JP2007001812A - Method and apparatus for manufacturing quartz glass rod - Google Patents

Method and apparatus for manufacturing quartz glass rod Download PDF

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Publication number
JP2007001812A
JP2007001812A JP2005184284A JP2005184284A JP2007001812A JP 2007001812 A JP2007001812 A JP 2007001812A JP 2005184284 A JP2005184284 A JP 2005184284A JP 2005184284 A JP2005184284 A JP 2005184284A JP 2007001812 A JP2007001812 A JP 2007001812A
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quartz glass
rod
forming
glass rod
outer diameter
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JP4464321B2 (en
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Makoto Mitani
真 三谷
Yuichi Miyagishi
裕一 宮岸
Sadanobu Yamada
定信 山田
Yukio Doura
幸夫 堂浦
Koichi Nishihata
浩一 西端
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Nippon Steel Corp
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Sumitomo Metal Industries Ltd
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    • CCHEMISTRY; METALLURGY
    • C03GLASS; MINERAL OR SLAG WOOL
    • C03BMANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
    • C03B37/00Manufacture or treatment of flakes, fibres, or filaments from softened glass, minerals, or slags
    • C03B37/01Manufacture of glass fibres or filaments
    • C03B37/012Manufacture of preforms for drawing fibres or filaments
    • C03B37/01205Manufacture of preforms for drawing fibres or filaments starting from tubes, rods, fibres or filaments
    • C03B37/01225Means for changing or stabilising the shape, e.g. diameter, of tubes or rods in general, e.g. collapsing
    • C03B37/0124Means for reducing the diameter of rods or tubes by drawing, e.g. for preform draw-down
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P40/00Technologies relating to the processing of minerals
    • Y02P40/50Glass production, e.g. reusing waste heat during processing or shaping
    • Y02P40/57Improving the yield, e-g- reduction of reject rates

Abstract

<P>PROBLEM TO BE SOLVED: To provide a method and an apparatus for manufacturing a quartz glass rod having remarkably excellent dimensional precision of the outer diameter at high yield. <P>SOLUTION: The method of manufacturing the quartz glass rod is carried out by heating and softening a rod like quartz glass base material 11 successively from one side while rotating and moving along the axial direction while controlling the moving rate to control the outer diameter of the quartz glass rod. The apparatus for manufacturing the quartz glass rod comprises a chuck 15 for grasping the rod like quartz glass base material to be rotatable and moving in the axial direction, a heating means 17 for heating the rod like quartz glass base material, a forming and drawing die 20 for forming the heated and softened part of the rod like quartz glass base material into a prescribed shape by injecting into the die, and a chuck 16 for grasping the formed quartz glass rod to be rotatable and moving the quartz glass rod in the axial direction. The cross-sectional shape of the inner wall of the forming and drawing die comprising an inlet side opening part, a drawing part and a hole part is curved at the drawing part. <P>COPYRIGHT: (C)2007,JPO&INPIT

Description

本発明は、石英ガラス棒を高寸法精度で、かつ歩留まり良く製造するための製造方法及び製造装置に関する。   The present invention relates to a manufacturing method and a manufacturing apparatus for manufacturing a quartz glass rod with high dimensional accuracy and high yield.

近年、光通信技術の進展に伴い、光ファイバの利用が高まってきている。その光ファイバは、通常、光ファイバプリフォームと呼ばれる光ファイバ母材を線引きすることによって製造される。   In recent years, with the progress of optical communication technology, the use of optical fibers has increased. The optical fiber is usually manufactured by drawing an optical fiber preform called an optical fiber preform.

一般的な光ファイバプリフォーム(線引きする前の母材)は、主として、VAD法(Vapor phase Axial Deposition Method;気相軸付け法)、OVD法(Outside Vapor Phase Deposition Method;外付け法)、MCVD法(Modified Chemical Vapor Deposition Method;内付け法)等により製造される。そして、この光ファイバプリフォームを高速で線引きすることによって、目的の外径を有する光ファイバが得られるのである。   Common optical fiber preforms (base materials before drawing) are mainly VAD method (Vapor phase Axial Deposition Method), OVD method (Outside Vapor Phase Deposition Method), MCVD Manufactured by the method (Modified Chemical Vapor Deposition Method). Then, by drawing this optical fiber preform at a high speed, an optical fiber having a target outer diameter can be obtained.

例えば、VAD法の場合、実際に光が通るコアガラスロッドを出発ガラスロッドとし、出発ガラスロッドの外周に、ガラス微粒子を堆積させてコアロッド/ガラス微粒子堆積体の複合体を合成し、この複合体を加熱炉にて焼結してガラス体とし、ガラス体を延伸工程に付して、ファイバプリフォームを形成した後、プリフォームを線引き炉で線引きすることによって、光ファイバを製造する。この方法においては、出発ガラスロッドの両端に円柱状のダミー棒と呼ばれる石英ガラス棒が溶着接続され使用されている。また、この石英ガラス棒は、コアロッド/ガラス微粒子堆積体の複合体合成時にその複合体を吊り下げるシャフトとしても使用される。そして、このようにして使用される石英ガラス棒は、出発ガラスロッドと外径差がないこと、回転させた状態で使用されるため曲がりが少ないことなど、非常に厳しい寸法精度が要求されている。また、一方では、光通信コスト削減の観点から、特に消耗品であるダミー棒については安価であることが要求されている。   For example, in the case of the VAD method, a core glass rod through which light actually passes is used as a starting glass rod, and a composite of core rod / glass fine particles is synthesized by depositing glass particles on the outer periphery of the starting glass rod. After the glass body is sintered in a heating furnace to form a glass body, the glass body is subjected to a drawing process to form a fiber preform, and then the preform is drawn in a drawing furnace to produce an optical fiber. In this method, a quartz glass rod called a cylindrical dummy rod is welded and connected to both ends of a starting glass rod. The quartz glass rod is also used as a shaft for suspending the composite when synthesizing the core rod / glass fine particle composite. And the quartz glass rod used in this way is required to have very strict dimensional accuracy such as no difference in outer diameter from the starting glass rod and less bending because it is used in a rotated state. . On the other hand, from the viewpoint of reducing optical communication costs, it is required that the dummy rod, which is a consumable item, be inexpensive.

特許文献1には、石英ガラス棒を製造する方法が開示されている。この方法は、母材となる石英ガラスインゴットを加熱炉にて軟化させ、加熱炉下部に設置された延伸駆動ローラーによって鉛直方向に延伸する方法である。そして、延伸駆動部のトルクを一定範囲に制御することによって、外径精度を高めた石英ガラス棒を製造しようとするものである。   Patent Document 1 discloses a method for producing a quartz glass rod. This method is a method in which a quartz glass ingot serving as a base material is softened in a heating furnace and is stretched in the vertical direction by a stretching drive roller installed in the lower part of the heating furnace. And it is going to manufacture the quartz glass stick | rod which raised the outer diameter precision by controlling the torque of an extending | stretching drive part to a fixed range.

特許文献2には、他の石英ガラス棒の製造方法が開示されている。この方法は、石英ガラスインゴットの両端をそれぞれ固定側チャック、移動側チャックに把持し、加熱炉で局所的に軟化させた後、移動側チャックの位置を移動することにより延伸する方法である。ここでは、実際に延伸されている石英ガラス棒の外径をモニターし、移動側チャックの移動速度を調整することにより外径が制御される。   Patent Document 2 discloses another method for producing a quartz glass rod. In this method, both ends of the quartz glass ingot are held by a fixed chuck and a moving chuck, respectively, softened locally in a heating furnace, and then stretched by moving the position of the moving chuck. Here, the outer diameter of the quartz glass rod that is actually stretched is monitored, and the outer diameter is controlled by adjusting the moving speed of the moving side chuck.

さらに、特許文献3には、加熱した石英ガラス素材を回転させつつ成形ダイスに圧入することによって、石英ガラスインゴットを成形する方法が開示されている。石英ガラス素材を回転させながら加熱装置を通過させるので、石英ガラス素材を径方向で均一に加熱することができ、また加熱された石英ガラス素材の変形を防止することができる。   Furthermore, Patent Document 3 discloses a method of forming a quartz glass ingot by press-fitting a heated quartz glass material into a forming die while rotating it. Since the quartz glass material is passed through the heating device while being rotated, the quartz glass material can be heated uniformly in the radial direction, and deformation of the heated quartz glass material can be prevented.

特開平3−115131号公報JP-A-3-115131 特開平2−275723号公報JP-A-2-275723 特開2000−67411号公報JP 2000-67411 A

上記特許文献1に記載された垂直方向延伸法の場合、実際延伸されている石英ガラス棒の外径をモニターし、延伸駆動ローラーの回転数を調整するため、外径はある一定の範囲内には収まるものの、その範囲内において外径変動が発生する。また、母材となる石英ガラスインゴットは鉛直方向にのみ移動するため、石英ガラスインゴットと延伸駆動ローラーの中心軸はより高精度に一致させておく必要がある。さもないと、加熱炉の断面内での温度分布の影響を受けるので、石英ガラスインゴットの断面内で粘性差が生じ、延伸中の石英ガラス棒に曲がりや非円形部分が発生する。   In the case of the vertical stretching method described in Patent Document 1, the outer diameter of the quartz glass rod that is actually stretched is monitored, and the outer diameter is within a certain range in order to adjust the rotation speed of the stretching drive roller. However, the outer diameter fluctuates within that range. In addition, since the quartz glass ingot as a base material moves only in the vertical direction, it is necessary to match the central axes of the quartz glass ingot and the stretching drive roller with higher accuracy. Otherwise, since it is affected by the temperature distribution in the cross section of the heating furnace, a viscosity difference is generated in the cross section of the quartz glass ingot, and a bent or non-circular portion is generated in the quartz glass rod being drawn.

そして、上記特許文献2に記載された方法の場合、実際に延伸されている石英ガラス棒の外径をモニターし、移動側チャックの移動速度を調整するため、外径はある一定の範囲内には収まるものの、その範囲内において外径変動が発生する。また、曲がり部分や非円形部分については、石英ガラスインゴットを回転させているため、石英ガラスインゴットの断面内で粘性差を抑制することが可能であり、延伸中の石英ガラス棒の非円形部分の発生は抑制できるものの、延性に対する移動側チャックの移動速度の調整が非常に困難であるため、延伸中に垂れが生じ、結果として曲がりが発生してしまうことがある。   In the case of the method described in Patent Document 2, the outer diameter of the quartz glass rod that is actually stretched is monitored, and the outer diameter is within a certain range in order to adjust the moving speed of the moving side chuck. However, the outer diameter fluctuates within that range. In addition, since the quartz glass ingot is rotated for the bent part and the non-circular part, it is possible to suppress the viscosity difference in the cross section of the quartz glass ingot. Although generation | occurrence | production can be suppressed, since adjustment of the moving speed of the movement side chuck | zipper with respect to ductility is very difficult, dripping arises during extending | stretching and bending may be generated as a result.

したがって、いずれの製造方法も、外径変動が少なく、かつ曲がりの少ない寸法精度の優れた石英ガラス棒を得ることは困難である。また、延伸開始時の外径をモニターして外径を制御するため、延伸開始時から目的とする外径に到達するまでの間に延伸されてしまった部分については、目的とする外径の石英ガラス棒とはならないため、この分だけ歩留まりが悪くなる。   Therefore, it is difficult to obtain a quartz glass rod having excellent dimensional accuracy with little fluctuation in outer diameter and little bending in any of the manufacturing methods. In addition, in order to control the outer diameter by monitoring the outer diameter at the start of stretching, the portion that has been stretched from the start of stretching until reaching the target outer diameter, Since it is not a quartz glass rod, the yield is reduced by this amount.

さらに、上記特許文献3に記載された方法は、石英ガラス素材を径方向で均一に加熱するので、石英ガラス素材の変形を防止することができるが、成形後の石英ガラス棒の外径の寸法精度や歩留まりについては、言及されていない。   Furthermore, since the method described in Patent Document 3 uniformly heats the quartz glass material in the radial direction, the quartz glass material can be prevented from being deformed. There is no mention of accuracy or yield.

本発明の目的は、このような問題点を解決して、石英ガラス棒を寸法精度良くかつ歩留まり良く製造するための方法及び製造装置を提供することにある。   An object of the present invention is to solve such problems and to provide a method and a manufacturing apparatus for manufacturing a quartz glass rod with high dimensional accuracy and high yield.

本発明にかかる石英ガラス棒の製造方法は、次の(1)から(4)までのいずれかであり、そして、本発明にかかる石英ガラス棒の製造装置は次の(5)である。以下、これらを総称して本発明ということがある。   The method for producing a quartz glass rod according to the present invention is any of the following (1) to (4), and the apparatus for producing a quartz glass rod according to the present invention is the following (5). Hereinafter, these may be collectively referred to as the present invention.

(1)棒状の石英ガラス素材を回転させつつ片端から順次加熱軟化させて軸方向に移動させ、その加熱軟化部分を成形延伸ダイスに送り込むことにより石英ガラス棒を製造する方法であって、石英ガラス素材の送り込み速度を調整することにより石英ガラス棒の外径を制御することを特徴とする石英ガラス棒の製造方法。   (1) A method for producing a quartz glass rod by rotating a rod-like quartz glass material while heating and softening sequentially from one end and moving it in the axial direction, and feeding the heated and softened portion into a forming and drawing die, A method for producing a quartz glass rod, wherein the outer diameter of the quartz glass rod is controlled by adjusting a feed rate of the material.

(2)棒状の石英ガラス素材の成形状態の観察結果を用いて石英ガラス素材の送り込み速度を調整することを特徴とする、上記(1)の石英ガラス棒の製造方法。   (2) The method for producing a quartz glass rod according to (1), wherein the feeding speed of the quartz glass material is adjusted using the observation result of the molding state of the rod-like quartz glass material.

(3)棒状の石英ガラス素材の加熱軟化部分を成形延伸ダイスに送り込む際に、成形延伸ダイスの入口側開口部においてその加熱軟化部分の外径を一旦大きくした後、成形延伸ダイスの延伸部を経て孔部に送り込むことを特徴とする、上記(1)又は(2)の石英ガラス棒の製造方法。   (3) When the heat-softened portion of the rod-shaped quartz glass material is fed into the forming and drawing die, the outer diameter of the heat-softening portion is once increased at the opening on the inlet side of the forming and drawing die, and then the extending portion of the forming and drawing die is The method for producing a quartz glass rod according to the above (1) or (2), wherein the quartz glass rod is fed into the hole.

(4)成形延伸ダイスの内壁の軸方向の断面形状が、成形延伸ダイスの延伸部において曲線である成形延伸ダイスを用いることを特徴とする、上記(1)〜(3)のいずれかの石英ガラス棒の製造方法。   (4) The quartz according to any one of (1) to (3) above, wherein the shape-drawing die is such that the cross-sectional shape in the axial direction of the inner wall of the shape-drawing die is a curve in the drawing portion of the shape-drawing die. A method of manufacturing a glass rod.

(5)棒状の石英ガラス素材を回転可能な状態で把持するとともに軸方向に移動させるチャックと、棒状の石英ガラス素材を加熱するための加熱手段と、棒状の石英ガラス素材の加熱軟化部分を圧入させ所定の形状に成形するための成形延伸ダイスと、成形後の石英ガラス棒を回転可能な状態で把持するとともに軸方向に移動させるチャックを有する石英ガラス棒の製造装置であって、入口側開口部と延伸部と孔部からなる成形延伸ダイスの内壁の軸方向の断面形状が入口側開口部から孔部にかけて曲線であることを特徴とする石英ガラス棒の製造装置。   (5) Gripping the rod-shaped quartz glass material in a rotatable state and moving it in the axial direction, heating means for heating the rod-shaped quartz glass material, and heat-softening part of the rod-shaped quartz glass material are press-fitted A quartz glass rod manufacturing apparatus having a molding drawing die for molding into a predetermined shape and a chuck for holding the molded quartz glass rod in a rotatable state and moving it in the axial direction. An apparatus for producing a quartz glass rod, characterized in that the cross-sectional shape in the axial direction of the inner wall of a forming and drawing die comprising a part, an extending part and a hole is a curve from the opening on the inlet side to the hole.

本発明によれば、外径寸法精度の極めて良好な石英ガラス棒を、歩留まり良く製造することができる。   According to the present invention, it is possible to manufacture a quartz glass rod having a very good outer diameter dimensional accuracy with a high yield.

本発明に係る石英ガラス棒の製造方法は、棒状の石英ガラス素材を回転させつつ片端から順次加熱軟化させて軸方向に沿って移動させ、その加熱軟化部分を成形延伸ダイスに圧入する際に、石英ガラス素材の送り込み速度を調整するものである。   The method for producing a quartz glass rod according to the present invention is to heat and soften sequentially from one end while rotating a rod-like quartz glass material and move it along the axial direction, and press-fit the heat-softened part into a forming and drawing die. This adjusts the feeding speed of the quartz glass material.

以下に、図面を用いて、本発明を説明する。   The present invention will be described below with reference to the drawings.

図1は、本発明に用いる石英ガラス棒の製造装置の縦断面図である。   FIG. 1 is a longitudinal sectional view of an apparatus for producing a quartz glass rod used in the present invention.

この装置において、まず、棒状の石英ガラス素材11が、入側ダミー材13及び出側ダミー材14を介して、それぞれ入側チャック15及び出側チャック16に把持される。ダミー材としては、例えば石英ガラスロッドやパイプなどを用いることができ、これを棒状の石英ガラス素材の両端に溶着等により取り付ける。入側チャック15及び出側チャック16に把持された棒状の石英ガラス素材11は、回転しながら成形延伸ダイス20の方向へ(図1では左から右へ)送り出される。   In this apparatus, first, a rod-shaped quartz glass material 11 is gripped by an entrance side chuck 15 and an exit side chuck 16 via an entrance side dummy material 13 and an exit side dummy material 14, respectively. As the dummy material, for example, a quartz glass rod or a pipe can be used, and this is attached to both ends of a rod-like quartz glass material by welding or the like. The rod-shaped quartz glass material 11 gripped by the inlet side chuck 15 and the outlet side chuck 16 is sent out in the direction of the forming and drawing die 20 while rotating (from left to right in FIG. 1).

入側チャック15の走行速度と出側チャック16の走行速度の比は、棒状の石英ガラス素材11の横断面積と、所定の外径寸法を有する成形後の石英ガラス棒12の横断面積の比の逆数に設定される。ここで、入側チャック15の回転速度と出側チャック16の回転速度は、同じであることが好ましい。なぜならば、回転速度差を持たせると成形後の石英ガラス棒12の外表面に捻れ模様が発生しやすいためである。   The ratio of the traveling speed of the entrance side chuck 15 and the traveling speed of the exit side chuck 16 is the ratio of the transverse area of the rod-shaped quartz glass material 11 and the transverse area of the quartz glass rod 12 after molding having a predetermined outer diameter. Set to the reciprocal. Here, it is preferable that the rotational speed of the entrance side chuck 15 and the rotational speed of the exit side chuck 16 are the same. This is because a twisted pattern is likely to occur on the outer surface of the quartz glass rod 12 after forming if a rotational speed difference is provided.

入側チャック15と出側チャック16の間にはヒータ17が設置されており、棒状の石英ガラス素材11の一部は順次ヒータ17によって軟化点以上に加熱されて加熱軟化部分となり、成形延伸ダイス20に送り込まれる。成形延伸ダイス20の入口側開口部21と孔部23の内径は、使用する棒状の石英ガラス素材11の外径と、目的とする石英ガラス棒12の外径に対応して設定される。   A heater 17 is installed between the entrance side chuck 15 and the exit side chuck 16, and a part of the rod-like quartz glass material 11 is sequentially heated above the softening point by the heater 17 to become a heat-softening part, and a mold drawing die. 20 is sent. The inner diameters of the inlet-side opening 21 and the hole 23 of the forming and drawing die 20 are set in accordance with the outer diameter of the rod-shaped quartz glass material 11 to be used and the outer diameter of the target quartz glass rod 12.

棒状の石英ガラス素材の加熱軟化部分は、成形延伸ダイス20を通すことによって成形延伸され、目的とする外径を有する石英ガラス棒12が得られる。   The heat-softened portion of the rod-shaped quartz glass material is molded and stretched by passing the molding and drawing die 20 to obtain a quartz glass rod 12 having a target outer diameter.

図2は、本発明において棒状の石英ガラス素材11の加熱軟化部分が成形延伸されて、石英ガラス棒12が製造される工程を示す縦断面図である。   FIG. 2 is a longitudinal sectional view showing a process in which the heat-softened portion of the rod-shaped quartz glass material 11 is formed and stretched in the present invention to manufacture the quartz glass rod 12.

加熱軟化した石英ガラス素材11は回転しながら成形延伸ダイス20に送り込まれる。成形延伸ダイス20の内壁は、入口開口部21と延伸部22と孔部23からなっている。送り込まれた加熱軟化した石英ガラス素材11は、成形延伸ダイス20の入口側開口部21に当たり、ここで一旦成形されてから、延伸部22において延伸され、その後、孔部23の出口から引き抜かれて、目的とする外径を有する石英ガラス棒12が形成される。   The heat-softened quartz glass material 11 is fed into the forming and drawing die 20 while rotating. The inner wall of the forming and extending die 20 includes an inlet opening 21, an extending portion 22, and a hole 23. The heat-softened quartz glass material 11 that has been sent hits the opening 21 on the inlet side of the forming and drawing die 20, and once formed here, it is drawn in the drawing portion 22, and then pulled out from the outlet of the hole portion 23. A quartz glass rod 12 having a desired outer diameter is formed.

このとき、引抜速度は一旦所定の値に設定すれば、その後は調整の必要がない。すなわち、引き抜かれて形成される石英ガラス棒12の、引抜速度は、成形延伸ダイスに送り込まれる加熱軟化した石英ガラス素材11が成形延伸ダイス20の入口側開口部21に当たって成形されるときの外径を調整することによって決定される。そして、加熱軟化した石英ガラス素材11が成形延伸ダイス20の入口側開口部21に当たって成形されるときの外径の調整は、石英ガラス素材11の送り込み速度を調整することによって可能である。   At this time, once the drawing speed is set to a predetermined value, there is no need for adjustment thereafter. That is, the drawing speed of the quartz glass rod 12 formed by drawing is the outer diameter when the heat-softened quartz glass material 11 fed into the forming and drawing die hits the inlet-side opening 21 of the forming and drawing die 20. Is determined by adjusting. The outer diameter of the quartz glass material 11 that has been softened by heating can be adjusted by adjusting the feeding speed of the quartz glass material 11 when the quartz glass material 11 is molded by hitting the inlet-side opening 21 of the forming and drawing die 20.

なお、棒状の石英ガラス素材11の送り込み速度の調整方法は特に限定されるものではないが、棒状の石英ガラス素材11の外径等の成形状態の観察結果を用いるのが好ましい。この石英ガラス素材11の外径等の成形状態は例えばCCDカメラなどを用いて観察すればよい。   The method for adjusting the feeding speed of the rod-shaped quartz glass material 11 is not particularly limited, but it is preferable to use the observation result of the molding state such as the outer diameter of the rod-shaped quartz glass material 11. The molding state such as the outer diameter of the quartz glass material 11 may be observed using, for example, a CCD camera.

このように、引抜速度を調整することなく送り込み速度を調整すること、すなわち成形延伸ダイスにおいて石英ガラス素材の供給側の制御により、目的とする外径を有する石英ガラス棒12を均一にかつ連続的に形成することができ、外径精度の優れた石英ガラス棒12を製造することができる。また、本発明の場合、成形延伸ダイス20を介して目的とする外径の石英ガラス棒12に成形延伸されるため、石英ガラス素材11の先端から後端までの全域を、無駄なく、目的とする外径の石英ガラス棒12に加工することができるので、従来の方法と比較すると大幅に歩留まりが向上する。   Thus, by adjusting the feeding speed without adjusting the drawing speed, that is, by controlling the supply side of the quartz glass material in the forming and drawing die, the quartz glass rod 12 having the target outer diameter is made uniform and continuous. The quartz glass rod 12 with excellent outer diameter accuracy can be manufactured. Further, in the case of the present invention, since it is molded and stretched to the quartz glass rod 12 having a desired outer diameter through the molding and stretching die 20, the entire area from the front end to the rear end of the quartz glass material 11 can be used without waste. Therefore, the yield can be greatly improved as compared with the conventional method.

なお、送り込まれた加熱軟化した石英ガラス素材11が成形延伸ダイス20の入口側開口部21に当たって成形されるときの外径を、図2に示すように、棒状の石英ガラス素材11の外径よりも少し大きくすると、加熱軟化した石英ガラス素材11が成形延伸ダイス20の内壁に沿って十分に供給されていることが確認できるため、間接的に延伸部22での延伸が十分になされているか否かを確認することができる。   Note that the outer diameter of the heat-softened quartz glass material 11 that is fed into the inlet-side opening 21 of the forming and drawing die 20 is formed from the outer diameter of the rod-shaped quartz glass material 11 as shown in FIG. If it is a little larger, it can be confirmed that the heat-softened quartz glass material 11 is sufficiently supplied along the inner wall of the forming and drawing die 20, so whether or not the drawing portion 22 is sufficiently drawn indirectly. Can be confirmed.

したがって、成形延伸ダイス20の入口側開口部21においてその加熱軟化部分の外径を一旦大きくした後延伸部22を介して孔部23に送り込むことが好ましい。棒状の石英ガラス素材の外径よりも、直径で10〜20mm程度大きくすることが好ましい。   Therefore, it is preferable to increase the outer diameter of the heat-softened portion at the inlet-side opening 21 of the forming and drawing die 20 and then feed it into the hole 23 through the extending portion 22. It is preferable to make the diameter about 10 to 20 mm larger than the outer diameter of the rod-shaped quartz glass material.

棒状の石英ガラス素材を構成する石英ガラス材としては、VAD法などで製造される合成石英ガラスに限定されることなく、水晶粉などを原料にした天然石英ガラスなど他の石英ガラスも用いることができる。   The quartz glass material constituting the rod-shaped quartz glass material is not limited to synthetic quartz glass manufactured by the VAD method or the like, and other quartz glass such as natural quartz glass made from quartz powder or the like can be used. it can.

棒状の石英ガラス素材の加熱軟化温度は、石英ガラス素材のOH基濃度やCl濃度などによって、軟化点が大きく変化するので、それに合わせて、ヒーターを適正な温度条件に設定すればよい。成形延伸中の石英ガラス素材の温度は測定が困難であるが、ヒーターの設定温度としては、2000〜2500℃程度である。   Since the softening point of the heat-softening temperature of the rod-shaped quartz glass material varies greatly depending on the OH group concentration, Cl concentration, etc. of the quartz glass material, the heater may be set to an appropriate temperature condition accordingly. Although it is difficult to measure the temperature of the quartz glass material during forming and stretching, the set temperature of the heater is about 2000 to 2500 ° C.

また、成形延伸ダイスに送り込まれる加熱軟化した石英ガラス素材の温度は、ヒーターによって加熱された石英ガラス素材の最高温度よりも少し低いことが好ましい。すなわち、ヒーターによって、石英ガラス素材はチャック側から徐々に温度が高くなり、成形延伸ダイスに送り込まれる直前で最も高い温度となり、それよりもやや温度が下がった時点で成形延伸ダイスに接して成形延伸されることが好ましい。このように、石英ガラス素材の温度を一旦高くしておいて、その後でそれよりもやや低い温度で成形延伸すると、石英ガラス棒のさらなる変形を防止することができる。このときは、寸法精度の面で特に優れた石英ガラス棒を製造することが可能となる。   Moreover, it is preferable that the temperature of the heat-softened quartz glass material fed into the forming and drawing die is slightly lower than the maximum temperature of the quartz glass material heated by the heater. In other words, the temperature of the quartz glass material gradually increases from the chuck side by the heater, reaches the highest temperature immediately before being fed into the forming and drawing die, and contacts the forming and drawing die when the temperature drops slightly. It is preferred that Thus, if the temperature of the quartz glass material is once increased and then formed and stretched at a temperature slightly lower than that, further deformation of the quartz glass rod can be prevented. At this time, it becomes possible to manufacture a quartz glass rod particularly excellent in terms of dimensional accuracy.

ヒーターの設定温度が上述のように2000〜2500℃程度になると、成形延伸ダイスなどの治工具に適用できる材料は限定される。具体的には、Al23、MgO、ZrO2系の酸化物や、黒鉛、W、Moなどを用いることができるが、その中では高温域での強度並びに純度の面から、黒鉛が最も好ましい。なお、成形延伸ダイスは直接石英ガラス素材と接触するため、製造された石英ガラス棒の不純物汚染が懸念されるときは、不純物の少ない純化処理された黒鉛の材料を用いるのが好ましい。また、延伸は酸化防止のため不活性雰囲気中で実施するのが好ましい。 When the set temperature of the heater is about 2000 to 2500 ° C. as described above, materials that can be applied to jigs and tools such as forming and drawing dies are limited. Specifically, Al 2 O 3 , MgO, ZrO 2 -based oxides, graphite, W, Mo and the like can be used. Among them, graphite is the most in view of strength and purity in a high temperature range. preferable. In addition, since the forming and drawing die is in direct contact with the quartz glass material, when there is a concern about impurity contamination of the manufactured quartz glass rod, it is preferable to use a purified graphite material with few impurities. In addition, the stretching is preferably performed in an inert atmosphere to prevent oxidation.

次に、本発明に用いる成形延伸ダイスの好ましい形状を、図3の実施例に基づいて説明する。   Next, the preferable shape of the shaping | molding extending | stretching die used for this invention is demonstrated based on the Example of FIG.

図3は、成形延伸ダイスの内壁の軸方向断面図を示す。   FIG. 3 shows an axial sectional view of the inner wall of the forming and drawing die.

成形延伸ダイス20は、入口開口21と延伸部22と孔部23からなっている。図3に示したように、送り込まれた加熱軟化した石英ガラス素材11は、上述のとおり、成形延伸ダイス20の入口側開口部21に当たり、ここで一旦成形されてから、延伸部22において延伸され、その後、孔部23の出口から引き抜かれて、目的とする外径を有する石英ガラス棒12が形成される。このように、延伸部22において、加熱軟化した石英ガラス素材11は変形加工を受ける。   The forming and extending die 20 includes an inlet opening 21, an extending portion 22, and a hole portion 23. As shown in FIG. 3, the heat-softened quartz glass material 11 that has been fed hits the inlet-side opening 21 of the molding and drawing die 20 as described above, and once formed here, it is stretched at the stretching portion 22. Thereafter, the quartz glass rod 12 having the desired outer diameter is formed by being pulled out from the outlet of the hole 23. Thus, in the extending | stretching part 22, the heat-softened quartz glass raw material 11 receives a deformation process.

したがって、この際に内壁面に沿って加熱軟化した石英ガラス素材11が破断することなく移動することが好ましく、そのためには、成形延伸ダイス20の内壁の軸方向の断面形状は、延伸部22において、曲線であることが好ましい。   Therefore, it is preferable that the quartz glass material 11 heated and softened along the inner wall surface moves without breaking at this time, and for this purpose, the axial cross-sectional shape of the inner wall of the forming and drawing die 20 is set at the extending portion 22. A curve is preferred.

成形延伸ダイス20の入口開口部21の内径Aは、棒状の石英ガラス素材11の外径よりも大きくしておく必要があり、孔部の内径Bは、目的とする石英ガラス棒12の外径の寸法に合わせておく必要がある。   The inner diameter A of the inlet opening 21 of the forming and drawing die 20 needs to be larger than the outer diameter of the rod-shaped quartz glass material 11, and the inner diameter B of the hole is the outer diameter of the target quartz glass rod 12. It is necessary to match with the dimensions.

上述のとおり、加熱軟化した石英ガラス素材11が成形延伸ダイス20の入口側開口部21に当たって成形されるときの外径の調整は、石英ガラス素材11の送り込み速度を調整することによって可能であるが、適正な調整域を確保するために、入口開口部21の内径Aは棒状の石英ガラス素材11の外径よりも、30〜50mm程度大きいことが望ましい。   As described above, adjustment of the outer diameter when the heat-softened quartz glass material 11 strikes the inlet-side opening 21 of the forming and drawing die 20 is possible by adjusting the feeding speed of the quartz glass material 11. In order to ensure an appropriate adjustment range, the inner diameter A of the inlet opening 21 is desirably about 30 to 50 mm larger than the outer diameter of the rod-shaped quartz glass material 11.

また、成形延伸ダイス20の孔部23の長さCは、加熱軟化した石英ガラス素材11が成形延伸ダイス20に接する温度や目的とする石英ガラス棒の引抜速度等に応じて適正な長さにすればよい。ただし、孔部23の長さCが短すぎて、延伸部22がヒータ17出口に極端に近づく構成となると、加熱軟化した石英ガラス素材11の温度が軟化点以下に低下してしまう可能性があり、その場合、成形延伸ダイス内20で石英ガラス棒12が破断してしまうおそれがある。逆に、孔部の長さCが長すぎると、延伸部22及び孔部23の前半部がヒータ17中央部に近づき、石英ガラス素材の粘性が低下するため、成形延伸後にさらに変形が進んでしまい、目的とする外径を確保できない可能性がある。   Further, the length C of the hole 23 of the forming and drawing die 20 is set to an appropriate length according to the temperature at which the heat-softened quartz glass material 11 is in contact with the forming and drawing die 20, the drawing speed of the target quartz glass rod, and the like. do it. However, if the length C of the hole 23 is too short and the extending portion 22 is extremely close to the outlet of the heater 17, the temperature of the heat-softened quartz glass material 11 may be lowered below the softening point. In such a case, the quartz glass rod 12 may be broken in the forming and drawing die 20. Conversely, if the length C of the hole is too long, the stretched portion 22 and the front half of the hole 23 come closer to the center of the heater 17 and the viscosity of the quartz glass material decreases, so that the deformation further proceeds after forming and stretching. Therefore, the target outer diameter may not be ensured.

さらに、図3に示すように、成形延伸ダイス20の内面に、例えば、窒素ガスのような不活性ガスの導入孔30を設けることが好ましく、不活性ガスを導入することによって、石英ガラス棒12が成形延伸される直前及び/又は直後の冷却効果を高めることが可能となる。これにより、成形延伸後のさらなる変形を防止することができる。冷却用の不活性ガス導入孔については、孔径、個数、位置等は特に限定されることはなく、処理される温度、引抜速度等によって適正な条件とすればよい。なお、冷却用の不活性ガス導入孔を設置する場合は、各面が均等に冷却されるように設置することが好ましい。   Furthermore, as shown in FIG. 3, it is preferable to provide, for example, an inert gas introduction hole 30 such as nitrogen gas on the inner surface of the forming and drawing die 20, and the quartz glass rod 12 is introduced by introducing the inert gas. It is possible to enhance the cooling effect immediately before and / or immediately after the film is stretched. Thereby, the further deformation | transformation after shaping | molding extending | stretching can be prevented. As for the inert gas introduction hole for cooling, the hole diameter, the number, the position and the like are not particularly limited, and may be set appropriately depending on the processing temperature, the drawing speed and the like. In addition, when installing the inert gas introduction hole for cooling, it is preferable to install so that each surface may be cooled equally.

次に、本発明に用いる成形延伸ダイスの内壁の曲線の例について説明する。   Next, the example of the curve of the inner wall of the shaping | molding extending | stretching die | dye used for this invention is demonstrated.

図4は、本発明に用いる成形延伸ダイスの内壁の例を示す軸方向断面図である。(a)の成形延伸ダイス内壁の曲線は、入口開口部を形成する直線と孔部を形成する直線にて形成されるコーナー部を角丸めしたものである。(b)の成形延伸ダイス内壁の曲線は、入口開口部と孔部の間を3本の直線で形成し、各々のコーナー部を角丸めしたものである。入口開口部と孔部の間を形成する直線の数は3本に限らず4本以上としてもよいが、少なくとも延伸部を形成するコーナー部は角丸めされる。(c)の成形延伸ダイス内壁の曲線は、楕円弧を組み合わせることにより形成したものである。(d)の成形延伸ダイスの内壁の曲線は円弧と楕円弧の組み合わせにより形成したものである。なお、(a)〜(d)のいずれの場合も、各曲線を構成する直線の長さや円弧及び楕円弧の長さは、石英ガラス素材の外径及び製造される石英ガラス棒の外径などにより設計すればよい。また、角丸めの大きさは、製造される石英ガラス棒の外径にもよるが、製造される石英ガラス棒の半径の2〜20倍程度であり、8〜12倍程度が好ましい。   FIG. 4 is an axial sectional view showing an example of the inner wall of the forming and drawing die used in the present invention. The curve of the inner wall of the forming and drawing die (a) is obtained by rounding a corner formed by a straight line that forms the inlet opening and a straight line that forms the hole. The curve of the inner wall of the forming and drawing die (b) is formed by forming three straight lines between the inlet opening and the hole, and rounding each corner. The number of straight lines that form between the inlet opening and the hole is not limited to three, but may be four or more, but at least the corner that forms the extension is rounded off. The curve of the inner wall of the forming and drawing die (c) is formed by combining elliptical arcs. The curve of the inner wall of the forming and drawing die (d) is formed by a combination of an arc and an elliptical arc. In any case of (a) to (d), the length of the straight line constituting each curve, the length of the arc and the elliptical arc depends on the outer diameter of the quartz glass material and the outer diameter of the manufactured quartz glass rod. Just design. Moreover, although the magnitude | size of a rounded corner is based also on the outer diameter of the manufactured quartz glass rod, it is about 2 to 20 times the radius of the manufactured quartz glass rod, and about 8 to 12 times is preferable.

成形延伸ダイス内壁の曲線形状は、図4にも示した通り、種々様々な形状とすることができるが、あまり複雑な曲線とすると製造コストが高くなる。そこで、図4(a)に示した入口開口部を形成する直線と孔部を形成する直線にて形成されるコーナー部を角丸めしたものが、好ましい。   As shown in FIG. 4, the curved shape of the inner wall of the formed drawing die can be variously varied. However, if the curve is too complicated, the manufacturing cost becomes high. Therefore, it is preferable to round the corner portion formed by the straight line forming the inlet opening and the straight line forming the hole shown in FIG.

(本発明例)
高純度の水晶粉(シリカ粉)を酸水素火炎にて溶融しながら垂直方向に堆積させて、天然石英ガラスインゴットを作製した。そして、外周を研削して、棒状の石英ガラス素材を得た。
(Example of the present invention)
A high-purity quartz powder (silica powder) was deposited in the vertical direction while melting in an oxyhydrogen flame to produce a natural quartz glass ingot. And the outer periphery was ground and the rod-shaped quartz glass raw material was obtained.

この石英ガラス素材(外径140mm、長さ750mm)から、図1の製造装置を用いて、本発明の方法に従って、外径50.15mmを目標にして、石英ガラス棒を製造した。ヒーターの設定温度は2300℃、回転速度は10rpmとし、棒状の石英ガラス素材の送り込み速度を14.76mm/min、生成した石英ガラス棒の引抜速度を115.06mm/minに設定し、成形延伸を行った。なお、成形延伸ダイスは、図3のものを用いた。成形延伸ダイスの入口開口部の内径Aは170mm、孔部の内径Bは50.15mm、そして、孔部23の長さCは120mmであった。また、延伸部の曲線は、図4(a)に示した入口開口部を形成する直線と孔部を形成する直線にて形成されるコーナー部をR200に角丸めしたものとした。   From this quartz glass material (outer diameter 140 mm, length 750 mm), a quartz glass rod was manufactured by using the manufacturing apparatus of FIG. 1 and targeting an outer diameter of 50.15 mm according to the method of the present invention. The set temperature of the heater is 2300 ° C., the rotation speed is 10 rpm, the feeding speed of the rod-shaped quartz glass material is set to 14.76 mm / min, the drawing speed of the generated quartz glass rod is set to 115.06 mm / min, went. In addition, the thing of FIG. 3 was used for the forming and drawing die. The inner diameter A of the inlet opening of the forming and drawing die was 170 mm, the inner diameter B of the hole was 50.15 mm, and the length C of the hole 23 was 120 mm. Moreover, the curve of the extending part was obtained by rounding a corner part formed by the straight line forming the inlet opening and the straight line forming the hole shown in FIG.

成形延伸開始から終了までの間、生成中の石英ガラス棒の外径はモニターしたが、引抜速度は一切調整せず、棒状の石英ガラス素材の送り込み側から、石英ガラス素材の加熱軟化部分の成形状態を観察しながら、棒状の石英ガラス素材の送り込み速度を14.30〜15.00mm/minの間で微調整した。   The outer diameter of the quartz glass rod being produced was monitored from the beginning to the end of molding, but the drawing speed was not adjusted at all, and the heating softening part of the quartz glass material was molded from the feed side of the rod-shaped quartz glass material. While observing the state, the feeding speed of the rod-shaped quartz glass material was finely adjusted between 14.30 and 15.00 mm / min.

図5に、本発明例において製造した石英ガラス棒の外径の変動状況を示す。この結果は、平均外径50.15mm、最大外径50.21mm、最小外径50.06mm、標準偏差0.02mmであった。このように、棒状の石英ガラス素材の送り込み速度を微調整するだけで、延伸開始時から終了までの間、安定して目標通りの外径の石英ガラス棒が得られた。   In FIG. 5, the fluctuation | variation state of the outer diameter of the quartz glass rod manufactured in the example of this invention is shown. As a result, the average outer diameter was 50.15 mm, the maximum outer diameter was 50.21 mm, the minimum outer diameter was 50.06 mm, and the standard deviation was 0.02 mm. Thus, only by finely adjusting the feeding speed of the rod-shaped quartz glass material, a quartz glass rod having a target outer diameter was stably obtained from the start to the end of stretching.

次に、製造した石英ガラス棒の曲がりを測定するため、製造した石英ガラス棒を1000mmに切断し、両端をVブロックで固定し、その石英ガラス棒の中央部の変位量をダイヤルゲージで測定し、下式(1)により算出したところ、曲がりは0.04mmであった。   Next, in order to measure the bending of the manufactured quartz glass rod, the manufactured quartz glass rod is cut into 1000 mm, both ends are fixed with V blocks, and the displacement of the central portion of the quartz glass rod is measured with a dial gauge. When calculated by the following equation (1), the bending was 0.04 mm.

曲がり(mm)=(石英ガラス棒中央部の変位量)/2
また、上記において、通常の外径公差を±0.5mmとした場合、全延伸長に対する良品部分の歩留まりは、100%であった。
Bend (mm) = (Displacement at the center of quartz glass rod) / 2
In the above description, when the normal outer diameter tolerance is ± 0.5 mm, the yield of the non-defective part with respect to the total stretched length was 100%.

(比較例)
この本発明例に係る石英ガラス棒の製造方法に対して、特許文献1に記載された鉛直遠心法に従って、外径50.15mmを目標にして、石英ガラス棒に加工した。
(Comparative example)
With respect to the method for producing a quartz glass rod according to the present invention example, a quartz glass rod was processed according to the vertical centrifugal method described in Patent Document 1 with an outer diameter of 50.15 mm as a target.

石英ガラス素材は、本発明例と同じく、高純度の水晶粉(シリカ粉)を酸水素火炎にて溶融しながら垂直方向に堆積させて、天然石英ガラスインゴットを作成した。そして、外周を研削することによって得られた、棒状の石英ガラス素材(外径140mm、長さ750mm)を用いた。   As for the quartz glass material, a natural quartz glass ingot was prepared by depositing high-purity quartz powder (silica powder) in the vertical direction while melting with an oxyhydrogen flame, as in the present invention example. And the rod-shaped quartz glass raw material (outer diameter 140mm, length 750mm) obtained by grinding the outer periphery was used.

加熱温度は2300℃、棒状の石英ガラス素材の送り込み速度を14.76mm/min、生成した石英ガラス棒の引抜速度を115.06mm/min(延伸駆動ローラ回転数で0.30rpm)に設定し、延伸を行った。延伸開始から終了までの間、生成した石英ガラス棒の外径をモニターしながら、目的とする外径に近づけるため、石英ガラス棒の引抜速度を95〜140mm/min(延伸駆動ローラ回転数で0.25〜0.37rpm)の間で調整した。   The heating temperature is set to 2300 ° C., the feeding speed of the rod-shaped quartz glass material is set to 14.76 mm / min, and the drawing speed of the generated quartz glass bar is set to 115.06 mm / min (the stretching drive roller speed is 0.30 rpm), Stretching was performed. In order to approach the target outer diameter while monitoring the outer diameter of the generated quartz glass rod from the start to the end of stretching, the pulling speed of the quartz glass rod is 95 to 140 mm / min (0 at the rotation speed of the stretching drive roller). .25 to 0.37 rpm).

図6に、比較例において製造された石英ガラス棒の外径の変動状況を示す。この結果は、平均外径50.71mm、最大外径58.19mm、最小外径49/53mm、標準偏差1.08mmであった。このように、石英ガラスの外径をモニターしながら引抜速度を調整したが、目標の外径に達するまでにかなりの時間を要するだけでなく、目標外径に近づいた後も、絶えず外径が変動した。   In FIG. 6, the fluctuation | variation state of the outer diameter of the quartz glass rod manufactured in the comparative example is shown. As a result, the average outer diameter was 50.71 mm, the maximum outer diameter was 58.19 mm, the minimum outer diameter was 49/53 mm, and the standard deviation was 1.08 mm. In this way, the drawing speed was adjusted while monitoring the outer diameter of the quartz glass, but not only did it take a considerable amount of time to reach the target outer diameter, but the outer diameter constantly increased after approaching the target outer diameter. It fluctuated.

次に、延伸された石英ガラス棒の曲がりを測定するため、延伸された石英ガラス棒を1000mmに切断し、両端をVブロックで固定し、石英ガラス棒の中央部の変位量をダイヤルゲージで測定し、下式(1)により算出したところ、曲がりは0.38mmであった。   Next, in order to measure the bending of the drawn quartz glass rod, the drawn quartz glass rod is cut into 1000 mm, both ends are fixed with V blocks, and the displacement amount at the center of the quartz glass rod is measured with a dial gauge. The bending was 0.38 mm as calculated by the following formula (1).

曲がり(mm)=(石英ガラス棒中央部の変位量)/2
また、上記において、通常の外径公差を±0.5mmとした場合、全延伸長に対する良品部分の歩留まりは、68%であった。
Bend (mm) = (Displacement at the center of quartz glass rod) / 2
In the above, when the normal outer diameter tolerance is ± 0.5 mm, the yield of the non-defective part with respect to the total stretched length was 68%.

図6は、本発明例及び比較例において製造された石英ガラス棒の外径の変動状況の両方を、同スケールにて、示すものである。本発明例によれば、外径寸法精度の極めて良好な石英ガラス棒を、歩留まり良く製造することができることが確認できた。   FIG. 6 shows, on the same scale, both fluctuations in the outer diameter of the quartz glass rods produced in the present invention example and the comparative example. According to the example of the present invention, it has been confirmed that a quartz glass rod with extremely good outer diameter dimensional accuracy can be manufactured with high yield.

本発明によれば、外径寸法精度の極めて良好な石英ガラス棒を、歩留まり良く製造することができる。   According to the present invention, it is possible to manufacture a quartz glass rod having a very good outer diameter dimensional accuracy with a high yield.

本発明に係る石英ガラス棒の製造装置の縦断面図である。It is a longitudinal cross-sectional view of the manufacturing apparatus of the quartz glass rod which concerns on this invention. 本発明において石英ガラス素材が成形かつ延伸されて石英ガラス棒が製造される工程を示す縦断面図である。It is a longitudinal cross-sectional view which shows the process in which a quartz glass raw material is shape | molded and extended | stretched in this invention, and a quartz glass rod is manufactured. 本発明に用いる成形延伸ダイスの内壁を示す軸方向断面図である。It is an axial sectional view showing the inner wall of the forming and drawing die used in the present invention. 本発明に用いる成形延伸ダイスの内壁の例を示す軸方向断面図である。It is an axial direction sectional view showing an example of an inner wall of a forming extension die used for the present invention. 本発明例において製造された石英ガラス棒の外径の変動状況を示す。The fluctuation | variation state of the outer diameter of the quartz glass rod manufactured in the example of this invention is shown. 比較例において製造された石英ガラス棒の外径の変動状況を示す。The fluctuation | variation state of the outer diameter of the quartz glass rod manufactured in the comparative example is shown. 本発明例及び比較例において製造された石英ガラス棒の外径の変動状況の両方を、同スケールにて、示すものである。Both the fluctuation | variation conditions of the outer diameter of the quartz glass rod manufactured in this invention example and the comparative example are shown by the same scale.

符号の説明Explanation of symbols

11 石英ガラス素材
12 石英ガラス棒
13 入側ダミー材
14 出側ダミー材
15 入側チャック
16 出側チャック
17 ヒーター
20 成形延伸ダイス
21 入口開口部
22 延伸部
23 孔部
30 不活性ガスの導入孔
A 入口開口部の内径
B 孔部の内径
C 孔部の長さ
DESCRIPTION OF SYMBOLS 11 Quartz glass raw material 12 Quartz glass rod 13 Inlet side dummy material 14 Outlet side dummy material 15 Inlet side chuck 16 Outlet side chuck 17 Heater 20 Molding extending | stretching die 21 Inlet opening part 22 Extending part 23 Hole part 30 Inert gas introduction hole A Inner diameter of inlet opening B Inner diameter of hole C Length of hole

Claims (5)

棒状の石英ガラス素材を回転させつつ片端から順次加熱軟化させて軸方向に移動させ、その加熱軟化部分を成形延伸ダイスに送り込むことにより石英ガラス棒を製造する方法であって、石英ガラス素材の送り込み速度を調整することにより石英ガラス棒の外径を制御することを特徴とする石英ガラス棒の製造方法。   A method for producing a quartz glass rod by rotating a rod-like quartz glass material from one end while rotating and softening the rod-shaped quartz glass material in the axial direction, and feeding the heated and softened portion to a forming and drawing die. A method for producing a quartz glass rod, wherein the outer diameter of the quartz glass rod is controlled by adjusting the speed. 棒状の石英ガラス素材の成形状態の観察結果を用いて石英ガラス素材の送り込み速度を調整することを特徴とする、請求項1に記載の石英ガラス棒の製造方法。   The method for producing a quartz glass rod according to claim 1, wherein the feeding speed of the quartz glass material is adjusted using an observation result of a molding state of the rod-like quartz glass material. 棒状の石英ガラス素材の加熱軟化部分を成形延伸ダイスに送り込む際に、成形延伸ダイスの入口側開口部においてその加熱軟化部分の外径を一旦大きくした後、成形延伸ダイスの延伸部を経て孔部に送り込むことを特徴とする、請求項1又は2に記載の石英ガラス棒の製造方法。   When the heat-softened portion of the rod-shaped quartz glass material is fed into the forming and drawing die, the outer diameter of the heat-softening portion is once increased at the inlet side opening of the forming and drawing die, and then the hole is passed through the extending portion of the forming and drawing die. The method for producing a quartz glass rod according to claim 1, wherein the quartz glass rod is fed to the quartz glass rod. 成形延伸ダイスの内壁の軸方向の断面形状が、成形延伸ダイスの延伸部において曲線である成形延伸ダイスを用いることを特徴とする、請求項1から3までのいずれかに記載の石英ガラス棒の製造方法。   The quartz glass rod according to any one of claims 1 to 3, wherein a shape-drawing die having a cross-sectional shape in an axial direction of an inner wall of the shape-drawing die is a curve at a drawing portion of the shape-drawing die. Production method. 棒状の石英ガラス素材を回転可能な状態で把持するとともに軸方向に移動させるチャックと、棒状の石英ガラス素材を加熱するための加熱手段と、棒状の石英ガラス素材の加熱軟化部分を圧入させ所定の形状に成形するための成形延伸ダイスと、成形後の石英ガラス棒を回転可能な状態で把持するとともに軸方向に移動させるチャックを有する石英ガラス棒の製造装置であって、入口側開口部と延伸部と孔部からなる成形延伸ダイスの内壁の軸方向の断面形状が延伸部において曲線であることを特徴とする石英ガラス棒の製造装置。
A chuck for holding the rod-shaped quartz glass material in a rotatable state and moving it in the axial direction, a heating means for heating the rod-shaped quartz glass material, and a heating softening portion of the rod-shaped quartz glass material are press-fitted into a predetermined A quartz glass rod manufacturing apparatus having a forming and drawing die for forming into a shape and a chuck that holds the formed quartz glass rod in a rotatable state and moves it in the axial direction. An apparatus for producing a quartz glass rod, wherein an axial cross-sectional shape of an inner wall of a forming and drawing die comprising a portion and a hole is a curve in the extending portion.
JP2005184284A 2005-06-24 2005-06-24 Method and apparatus for producing quartz glass rod Active JP4464321B2 (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110540358A (en) * 2019-08-19 2019-12-06 湖州维德光电科技有限公司 Device for integrally forming bat

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110540358A (en) * 2019-08-19 2019-12-06 湖州维德光电科技有限公司 Device for integrally forming bat

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