JP2008076243A5 - - Google Patents
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- JP2008076243A5 JP2008076243A5 JP2006256113A JP2006256113A JP2008076243A5 JP 2008076243 A5 JP2008076243 A5 JP 2008076243A5 JP 2006256113 A JP2006256113 A JP 2006256113A JP 2006256113 A JP2006256113 A JP 2006256113A JP 2008076243 A5 JP2008076243 A5 JP 2008076243A5
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- 238000004458 analytical method Methods 0.000 claims 25
- 238000001514 detection method Methods 0.000 claims 24
- 238000002347 injection Methods 0.000 claims 14
- 239000007924 injection Substances 0.000 claims 14
- 238000000926 separation method Methods 0.000 claims 5
- 238000010521 absorption reaction Methods 0.000 claims 1
- 239000007788 liquid Substances 0.000 claims 1
Claims (8)
前記試料注入部により注入された前記分析試料を成分毎に分離する分離カラムと、
前記分離カラムにより分離された前記分析試料の成分を検出する検出器と、
前記分析試料の数を入力する入力部と、
前記入力部で指定された分析試料数の分析を行うように前記試料注入部、前記分離カラム、前記検出器、および入力部等の各ユニットを制御する制御部と、
分析により得られるクロマトグラムを記録する記録部とを備えた液体クロマトグラフを含むクロマトグラフ装置において、
前記成分の検知開始から終了までの検出時間範囲を記憶する記憶手段と、
前記記憶手段に記憶された検出時間範囲を基に複数の前記分析試料を前記試料注入部に注入する注入間隔を算出する処理手段と、
前記注入間隔を適用して前記複数の分析試料の分析が行われるように各ユニットを制御する制御手段を有することを特徴とするクロマトグラフ装置。 A sample injection part for injecting an analysis sample;
A separation column for separating the analysis sample injected by the sample injection unit into components;
A detector for detecting a component of the analysis sample separated by the separation column;
An input unit for inputting the number of the analysis samples;
A control unit that controls each unit such as the sample injection unit, the separation column, the detector, and the input unit so as to perform analysis of the number of analysis samples specified by the input unit;
In a chromatograph apparatus including a liquid chromatograph provided with a recording unit for recording a chromatogram obtained by analysis,
Storage means for storing a detection time range from the detection start to the end of the component;
Processing means for calculating an injection interval for injecting a plurality of the analysis samples into the sample injection unit based on the detection time range stored in the storage means;
A chromatographic apparatus comprising control means for controlling each unit so that the analysis of the plurality of analysis samples is performed by applying the injection interval.
前記検出器として質量分析計を用い、
前記質量分析計で分析検知された成分の質量電荷比と前記検出時間範囲とを前記記憶手段に記憶し、
前記処理手段は前記検出時間範囲のうち、最大の検出時間範囲幅以上の時間間隔を前記注入間隔とすることを特徴とするクロマトグラフ装置。 The chromatographic apparatus according to claim 1,
Using a mass spectrometer as the detector,
The mass-to-charge ratio of the component analyzed and detected by the mass spectrometer and the detection time range are stored in the storage means,
The said processing means makes the time interval more than the largest detection time range width | variety among the said detection time ranges as the said injection | pouring interval, The chromatograph apparatus characterized by the above-mentioned.
同じ分析試料中に含まれる質量電荷比が同一または所定近似値以内にある複数成分について、前記複数成分の検知時間範囲を全て包含する複数成分検出時間範囲を新たに設定する機能を有することを特徴とするクロマトグラフ装置。 The chromatographic apparatus according to claim 2, wherein
A function of newly setting a multi-component detection time range including all the detection time ranges of the multi-components for a plurality of components having the same mass-to-charge ratio contained in the same analysis sample or within a predetermined approximate value. A chromatographic apparatus.
前記分析試料に含まれる検出対象成分の中からユーザが選択する任意の複数成分に跨がるユーザ選択複数成分検出時間範囲を新たに設定し、このユーザ選択複数成分検出時間範囲、および前記検出時間範囲から最も長い検出時間範囲を前記注入時間間隔とすることを特徴とするクロマトグラフ装置。 The chromatographic apparatus according to claim 2, wherein
A user-selected multi-component detection time range that extends over any of a plurality of components selected by the user from the detection target components included in the analysis sample is newly set, and the user-selected multi-component detection time range and the detection time A chromatograph apparatus characterized in that a longest detection time range from the range is the injection time interval.
前記分析試料の注入時刻と、前記分析試料に含まれる検出対象成分の質量電荷比と、前記検出対象成分の検出時間範囲を基に、前記検出対象成分が前記検出器に到達する検出予定時刻を算出する機能を備えることを特徴とするクロマトグラフ装置。 The chromatographic apparatus according to claim 2, wherein
Based on the injection time of the analysis sample, the mass-to-charge ratio of the detection target component contained in the analysis sample, and the detection time range of the detection target component, the detection scheduled time when the detection target component reaches the detector A chromatographic apparatus comprising a function for calculating.
前記検出予定時刻と、分析により得られる成分の検出時刻を基に、検出された検出成分を前記分析試料に帰属して記録する機能を備えることを特徴とするクロマトグラフ装置。 The chromatographic apparatus according to claim 5, wherein
A chromatograph apparatus comprising a function of recording a detected detected component belonging to the analysis sample based on the scheduled detection time and a detection time of a component obtained by analysis.
前記検出器としてDAD検出器を用い、
前記記憶手段は前記分析試料に含まれる成分の吸収波長と検出時間範囲とを各々記憶し、
前記処理手段は前記分析試料に含まれる成分の検出時間範囲のうち、最大の時間幅以上の時間間隔を前記注入間隔とすることを特徴とするクロマトグラフ装置。 The chromatographic apparatus according to claim 1,
Using a DAD detector as the detector,
The storage means stores an absorption wavelength and a detection time range of each component contained in the analysis sample,
The chromatographic apparatus characterized in that the processing means sets a time interval equal to or greater than a maximum time width in the detection time range of components contained in the analysis sample as the injection interval.
前記試料注入部により注入された前記分析試料を成分毎に分離する分離カラムと、
前記分離カラムにより分離された前記分析試料の成分を検出する検出器を備えた分析方法において、
前記分析試料の各成分検出の開始から終了までにかかる検出時間範囲を基に複数の前記分析試料を前記試料注入部に注入する注入間隔を算出することを特徴とする分析方法。 A sample injection part for injecting an analysis sample;
A separation column for separating the analysis sample injected by the sample injection unit into components;
In an analysis method comprising a detector for detecting a component of the analysis sample separated by the separation column,
An analysis method characterized in that an injection interval for injecting a plurality of the analysis samples into the sample injection section is calculated based on a detection time range required from the start to the end of detection of each component of the analysis sample.
Priority Applications (1)
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JP2006256113A JP4861107B2 (en) | 2006-09-21 | 2006-09-21 | Chromatograph apparatus and analysis method |
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JP2006256113A JP4861107B2 (en) | 2006-09-21 | 2006-09-21 | Chromatograph apparatus and analysis method |
Publications (3)
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JP2008076243A JP2008076243A (en) | 2008-04-03 |
JP2008076243A5 true JP2008076243A5 (en) | 2008-07-17 |
JP4861107B2 JP4861107B2 (en) | 2012-01-25 |
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JP2006256113A Expired - Fee Related JP4861107B2 (en) | 2006-09-21 | 2006-09-21 | Chromatograph apparatus and analysis method |
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Families Citing this family (10)
Publication number | Priority date | Publication date | Assignee | Title |
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JP4980740B2 (en) * | 2007-01-31 | 2012-07-18 | 株式会社 資生堂 | Two-dimensional liquid chromatography analysis method and sorting flow path switching unit |
JP5445149B2 (en) * | 2010-01-08 | 2014-03-19 | 株式会社島津製作所 | ANALYZER CONTROL SYSTEM AND PROGRAM FOR THE SYSTEM |
JP5545494B2 (en) * | 2011-04-05 | 2014-07-09 | 横河電機株式会社 | Chromatograph |
US8669519B2 (en) * | 2011-12-05 | 2014-03-11 | Quest Diagnostics Investments, Inc. | Methods for detecting reverse triiodothyronine by mass spectrometry |
TWI613445B (en) * | 2016-04-01 | 2018-02-01 | 行政院農業委員會農業藥物毒物試驗所 | Method and system for inspecting pesticide residue in argicultural products using mass spectrometry imaging analysis |
US11828737B2 (en) | 2017-04-05 | 2023-11-28 | Shimadzu Corporation | Preparative liquid chromatograph |
CN111398611A (en) * | 2019-01-03 | 2020-07-10 | 深圳迈瑞生物医疗电子股份有限公司 | Sample detection time estimation method and device, sample analyzer and storage medium |
CN111289640B (en) * | 2020-02-27 | 2022-12-13 | 南京凯通粮食生化研究设计有限公司 | Liquid chromatography detection method for improving detection efficiency by advancing sample introduction |
JP2022123952A (en) * | 2021-02-15 | 2022-08-25 | 株式会社島津製作所 | liquid chromatograph |
CN115453030A (en) * | 2022-09-28 | 2022-12-09 | 博莱克科技(武汉)有限公司 | Method for improving gas chromatography detection efficiency |
Family Cites Families (3)
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JP3180391B2 (en) * | 1991-12-09 | 2001-06-25 | 株式会社島津製作所 | Liquid chromatograph |
JP3700368B2 (en) * | 1998-01-12 | 2005-09-28 | 株式会社島津製作所 | Chromatographic data processor |
JP3938086B2 (en) * | 2003-04-04 | 2007-06-27 | 株式会社島津製作所 | Chromatographic data processor |
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