に従って安定率Bを求めたところ18.4%であり、安定性改善効果があることがわかった。
安定率B(%)={(β2−α2)/α2}×100
ここで、α2:セロオリゴ糖を配合しないホイップドクリームXの離水率(%)、β2:セロオリゴ糖を配合したホイップドクリームBの離水率(%)である。
[Example 2]
In place of 12.5% by mass of cellooligosaccharide of Example 1, 8% by mass of cellooligosaccharide, 4.498% by mass of granulated sugar, and 0.002% by mass of aspartame were added. The method produced whipped cream B and filled it into a cylindrical sample bottle. The milk fat content was 42%.
After the production, the water separation rate of whipped cream B obtained after storage at 40 ° C. for 1 hour was 10.2%. From the water separation rate of the whipped cream B and the water separation rate of 12.5% of the whipped cream X of Comparative Example 1, when the stability rate B was determined according to the following formula, it was 18.4% and had a stability improving effect. I understood.
Stability rate B (%) = {(β2-α2) / α2} × 100
Here, α2: water separation rate (%) of whipped cream X not containing cellooligosaccharide, and β2: water separation rate (%) of whipped cream B containing cellooligosaccharide.
また製造後、−20℃で12時間、さらに10℃の雰囲気下で1時間保存したホイップドクリームBの強度は、253mNであった。ホイップドクリームBの強度と、比較例1のホイップドクリームXの強度163mNから、次式に従って保形率Bを求めたところ55.2%であり、保形性改善効果が認められた。
保形率B(%)={(δ2−γ2)/γ2}×100
ここで、γ2:セロオリゴ糖を配合しないホイップドクリームXの強度(mN)、δ2:セロオリゴ糖を配合したホイップドクリームBの強度(mN)である
Moreover, the intensity | strength of the whipped cream B preserve | saved for 12 hours at -20 degreeC after manufacture and also 1 hour in the atmosphere of 10 degreeC was 253 mN. From the strength of whipped cream B and the strength of 163 mN of whipped cream X of Comparative Example 1, the shape retention ratio B was determined according to the following formula and found to be 55.2%, and an effect of improving shape retention was recognized.
Shape retention B (%) = {(δ2-γ2) / γ2} × 100
Here, γ2 is the strength (mN) of whipped cream X not containing cellooligosaccharide, and δ2 is the strength (mN) of whipped cream B containing cellooligosaccharide.
[実施例3]
85質量%の実施例1のクリームを、5℃に調整後、攪拌装置(株式会社愛工舎製作所製、「ケンミックス アイコーPRO、型式:KM−600」、付属アタッチメントとしてホイッパーを装着したもの)のボールに投入し、さらに13質量%のセロオリゴ糖を添加して、目盛4で4分間、ホイップした。乳脂肪分は、40.8%であった。
次に、2質量%のココア粉末を添加し、さらに目盛4で1分間ホイップし、チョコレートクリームCを製造した。
チョコレートクリームCを、星型の口金を付けた絞り袋に充填し、市販のスポンジ生地を、直径10cm×高さ3cmに切り出したものの上に5g分絞り出し、チョコレートケーキDを得た。30℃で12時間保存して、チョコレートケーキDの外観を観察したが、チョコレートクリームのダレはなく、ツノが立った状態であった。
[Example 3]
After the 85 mass% cream of Example 1 was adjusted to 5 ° C., a stirring device (manufactured by Aikosha Mfg. Co., Ltd., “Kenmix Aiko PRO, model: KM-600”, with attached whipper as an attached attachment) The mixture was put into a bowl, and further 13% by mass of cellooligosaccharide was added and whipped with a scale 4 for 4 minutes. The milk fat content was 40.8%.
Next, 2% by mass of cocoa powder was added, and further whipped on scale 4 for 1 minute to produce chocolate cream C.
Chocolate cream C was filled into a squeezed bag with a star-shaped mouthpiece, and a commercially available sponge dough was squeezed out by 5 g onto a piece cut into a diameter of 10 cm and a height of 3 cm to obtain a chocolate cake D. Although it preserve | saved at 30 degreeC for 12 hours and observed the external appearance of chocolate cake D, there was no dripping of chocolate cream and it was in the state where the horn stood.
[比較例1]
実施例1のセロオリゴ糖の代わりに、グラニュー糖を添加して、実施例1と同様の方法でホイップドクリームXを製造し、評価した。乳脂肪分は42%であった。
ホイップドクリームXの離水率は12.5%、強度は163mNと、実施例1および2と比較して、安定性や保形性に劣るものであった。
[Comparative Example 1]
Instead of the cellooligosaccharide of Example 1, granulated sugar was added, and whipped cream X was produced and evaluated in the same manner as in Example 1. The milk fat content was 42%.
The whipped cream X had a water separation rate of 12.5% and a strength of 163 mN, which was inferior in stability and shape retention compared to Examples 1 and 2.
[比較例2]
実施例3のセロオリゴ糖の代わりに、グラニュー糖を使用して、実施例3と同様の方法でチョコレートクリームYとチョコレートケーキZを製造し、評価した。
チョコレートケーキZの外観を観察したところ、チョコレートクリームのダレが発生し、部分的にツノが消失してしまった。
[Comparative Example 2]
Chocolate cream Y and chocolate cake Z were produced and evaluated in the same manner as in Example 3 using granulated sugar instead of the cellooligosaccharide of Example 3.
When the appearance of the chocolate cake Z was observed, sagging of the chocolate cream occurred and the horns disappeared partially.
本発明は、難消化性であるセロオリゴ糖を配合することで、低カロリーで安定性が高く、且つ、保形性に優れたホイップドクリーム、およびそれを配合した食品または医薬品組成物が提供可能である。つまり外観に優れ、商品価値の高い製品を提供することができる。 The present invention can provide a low-calorie, high stability and excellent shape-retaining whipped cream and a food or pharmaceutical composition containing the same by blending cellooligosaccharide which is indigestible It is. That is, it is possible to provide a product having an excellent appearance and a high commercial value.
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Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
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JP2012075353A (en) * | 2010-09-30 | 2012-04-19 | Ogawa & Co Ltd | Flavor improving agent of soy milk or food and drink containing soy milk |
JP2014533522A (en) * | 2011-12-03 | 2014-12-15 | カヴァリエ ナームローゼ フェンノートシャップCavalier N.V. | Fiber reinforced filling composition for chocolate products |
JP2018531030A (en) * | 2015-10-22 | 2018-10-25 | ジボダン エス エー | How to mask off taste with cellobiose and / or psicose |
CN117481213A (en) * | 2024-01-02 | 2024-02-02 | 内蒙古蒙牛乳业(集团)股份有限公司 | Acidified cream and preparation method thereof |
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JP2002105093A (en) * | 2000-09-27 | 2002-04-10 | Nippon Paper Industries Co Ltd | New saccharide derivative, method for producing the same and use thereof |
WO2006011479A1 (en) * | 2004-07-27 | 2006-02-02 | Asahi Kasei Chemicals Corporation | Processes for producing cellooligosaccharide |
WO2007037249A1 (en) * | 2005-09-27 | 2007-04-05 | Asahi Kasei Chemicals Corporation | Cellooligosaccharide-containing composition |
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JPH0759532A (en) * | 1993-08-23 | 1995-03-07 | Kao Corp | Normal temperature-resistant cream with high resistance to bacteria |
JP2002105093A (en) * | 2000-09-27 | 2002-04-10 | Nippon Paper Industries Co Ltd | New saccharide derivative, method for producing the same and use thereof |
WO2006011479A1 (en) * | 2004-07-27 | 2006-02-02 | Asahi Kasei Chemicals Corporation | Processes for producing cellooligosaccharide |
WO2007037249A1 (en) * | 2005-09-27 | 2007-04-05 | Asahi Kasei Chemicals Corporation | Cellooligosaccharide-containing composition |
Cited By (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP2012075353A (en) * | 2010-09-30 | 2012-04-19 | Ogawa & Co Ltd | Flavor improving agent of soy milk or food and drink containing soy milk |
JP2014533522A (en) * | 2011-12-03 | 2014-12-15 | カヴァリエ ナームローゼ フェンノートシャップCavalier N.V. | Fiber reinforced filling composition for chocolate products |
JP2018064574A (en) * | 2011-12-03 | 2018-04-26 | カヴァリエ ナームローゼ フェンノートシャップCavalier N.V. | Fiber reinforced filling composition for chocolate product |
JP2018531030A (en) * | 2015-10-22 | 2018-10-25 | ジボダン エス エー | How to mask off taste with cellobiose and / or psicose |
CN117481213A (en) * | 2024-01-02 | 2024-02-02 | 内蒙古蒙牛乳业(集团)股份有限公司 | Acidified cream and preparation method thereof |
CN117481213B (en) * | 2024-01-02 | 2024-03-15 | 内蒙古蒙牛乳业(集团)股份有限公司 | Acidified cream and preparation method thereof |
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