JP2005193405A - Fluffy bamboo fiber manufacturing method - Google Patents

Fluffy bamboo fiber manufacturing method Download PDF

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JP2005193405A
JP2005193405A JP2003435317A JP2003435317A JP2005193405A JP 2005193405 A JP2005193405 A JP 2005193405A JP 2003435317 A JP2003435317 A JP 2003435317A JP 2003435317 A JP2003435317 A JP 2003435317A JP 2005193405 A JP2005193405 A JP 2005193405A
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bamboo
temperature
steamed
fiber
defibrated
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JP4314569B2 (en
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Katsuhiro Nakahara
勝弘 中原
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Kiyomoto Iron & Machinery Work
Kiyomoto Iron and Machinery Works Co Ltd
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Kiyomoto Iron and Machinery Works Co Ltd
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Abstract

<P>PROBLEM TO BE SOLVED: To provide a fluffy bamboo fiber manufacturing method capable of efficiently obtaining a fluffy bamboo fiber bundle suitable for manufacturing a fiberboard. <P>SOLUTION: A bamboo material cut so as to leave an interval in its longitudinal direction is compressed and torn to be formed into a flat plate shape under compression. The flat plate-shaped bamboo material formed under compression is steamed under a heated steam atmosphere and the steamed bamboo material is fibrillated under normal pressure at a temperature higher than the normal temperature to manufacture fluffy bamboo fibers. The bamboo fibers can be easily entangled with each other by forming the bamboo fibers into a fluffy state. <P>COPYRIGHT: (C)2005,JPO&NCIPI

Description

本発明は、綿状の竹繊維の製造方法に関し、特に、高質の繊維板の製造に適した綿状の竹繊維の製造方法に関する。   The present invention relates to a method for producing cotton-like bamboo fibers, and more particularly to a method for producing cotton-like bamboo fibers suitable for producing high-quality fiberboard.

繊維板、例えば、中質繊維板〔ミディアムデンシティファイバーボード、即ちMDF(JIS A 5905参照)〕は、木材又は木材以外の植物繊維を原料として、合成樹脂接着剤を繊維同士を接着する接着剤として加えて熱圧縮加工により成形した繊維板であり、密度が0.35g/cm以上0.80g/cm未満と軽く、均質で方向性がなく、加工性及び表面平滑性に優れている。しかし、使用される繊維の長さが短いために、水平方向に繊維が並ぶ合板に比して強度が劣る点が欠点とされている。また、このような繊維板を製造する原料となる繊維は、多くは木の伐採により得られている。しかし、木は炭酸同化作用により、空気中の二酸化炭素を取入れて、有機物を合成し、酸素を放出するために、空気中の二酸化炭素濃度の低減及び酸素の再生といった地球環境の保護の上で貴重とされており、しかも、木は伐採できるまでに要する生長期間が数十年と長く、伐採後の森林の回復には長い年月を要することとなるために、伐採して木材資源を得ることが難しくなっている。これに対して、竹は、木に比して生長が早く、しかも、竹の稈を挿して簡単に増殖することができ、寿命は60年とも100年とも言われ、木材繊維の代替として注目されている。 A fiberboard, for example, a medium fiberboard (medium density fiberboard, that is, MDF (see JIS A 5905)) is made of wood or plant fibers other than wood as a raw material, and a synthetic resin adhesive is used as an adhesive for bonding the fibers together. In addition, it is a fiberboard formed by hot compression processing. The density is as light as 0.35 g / cm 2 or more and less than 0.80 g / cm 2 , is homogeneous and has no directionality, and has excellent workability and surface smoothness. However, since the length of the fiber used is short, the strength is inferior to the plywood in which the fibers are arranged in the horizontal direction. Moreover, many of the fibers that are the raw materials for producing such fiberboard are obtained by cutting down trees. However, because of the carbon dioxide assimilation effect, trees take in carbon dioxide in the air, synthesize organic matter, and release oxygen. In order to protect the global environment, such as reducing the concentration of carbon dioxide in the air and regenerating oxygen. It is considered valuable, and it takes a long period of time, which is several decades, until trees can be cut down, and it takes a long time to recover the forest after cutting down. It has become difficult. On the other hand, bamboo grows faster than wood, and can be easily propagated by inserting bamboo shoots. Its lifespan is said to be 60 years or 100 years. Has been.

そこで、竹繊維は、例えば、所定長さに切断された竹を、ロールで押し潰し、この押し潰された竹を、ハンマーミル等で叩いて解繊して製造する方法、及び竹を押し潰した状態の短冊状竹片とした上で解繊機の側面から解繊機内に送り込み短冊状竹片を解繊して所定の径まで解繊された竹繊維を製造する方法が示されている(例えば、特開2000−71209号公報参照)。また、竹を所定長さに切断し、切断された竹を圧力容器内に充填し、この圧力容器内に加熱加圧された水蒸気を導入して、竹を加熱加圧状態とし、瞬時に非加圧状態に圧力を低下させて、竹を爆砕して、竹繊維を製造し、この竹繊維を補強繊維とする補強繊維プラスチック成形体が提案されている(例えば、特開2003−253011公報参照)。またその他に、椰子、麻、砂糖黍、竹、稲又はケナフなどのリグノセルロース繊維は、熱水で処理して、熱水可溶成分を溶解除去して取出すことができ、この取出されたリグノセルロース繊維を接着剤と混合して、熱及び圧力を加えて板状に形成した繊維板とする方法が提案されている(特開2000−102910号公報参照)。
特開2000−102910号公報 特開2000−71209号公報 特開2003−253011号公報
Therefore, the bamboo fiber is produced by, for example, crushing bamboo cut into a predetermined length with a roll, and smashing the crushed bamboo with a hammer mill or the like, and crushing the bamboo. A method for producing bamboo fiber that has been defibrated to a predetermined diameter by sending it into the defibrator from the side of the defibrating machine and then defibrating the strip-shaped bamboo slab after having been made into a strip-shaped bamboo piece in a state of being in a state ( For example, refer to Japanese Unexamined Patent Publication No. 2000-71209. In addition, the bamboo is cut into a predetermined length, the cut bamboo is filled into a pressure vessel, and steam heated and pressurized is introduced into the pressure vessel to bring the bamboo into a heated and pressurized state. There has been proposed a reinforced fiber plastic molding in which pressure is reduced to a pressurized state, bamboo is crushed to produce bamboo fibers, and the bamboo fibers are used as reinforcing fibers (see, for example, Japanese Patent Application Laid-Open No. 2003-253011). ). In addition, lignocellulosic fibers such as coconut, hemp, sugar cane, bamboo, rice or kenaf can be removed by treating with hot water to dissolve and remove hot water soluble components. A method has been proposed in which fibers are mixed with an adhesive to form a fiberboard formed by applying heat and pressure to form a fiberboard (see Japanese Patent Application Laid-Open No. 2000-102910).
JP 2000-102910 A JP 2000-71209 A JP 2003-253011 A

しかし、竹をハンマーミルにより解繊する場合、一般には、供給口が、回転するハンマーの刃の面に向けて略垂直に設けられるので、破砕される押し潰された竹片は、ハンマーミルの回転するハンマーの刃の面前に突き出るように供給されることになり、押し潰された竹片はその長手方向で破断されて、ほとんどが短繊維や粉末となり、10mmを越える竹の長繊維を製造することが難しい。このような短繊維で作られた繊維板は、繊維長が比較的短いために、合板に比して強度が小さく問題とされている。そこで、押し潰された竹片をハンマーミルの回転するハンマーの刃に並行に供給して竹の長繊維を製造することが提案されている(特開2000−71209号公報参照)。しかし、このようにしても、得られた竹繊維は比較的直線状で折れ易く、30mmを越える長い竹繊維を歩留まり良く得ることは難しく問題とされている。そこで、所定長さに切断した竹材を圧力釜内で100℃以上の温度及び該温度に対応する水蒸気圧下に加熱及び加圧する加熱加圧操作と、圧力缶内の圧力を急速に解放する減圧操作とを繰り返し行って、竹繊維を痛めることなく相互に分離して、所定長さの竹繊維を得ることが提案されている(特開2003−155677号公報参照)。しかし、加熱加圧操作と減圧操作の繰り返し回数が多く、得られるのは繊維間を引き裂いて得られる所定長さの長繊維の束であり、径が0.1ミリメートル乃至数十ミクロンの全体的に綿状を呈する絡み具合の良い繊維板の原料に適した比較的長い竹繊維束を得ることは難しい。
本発明は、従来の繊維板の製造に使用される竹繊維に係る問題点を解決することを目的としている。
However, when bamboo is defibrated by a hammer mill, the supply port is generally provided substantially perpendicularly to the surface of the rotating hammer blade, so that the crushed bamboo pieces to be crushed are The crushed bamboo pieces will be broken in the longitudinal direction and become mostly short fibers and powder, producing bamboo long fibers exceeding 10 mm. Difficult to do. A fiberboard made of such short fibers has a relatively short fiber length, and therefore has a problem that its strength is smaller than that of plywood. Therefore, it has been proposed to produce bamboo long fibers by supplying the crushed bamboo pieces in parallel to the rotating hammer blade of a hammer mill (see Japanese Patent Laid-Open No. 2000-71209). However, even in this case, the obtained bamboo fiber is relatively straight and easily broken, and it is difficult to obtain a long bamboo fiber exceeding 30 mm with a good yield. Therefore, a heating and pressurizing operation for heating and pressurizing bamboo cut into a predetermined length in a pressure cooker at a temperature of 100 ° C. or higher and a water vapor pressure corresponding to the temperature, and a depressurizing operation for rapidly releasing the pressure in the pressure can It is proposed that the bamboo fibers are separated from each other without damaging them to obtain bamboo fibers having a predetermined length (see Japanese Patent Application Laid-Open No. 2003-155679). However, the number of repetitions of the heating and pressurizing operation and the depressurizing operation is large, and what is obtained is a bundle of long fibers of a predetermined length obtained by tearing between the fibers, and the overall diameter is 0.1 millimeters to several tens of microns. It is difficult to obtain a relatively long bamboo fiber bundle suitable for a raw material for a fiberboard having a good entanglement condition.
An object of this invention is to solve the problem concerning the bamboo fiber used for manufacture of the conventional fiber board.

本発明は、繊維板を製造するのに適した綿状の竹繊維束を効率よく得ることができる竹繊維の製造方法を提供する。
即ち、本発明は、竹材を高温高圧水蒸気の存在下に蒸煮し、蒸煮された竹材を常圧下で常温を越える温度下で解繊することを特徴とする綿状の竹繊維の製造方法にあり、また、本発明は、長手方向に間隔を以って裁断された竹材を圧縮して、開裂させて、平板状に圧縮形成し、圧縮形成された平板状の竹材を、加熱水蒸気の雰囲気下で蒸煮し、蒸煮された竹材を、常圧下で、常温より高い温度下で解繊することを特徴とする綿状の竹繊維の製造方法にあり、さらに、本発明は、200cm以下の長さに裁断された竹材を圧縮して、開裂させて、厚さ20mm以下の平板状に圧縮形成し、圧縮形成された平板状の竹材を、加熱水蒸気の雰囲気下で蒸煮し、蒸煮された竹材を、1分以上の時間を掛けて常圧にまで圧力を下げ、常圧下で、常温より高い温度で解繊することを特徴とする綿状の竹繊維の製造方法にあり、さらにまた、本発明は、長さ10乃至200cmに分割切断された竹材を圧縮して、開裂させて、厚さ5乃至20mmの平板状に形成し、圧縮されて平板状に形成された竹材を、100乃至200℃の温度及び0.1乃至1.6MPaの圧力を有する加熱水蒸気の雰囲気内で蒸煮し、蒸煮された竹材を1分以上の時間を掛けて減圧し、次いで、大気圧及び50℃以上の温度を有する雰囲気内で、解繊することを特徴とする綿状の竹繊維の製造方法にあり、さらに加えて、本発明は、長さ10乃至200cmに分割切断された竹材を圧縮して、開裂させて、厚さ5乃至20mmの平板状に形成し、圧縮されて平板状に形成された竹材を、100乃至200℃の温度及び0.1乃至1.6MPaの圧力を有する加熱水蒸気の雰囲気内で5乃至60分間蒸煮し、蒸煮された竹材を5乃至10分間で常圧まで減圧して、50乃至100℃の温度及び10乃至30重量%の含水率を有する状態にして、少なくとも一方の切刃が回転刃である粗解繊機により、粗解繊を行って、厚さが0.1乃至1.0mmの粗解繊繊維束を形成し、次いで、この粗解繊繊維束を、大気圧下で、50乃至100℃の温度及び10乃至30重量%の含水率を有する状態にして、少なくとも一方の解繊刃が回転刃である精解繊装置による高速回転により、さらに精解繊して、直径が0.01乃至0.2mmの繊維束を製造することを特徴とする綿状の竹繊維の製造方法にあり、さらにこれらの他に、本発明は、長さ10乃至200cmに分割切断された竹材を圧縮して、開裂させて、厚さ5乃至20mmの平板状に形成し、圧縮されて平板状に形成された竹材を、100乃至200℃の温度及び0.1乃至1.6MPaの圧力を有する加熱水蒸気の雰囲気内で5乃至60分間蒸煮し、蒸煮された竹材を5乃至10分間で常圧まで減圧して、50乃至100℃の温度及び10乃至30重量%の含水率を有する状態にして、少なくとも一方の切刃が回転刃である粗解繊機により、粗解繊を行って、厚さが0.1乃至1.0mmの粗解繊繊維束を形成し、次いで、この粗解繊繊維束を、大気圧下で、50℃以上の温度及び10乃至30重量%の含水率を有する状態にして、少なくとも一方の切刃が棒状の回転刃である精解繊装置による高速回転により、さらに精解繊して、直径が0.01乃至0.2mmで、長さが1乃至100mmの精解繊繊維束を製造することを特徴とする綿状の竹繊維の製造方法にある。本発明において、蒸煮雰囲気を、130乃至160℃の温度及び0.28乃至0.64MPaの圧力を有する雰囲気とすることが好ましく、また、竹材の解繊は、切削角度が50乃至80度で予め粗解繊を行い、次いで、1000乃至6000rpmの回転数で行われることが好ましい。本発明において、竹繊維は、綿状を呈するものであり、直径が10乃至200ミクロン又は直径が10乃至200ミクロン及び長さが1乃至100mmの綿繊維状とするのが好ましい。
The present invention provides a method for producing bamboo fiber, which can efficiently obtain a cotton-like bamboo fiber bundle suitable for producing a fiberboard.
That is, the present invention lies in a method for producing cotton-like bamboo fibers, characterized in that bamboo is steamed in the presence of high-temperature and high-pressure steam, and the steamed bamboo is defibrated at a temperature exceeding normal temperature under normal pressure. Further, the present invention compresses bamboo material cut at intervals in the longitudinal direction, cleaves it, compresses it into a flat plate, and forms the compressed flat bamboo material under the atmosphere of heated steam. In the method for producing cotton-like bamboo fiber, characterized in that the bamboo material cooked and steamed at room temperature is defibrated under normal pressure and at a temperature higher than room temperature, and the present invention has a length of 200 cm or less. The bamboo material cut into pieces is compressed and cleaved to form a flat plate with a thickness of 20 mm or less, and the compressed flat plate-like bamboo material is cooked in a heated steam atmosphere. Take the time of 1 minute or more to lower the pressure to normal pressure. The present invention relates to a method for producing cotton-like bamboo fibers characterized by defibration at a high temperature. Furthermore, the present invention compresses and cleaves bamboo material that has been divided and cut to a length of 10 to 200 cm, The bamboo material formed into a flat plate shape of 5 to 20 mm and compressed into a flat plate shape is cooked in an atmosphere of heated steam having a temperature of 100 to 200 ° C. and a pressure of 0.1 to 1.6 MPa, There is a method for producing cotton-like bamboo fibers, characterized in that steamed bamboo is depressurized over a period of one minute or longer and then defibrated in an atmosphere having an atmospheric pressure and a temperature of 50 ° C. or higher. In addition, in the present invention, bamboo material divided and cut to a length of 10 to 200 cm is compressed and cleaved to form a flat plate having a thickness of 5 to 20 mm, and compressed into a flat plate. Bamboo wood is heated at a temperature of 100 to 200 ° C. and 0. Steamed in an atmosphere of heated steam having a pressure of 1 to 1.6 MPa for 5 to 60 minutes, and the steamed bamboo material is decompressed to normal pressure in 5 to 10 minutes to a temperature of 50 to 100 ° C. and 10 to 30% by weight. In a state having a water content of at least one of the cutting blades, a rough defibrating machine having a rotary blade is used to perform rough defibrating to form a defibrated fiber bundle having a thickness of 0.1 to 1.0 mm. Then, this coarse defibrated fiber bundle is brought into a state having a temperature of 50 to 100 ° C. and a moisture content of 10 to 30% by weight under atmospheric pressure, and at least one defibrating blade is a rotary blade. A cotton-like bamboo fiber manufacturing method characterized in that a fiber bundle having a diameter of 0.01 to 0.2 mm is manufactured by further fine disentanglement by high-speed rotation by a fiber device. The present invention is divided and cut into lengths of 10 to 200 cm. The bamboo material is compressed and cleaved to form a flat plate having a thickness of 5 to 20 mm, and the compressed bamboo material is formed into a flat plate with a temperature of 100 to 200 ° C. and 0.1 to 1.6 MPa. Steamed in an atmosphere of heated steam having a pressure of 5 to 60 minutes and reduced the steamed bamboo material to normal pressure in 5 to 10 minutes to a temperature of 50 to 100 ° C. and a moisture content of 10 to 30% by weight. In a state of having a rough defibrating fiber bundle having a thickness of 0.1 to 1.0 mm by performing rough defibrating with a rough defibrating machine in which at least one of the cutting blades is a rotary blade, A high speed by a fine defibrating apparatus in which a crude defibrated fiber bundle is brought into a state having a temperature of 50 ° C. or higher and a moisture content of 10 to 30% by weight at atmospheric pressure, and at least one of the cutting edges is a rod-shaped rotary blade Further defibration by rotation, the diameter is 0.01 to 0 In 2 mm, in the manufacturing method of the shaped bamboo fiber cotton, characterized in that the length to produce a fine fibrillated fiber bundle 1 to 100 mm. In the present invention, the steaming atmosphere is preferably an atmosphere having a temperature of 130 to 160 ° C. and a pressure of 0.28 to 0.64 MPa, and the bamboo material is defibrated in advance at a cutting angle of 50 to 80 degrees. It is preferable that rough defibration is performed and then performed at a rotational speed of 1000 to 6000 rpm. In the present invention, the bamboo fiber has a cotton shape, and preferably has a diameter of 10 to 200 microns or a diameter of 10 to 200 microns and a length of 1 to 100 mm.

本発明は、長手方向に間隔を以って裁断された竹材を圧縮して、開裂させて、平板状に圧縮形成し、圧縮形成された平板状の竹材を、加熱水蒸気の雰囲気下で蒸煮し、蒸煮された竹材を、常圧下で、常温より高い温度下で粗解繊し、次いで精解繊することにより竹繊維を製造するので、互いに絡み易く、繊維板の補強繊維に適した比較的細い綿状の竹繊維を製造することができる。   The present invention compresses bamboo material cut at intervals in the longitudinal direction, cleaves it, compresses it into a flat plate shape, and steams the compression-formed flat bamboo material in an atmosphere of heated steam. The bamboo fiber is produced by rough defibration of the cooked bamboo under normal pressure at a temperature higher than room temperature, and then finely defibrating. Fine cotton-like bamboo fibers can be produced.

本発明において、竹繊維は、繊維板の強度を大きくするために、互いに絡み易いように綿状に形成される。本発明において、竹繊維を綿状に形成するために、竹は長さ10乃至200cmに輪切りに切断される。輪切りにされた円筒状の竹を、直径方向に押圧することにより圧砕して、厚さが5乃至20mmの平板状の竹材を形成する。このように形成された竹材は、水分を含有して柔軟になるように高温及び高圧下において蒸煮される。この竹材の蒸煮処理は、100乃至200℃、好ましくは、130乃至160℃の蒸煮温度、及び0.1乃至1.6MPa、好ましくは、0.28乃至0.64MPaの蒸煮加熱蒸気圧力を有する雰囲気内に、5乃至60分間、好ましくは20乃至30分間の蒸煮時間の間放置させて、蒸煮処理される。   In the present invention, the bamboo fibers are formed in a cotton shape so as to be easily entangled with each other in order to increase the strength of the fiberboard. In the present invention, in order to form bamboo fibers into a cotton shape, the bamboo is cut into a length of 10 to 200 cm. The cylindrical bamboo cut into circles is crushed by pressing in the diametrical direction to form a flat bamboo material having a thickness of 5 to 20 mm. The bamboo material thus formed is steamed under high temperature and high pressure so as to be soft and contain moisture. The bamboo is steamed in an atmosphere having a steaming temperature of 100 to 200 ° C., preferably 130 to 160 ° C., and steaming steam pressure of 0.1 to 1.6 MPa, preferably 0.28 to 0.64 MPa. It is allowed to stand for 5 to 60 minutes, preferably 20 to 30 minutes, and is cooked.

本発明において、蒸煮により水分を含有して柔軟になった平板状の竹材は、柔軟性を保持させながら、粗解繊され、次いで精解繊される。蒸煮処理は、単一式又は連続式に行うことができる。単一式の場合、蒸煮装置内は、蒸煮処理後に開放されて、蒸煮処理温度及び圧力は、常温及び常圧に戻される。本発明者は、蒸煮処理された平板状の竹材の保有温度が常温に低下させ、またその含水率を10%よりに低下させると、解繊しても絡み合い易い綿状の竹繊維が得られないことを発見した。   In the present invention, the flat bamboo material softened by containing moisture by steaming is roughly defibrated and then finely defibrated while maintaining flexibility. The steaming process can be performed in a single mode or a continuous mode. In the case of a single type, the inside of the cooking apparatus is opened after the steaming process, and the steaming process temperature and pressure are returned to room temperature and normal pressure. The inventor of the present invention can obtain a cotton-like bamboo fiber that is easily entangled even when fibrillated when the holding temperature of the steamed flat bamboo material is lowered to room temperature and the moisture content is reduced to less than 10%. I found no.

そこで、本発明においては、蒸煮処理された竹材は、蒸煮後において、その含有水分を外気に逃散して柔軟さを失わないように、例えば、蒸煮装置内で保温及び保湿されるのが好ましい。この場合、蒸煮装置内の圧力及び温度は、蒸煮処理後、常圧及び常温に降下させるが、蒸煮された平板状の竹材が、含有水分が外気に逃散して、柔軟さが失われないように、例えば、その保有水分が、10%以上、好ましくは10乃至30%の範囲内に保たれ、保有温度が、50℃以上、好ましくは50乃至100℃の温度範囲内にあるように、保温及び保湿される。このために、蒸煮された平板状の竹材を収容する蒸煮装置内は、1乃至20分、好ましくは、5乃至10分掛けて、常圧にまで減圧され、放冷され、放湿される。   Therefore, in the present invention, it is preferable that the steamed bamboo material is kept warm and moisturized in, for example, a steaming apparatus so that the moisture contained in the steamed material escapes to the outside air and does not lose flexibility. In this case, the pressure and temperature in the steaming device are lowered to normal pressure and room temperature after the steaming process, but the steamed flat bamboo material does not lose its flexibility because the contained moisture escapes to the outside air. In addition, for example, the retained moisture is kept within a range of 10% or more, preferably 10 to 30%, and the retained temperature is within a temperature range of 50 ° C. or more, preferably 50 to 100 ° C. And moisturized. For this purpose, the inside of the steaming apparatus for storing the cooked flat bamboo material is reduced to normal pressure over 1 to 20 minutes, preferably 5 to 10 minutes, allowed to cool, and then dried.

本発明において、蒸煮された平板状の竹材は、粗解繊装置により粗解繊される。この粗解繊装置は、従来の解繊装置を使用することができる。本発明において、粗解繊装置により解繊される平板状の竹材は、綿状の竹繊維を得るためには、その保有水分が、10%以上、好ましくは10乃至30%の範囲内で、保有温度が、50℃以上、好ましくは50乃至100℃の温度範囲内にあることが必要であることが分かった。そこで。本発明においては、粗解繊装置により解繊される平板状の竹材は、保管室又は保温保湿装置において、その保有水分が10%以上、好ましくは10乃至30%の範囲内で、保有温度が50℃以上、好ましくは50乃至100℃の温度範囲内にあるように、保温保湿される。保有水分、即ち、含水率が10%より低いと綿状の竹繊維を製造するのが難しく、また、保有水分、即ち、含水率が30%より高くする綿状の竹繊維を得るのが難しい。   In the present invention, the cooked flat bamboo material is coarsely defibrated by a coarse defibrating device. This rough defibrating apparatus can use a conventional defibrating apparatus. In the present invention, the flat bamboo material to be defibrated by the coarse defibrating apparatus has a moisture content of 10% or more, preferably 10 to 30%, in order to obtain cotton-like bamboo fibers. It has been found that the holding temperature needs to be in the temperature range of 50 ° C. or higher, preferably 50 to 100 ° C. there. In the present invention, the flat bamboo material to be defibrated by the coarse defibrating device has a retained water content of 10% or more, preferably 10 to 30% in the storage room or the heat and moisture retaining device, and has a retained temperature. It is kept warm and moisturized so that it is in the temperature range of 50 ° C. or higher, preferably 50 to 100 ° C. It is difficult to produce cotton-like bamboo fibers when the moisture content, ie, the moisture content is lower than 10%, and it is difficult to obtain cotton-like bamboo fibers whose moisture content, ie, the moisture content is higher than 30%. .

このように保温保湿された平板状の竹材は、例えば、内側に切刃が形成されているスクリーンを備える外筒と、外筒内で回動可能に設けられ、外側に切刃が設けられ回転可能に設けられている内筒を備える粗解繊装置により粗解繊される。この粗解繊装置の粗解繊時において、外筒は静止して、固定刃として作用し、内筒は、回転させて回転刃として作用させることができる。この粗解繊装置は、外筒の固定刃と内筒の回転刃が、夫々の刃筋の交差角度(切削角度)、が50°以上、好ましくは50乃至80°の角度となるように配置されているのが好ましく、回転刃の切込み厚さが、0.1mm以上、好ましくは0.1乃至1.0mmの繊維束を通すスクリーンを備えているのが好ましい。しかし、本発明において、粗解繊装置においては、外筒と内筒を共に回転刃に形成することができる。   The flat bamboo material that is kept warm and moisturized in this way is provided, for example, with an outer cylinder having a screen with a cutting blade formed on the inner side and a rotatable inside the outer cylinder, and with a cutting blade provided on the outer side and rotating. Rough defibrating is performed by a rough defibrating apparatus having an inner cylinder provided as possible. At the time of rough defibration of this rough defibrating apparatus, the outer cylinder can be stationary and act as a fixed blade, and the inner cylinder can be rotated to act as a rotary blade. This rough defibrating apparatus is arranged so that the fixed blade of the outer cylinder and the rotary blade of the inner cylinder have an angle of intersection (cutting angle) of their respective blade lines of 50 ° or more, preferably 50 to 80 °. It is preferable to provide a screen for passing a fiber bundle having a cutting blade thickness of 0.1 mm or more, preferably 0.1 to 1.0 mm. However, in the present invention, in the coarse defibrating apparatus, both the outer cylinder and the inner cylinder can be formed on the rotary blade.

本発明において、粗解繊された繊維束は、精解繊装置によりさらに細い竹繊維に解繊される。この精解繊装置は、従来の細かい繊維束に解繊できる精解繊装置を使用することができる。本発明において、精解繊装置は、例えば、棒状に形成されている解繊ピンが固定されて、互いに対向する板状乃至薄い皿型の回転体と、その外周にスクリーンを備えており、解繊時には、互いに対向する板状又は薄い皿型の回転体の夫々に設けられている解繊ピン間の剪断作用により綿状に解繊される。この精解繊装置において、解繊ピンは、互いに対向する板状乃至薄い皿型の回転体に一以上設けられる。この場合、解繊ピンは複数個を設けることができる。解繊ピンを複数個設ける場合には、複数個を一列に設けてもよく、また同心状に複数段に設けてもよい。何れの精解繊装置においても、解繊時、解繊ピンを備える板状回転体は、1,000rpm以上、好ましくは、1,000乃至6,000rpmの回転数で回転され、粗解繊された繊維束は、対向する板状乃至薄い皿型の回転体の解繊ピンの剪断作用により、例えば、直径が10乃至200μ(ミクロン)の繊維束又は直径が10乃至200μで長さが1乃至100mmの繊維束に解繊される。本発明において、精解繊装置のスクリーンは、これらの精解繊された細い繊維束を通すように形成される。本発明において、互いに対向する板状乃至薄い皿型の回転体を備える精解繊装置により精解繊を行う場合には、一方の板状乃至薄い皿型の回転体を停止した状態とし、他方の板状乃至薄い皿型の回転体のみを高速回転させても良いが、双方の板状乃至薄い皿型の回転体を互いに異なる方向に回転させても良い。   In the present invention, the coarsely defibrated fiber bundle is defibrated into finer bamboo fibers by a fine defibrating device. As this defibrating device, a defibrating device that can be defibrated into a conventional fine fiber bundle can be used. In the present invention, the defibrating apparatus includes, for example, a plate-shaped or thin dish-shaped rotating body that is fixed to a defibrating pin formed in a bar shape, and a screen on the outer periphery thereof. At the time of fibering, the fibers are defibrated in a cotton shape by a shearing action between defibrating pins provided in each of plate-like or thin dish-shaped rotating bodies facing each other. In this fine defibrating apparatus, one or more defibrating pins are provided on plate-shaped or thin dish-shaped rotating bodies facing each other. In this case, a plurality of defibrating pins can be provided. When a plurality of defibration pins are provided, the plurality may be provided in a row, or may be provided concentrically in a plurality of stages. In any fine defibrating apparatus, at the time of defibrating, the plate-like rotating body provided with the defibrating pins is rotated at a rotational speed of 1,000 rpm or more, preferably 1,000 to 6,000 rpm, and is roughly defibrated. The fiber bundle is, for example, a fiber bundle having a diameter of 10 to 200 μm (micron) or a diameter of 10 to 200 μ and a length of 1 to 1 due to the shearing action of the defibration pins of the opposing plate-shaped or thin dish-shaped rotating body. It is defibrated into a 100 mm fiber bundle. In the present invention, the screen of the fine fiber apparatus is formed so as to pass these fine fiber bundles that have been fine fiber. In the present invention, when fine defibrating is performed by a fine defibrating apparatus including plate-shaped or thin dish-shaped rotating bodies facing each other, one plate-shaped or thin dish-shaped rotating body is stopped and the other Only the plate-shaped or thin dish-shaped rotating body may be rotated at high speed, but both the plate-shaped or thin dish-shaped rotating bodies may be rotated in different directions.

以下に、例を示して、本発明の実施の態様を説明するが、本発明は以下の例示及び説明により何ら限定されるものではない。   Hereinafter, embodiments of the present invention will be described with reference to examples, but the present invention is not limited to the following examples and explanations.

1.竹材の分割切断と圧砕
長さ30cmに切出した肉厚が10mm程度の円筒状の竹材を、縦に6分割して、1個の切出した竹材当たり、6個の円弧状の竹片を得た。この円弧状の竹片の内側の節を取除き、押し潰すようにして圧砕し、平板状の竹片を製造した。
1. Divided cutting and crushing of bamboo material Cylindrical bamboo material with a thickness of about 10 mm, cut to a length of 30 cm, was divided vertically into 6 pieces to obtain 6 arc-shaped bamboo pieces per piece of bamboo material cut out. . The arc-shaped bamboo pieces were removed from the inner nodes, and crushed and crushed to produce flat bamboo pieces.

2.蒸煮処理
圧砕された竹片を蒸煮装置に入れて、0.43MPaの加圧飽和水蒸気を蒸煮装置内に供給した。蒸煮装置内に加圧飽和水蒸気を10分程供給して、蒸煮装置内の温度を、145℃に上昇させた。その後、蒸煮装置内を、温度145℃、圧力0.43MPaに約20分間維持して竹片を蒸煮処理した。竹片蒸煮処理を終えたところで、蒸煮処理装置内を徐々に降圧して、約5分間で大気に開放した。大気解放後の竹片は、保有温度が70℃で水分含有率が15重量%で、その侭保温保湿した。
2. Steaming treatment The crushed bamboo pieces were put into a steaming apparatus, and 0.43 MPa pressurized saturated steam was supplied into the steaming apparatus. Pressure saturated steam was supplied into the steaming apparatus for about 10 minutes, and the temperature in the steaming apparatus was raised to 145 ° C. Then, the bamboo piece was steamed by maintaining the inside of the steaming apparatus at a temperature of 145 ° C. and a pressure of 0.43 MPa for about 20 minutes. When the bamboo piece steaming process was completed, the pressure in the steaming apparatus was gradually reduced and released to the atmosphere in about 5 minutes. The bamboo pieces after release to the atmosphere were kept at 70 ° C. and a moisture content of 15% by weight, and kept warm and moist.

3.解繊処理
温度が70℃で水分含有率が15重量%の竹片を粗解繊機に入れて祖解繊した。粗解繊は、固定刃と回転刃の刃間隔が1mm程度で、厚さ0.5mm以下の薄片に切削し、切り裂いて細長い粗解繊の繊維束を製造した。次に、この切り裂かれた細長い粗解繊の繊維束を、複数個の解繊ピンを二段に夫々固定した互いに対向する一対の板状回転体を備える精解繊装置により精解繊した。本例において、精解繊は、前記精解繊装置の一方の板状回転体を固定し、もう一方の板状回転体を、約3000rpmの回転数で高速回転させて行なわれ、固定した板状回転体の解繊ピンと高速回転する板状回転体の解繊ピンとの間の剪断作用により、粗解繊の繊維束をより細かく解繊して、綿状の竹繊維を製造した。精解繊された綿状の竹繊維は、端部に設けられているスクリーンを通して得られた。本例においては、互いに対向する一対の板状回転体の一方の板状回転体を停止して、他方の板状回転体を回転させて精解繊を行っているが、双方の板状回転体を互いに逆方向に回転させて精解繊を行うことができる。
3. Defibration treatment Bamboo pieces having a temperature of 70 ° C. and a moisture content of 15% by weight were placed in a coarse defibrating machine and defibrated. In the coarse defibration, the fixed blade and the rotary blade have a gap of about 1 mm, cut into a thin piece having a thickness of 0.5 mm or less, and cut to produce an elongated coarse defibrated fiber bundle. Next, the elongated, loosely defibrated fiber bundle that was torn was finely defibrated by a defibrating device having a pair of plate-like rotating bodies facing each other, each having a plurality of defibrating pins fixed in two stages. In this example, the fine defibrating is performed by fixing one plate-like rotating body of the fine-defining device and rotating the other plate-like rotating body at a high speed of about 3000 rpm. The coarse defibrated fiber bundle was further finely deflated by a shearing action between the defibrating pin of the rotator and the defibrating pin of the plate rotator rotating at high speed to produce cotton-like bamboo fibers. Refined cotton-like bamboo fiber was obtained through a screen provided at the end. In this example, one plate-shaped rotating body of a pair of plate-shaped rotating bodies facing each other is stopped and the other plate-shaped rotating body is rotated to perform fine defibration. Fine defibration can be performed by rotating the body in opposite directions.

繊維板の加工
例1で製造した綿状の竹繊維の含水率を10重量%に調整した。含水率が調整された綿状の竹繊維に、竹繊維に対し、6乃至8重量%の合成樹脂接着剤を加えて混合し、合成樹脂接着剤を均等に分散させる。この接着剤が分散された竹繊維を、型枠内に入れて予備加圧成形して板状成形体を製造する。製造された板状成形体を型枠内に積み重ねて、プレス温度160℃、プレス圧50kg/cm及びプレス時間5分のプレス条件で熱圧縮成形して、幅300mm、長さ300mm、厚さ10mmの繊維板を製造した。
Processing of fiberboard The moisture content of the cotton-like bamboo fiber produced in Example 1 was adjusted to 10% by weight. A synthetic resin adhesive of 6 to 8% by weight with respect to the bamboo fiber is added to and mixed with the cotton-like bamboo fiber whose water content is adjusted, and the synthetic resin adhesive is uniformly dispersed. The bamboo fiber in which the adhesive is dispersed is put in a mold and pre-press-molded to produce a plate-like molded body. The produced plate-like molded bodies are stacked in a mold, and are subjected to hot compression molding under a press temperature of 160 ° C., a press pressure of 50 kg / cm 2 and a press time of 5 minutes, and are 300 mm wide, 300 mm long, and thick. A 10 mm fiberboard was produced.

繊維板の曲げヤング率
前記製造された幅300mm、長さ300mm及び厚さ10mmの繊維板について、幅50mm及び長さ200mmの試験体を切出して曲げヤング率の測定用試験体とし、この試験体により繊維板の曲げヤング率を測定した。測定された繊維板の曲げヤング率は2518N/mmであった。この測定された繊維板の曲げヤング率の値は、繊維板MDFの曲げヤング率の基準値の800乃至2518N/mm以上を満たすものであった。
Bending Young's modulus of fiberboard About the manufactured fiberboard having a width of 300 mm, a length of 300 mm and a thickness of 10 mm, a specimen having a width of 50 mm and a length of 200 mm was cut out to obtain a specimen for measuring a bending Young's modulus. Was used to measure the bending Young's modulus of the fiberboard. The measured bending Young's modulus of the fiberboard was 2518 N / mm 2 . The measured value of the bending Young's modulus of the fiberboard satisfies the standard value of 800 to 2518 N / mm 2 or more of the bending Young's modulus of the fiberboard MDF.

繊維板の剥離強さ
前記の製造された幅300mm、長さ300mm及び厚さ10mmの繊維板について、幅50mm及び長さ50mmの試験体を切出して繊維板の剥離強さの測定用試験体を調製した。測定された繊維板の剥離強さは1.20N/mmであった。この測定された繊維板の剥離強さの値は、繊維板MDFの剥離強さの基準値の0.2乃至0.5N/mm以上を満たすものであった。
Peel strength of fiber board About the manufactured fiber board of width 300mm, length 300mm, and thickness 10mm, the test body for width 50mm and length 50mm was cut out, and the test body for measuring the peel strength of fiber board was used. Prepared. The measured peel strength of the fiberboard was 1.20 N / mm 2 . The measured value of the peel strength of the fiberboard satisfies the reference value of 0.2 to 0.5 N / mm 2 or more of the peel strength of the fiberboard MDF.

繊維板の吸水厚さ膨張率
前記の製造された幅300mm、長さ300mm及び厚さ10mmの繊維板について、幅50mm及び長さ50mmの試験体を切出して繊維板の吸水厚さ膨張率の測定用試験体を調製した。測定された繊維板の吸水厚さ膨張率は5.3%であった。この測定された値は、繊維板MDFの吸水厚さ膨張率の基準値の10乃至17%以下の各基準値を満たすものであった。
Measurement of the water absorption thickness expansion coefficient of the fiber board by cutting out a specimen having a width of 50 mm and a length of 50 mm from the manufactured fiber board having a width of 300 mm, a length of 300 mm and a thickness of 10 mm. A test specimen was prepared. The measured water absorption thickness expansion coefficient of the fiberboard was 5.3%. This measured value satisfied each reference value of 10 to 17% or less of the reference value of the water absorption thickness expansion coefficient of the fiberboard MDF.

本発明は、竹材を高温高圧水蒸気の存在下に蒸煮し、蒸煮された竹材を常圧下で常温を越える温度下で解繊することにより、相互に絡み易く綿状の竹繊維を製造することができる。本発明においては、竹繊維を綿状に形成するので、成形段階で相互に絡ませることができ、繊維板に使用して、繊維長の短い繊維を使用する繊維板の強度に係る欠点を改良することができる。また、竹繊維を相互に絡ませるために、接着剤の使用量は、6乃至8重量%であり、この接着剤の使用量は、木繊維の繊維板の接着剤の使用量の10乃至13重量%に比して著しく少なく、接着剤の使用量を節約でき、経済性に優れる。

The present invention can produce cotton-like bamboo fibers that are easily entangled with each other by cooking bamboo in the presence of high-temperature and high-pressure steam and defibrating the cooked bamboo at a temperature exceeding normal temperature under normal pressure. it can. In the present invention, the bamboo fibers are formed in a cotton shape, so that they can be entangled with each other in the molding stage, and used for the fiberboard to improve the defect related to the strength of the fiberboard using fibers with a short fiber length. can do. In order to entangle bamboo fibers with each other, the amount of the adhesive used is 6 to 8% by weight. The amount of the adhesive used is 10 to 13 of the amount of the adhesive used for the fiberboard of the wood fiber. It is remarkably small compared to the weight%, and the amount of adhesive used can be saved, resulting in excellent economic efficiency.

Claims (9)

竹材を高温高圧水蒸気の存在下に蒸煮し、蒸煮された竹材を常圧下で常温を越える温度下で解繊することを特徴とする綿状の竹繊維の製造方法。 A method for producing cotton-like bamboo fibers, characterized in that bamboo materials are steamed in the presence of high-temperature and high-pressure steam, and the steamed bamboo materials are defibrated at a temperature exceeding normal temperature under normal pressure. 長手方向に間隔を以って裁断された竹材を圧縮して、開裂させて、平板状に圧縮形成し、圧縮形成された平板状の竹材を、加熱水蒸気の雰囲気下で蒸煮し、蒸煮された竹材を、常圧下で、常温より高い温度下で解繊することを特徴とする綿状の竹繊維の製造方法。 Bamboo material cut at intervals in the longitudinal direction was compressed, cleaved, compressed into a flat plate shape, and the flat formed bamboo material was steamed and steamed in an atmosphere of heated steam A method for producing cotton-like bamboo fibers, characterized in that bamboo material is defibrated under normal pressure and at a temperature higher than room temperature. 200cm以下の長さに裁断された竹材を圧縮して、開裂させて、厚さ20mm以下の平板状に圧縮形成し、圧縮形成された平板状の竹材を、加熱水蒸気の雰囲気下で蒸煮し、蒸煮された竹材を、1分以上の時間を掛けて常圧にまで圧力を下げ、常圧下で、常温より高い温度で解繊することを特徴とする綿状の竹繊維の製造方法。 Bamboo material cut to a length of 200 cm or less is compressed and cleaved, and compressed into a flat plate with a thickness of 20 mm or less. The compressed flat bamboo material is cooked in an atmosphere of heated steam, A method for producing cotton-like bamboo fibers, characterized in that steamed bamboo is reduced to normal pressure over a period of 1 minute or longer, and defibrated at a temperature higher than normal temperature under normal pressure. 長さ10乃至200cmに分割切断された竹材を圧縮して、開裂させて、厚さ5乃至20mmの平板状に形成し、圧縮されて平板状に形成された竹材を、100乃至200℃の温度及び0.1乃至1.6MPaの圧力を有する加熱水蒸気の雰囲気内で蒸煮し、蒸煮された竹材を1分以上の時間を掛けて減圧し、次いで、大気圧及び50℃以上の温度を有する雰囲気内で、解繊することを特徴とする綿状の竹繊維の製造方法。 Bamboo material divided and cut into lengths of 10 to 200 cm is compressed and cleaved to form a flat plate with a thickness of 5 to 20 mm, and the bamboo formed into a flat plate with a thickness of 100 to 200 ° C. And steamed in an atmosphere of heated steam having a pressure of 0.1 to 1.6 MPa, the steamed bamboo material is depressurized over a period of 1 minute, and then an atmosphere having an atmospheric pressure and a temperature of 50 ° C. or higher Inside, a method for producing cotton-like bamboo fiber, which is defibrated. 長さ10乃至200cmに分割切断された竹材を圧縮して、開裂させて、厚さ5乃至20mmの平板状に形成し、圧縮されて平板状に形成された竹材を、100乃至200℃の温度及び0.1乃至1.6MPaの圧力を有する加熱水蒸気の雰囲気内で5乃至60分間蒸煮し、蒸煮された竹材を5乃至10分間で常圧まで減圧して、50乃至100℃の温度及び10乃至30重量%の含水率を有する状態にして、少なくとも一方の切刃が回転刃である粗解繊機により、粗解繊を行って、厚さが0.1乃至1.0mmの粗解繊繊維束を形成し、次いで、この粗解繊繊維束を、大気圧下で、50乃至100℃の温度及び10乃至30重量%の含水率を有する状態にして、少なくとも一方の解繊刃が回転刃である精解繊装置による高速回転により、さらに精解繊して、直径が0.01乃至0.2mmの精解繊繊維束を製造することを特徴とする綿状の竹繊維の製造方法。 Bamboo material divided and cut into lengths of 10 to 200 cm is compressed and cleaved to form a flat plate with a thickness of 5 to 20 mm, and the bamboo formed into a flat plate with a thickness of 100 to 200 ° C. And steamed in an atmosphere of heated steam having a pressure of 0.1 to 1.6 MPa for 5 to 60 minutes, and the steamed bamboo material is decompressed to normal pressure in 5 to 10 minutes to a temperature of 50 to 100 ° C. and 10 A coarse defibrated fiber having a thickness of 0.1 to 1.0 mm by performing rough defibration using a rough defibrating machine having a moisture content of thirty to 30% by weight and at least one cutting blade being a rotary blade. A bundle is formed, and then this coarse defibrated fiber bundle is brought into a state having a temperature of 50 to 100 ° C. and a moisture content of 10 to 30% by weight at atmospheric pressure, and at least one defibrating blade is a rotary blade The high-speed rotation by Seikai fiber to method for producing a cotton-like bamboo fiber characterized by a diameter to produce a fine fibrillated fiber bundle of 0.01 to 0.2mm in. 長さ10乃至200cmに分割切断された竹材を圧縮して、開裂させて、厚さ5乃至20mmの平板状に形成し、圧縮されて平板状に形成された竹材を、100乃至200℃の温度及び0.1乃至1.6MPaの圧力を有する加熱水蒸気の雰囲気内で5乃至60分間蒸煮し、蒸煮された竹材を5乃至10分間で常圧まで減圧して、50乃至100℃の温度及び10乃至30重量%の含水率を有する状態にして、少なくとも一方の切刃が回転刃である粗解繊機により、粗解繊を行って、厚さが0.1乃至1.0mmの粗解繊繊維束を形成し、次いで、この粗解繊繊維束を、大気圧下で、50℃以上の温度及び10乃至30重量%の含水率を有する状態にして、少なくとも一方の切刃が棒状の回転刃である精解繊装置による高速回転により、さらに精解繊して、直径が0.01乃至0.2mmで、長さが1乃至100mmの精解繊繊維束を製造することを特徴とする綿状の竹繊維の製造方法。 Bamboo material divided and cut into lengths of 10 to 200 cm is compressed and cleaved to form a flat plate with a thickness of 5 to 20 mm, and the bamboo formed into a flat plate with a thickness of 100 to 200 ° C. And steamed in an atmosphere of heated steam having a pressure of 0.1 to 1.6 MPa for 5 to 60 minutes, and the steamed bamboo material is decompressed to normal pressure in 5 to 10 minutes to a temperature of 50 to 100 ° C. and 10 A coarse defibrated fiber having a thickness of 0.1 to 1.0 mm by performing rough defibration using a rough defibrating machine having a moisture content of thirty to 30% by weight and at least one cutting blade being a rotary blade. A bundle is formed, and then the crude defibrated fiber bundle is brought to a state having a temperature of 50 ° C. or higher and a moisture content of 10 to 30% by weight at atmospheric pressure, and at least one of the cutting blades is a rod-shaped rotary blade The high-speed rotation by And fine defibration, a diameter of 0.01 to 0.2 mm, the manufacturing method of the cotton-like bamboo fiber, wherein a length to produce a fine fibrillated fiber bundle 1 to 100 mm. 蒸煮雰囲気が、130乃至160℃の温度及び0.28乃至0.64MPaの圧力を有する雰囲気であることを特徴とする綿状の竹繊維の製造方法。 A method for producing cotton-like bamboo fibers, wherein the steaming atmosphere is an atmosphere having a temperature of 130 to 160 ° C. and a pressure of 0.28 to 0.64 MPa. 竹材の粗解繊が、粗解繊機の一方の切刃と他方の切刃が交差する角度が50乃至80度で行われることを特徴とする請求項1乃至7の何れか一項に記載の綿状の竹繊維の製造方法。 The rough defibration of the bamboo material is performed at an angle of 50 to 80 degrees where one cutting edge of the rough defibrating machine and the other cutting edge intersect each other. A method for producing cotton-like bamboo fiber. 竹材の粗解繊に続く精解繊が、一対切刃が共に棒状であり、少なくとも一方の切刃が回転刃である精解繊装置により、1000rpm以上の回転刃の回転により行われることを特徴とする請求項1乃至8の何れか一項に記載の綿状の竹繊維の製造方法。
The fine defibrating following the rough defibration of the bamboo material is performed by rotating the rotary blade at 1000 rpm or more by a fine defibrating device in which the pair of cutting blades are both rod-shaped and at least one of the cutting blades is a rotary blade. The manufacturing method of the cotton-like bamboo fiber as described in any one of Claims 1 thru | or 8.
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