JP2006193430A5 - - Google Patents
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- Publication number
- JP2006193430A5 JP2006193430A5 JP2005003718A JP2005003718A JP2006193430A5 JP 2006193430 A5 JP2006193430 A5 JP 2006193430A5 JP 2005003718 A JP2005003718 A JP 2005003718A JP 2005003718 A JP2005003718 A JP 2005003718A JP 2006193430 A5 JP2006193430 A5 JP 2006193430A5
- Authority
- JP
- Japan
- Prior art keywords
- organic solvent
- carboxylic acid
- containing compound
- unsaturated carboxylic
- vinyl group
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000003960 organic solvent Substances 0.000 claims description 10
- 150000001875 compounds Chemical class 0.000 claims description 8
- 238000004519 manufacturing process Methods 0.000 claims description 6
- 125000000391 vinyl group Chemical group [H]C([*])=C([H])[H] 0.000 claims description 6
- UHOVQNZJYSORNB-UHFFFAOYSA-N benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 claims description 4
- HEDRZPFGACZZDS-UHFFFAOYSA-N chloroform Chemical compound ClC(Cl)Cl HEDRZPFGACZZDS-UHFFFAOYSA-N 0.000 claims description 4
- YMWUJEATGCHHMB-UHFFFAOYSA-N methylene dichloride Chemical compound ClCCl YMWUJEATGCHHMB-UHFFFAOYSA-N 0.000 claims description 4
- 239000000243 solution Substances 0.000 claims description 4
- YXFVVABEGXRONW-UHFFFAOYSA-N toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 claims description 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 4
- WSLDOOZREJYCGB-UHFFFAOYSA-N 1,2-dichloroethane Chemical compound ClCCCl WSLDOOZREJYCGB-UHFFFAOYSA-N 0.000 claims description 2
- FDPIMTJIUBPUKL-UHFFFAOYSA-N 3-Pentanone Chemical compound CCC(=O)CC FDPIMTJIUBPUKL-UHFFFAOYSA-N 0.000 claims description 2
- JHIVVAPYMSGYDF-UHFFFAOYSA-N Cyclohexanone Chemical compound O=C1CCCCC1 JHIVVAPYMSGYDF-UHFFFAOYSA-N 0.000 claims description 2
- NTIZESTWPVYFNL-UHFFFAOYSA-N Methyl isobutyl ketone Chemical compound CC(C)CC(C)=O NTIZESTWPVYFNL-UHFFFAOYSA-N 0.000 claims description 2
- 239000007864 aqueous solution Substances 0.000 claims description 2
- FUZZWVXGSFPDMH-UHFFFAOYSA-M caproate Chemical compound CCCCCC([O-])=O FUZZWVXGSFPDMH-UHFFFAOYSA-M 0.000 claims description 2
- 238000004140 cleaning Methods 0.000 claims description 2
- UFHFLCQGNIYNRP-UHFFFAOYSA-N hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims description 2
- 229910052739 hydrogen Inorganic materials 0.000 claims description 2
- 239000001257 hydrogen Substances 0.000 claims description 2
- FGKJLKRYENPLQH-UHFFFAOYSA-M isocaproate Chemical compound CC(C)CCC([O-])=O FGKJLKRYENPLQH-UHFFFAOYSA-M 0.000 claims description 2
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 claims description 2
- CTQNGGLPUBDAKN-UHFFFAOYSA-N o-xylene Chemical compound CC1=CC=CC=C1C CTQNGGLPUBDAKN-UHFFFAOYSA-N 0.000 claims description 2
- 230000002194 synthesizing Effects 0.000 claims description 2
- 238000005406 washing Methods 0.000 claims description 2
- 239000008096 xylene Substances 0.000 claims description 2
- 150000001732 carboxylic acid derivatives Chemical class 0.000 claims 3
- 239000002184 metal Substances 0.000 claims 2
- 150000003839 salts Chemical class 0.000 claims 2
- 239000011780 sodium chloride Substances 0.000 claims 2
- 230000000875 corresponding Effects 0.000 claims 1
- 229920000647 polyepoxide Polymers 0.000 claims 1
Description
で表される化合物を合成する工程、その後その反応液に有機溶媒を添加し、該溶液に対して水溶液及び／または純水で１回以上洗浄する工程を含むビニル基含有化合物の製造方法であって、該洗浄工程で用いる有機溶媒として、溶解度パラメータが８．３以上、かつ該有機溶媒の水への溶解度が３％以下の有機溶媒を用いることを特徴とするビニル基含有化合物の製造方法、
（ここで、Ｒ１は水素またはメチル基を表す。）
（２）前記の有機溶媒がベンゼン、トルエン、キシレン、ジクロロメタン、クロロホルム、ジクロロエタン、メチルイソブチルケトン、ジエチルケトン、シクロヘキサノン、酢酸ｎ−ブチル、酢酸イソブチルからなる群から選ばれた少なくとも１種であることを特徴とする前記（１）に記載のビニル基含有化合物の製造方法、である。
A method for producing a vinyl group-containing compound, which comprises a step of synthesizing the compound represented by the formula, then adding an organic solvent to the reaction solution , and washing the solution with an aqueous solution and / or pure water at least once. Te, as the organic solvent used in the cleaning step, the solubility parameter is 8.3 or more, and a manufacturing method of a vinyl group-containing compound whose solubility in water of the organic solvent is characterized by using a 3% organic solvents,
(Here, R 1 represents hydrogen or a methyl group.)
(2) The organic solvent is at least one selected from the group consisting of benzene, toluene, xylene, dichloromethane, chloroform, dichloroethane, methyl isobutyl ketone, diethyl ketone, cyclohexanone, n-butyl acetate, and isobutyl acetate. A method for producing a vinyl group-containing compound as described in (1) above.
Claims (2)
（ここで、Ｒ１は水素またはメチル基を表す。） The following formula (a1)
(Here, R 1 represents hydrogen or a methyl group.)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2005003718A JP4572684B2 (en) | 2005-01-11 | 2005-01-11 | Method for producing vinyl group-containing compound |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2005003718A JP4572684B2 (en) | 2005-01-11 | 2005-01-11 | Method for producing vinyl group-containing compound |
Related Child Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2010144705A Division JP5370283B2 (en) | 2010-06-25 | 2010-06-25 | Manufacturing method of medical device |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2006193430A JP2006193430A (en) | 2006-07-27 |
| JP2006193430A5 true JP2006193430A5 (en) | 2008-02-28 |
| JP4572684B2 JP4572684B2 (en) | 2010-11-04 |
Family
ID=36799785
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2005003718A Active JP4572684B2 (en) | 2005-01-11 | 2005-01-11 | Method for producing vinyl group-containing compound |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JP4572684B2 (en) |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US8569538B2 (en) * | 2006-06-30 | 2013-10-29 | Johnson & Johnson Vision Care, Inc. | Acryloyl materials for molded plastics |
| JP5370283B2 (en) * | 2010-06-25 | 2013-12-18 | 東レ株式会社 | Manufacturing method of medical device |
| JP5811133B2 (en) * | 2013-04-26 | 2015-11-11 | 東レ株式会社 | Method for producing vinyl group-containing compound |
Family Cites Families (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS60336B2 (en) * | 1975-01-23 | 1985-01-07 | 東亞合成株式会社 | Production method of ester |
| JP2000297062A (en) * | 1999-04-14 | 2000-10-24 | Dainippon Ink & Chem Inc | Production of hydroxyalkyl (meth)acrylate |
-
2005
- 2005-01-11 JP JP2005003718A patent/JP4572684B2/en active Active
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