JP2007144922A - Manufacturing method of ceramic honeycomb structure - Google Patents

Manufacturing method of ceramic honeycomb structure Download PDF

Info

Publication number
JP2007144922A
JP2007144922A JP2005345412A JP2005345412A JP2007144922A JP 2007144922 A JP2007144922 A JP 2007144922A JP 2005345412 A JP2005345412 A JP 2005345412A JP 2005345412 A JP2005345412 A JP 2005345412A JP 2007144922 A JP2007144922 A JP 2007144922A
Authority
JP
Japan
Prior art keywords
cup
honeycomb structure
peripheral side
face
ceramic honeycomb
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
JP2005345412A
Other languages
Japanese (ja)
Inventor
Shunji Okazaki
俊二 岡崎
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Proterial Ltd
Original Assignee
Hitachi Metals Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Hitachi Metals Ltd filed Critical Hitachi Metals Ltd
Priority to JP2005345412A priority Critical patent/JP2007144922A/en
Publication of JP2007144922A publication Critical patent/JP2007144922A/en
Pending legal-status Critical Current

Links

Images

Landscapes

  • Processing Of Stones Or Stones Resemblance Materials (AREA)
  • Filtering Materials (AREA)
  • Polishing Bodies And Polishing Tools (AREA)

Abstract

<P>PROBLEM TO BE SOLVED: To provide a manufacturing method of a ceramic honeycomb structure capable of preventing a partition from chipping in processing the end face of the ceramic honeycomb structure with a cup-type abrasive wheel. <P>SOLUTION: The manufacturing method of a ceramic honeycomb structure comprises the step of processing the end face of the ceramic honeycomb structure having a large number of cells formed by porous partitions by using the cup-type abrasive wheel. The cup-type abrasive wheel has a step on the outer peripheral side end face to the inner peripheral side end face at the axial direction attaching part side of the cup-type abrasive wheel, that the cup-type abrasive wheel has an abrasive particle layer at a grinding part thereof, and that the abrasive particle layer is composed of abrasive particle layers having different particle size each other with regard to the outer peripheral side and the inner peripheral side, that is, an abrasive particle layer having a relatively larger particle size is formed at the outer peripheral side and an abrasive particle layer having a relatively smaller particle size is formed at the outer peripheral side. <P>COPYRIGHT: (C)2007,JPO&INPIT

Description

本発明は、セラミックハニカム構造体の端面を加工する製造方法に関する。   The present invention relates to a manufacturing method for processing an end face of a ceramic honeycomb structure.

ディーゼルエンジンなどの排気ガス中には炭素を主体とするPM(微粒子状物質)が多量に含まれており、これが大気中に放出されると、人体や環境に悪影響を与える。このため、ディーゼルエンジンなどの排気系部品には、PMを捕集するためのフィルタが搭載されている。図4は、自動車の排気ガス中のPMを捕集、浄化するフィルタに用いられるハニカム構造体の一例を示したものであり、(a)は正面模式図、(b)は側断面模式図である。図4(a)(b)において、ハニカム構造体20は、多孔質セラミックからなり、外周壁21と、この外周壁21の内側に各々直交する隔壁22で仕切られた複数のセル23、24を有しており、セル23、24は、排気ガスの流入側端面27と流出側端面28において交互に封止部25、26で封止されている。また、外周壁21は、金属メッシュあるいはセラミックス製のマットなどで形成された把持部材(図示せず)で使用中に動かないように把持され、金属製の収納容器(図示せず)に配置されている。   Exhaust gas from diesel engines and the like contains a large amount of PM (particulate matter) mainly composed of carbon, and if this is released into the atmosphere, it will adversely affect the human body and the environment. For this reason, exhaust system parts, such as a diesel engine, are equipped with a filter for collecting PM. FIG. 4 shows an example of a honeycomb structure used for a filter for collecting and purifying PM in automobile exhaust gas, (a) is a schematic front view, and (b) is a schematic side sectional view. is there. 4 (a) and 4 (b), the honeycomb structure 20 is made of porous ceramic and includes an outer peripheral wall 21 and a plurality of cells 23 and 24 partitioned by partition walls 22 orthogonal to the inner side of the outer peripheral wall 21, respectively. The cells 23 and 24 are alternately sealed by the sealing portions 25 and 26 at the exhaust gas inflow side end surface 27 and the outflow side end surface 28. The outer peripheral wall 21 is gripped so as not to move during use by a gripping member (not shown) formed of a metal mesh or a ceramic mat, and is disposed in a metal storage container (not shown). ing.

このようなフィルタに用いられるセラミックハニカム構造体は、セラミック原料を混合、混練して粘土質素材とし、この粘土質素材を押出し成形後、例えば、特許文献1に記載の極細鋼線で切断し、乾燥、焼成して得られる。焼成して得られたセラミックハニカム構造体の端面にフィルムもしくはマスクを貼り付け、封止部を形成するセルのフィルムもしくはマスクを開孔し、開孔されたセルに目封止用スラリーを充填して封止部を形成し、セラミックハニカムフィルタが得られる。このセラミックハニカム構造体は、PMの捕集性能と低い圧力損失の実現のために、最近では高気孔率のものが使用されてきている。   The ceramic honeycomb structure used for such a filter is made by mixing and kneading ceramic raw materials into a clay material, and after extruding the clay material, for example, cutting with an ultrafine steel wire described in Patent Document 1, Obtained by drying and firing. A film or mask is attached to the end face of the ceramic honeycomb structure obtained by firing, the film or mask of the cell forming the sealing portion is opened, and the plugged slurry is filled in the opened cell. Thus, a sealing portion is formed, and a ceramic honeycomb filter is obtained. This ceramic honeycomb structure has recently been used with a high porosity in order to achieve PM collection performance and low pressure loss.

ところで、特許文献1に記載の極細鋼線で切断して得られたセラミックハニカム構造体は、切断時に端面での隔壁の変形や欠けが生じていることがあるので、端面の研削を行い、最終的な長さにすることが必要である。端面でセルが変形していたり、隔壁に欠けが生じていると、封止部を形成する工程において、セラミックハニカム構造体の端面と、その端面に貼り付けたフィルムもしくはマスクとの間に隙間が生じる。そして、目封止用スラリーを充填する際に、その隙間から、本来、封止部を形成すべきでない隣接するセルに目封止用スラリーが漏洩する。これにより、本来、封止部を形成すべきでないセルが塞がれてしまうので、フィルタとして使用した場合に、圧力損失が大きくなるという問題を生じるからである。   By the way, since the ceramic honeycomb structure obtained by cutting with the ultra fine steel wire described in Patent Document 1 may have deformation or chipping of the partition wall at the end face at the time of cutting, the end face is ground, It is necessary to make it as long as possible. If the cell is deformed at the end face or the partition wall is chipped, a gap is formed between the end face of the ceramic honeycomb structure and the film or mask attached to the end face in the step of forming the sealing portion. Arise. When the plugging slurry is filled, the plugging slurry leaks from the gap to the adjacent cells where the sealing portion should not be originally formed. As a result, the cells that should not originally form the sealing portion are blocked, and therefore, when used as a filter, the problem of increased pressure loss arises.

そこで、これを避けるため、本発明者は、特願2005−101978号において、カップ形砥石を用いて該カップ形砥石の端面がセラミックハニカム構造体の端面に略平行となるように研削加工を行うセラミックハニカム構造体の製造方法を提案している。これにより、加工に要する時間を短縮することができるとともに、隔壁に欠けを生じ難くすることができるとしている。そして、図5(a)(b)に示すように、カップ形砥石の外周面とセラミックハニカム構造体の端面とのなす角度θが、90°以上の場合と90°未満の場合があって、90°未満とすることで、隔壁に欠けをより生じ難く加工することができるとしている。   Therefore, in order to avoid this, in the Japanese Patent Application No. 2005-101978, the present inventor uses a cup-shaped grindstone to perform grinding so that the end face of the cup-shaped grindstone is substantially parallel to the end face of the ceramic honeycomb structure. A method for manufacturing a ceramic honeycomb structure is proposed. Thereby, the time required for processing can be shortened, and the partition wall can be made less likely to be chipped. And as shown to Fig.5 (a) (b), the angle (theta) which the outer peripheral surface of a cup-shaped grindstone and the end surface of a ceramic honeycomb structure make may be 90 degrees or more, and may be less than 90 degrees, By setting it to less than 90 °, it is said that the partition wall can be processed with less difficulty in chipping.

また、特許文献2には、平面部を研削する際に用いられるカップ形砥石に関し、砥石主軸に直交する砥石面を備えたカップ形砥石において、リング状の砥石面を同心状に複数形成し、砥石面の高さを周方向外側から内側にかけて漸次高くしたことを特徴とするカップ形砥石が開示されている。   In addition, Patent Document 2 relates to a cup-shaped grindstone used when grinding a flat surface portion. A cup-shaped grindstone is disclosed in which the height of the grindstone surface is gradually increased from the outer side to the inner side in the circumferential direction.

特公平4−60402号公報Japanese Patent Publication No. 4-60402 特開平5−92371号公報Japanese Patent Laid-Open No. 5-92371

しかしながら、本発明者が特願2005−101978号において提案した製造方法では、次のような不具合を十分に防ぐことはできなかった。
つまり、図5(a)に示すような、カップ形砥石の外周面とセラミックハニカム構造体の端面とのなす角度θが、90°以上や90°未満のカップ形砥石を用いてセラミックハニカム構造体の端面を加工した場合、加工が終了する直前に、未研削部の隔壁や外周壁が欠けて飛散してしまい、加工終了位置付近の外周に生じる欠けを十分に防ぐことはできなかったり、加工された後の切粉がセル内に詰まり易くなり、セルに詰まった切粉に加工時の力が隔壁に過剰に作用し、隔壁に生じる微小な欠け(チッピング)を十分に防ぐことができなかった。また、カップ砥石の端面側と外周側に2種類の砥粒を用いて加工することが記載されているが、2種類の砥粒のうち、相対的に粒径の大きい砥粒層が外周側に、相対的に粒径の小さい砥粒層がカップ砥石の端面側に形成されていることで、粒径の大きい砥粒層がハニカム構造体の端面を加工した後に、粒径の小さい砥粒層で加工する加工しろは必然的に小さくなり、粒径の大きい砥粒層がハニカム構造体の端面を加工した際に生じた欠けを十分に取り除くことはできなかった。
However, the manufacturing method proposed by the present inventor in Japanese Patent Application No. 2005-101978 cannot sufficiently prevent the following problems.
That is, as shown in FIG. 5A, a ceramic honeycomb structure using a cup-shaped grindstone having an angle θ between the outer peripheral surface of the cup-shaped grindstone and the end face of the ceramic honeycomb structure of 90 ° or more and less than 90 °. When machining the end face, the partition wall and outer peripheral wall of the unground part are chipped and scattered immediately before the end of processing, and it is not possible to sufficiently prevent the chipping generated on the outer periphery near the processing end position. The chip after clogging is easily clogged in the cell, and the processing force is excessively applied to the partition wall of the cell clog, and the minute chipping (chipping) generated in the partition wall cannot be prevented sufficiently. It was. In addition, it is described that processing is performed using two types of abrasive grains on the end face side and the outer peripheral side of the cup grindstone, but among the two types of abrasive grains, the abrasive grain layer having a relatively large particle diameter is the outer peripheral side. In addition, since the abrasive grain layer having a relatively small particle diameter is formed on the end face side of the cup grindstone, the abrasive grain having a small grain diameter is processed after the abrasive grain layer having a large particle diameter has processed the end face of the honeycomb structure. The machining margin to be processed by the layer is inevitably small, and the chip generated when the abrasive grain layer having a large particle diameter processes the end face of the honeycomb structure cannot be sufficiently removed.

そこで、前記したような問題を改善するために、特許文献2に開示されるようなカップ形砥石を用いて、セラミックハニカム構造体の端面を研削加工してみたが、セラミックハニカム構造体は多孔質の隔壁で形成されるので、微小な欠けの発生を十分には防ぐことができなかった。そして、欠けが生じた場合は、砥粒の細かい仕上げ用の砥石を用いて再度加工をする必要があり、加工に多くの時間を要していた。   Thus, in order to improve the above-described problems, the end face of the ceramic honeycomb structure was ground using a cup-shaped grindstone as disclosed in Patent Document 2, but the ceramic honeycomb structure is porous. Therefore, the generation of minute chips could not be sufficiently prevented. And when a chip | tip generate | occur | produced, it was necessary to process again using the grindstone for finishing with a fine abrasive grain, and processing required much time.

本発明の課題は、セラミックハニカム構造体の端面をカップ形砥石を用いて加工する際に、隔壁に生じる欠けを防止することができるセラミックハニカム構造体の製造方法を得ることにある。   An object of the present invention is to obtain a method for manufacturing a ceramic honeycomb structure capable of preventing chipping generated in partition walls when the end face of the ceramic honeycomb structure is processed using a cup-shaped grindstone.

上記課題を解決する為、具体的に本発明は、多孔質の隔壁により形成されるセルを多数有するセラミックハニカム構造体の端面を、カップ形砥石を用いて加工を行うセラミックハニカム構造体の製造方法において、前記カップ形砥石はその外周側の端面が、内周側の端面に対して、前記カップ形砥石の軸方向取付部側に段差を有し、前記カップ形砥石の研削部位に砥粒層を有し、前記砥粒層は、前記カップ形砥石の外周側と内周側で、それぞれ粒径の異なる砥粒の砥粒層であり、前記砥粒のうち相対的に粒径の大きい砥粒層を外周側に形成し、相対的に粒径の小さい砥粒層を内周側に形成されていることを特徴とする。   In order to solve the above-described problems, the present invention specifically relates to a method for manufacturing a ceramic honeycomb structure in which an end face of a ceramic honeycomb structure having a large number of cells formed by porous partition walls is processed using a cup-shaped grindstone. The cup-shaped grindstone has a step on the outer peripheral side of the cup-shaped grindstone with respect to the inner circumferential side end surface on the axial mounting portion side of the cup-shaped grindstone. The abrasive layer is an abrasive layer of abrasive grains having different particle sizes on the outer peripheral side and the inner peripheral side of the cup-shaped grindstone, and the abrasive grains having a relatively large particle size among the abrasive grains. The grain layer is formed on the outer peripheral side, and the abrasive grain layer having a relatively small particle diameter is formed on the inner peripheral side.

本発明において、前記段差が0.1〜5.0mmであることが好ましい。   In the present invention, the step is preferably 0.1 to 5.0 mm.

さらに、本発明において、前記カップ形砥石の外周側の端面と、内周側の端面との間に凹部を有していることが好ましい。   Furthermore, in this invention, it is preferable to have a recessed part between the outer peripheral side end surface of the said cup-shaped grindstone, and an inner peripheral side end surface.

さらに、本発明において、外周側の端面と、内周側の端面にR部を有することが好ましい。   Furthermore, in this invention, it is preferable to have R part in the end surface of an outer peripheral side, and the end surface of an inner peripheral side.

次に、本発明の作用効果について図1〜3に基き説明する。
本発明は、カップ形砥石の外周側の端面151が、内周側の端面152に対して、前記カップ形砥石の軸方向取付部14側に段差Hを有し、カップ形砥石の研削部位15に砥粒層17を有し、砥粒層17を、図1(c)に示すように、外周側の端面151と内周側の端面152に、それぞれ粒径の異なる砥粒の砥粒層17A、砥粒層17Bとし、相対的に粒径の大きい砥粒層17Aを外周側の端面151側に形成し、相対的に粒径の小さい砥粒層17Bを内周側の端面152側に形成さることで、次のような作用効果を有する。図1で、カップ型砥石10は、図1(b)で示すように切り込み量tを設定した後に、回転をしながらハニカム構造体の端面27に対して矢印の方向に相対的に移動して研削を行う。そして、カップ型砥石10の外周側の端面151の砥粒層17Aが、まずハニカム構造体の端面27を研削加工し、次いで、端面151の砥粒層17Aが加工した後に段差Hだけ残ったハニカム構造体の端面を、カップ型砥石の内周側の端面152の砥粒層17Bが研削加工を行う。この場合、砥粒層17Aで研削された部位は、ハニカム構造体としては不要な部位であるので、粉砕粉として排出できればよいので砥粒層17Aは2種類の砥粒のうち相対的に粒径の大きい砥粒を用いることができ、砥粒層17Bを2種類の砥粒のうち相対的に粒径の小さい砥粒層17Bで研削することで、仕上加工することになる。これにより、カップ型砥石10の外周側の端面151の砥粒層17Aが研削した際に生じた欠けを、次にカップ型砥石の内周側の端面152の砥粒層17Bが仕上げ加工をすることで、ハニカム構造体の端面部で隔壁の欠けが生じ難くなり、良好に加工することができる。さらに、セラミックハニカム構造体の端面27からの切り込み量tが、外周側の端面151での切り込み量t1と内周側の端面152での切り込み量t2の和となるので、一つの砥粒層での切り込み量を小さくでき、セラミックハニカム構造体の端面に生じる加工負荷を小さくでき、隔壁の欠けを防止することができる。さらに、切り込み量tが大きい場合に、隔壁との接触面が大きくなることで、砥粒層17Aで加工される際に伴う負荷が大きくなり隔壁に欠けが生じた場合であっても、砥粒層17Bが仕上加工するので、砥粒層17Aで加工された際に生じた欠けを砥粒層17Bが除去するので欠けを生じ難くすることができる。これは、特に、ハニカム構造体の気孔率が55%以上と高い気孔率で、隔壁が脆い場合であっても、欠けを生じ難く良好に加工をすることができるのである。
ここで、カップ型砥石の内周側の内周側の端面152が、段差Hだけ残ったハニカム構造体の端面の研削加工を行う際に、セラミックハニカム構造体の端面に生じる加工負荷を小さくでき、隔壁の欠けを十分防止するためには、段差Hは0.1〜5.0mmであることが好ましい。段差Hが0.1mm未満である場合、カップ型砥石の外周側の端面151が、セラミックハニカム構造体の端面27を研削加工した際に生じた欠けを、内周側の端面152が研削加工で除去することが難くなるので、欠けを十分に防止することができなくなるので、0.1mm以上が好ましい。一方、段差Hが5.0mmを超えると、カップ型砥石の外周側の端面151が、ハニカム構造体の端面を研削加工した後に残った段差Hを、カップ型砥石の内周側の端面152が研削加工を行う際、隔壁に作用する負荷が大きくなり、隔壁に欠けが生じ易くなるので、5.0mm以下が好ましい。
なお、本発明において、カップ形砥石の外周面18とセラミックハニカム構造体の端面27とのなす角度θが略直角であると、加工した切粉がセル内に詰まり難くなり、隔壁に欠けが生じ難くなるので好ましい。ここで、カップ形砥石の外周面18とセラミックハニカム構造体の端面27とのなす角度θが略直角とは、θが75°〜105°の範囲のことを言う。
Next, the effect of this invention is demonstrated based on FIGS.
In the present invention, the end surface 151 on the outer peripheral side of the cup-shaped grindstone has a step H on the axial mounting portion 14 side of the cup-shaped grindstone with respect to the end surface 152 on the inner peripheral side. As shown in FIG. 1 (c), the abrasive layer 17 is provided on the outer peripheral end surface 151 and the inner peripheral end surface 152. 17A and the abrasive layer 17B, the abrasive layer 17A having a relatively large particle size is formed on the outer peripheral side end surface 151 side, and the abrasive particle layer 17B having a relatively small particle size is formed on the inner peripheral side end surface 152 side. By forming, it has the following effects. In FIG. 1, the cup-type grindstone 10 moves relative to the end face 27 of the honeycomb structure in the direction of the arrow while rotating after setting the cutting amount t as shown in FIG. 1 (b). Grind. Then, the abrasive grain layer 17A on the end face 151 on the outer peripheral side of the cup-type grindstone 10 first grinds the end face 27 of the honeycomb structure, and then the honeycomb in which only the step H remains after the abrasive grain layer 17A on the end face 151 is machined. The end surface of the structure is ground by the abrasive layer 17B of the end surface 152 on the inner peripheral side of the cup-type grindstone. In this case, since the part ground by the abrasive grain layer 17A is an unnecessary part as the honeycomb structure, the abrasive grain layer 17A has a relatively small particle diameter among the two kinds of abrasive grains. A large abrasive grain can be used, and the abrasive grain layer 17B is ground by the abrasive grain layer 17B having a relatively small grain diameter out of the two kinds of abrasive grains. As a result, the chip generated when the abrasive layer 17A on the outer peripheral side end surface 151 of the cup-type grindstone 10 is ground, and then the abrasive layer 17B on the end surface 152 on the inner peripheral side of the cup-type grindstone is finished. As a result, the partition wall is less likely to be chipped at the end face portion of the honeycomb structure and can be processed satisfactorily. Further, since the depth of cut t from the end surface 27 of the ceramic honeycomb structure, the sum of cut amount t 2 in the cutting depth t 1 and the inner circumferential end face 152 of the end surface 151 of the outer peripheral side, one of the abrasive grains The amount of cut in the layer can be reduced, the processing load generated on the end face of the ceramic honeycomb structure can be reduced, and the partition wall can be prevented from being chipped. Further, when the cutting amount t is large, the contact surface with the partition wall becomes large, so that the load accompanying processing with the abrasive grain layer 17A increases, and even if the partition wall is chipped, the abrasive grains Since the layer 17B is finished, since the abrasive layer 17B removes the chip generated when the abrasive layer 17A is processed, the chip can be made difficult to occur. This is particularly because the honeycomb structure has a high porosity of 55% or more, and even when the partition walls are brittle, chipping is unlikely to occur and processing can be performed satisfactorily.
Here, when the end face 152 of the inner peripheral side of the cup-type grindstone is ground on the end face of the honeycomb structure in which only the step H remains, the processing load generated on the end face of the ceramic honeycomb structure can be reduced. In order to sufficiently prevent the partition wall from being chipped, the step H is preferably 0.1 to 5.0 mm. When the level difference H is less than 0.1 mm, the end surface 151 on the outer peripheral side of the cup-type grindstone is chipped when the end surface 27 of the ceramic honeycomb structure is ground, and the end surface 152 on the inner peripheral side is ground. Since it becomes difficult to remove, chipping cannot be prevented sufficiently, so 0.1 mm or more is preferable. On the other hand, when the level difference H exceeds 5.0 mm, the end surface 151 on the outer peripheral side of the cup-type grindstone is replaced with the step H remaining after grinding the end surface of the honeycomb structure by the end surface 152 on the inner peripheral side of the cup-type grindstone. When grinding is performed, the load acting on the partition wall is increased, and chipping of the partition wall is likely to occur, so 5.0 mm or less is preferable.
In the present invention, if the angle θ formed between the outer peripheral surface 18 of the cup-shaped grindstone and the end surface 27 of the ceramic honeycomb structure is substantially a right angle, the processed chips are difficult to clog in the cell, and the partition wall is chipped. It is preferable because it becomes difficult. Here, the angle θ formed by the outer peripheral surface 18 of the cup-shaped grindstone and the end face 27 of the ceramic honeycomb structure is substantially a right angle means that θ is in the range of 75 ° to 105 °.

さらに、図2に示すように、カップ形砥石の外周側の端面151と、内周側の端面152との間に凹部16を有していることで、カップ型砥石の凹部16よりも外周側の端面151が、ハニカム構造体の端面を研削加工し、次いで、カップ型砥石の凹部16よりも内周側の端面152が、段差Hだけ残ったハニカム構造体の端面の研削加工を行う。この場合、端面151で研削されて生じた切粉は、凹部16にも集まり、集まった切粉はカップ型砥石の回転によってセラミックハニカム構造体の端面から排出されるので、切粉がセルに詰まることを防ぐことができ、隔壁に生じる欠けを防止することができる。
ここで、加工によって生じた切粉が凹部16に集まり、カップ型砥石の回転によってセラミックハニカム構造体の端面から十分に排出されるためには、凹部16の幅L1は端面15の幅Lに対して、L1/Lが0.1〜0.7であることが好ましい。また、凹部16の深さh1は、凹部16の幅L1に対して、h1/L1が0.5〜2.0であることが好ましい。凹部16の幅L1と端面15の幅Lとの比L1/Lが0.1未満の場合、加工によって生じた切粉が凹部16に集まり難くなるので、セル内へ切粉が詰まり易くなり、隔壁に欠けが生じ易くなるので0.1以上が好ましい。一方、L1/Lが0.7を超えると、カップ形砥石10の端面15が狭くなり、十分な研削加工を行うことができなくなるので0.7以下が好ましい。また、凹部16の深さh1と凹部16の幅L1の比h1/L1が0.5未満の場合、加工によって生じた切粉が凹部16に集まり難くなるので、セル内へ切粉が詰まり易くなり、隔壁に欠けが生じ易くなるので0.5以上が好ましい。一方、h1/L1が2.0を超えると、カップ形砥石10自体の強度が低下して研削加工ができなくなるので2.0以下が好ましい。
Furthermore, as shown in FIG. 2, it has the recessed part 16 between the end surface 151 of the outer peripheral side of a cup shape grindstone, and the end surface 152 of an inner peripheral side, Therefore The outer peripheral side rather than the recessed part 16 of a cup type grindstone The end surface 151 of the honeycomb structure grinds the end surface of the honeycomb structure, and then the end surface of the honeycomb structure in which the end surface 152 on the inner peripheral side of the concave portion 16 of the cup-type grindstone has a level difference H is ground. In this case, the chips produced by grinding at the end face 151 also gather in the recesses 16 and the collected chips are discharged from the end face of the ceramic honeycomb structure by the rotation of the cup-type grindstone, so that the chips are clogged in the cells. This can prevent the chipping caused in the partition wall.
Here, in order for the chips generated by the processing to collect in the recess 16 and be sufficiently discharged from the end face of the ceramic honeycomb structure by the rotation of the cup-type grindstone, the width L 1 of the recess 16 is set to the width L of the end face 15. in contrast, it is preferable L 1 / L is 0.1 to 0.7. Further, the depth h 1 of the recess 16 is preferably such that h 1 / L 1 is 0.5 to 2.0 with respect to the width L 1 of the recess 16. When the ratio L 1 / L between the width L 1 of the recess 16 and the width L of the end face 15 is less than 0.1, the chips generated by the processing are less likely to collect in the recess 16, so that the chips are easily clogged into the cell. Therefore, it is preferable that the partition wall be 0.1 or more. On the other hand, when L 1 / L exceeds 0.7, the end face 15 of the cup-shaped grindstone 10 becomes narrow and sufficient grinding cannot be performed, so 0.7 or less is preferable. Further, when the ratio h 1 / L 1 of width L 1 of the depth h 1 and the recess 16 of the recess 16 is less than 0.5, since chips generated by machining is less likely gather in the recess 16, switching into the cell 0.5 or more is preferable because the powder is likely to be clogged and the partition wall is likely to be chipped. On the other hand, if h 1 / L 1 exceeds 2.0, the strength of the cup-shaped grindstone 10 itself is lowered and grinding becomes impossible.

また、図3(a)(b)に示すように、外周側の端面151と、内周側の端面152にR部R1〜R4を有することで、カップ形砥石がハニカム構造体の隔壁を加工する際に、隔壁に作用する負荷が軽減され、隔壁の欠けがより生じ難くなるので好ましい。このR部は、R1〜R4の全てを有する必要は無く、少なくとも一箇所存在すればよいが、カップ形砥石の送り方向と一致する少なくともR1とR3に有していることが好ましい。ここで、R部の半径は、0.5〜3mmであることが好ましい。 Further, as shown in FIGS. 3A and 3B, the cup-shaped grindstone has a partition wall of the honeycomb structure by having R portions R 1 to R 4 on the outer end face 151 and the inner end face 152. This is preferable because the load acting on the partition wall is reduced and the partition wall is less likely to be chipped. The R portion does not need to have all of R 1 to R 4 , and may exist at least at one place, but preferably has at least R 1 and R 3 that coincide with the feeding direction of the cup-shaped grindstone. . Here, the radius of the R portion is preferably 0.5 to 3 mm.

本発明のセラミックハニカム構造体の製造方法によれば、セラミックハニカム構造体の端面をカップ形砥石を用いて加工する際に、隔壁に生じる欠けを防止することができるセラミックハニカム構造体を得ることができる。   According to the method for manufacturing a ceramic honeycomb structure of the present invention, it is possible to obtain a ceramic honeycomb structure capable of preventing chips generated in partition walls when the end face of the ceramic honeycomb structure is processed using a cup-shaped grindstone. it can.

以下、本発明の実施の形態を図1〜3をもとに詳細に説明する。
(実施の形態1)
図1において、セラミックハニカム構造体20は、次のようにして準備される。セラミック原料として、炭化珪素、窒化珪素、コージェライト、アルミナ、ムライト、ジルコニア、チタン酸アルミニウムあるいはこれらの組合せからなる群から選ばれた少なくとも一種のセラミックを用いる。このセラミック原料に、メチルセルロース及びヒドロキシプロポキシルメチルセルロース等のバインダー、界面活性剤、水、及び必要に応じてカーボン等の造孔剤を添加、混練して可塑性の坏土を作成する。この杯土を押出し成形することで、セルを多数有するセラミックハニカム構造の成形体を成形する。この成形体を所定の長さに極細鋼線で切断し、乾燥の後、焼成して多孔質の隔壁により形成されるセルを多数有するセラミックハニカム構造体20が得られる。
次に、カップ形砥石10は、炭素鋼、高速度鋼、ダイス鋼等の鋼材製の基台11と軸12で構成され、基台11の中央部には逃げ部13を有しており、その研削部位15には砥粒層17が形成されている。この砥粒層17に形成される砥粒の材質には、ダイヤモンド、立方晶窒化ほう素等を用いることができ、その粒度は、#50〜#270程度のものを用いることができる。そして、図1(c)に示すように、砥粒層17には2種類の砥粒を用い、2種類の砥粒のうち相対的に粒径の大きい砥粒層17Aを外周側の端面151の研削部位に形成し、2種類の砥粒のうち相対的に粒径の小さい砥粒層17Bを内周側の端面152の研削部位に形成させる。したがって、例えば、砥粒層17Aに粒度が#50〜#120程度の粗用のものを、砥粒層17Bに粒度が#100〜#270程度の仕上用のものを用いることができる。また、砥粒層17の厚さは0.5〜5mm程度とすることができる。そして、砥粒層17が形成されたその研削部位15において、外周側の端面151が、内周側の端面152に対して、カップ形砥石の軸方向取付部14側に段差Hを有している。尚、カップ形砥石10の外径は、セラミックハニカム構造体20の外径と同じか、それより大きい外径を有していると、セラミックハニカム構造体の端面全面を1回の加工で完了するので好ましい。
そして、このカップ形砥石によりセラミックハニカム構造体の端面は次のように加工される。
セラミックハニカム構造体20の外周を加工装置の取付具31で固定する。セラミックハニカム構造体20の一方の端面27からの切り込み量tが0.1〜5mmとなるように、カップ形砥石10の位置を決める。次いで、カップ形砥石10を回転させて送り(図中矢印)をかけ、セラミックハニカム構造体20の端面27を加工する。まず、カップ形砥石10の研削部位15に形成された砥粒層17Aが、ハニカム構造体20の隔壁を加工する。この場合、砥粒層17Aで研削される部位は、ハニカム構造体としては不要な部位であり、砥粒層17Aの粒度は、砥粒層17Bと比べて相対的に粗いので、容易に粉砕粉として排出される。次いで、砥粒層17Aにより粗加工されたハニカム構造体の隔壁を、砥粒層17Bが仕上加工していく。この場合、砥粒層17Aで研削された部位を2種類の砥粒のうち相対的に粒径の小さい砥粒層17Bで加工するので、ハニカム構造体20の端面27で隔壁の欠けが生じ難くなり、良好に加工することができる。このことは、特に、ハニカム構造体の気孔率が55%以上と高い気孔率で隔壁が脆く欠けが生じ易い場合であっても、欠けを生じず良好に加工をすることができるのである。そして、一方の端面27の加工が完了すると、取付具31を外して、セラミックハニカム構造体20を取付け直し、他方の端面28を同様にして加工を行う。このようにして加工されたセラミックハニカム構造体は、次に、端面27、28にフィルムを貼り付け、封止する所定のセルのフィルムをレーザー光等の熱で開孔し、開孔されたセルに目封止用スラリーを充填し、焼成してセラミックハニカムフィルタとする。
Hereinafter, embodiments of the present invention will be described in detail with reference to FIGS.
(Embodiment 1)
In FIG. 1, the ceramic honeycomb structure 20 is prepared as follows. As the ceramic raw material, at least one ceramic selected from the group consisting of silicon carbide, silicon nitride, cordierite, alumina, mullite, zirconia, aluminum titanate, or a combination thereof is used. To this ceramic raw material, a binder such as methyl cellulose and hydroxypropoxyl methyl cellulose, a surfactant, water and, if necessary, a pore-forming agent such as carbon are added and kneaded to prepare a plastic clay. A ceramic honeycomb structure formed body having a large number of cells is formed by extruding the clay. The formed body is cut to a predetermined length with an ultrafine steel wire, dried and fired to obtain a ceramic honeycomb structure 20 having a large number of cells formed by porous partition walls.
Next, the cup-shaped grindstone 10 is composed of a base 11 and a shaft 12 made of steel such as carbon steel, high-speed steel, die steel, etc., and has a relief portion 13 at the center of the base 11. An abrasive grain layer 17 is formed on the ground portion 15. As the material of the abrasive grains formed on the abrasive grain layer 17, diamond, cubic boron nitride or the like can be used, and those having a grain size of about # 50 to # 270 can be used. Then, as shown in FIG. 1C, two types of abrasive grains are used for the abrasive layer 17, and the abrasive layer 17A having a relatively large particle size is used as the end face 151 on the outer peripheral side among the two types of abrasive grains. The abrasive layer 17B having a relatively small particle size out of the two types of abrasive grains is formed on the grinding part of the end surface 152 on the inner peripheral side. Therefore, for example, a rough grain having a grain size of about # 50 to # 120 can be used for the abrasive grain layer 17A, and a finishing grain having a grain size of about # 100 to # 270 can be used for the abrasive grain layer 17B. Moreover, the thickness of the abrasive grain layer 17 can be about 0.5-5 mm. And in the grinding part 15 in which the abrasive grain layer 17 is formed, the end face 151 on the outer peripheral side has a step H on the axial mounting portion 14 side of the cup-shaped grindstone with respect to the end face 152 on the inner peripheral side. Yes. If the outer diameter of the cup-shaped grindstone 10 is the same as or larger than the outer diameter of the ceramic honeycomb structure 20, the entire end face of the ceramic honeycomb structure is completed by a single process. Therefore, it is preferable.
Then, the end face of the ceramic honeycomb structure is processed as follows by this cup-shaped grindstone.
The outer periphery of the ceramic honeycomb structure 20 is fixed with the fixture 31 of the processing apparatus. The position of the cup-shaped grindstone 10 is determined so that the cut amount t from one end face 27 of the ceramic honeycomb structure 20 is 0.1 to 5 mm. Next, the cup-shaped grindstone 10 is rotated and fed (arrow in the figure), and the end face 27 of the ceramic honeycomb structure 20 is processed. First, the abrasive grain layer 17 </ b> A formed in the grinding portion 15 of the cup-shaped grindstone 10 processes the partition walls of the honeycomb structure 20. In this case, the portion ground by the abrasive grain layer 17A is an unnecessary part for the honeycomb structure, and the grain size of the abrasive grain layer 17A is relatively coarse compared to the abrasive grain layer 17B. Discharged as. Next, the abrasive grain layer 17B finishes the partition walls of the honeycomb structure roughly processed by the abrasive grain layer 17A. In this case, since the portion ground by the abrasive grain layer 17A is processed by the abrasive grain layer 17B having a relatively small grain size out of the two types of abrasive grains, the partition wall is less likely to be chipped at the end face 27 of the honeycomb structure 20. It can be processed well. This means that even when the honeycomb structure has a high porosity of 55% or more and the partition walls are brittle and chipping is likely to occur, the honeycomb structure can be satisfactorily processed without chipping. When the processing of one end surface 27 is completed, the fixture 31 is removed, the ceramic honeycomb structure 20 is reattached, and the other end surface 28 is processed in the same manner. The ceramic honeycomb structure thus processed is then bonded to the end faces 27 and 28, and a film of a predetermined cell to be sealed is opened with heat such as laser light, and the opened cell is formed. Are filled with a slurry for plugging and fired to obtain a ceramic honeycomb filter.

(実施の形態2)
実施の形態1で示したカップ形砥石10を、図2に示すように、カップ形砥石の外周側の端面151と、内周側の端面152との間に凹部16を有するものを用いる。この凹部16は、その幅L1が端面15の幅Lに対して、L1/L=0.1〜0.7の範囲とし、その深さh1を凹部16の幅L1に対して、h1/L1=0.5〜2.0の範囲で形成する。本実施の形態2のカップ形砥石を用いることで、カップ形砥石10の端面151で研削されて生じた切粉は、凹部16にも集まり、集まった切粉はカップ型砥石の回転によってセラミックハニカム構造体の端面から排出されるので、切粉がセルに詰まることを防ぐことができ、隔壁に生じる欠けを防止することができる。
(Embodiment 2)
As the cup-type grindstone 10 shown in Embodiment 1, as shown in FIG. 2, a cup-type grindstone having a concave portion 16 between an outer peripheral end surface 151 and an inner peripheral end surface 152 is used. The recess 16 has a width L 1 in a range of L 1 /L=0.1 to 0.7 with respect to the width L of the end face 15, and a depth h 1 with respect to the width L 1 of the recess 16. H 1 / L 1 = 0.5 to 2.0. By using the cup-shaped grindstone of the second embodiment, the chips generated by grinding at the end surface 151 of the cup-shaped grindstone 10 also gather in the recess 16, and the collected chips are collected by the ceramic honeycomb by the rotation of the cup-shaped grindstone. Since it is discharged | emitted from the end surface of a structure, it can prevent that a chip | tip clogs a cell, and can prevent the chip | tip which arises in a partition.

(実施の形態3)
実施の形態1で示したカップ形砥石10を、図3に示すように、外周側の端面151と、内周側の端面152にR部R1〜R4を有するものを用いる。R部の半径は、0.5〜3mmとし、R部は、R1〜R4の全てを有する必要は無く、少なくとも一箇所存在すればよいが、カップ形砥石の送り方向と一致する少なくともR1とR3に有していて良い。本実施の形態3のカップ形砥石を用いることで、カップ形砥石がハニカム構造体の隔壁を加工する際に、隔壁に作用する負荷が軽減され、隔壁の欠けがより生じ難くなるのである。
(Embodiment 3)
As shown in FIG. 3, the cup-shaped grindstone 10 shown in the first embodiment is used that has R portions R 1 to R 4 on the outer peripheral end surface 151 and the inner peripheral end surface 152. The radius of the R portion is 0.5 to 3 mm, and the R portion does not need to have all of R 1 to R 4 , and may exist at least one place, but at least R that matches the feeding direction of the cup-shaped grindstone. 1 and R 3 may be present. By using the cup-shaped grindstone of the third embodiment, when the cup-shaped grindstone processes the partition walls of the honeycomb structure, the load acting on the partition walls is reduced and the partition wall chips are less likely to occur.

先ず、次のようにしてセラミックハニカム構造体を準備した。
カオリン、タルク、シリカ、アルミナなどの粉末を調整して、質量比で、SiO:48〜52%、Al:33〜37%、MgO:12〜15%を含むようなコージェライト生成原料粉末とし、この、コージェライト生成原料粉末に、メチルセルロース、ヒドロキシプロピルメチルセルロース等のバインダー、潤滑剤、造孔材としてグラファイトを添加し、乾式で十分混合した後、規定量の水を添加、十分な混練を行って可塑化したセラミック杯土を作製した。次に、押出し成形用金型を用いて坏土を押出し成形し、切断してハニカム構造を有する成形体とした。そして、この成形体を、乾燥、焼成させ、隔壁厚0.3mm、気孔率65%、平均細孔径20μm、ピッチ1.5mmで、外径D277mm、全長320mmのコージェライト質セラミックハニカム構造体とした。
First, a ceramic honeycomb structure was prepared as follows.
Kaolin, talc, silica, by adjusting the powder such as alumina, in a mass ratio, SiO 2: 48~52%, Al 2 O 3: 33~37%, MgO: cordierite generation such as those containing from 12 to 15% As a raw material powder, to this cordierite-producing raw material powder, a binder such as methylcellulose and hydroxypropylmethylcellulose, a lubricant, and graphite as a pore-forming material are added, and after mixing thoroughly in a dry process, a specified amount of water is added, and sufficient Kneaded to produce a plasticized ceramic clay. Next, the kneaded material was extruded using an extrusion mold and cut to obtain a formed body having a honeycomb structure. Then, the formed body is dried and fired, and a cordierite ceramic honeycomb structure having a partition wall thickness of 0.3 mm, a porosity of 65%, an average pore diameter of 20 μm, a pitch of 1.5 mm, an outer diameter of D 2 277 mm, and an overall length of 320 mm. It was.

次に、このセラミックハニカム構造体20を、図1に示すように、取付具31で固定する。そして、端面の加工に用いるカップ形砥石10は、その外径Dが300mm、端面部15の幅Lが30mmで、表1に示すように、外周側の端面151が内周側の端面152に対して段差Hが形成されたもの、外周側の端面151と、内周側の端面152との間に凹部16の有無とその寸法、砥粒層17の種類、及び、端面のR部の有無を変更させたものを用いて、セラミックハニカム構造体20の一方の端面27から所定の切り込み量5mmとなるように、カップ形砥石10の位置を決める。次いで、カップ形砥石10を400回転/分で回転させて1m/分の送りをかけ、セラミックハニカム構造体20の端面27を加工する。そして、取付具31を外して、セラミックハニカム構造体20を取付直し、他方の端面28を同様にして加工を行った。
そして、加工が完了したセラミックハニカム構造体の端面に隔壁の欠けの有無を評価した。結果を表1に示す。隔壁の欠けの有無の評価は、端面当りに生じた大きさ5mm以上の欠け発生数(個/端面)を、比較例1で発生した端面当りの欠け発生数(個/端面)を1としてその比率で表した。
Next, the ceramic honeycomb structure 20 is fixed with a fixture 31, as shown in FIG. The cup-shaped grinding wheel 10 for use in machining of the end surface has an outer diameter D 1 is 300 mm, the width L is 30mm of the end surface portion 15, as shown in Table 1, the outer peripheral side of the end surface 151 of the inner end surface 152 Between the outer peripheral end face 151 and the inner peripheral end face 152, the presence and size of the recess 16, the type of the abrasive layer 17, and the R portion of the end face. The position of the cup-shaped grindstone 10 is determined so as to have a predetermined cut amount of 5 mm from one end face 27 of the ceramic honeycomb structure 20 by using the one with the presence or absence changed. Next, the end face 27 of the ceramic honeycomb structure 20 is processed by rotating the cup-shaped grindstone 10 at 400 rpm and feeding it at 1 m / min. And the fixture 31 was removed, the ceramic honeycomb structure 20 was reattached, and the other end surface 28 was processed similarly.
And the presence or absence of a chip of a partition wall was evaluated on the end face of the ceramic honeycomb structure that had been processed. The results are shown in Table 1. The evaluation of the presence or absence of cracks in the partition wall was made by assuming that the number of chips generated per end face of 5 mm or more (pieces / end face) was 1, and that the number of chips generated per end face (pieces / end face) generated in Comparative Example 1 was 1. Expressed as a ratio.

Figure 2007144922
Figure 2007144922

表1に示す結果から、本発明の実施例1〜20のカップ形砥石は、カップ形砥石の外周側の端面が、内周側の端面に対して、カップ形砥石の軸方向取付部側に段差を有し、カップ形砥石の研削部位に砥粒層が形成され、その砥粒層が、相対的に粒径の大きい砥粒層を外周側に、相対的に粒径の小さい砥粒層を内周側に形成されているので、比較例1〜3のカップ形砥石を用いて研削加工したものと比べて、欠けの発生が小さいことがわかる。なかでも、実施例2〜8、10〜20のカップ形砥石は、段差が0.1〜5.0mmであるので、欠けの発生が小さくなった。さらに、実施例10〜20のカップ形砥石は、カップ形砥石の外周側の端面と、内周側の端面との間に凹部を有し、外周側の端面と、内周側の端面にR部を有しているので、欠けの発生が非常に小さいことがわかる。   From the results shown in Table 1, in the cup-type grindstones of Examples 1 to 20 of the present invention, the end surface on the outer peripheral side of the cup-shaped grindstone is closer to the axial mounting portion side of the cup-shaped grindstone than the end surface on the inner peripheral side. An abrasive layer is formed at the grinding site of the cup-shaped grindstone, and the abrasive layer has a relatively large grain layer on the outer peripheral side and a relatively small grain layer. Since it is formed on the inner peripheral side, it can be seen that the occurrence of chipping is small as compared with the case of grinding using the cup-shaped grindstones of Comparative Examples 1 to 3. Especially, since the level | step difference was 0.1-5.0 mm in the cup-shaped grindstone of Examples 2-8, 10-20, generation | occurrence | production of a chip | tip became small. Furthermore, the cup-shaped grindstones of Examples 10 to 20 have a recess between the outer peripheral end surface and the inner peripheral end surface of the cup-shaped grindstone, and the outer peripheral end surface and the inner peripheral end surface are R. It can be seen that the occurrence of chipping is very small.

本発明に係るセラミックハニカム構造体の加工を示した図。The figure which showed the process of the ceramic honeycomb structure which concerns on this invention. 本発明に係るセラミックハニカム構造体の加工に用いるカップ形砥石を示した図。The figure which showed the cup-shaped grindstone used for the process of the ceramic honeycomb structure which concerns on this invention. 本発明に係るセラミックハニカム構造体の加工に用いるカップ形砥石を示した図。The figure which showed the cup-shaped grindstone used for the process of the ceramic honeycomb structure which concerns on this invention. 自動車の排気ガス中のPMを捕集、浄化するフィルタに用いられるハニカム構造体を示した図。The figure which showed the honeycomb structure used for the filter which collects and purifies PM in the exhaust gas of a motor vehicle. セラミックハニカム構造体の端面の加工で従来技術を示した図。The figure which showed the prior art by the process of the end surface of a ceramic honeycomb structure.

符号の説明Explanation of symbols

10:カップ形砥石
11:基台
12:軸
13:逃げ部
14:取付部
15:カップ形砥石の研削部位
151:外周側の端面
152:内周側の端面
16:凹部
17:砥粒層
17A:砥粒層A
17B:砥粒層B
18:外周面
20:セラミックハニカム構造体
21:外周壁
22:隔壁
23、24:セル
25、26:封止部
27、28:セラミックハニカム構造体の端面
31:取付具
:カップ形砥石の外径
:ハニカム構造体の外径
H:段差
:凹部の深さ
:端面152からの位置
L:カップ形砥石の端面の幅
:凹部の幅
:カップ形砥石の外周側からの位置
t、t、t:切り込み量
、R、R、R:R部
θ:カップ形砥石の外周面とセラミックハニカム構造体の端面とのなす角度
DESCRIPTION OF SYMBOLS 10: Cup-shaped grindstone 11: Base 12: Shaft 13: Relief part 14: Mounting part 15: Grinding part 151 of cup-shaped grindstone 152: End face 152 on the outer peripheral side: End face 16 on the inner peripheral side: Recess 17: Abrasive grain layer 17A : Abrasive layer A
17B: Abrasive grain layer B
18: outer peripheral surface 20: ceramic honeycomb structure 21: outer peripheral wall 22: partition wall 23, 24: cell 25, 26: sealing portion 27, 28: end face 31 of ceramic honeycomb structure: fixture D 1 : cup-shaped grindstone Outer diameter D 2 : Outer diameter of honeycomb structure H: Step height h 1 : Depth of recess h 2 : Position from end face 152 L: Width of end face of cup-shaped grindstone L 1 : Width of recess L 2 : Cup-shaped grindstone Positions t, t 1 , t 2 from the outer peripheral side of: R cut amount R 1 , R 2 , R 3 , R 4 : R part θ: angle formed by the outer peripheral surface of the cup-shaped grindstone and the end surface of the ceramic honeycomb structure

Claims (4)

多孔質の隔壁により形成されるセルを多数有するセラミックハニカム構造体の端面を、カップ形砥石を用いて加工を行うセラミックハニカム構造体の製造方法において、前記カップ形砥石はその外周側の端面が、内周側の端面に対して、前記カップ形砥石の軸方向取付部側に段差を有し、前記カップ形砥石の研削部位に砥粒層を有し、前記砥粒層は、前記カップ形砥石の外周側と内周側で、それぞれ粒径の異なる砥粒の砥粒層であり、前記砥粒のうち相対的に粒径の大きい砥粒層を外周側に形成し、相対的に粒径の小さい砥粒層を内周側に形成されていることを特徴とするセラミックハニカム構造体の製造方法。 In a method for manufacturing a ceramic honeycomb structure in which an end face of a ceramic honeycomb structure having a large number of cells formed by porous partition walls is processed using a cup-shaped grindstone, the cup-shaped grindstone has an end face on its outer peripheral side, With respect to the end surface on the inner circumferential side, there is a step on the axial mounting portion side of the cup-shaped grindstone, and there is an abrasive layer at the grinding part of the cup-shaped grindstone, and the abrasive layer is the cup-shaped grindstone Abrasive grain layers having different grain sizes on the outer peripheral side and the inner peripheral side, and a relatively large abrasive grain layer is formed on the outer peripheral side among the abrasive grains. A method for manufacturing a ceramic honeycomb structure, wherein a small abrasive grain layer is formed on the inner peripheral side. 前記段差が0.1〜5.0mmであることを特徴とする請求項1に記載のセラミックハニカム構造体の製造方法。 The method for manufacturing a ceramic honeycomb structure according to claim 1, wherein the step is 0.1 to 5.0 mm. 前記カップ形砥石の外周側の端面と、内周側の端面との間に凹部を有していることを特徴とする請求項1ないし3のいずれかに記載のセラミックハニカム構造体の製造方法。 The method for manufacturing a ceramic honeycomb structure according to any one of claims 1 to 3, wherein a concave portion is provided between an end face on the outer peripheral side and an end face on the inner peripheral side of the cup-shaped grindstone. 前記外周側の端面と、内周側の端面にR部を有することを特徴とする請求項1ないし4のいずれかに記載のセラミックハニカム構造体の製造方法。
The method for manufacturing a ceramic honeycomb structure according to any one of claims 1 to 4, wherein the outer peripheral side end surface and the inner peripheral side end surface have an R portion.
JP2005345412A 2005-11-30 2005-11-30 Manufacturing method of ceramic honeycomb structure Pending JP2007144922A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP2005345412A JP2007144922A (en) 2005-11-30 2005-11-30 Manufacturing method of ceramic honeycomb structure

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP2005345412A JP2007144922A (en) 2005-11-30 2005-11-30 Manufacturing method of ceramic honeycomb structure

Publications (1)

Publication Number Publication Date
JP2007144922A true JP2007144922A (en) 2007-06-14

Family

ID=38206889

Family Applications (1)

Application Number Title Priority Date Filing Date
JP2005345412A Pending JP2007144922A (en) 2005-11-30 2005-11-30 Manufacturing method of ceramic honeycomb structure

Country Status (1)

Country Link
JP (1) JP2007144922A (en)

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2012206007A (en) * 2011-03-29 2012-10-25 Ngk Insulators Ltd Plugged honeycomb structure
JP2012206006A (en) * 2011-03-29 2012-10-25 Ngk Insulators Ltd Plugged honeycomb structure
WO2013096113A1 (en) * 2011-12-19 2013-06-27 Dow Global Technologies Llc Improved method and apparatus for preparing ceramic body segments
JP2016093866A (en) * 2014-11-14 2016-05-26 オリンパス株式会社 Processing device for optical element, grindstone member and processing method for optical element
WO2016121785A1 (en) * 2015-01-29 2016-08-04 イビデン株式会社 Method for manufacturing ceramic filter
US20200238470A1 (en) * 2019-01-24 2020-07-30 Ngk Insulators, Ltd. Processing method and processing device for ceramic honeycomb structure

Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH0592371A (en) * 1991-09-27 1993-04-16 Mitsubishi Heavy Ind Ltd Cup shape grinding wheel
JP2001191323A (en) * 2000-01-07 2001-07-17 Ibiden Co Ltd Cutting member for porous ceramic material
JP2001191240A (en) * 2000-01-07 2001-07-17 Ibiden Co Ltd Method of manufacturing for honeycomb structure
JP2002018290A (en) * 2000-07-12 2002-01-22 Hitachi Metals Ltd Carrier for ceramic honeycomb structure catalyst and ceramic honeycomb structure catalyst converter using the same
JP2002263937A (en) * 2001-03-06 2002-09-17 Noritake Super Abrasive:Kk Milling tool
JP2004291213A (en) * 2003-03-28 2004-10-21 Noritake Super Abrasive:Kk Grinding wheel
JP2004321851A (en) * 2003-04-21 2004-11-18 Ngk Insulators Ltd Honeycomb structure, its production method, mouth piece for molding and discharge fluid cleaning system
JP2004321848A (en) * 2003-04-21 2004-11-18 Ngk Insulators Ltd Honeycomb structure and its manufacturing method

Patent Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH0592371A (en) * 1991-09-27 1993-04-16 Mitsubishi Heavy Ind Ltd Cup shape grinding wheel
JP2001191323A (en) * 2000-01-07 2001-07-17 Ibiden Co Ltd Cutting member for porous ceramic material
JP2001191240A (en) * 2000-01-07 2001-07-17 Ibiden Co Ltd Method of manufacturing for honeycomb structure
JP2002018290A (en) * 2000-07-12 2002-01-22 Hitachi Metals Ltd Carrier for ceramic honeycomb structure catalyst and ceramic honeycomb structure catalyst converter using the same
JP2002263937A (en) * 2001-03-06 2002-09-17 Noritake Super Abrasive:Kk Milling tool
JP2004291213A (en) * 2003-03-28 2004-10-21 Noritake Super Abrasive:Kk Grinding wheel
JP2004321851A (en) * 2003-04-21 2004-11-18 Ngk Insulators Ltd Honeycomb structure, its production method, mouth piece for molding and discharge fluid cleaning system
JP2004321848A (en) * 2003-04-21 2004-11-18 Ngk Insulators Ltd Honeycomb structure and its manufacturing method

Cited By (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2012206007A (en) * 2011-03-29 2012-10-25 Ngk Insulators Ltd Plugged honeycomb structure
JP2012206006A (en) * 2011-03-29 2012-10-25 Ngk Insulators Ltd Plugged honeycomb structure
WO2013096113A1 (en) * 2011-12-19 2013-06-27 Dow Global Technologies Llc Improved method and apparatus for preparing ceramic body segments
US9987766B2 (en) 2011-12-19 2018-06-05 Dow Global Technologies Llc Method and apparatus for preparing ceramic body segments
JP2016093866A (en) * 2014-11-14 2016-05-26 オリンパス株式会社 Processing device for optical element, grindstone member and processing method for optical element
WO2016121785A1 (en) * 2015-01-29 2016-08-04 イビデン株式会社 Method for manufacturing ceramic filter
JP2016137476A (en) * 2015-01-29 2016-08-04 イビデン株式会社 Manufacturing method of ceramic filter
US20200238470A1 (en) * 2019-01-24 2020-07-30 Ngk Insulators, Ltd. Processing method and processing device for ceramic honeycomb structure
US11919128B2 (en) * 2019-01-24 2024-03-05 Ngk Insulators, Ltd. Processing method and processing device for ceramic honeycomb structure

Similar Documents

Publication Publication Date Title
JP4731993B2 (en) Manufacturing method of honeycomb structure
KR100628291B1 (en) Method of manufacturing honeycomb structural body
EP2724814B1 (en) Grinding Method of Honeycomb Structure
JP5475953B2 (en) Method for manufacturing perforated honeycomb structure
JP4908951B2 (en) Manufacturing method of honeycomb formed body and grinding apparatus thereof
KR102013760B1 (en) Ceramic honeycomb body fabrication method
JP4632125B2 (en) Method for manufacturing ceramic honeycomb structure
JP2007144922A (en) Manufacturing method of ceramic honeycomb structure
JP6407773B2 (en) Honeycomb structure manufacturing method and grinding wheel
JP4998346B2 (en) Method for manufacturing ceramic honeycomb structure
JP5052790B2 (en) Grinding method
JP3953245B2 (en) Manufacturing method of honeycomb structure
JP2003103181A (en) Honeycomb catalyst, method for manufacturing honeycomb intermediate and honeycomb catalyst
JPWO2009035049A1 (en) Manufacturing method of honeycomb filter
JP2019166484A (en) Honeycomb structure
JP5667346B2 (en) Manufacturing method of honeycomb structure
JP7082583B2 (en) Processing method and processing equipment for ceramic honeycomb structures
JP6196234B2 (en) Improved method and apparatus for making ceramic body segments
JP2015501744A5 (en)
JPH0571533B2 (en)
JP2001191323A (en) Cutting member for porous ceramic material
JP2021146307A (en) Honeycomb structure

Legal Events

Date Code Title Description
A621 Written request for application examination

Free format text: JAPANESE INTERMEDIATE CODE: A621

Effective date: 20081009

A977 Report on retrieval

Free format text: JAPANESE INTERMEDIATE CODE: A971007

Effective date: 20110128

A131 Notification of reasons for refusal

Free format text: JAPANESE INTERMEDIATE CODE: A131

Effective date: 20110218

A521 Written amendment

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20110418

A02 Decision of refusal

Free format text: JAPANESE INTERMEDIATE CODE: A02

Effective date: 20110513