JP2004121061A - Method for producing powder composition - Google Patents

Method for producing powder composition Download PDF

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Publication number
JP2004121061A
JP2004121061A JP2002288495A JP2002288495A JP2004121061A JP 2004121061 A JP2004121061 A JP 2004121061A JP 2002288495 A JP2002288495 A JP 2002288495A JP 2002288495 A JP2002288495 A JP 2002288495A JP 2004121061 A JP2004121061 A JP 2004121061A
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Prior art keywords
powder
polysorbate
water
method
powder composition
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JP2002288495A
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Japanese (ja)
Inventor
Ritsuko Kawabata
Yasuyuki Morita
Kazuhiko Nishimura
川畑 りつ子
森田 康幸
西村 和彦
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Sanei Gen Ffi Inc
三栄源エフ・エフ・アイ株式会社
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Priority to JP2002288495A priority Critical patent/JP2004121061A/en
Publication of JP2004121061A publication Critical patent/JP2004121061A/en
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Abstract

<P>PROBLEM TO BE SOLVED: To provide a method for producing a powder composition, comprising treating a powder raw material with polysorbate, by which the powder composition having improved dusting resistance and improved solubility / dispersibility in water is obtained. <P>SOLUTION: This method for producing the powder composition is characterized by treating the powder raw material with the polysorbate, whereby the improved dusting resistance and improved water solubility / dispersibility of the powder composition can be obtained. The powder composition can be used as a raw material for food products, medicines, quasi medicines, industrial products, cosmetics, feeds, and the like. <P>COPYRIGHT: (C)2004,JPO

Description

【発明の属する技術分野】本発明は、粉末組成物の製造に際し、ポリソルベートで処理することを特徴とする飛散性、水への溶解性・分散性が改善された粉末組成物の製造方法に関する。 BACKGROUND OF THE INVENTION The present invention is in the production of powder composition, fluffy, characterized in that the treatment with polysorbate, a method of manufacturing a powder composition solubility, dispersibility in water is improved.
【0001】 [0001]
【従来の技術】 BACKGROUND OF THE INVENTION
粉末原料の多くは、乾燥した微細な粒子の集合体であり、粉末原料を取扱う際には微細な粉体が空中に飛散する、いわゆる「粉立ち」が発生し、飛散した粉末を作業員が吸引してしまって、健康に害を与える恐れがあるという問題や、作業環境の悪化、例えば、飛散した粉体が作業場内の床等に沈降し、滑りやすくなったり、また、作業内の床等に溜まった粉体原料が水とが接触することによって更に滑りやすくなったり、また、これが菌の繁殖を引き起こす原因となって衛生上大きな問題を生じることがあった。 Many powdered material is an aggregate of the dried fine particles, when handling the powder material is fine powder is scattered in the air, so-called "dusting" occurs, the operator of the scattered powder and I got sucked, and the problem that there is a risk of harm to health, deterioration of the working environment, for example, to settle scattered powder on the floor or the like in the workplace, or slippery, also, the floor in the work may become more slippery by accumulated powder material at equal to contact with water, also this was sometimes cause hygienic big problem causing causing propagation of bacteria. また、粉立ちが過度の場合には、粉塵爆発等の危険も考えられる。 In addition, in case dusting is excessive is considered to be dangerous, such as a dust explosion.
【0002】 [0002]
このような粉末原料の粉立ちを防止するには、従来は、粉体自体を製造する際にその粉砕等を粗くして粒度を上げる方法や、造粒工程等を行い、粉体の粒径を大きくする方法、或いは、粉末の表面を加工する方法がある。 To prevent dusting of such powder materials are conventionally, when manufacturing the powder itself roughened the grinding or the like and a method of increasing the particle size, performs granulation step or the like, the powder particle size of methods for increasing or there is a method of processing the surface of the powder. しかし粒度を粗くする場合は、水溶性のものでも、完全に水和させるのに要する時間が多くかかるという欠点の他、完全に溶解しないものでは、その粒子の大きさより、ザラツキや沈殿などの問題が生じるため、特定分野でしか使用できない。 However, when roughening the particle size, also water-soluble ones, other disadvantage completely takes a long time required to hydrate, is one which does not completely dissolve, than the size of the particles, problems such as rough or precipitation in order to occur, it can not be used only in specific areas.
【0003】 [0003]
また、粉末原料を水に添加した場合、粉体自体が水中に分散しながら溶解するよりも、粉体が水との接触面だけで水和する方が早い場合には、接触面のみ水和が行われ、中に溶解していない粉末が生じるという、いわゆる「ままこ」が生成して、粉末原料が水に溶解し難くなるという問題がある。 Further, when the powder raw material is added to water, than the powder itself is dissolved while dispersing in water, when those who powder is hydrated with just the contact surface with water is fast, only the contact surface hydration is carried out, and that the powder undissolved in occurs, the so-called "lump" is generated, there is a problem that the powder material is less soluble in water. 粉末原料の種類にもよるが、一度できてしまった「ままこ」を完全に溶解させることは非常に困難である。 Depending on the type of powder raw materials, it is very difficult to completely dissolve the "lump" you've made once. この「ままこ」を防ぐには、粉末原料を使用の際、高速撹拌しながら徐々に添加する方法、数倍以上の「ままこ」にならない粉体と混合して用いる方法、粉体の粒径を大きくする方法或いは粉体の表面を被覆する方法が挙げられるが、手間及び溶解性の点で全てを満足させるものではない。 This prevents "lump" is, in use the powdered material, high speed agitation method of gradually adding, a method of using as a mixture with not not powder "lump" in the above several times, the powder particle and a method of coating the surface of a method or a powder to increase the size, but does not satisfy all in terms of labor and solubility.
【0004】 [0004]
一方、易溶性キサンタンガムの製造方法は既に文献に記載されており(特許文献1参照)、これにはキサンタンガムをHLB8以上のポリグリセリンまたはショ糖脂肪酸エステル、レシチン、リゾレシチンを乳化剤として処理することによって、キサンタンガムの水和性・分散性を改善した方法が記載されている。 On the other hand, it is (see Patent Document 1) is described in the manufacturing method already literature readily soluble xanthan gum, poly glycerin or sucrose fatty acid esters above HLB8 xanthan gum to this, by treating lecithin, lysolecithin as an emulsifier, method with improved xanthan gum hydration and dispersion properties is described. しかしながら、この方法は、上記問題を完全に解決したものではなく、また、ショ糖脂肪酸エステル、レシチンの乳化剤は、溶液が白濁してしまうという問題があった。 However, this method is not completely solve the above problems, also, sucrose fatty acid esters, emulsifiers lecithin has a problem solution will clouded. さらに、これらの方法では粉立ちについても解決されていない。 Furthermore, it not solved for dusting with these methods.
【0005】 [0005]
また、水溶性多糖類の粉体に、水溶性多糖類とソルビタンモノオレエート、ソルビタンモノラウレート、テトラグリセリンモノラウレート、テトラグリセリンモノオレエート等の乳化剤の混合液をバインダーとして使用し、造粒することを特徴とする造粒水溶性多糖類の製造方法がある(特許文献2参照)。 Further, the water-soluble polysaccharide powder, using water-soluble polysaccharide and sorbitan monooleate, sorbitan monolaurate, tetraglycerol monolaurate, a mixture of emulsifiers such as tetraglycerol monooleate as a binder, granulated there is granulated water-soluble polysaccharide production method characterized by particle (see Patent Document 2).
【0006】 [0006]
テトラグリセリンモノラウレート、テトラグリセリンモノオレエート等のポリグリセリンやレシチン、リゾレシチンを乳化剤として使用した場合では、乳化剤自体に風味の問題があり、添加量を多くすると臭いや風味に影響を与えるので、食品への使用用途や使用方法が限定されていた。 Tetraglycerol monolaurate, in the case where the polyglycerol and lecithin such as tetraglycerol monooleate, lysolecithin is used as an emulsifier, there are flavor problems emulsifier itself, so affecting the odor and flavor allowing a larger amount, use the application and use of the food has been limited. また、ショ糖脂肪酸エステル、レシチン、酵素処理レシチン、ソルビタンモノオレエート、ソルビタンモノステアレートでは、溶解性に問題があり、乳化剤自身を溶解した場合、白濁する若しくは長期保存により乳化剤が結晶化する等の問題があり、透明性が必要とされる用途や長期保存を行う用途では使用できなかった。 Further, sucrose fatty acid esters, lecithin, enzyme-treated lecithin, sorbitan monooleate, the sorbitan monostearate, there is a problem with solubility when dissolved an emulsifier itself, emulsifier cloudy to or long-term storage and the like to crystallize There are problems, could not be used in applications for performing applications and long-term storage where transparency is required.
【0007】 [0007]
上記の如く、粉末原料を水に溶解或いは分散させるには、多くの問題があり、現状の方法ではこれら問題を解決するには至っていない。 As described above, the powder raw material is dissolved or dispersed in water, there are many problems, not the current methods have yet to solve these problems.
【0008】 [0008]
【特許文献1】 [Patent Document 1]
特開昭63−230703号公報【特許文献2】 JP 63-230703 JP Patent Document 2]
特開2000−063402号公報【0009】 Japanese Unexamined Patent Publication No. 2000-063402 Publication [0009]
【発明が解決しようとする課題】本発明は、粉末原料の使用用途を限定することなく、水への溶解性・分散性に優れ、水への投入時の粉立ち及び「ままこ」の生成を有意に抑制された、作業性に優れる粉末組成物を製造する方法を提供することを目的とする。 [SUMMARY OF THE INVENTION The present invention, generation of without limiting the intended use of the powder material, excellent in solubility, dispersibility in water, dusting and "lump" when poured into water It was significantly suppressed, and an object thereof is to provide a method for producing a powder composition having excellent workability.
【0010】 [0010]
【課題を解決するための手段】本発明者らは、上記課題を解決すべく鋭意研究を重ねたところ、粉末原料をポリソルベートで処理することによって、粉体原料の水への溶解性・分散性、泡立ち性、粉立ち性が改善され、作業性に優れた粉末組成物を製造することができるということを見いだした。 Means for Solving the Problems The present inventors have made intensive studies to solve the above problems by treating the powder material polysorbate, solubility and dispersibility of the powder raw material in water , foaming properties, are dusting properties improved, it found that it is possible to manufacture an excellent powder composition workability. 本発明は、かかる知見に基づいて開発されたものである。 The present invention has been developed on the basis of this finding.
【0011】 [0011]
すなわち、本発明は下記にあげる粉末組成物の製造方法である。 That is, the present invention is a method of producing a powder composition listed below.
1. 1. 粉末原料をポリソルベートで処理することを特徴とする粉末組成物の製造方法。 Method of producing a powder composition which comprises treating the powder material in polysorbate.
2. 2. 粉末原料が、脱脂粉乳、全脂粉乳等の粉乳、分離大豆タンパク質・乳清タンパク質、カゼインナトリウム、アルブミン、ゼラチン等の水溶性タンパク質類、馬鈴薯等の澱粉類やそれらの加工デンプン、小麦粉・きな粉等の穀粉類、ココア・抹茶等の食用粉末、グァーガム等の水溶性多糖類等である項1. Powder raw material, skim milk, milk powder such as whole milk powder, soybean protein isolate, whey protein, sodium caseinate, albumin, water-soluble proteins such as gelatin, starches and their modified starches, such as potato, wheat flour, soybean flour, etc. cereal flour of claim 1 is a cocoa edible powder such as green tea, water-soluble polysaccharide such as guar gum. 記載の粉末組成物の製造方法。 Method of producing a powder composition.
3. 3. ポリソルベートがポリソルベート80あるいはポリソルベート60またはそれらの混合物から選ばれる請求項1に記載の粉末組成物の製造方法。 Method of producing a powder composition according to claim 1, polysorbate is selected from polysorbate 80 or polysorbate 60, or mixtures thereof.
また、本発明は下記にあげる粉末組成物である。 Further, the present invention is a powder composition listed below.
4. 4. 粉末原料をポリソルベートで処理することによって、水への溶解性・分散性が改善された粉末組成物。 By treating the powder material polysorbate, powder composition solubility, dispersibility in water is improved.
さらに、本発明は下記にあげる粉末原料の水への溶解性の改善方法である。 Furthermore, the present invention is a method for improving the solubility in water of the powder material listed below.
5. 5. 粉末原料をポリソルベートで処理することを特徴とする、粉末原料の水への溶解性の改善方法。 Characterized by treating the powder material in polysorbate, a method for improving the solubility of the powder raw material in water.
【0012】 [0012]
【発明の実施の形態】本発明における粉末原料とは、水に投入した際に、上述したような問題点を有するものであれば特に制限がないが、例えば、脱脂粉乳、全脂粉乳等の粉乳、分離大豆タンパク質・乳清タンパク質、カゼインナトリウム、アルブミン、ゼラチン等の水溶性タンパク質類、馬鈴薯等の澱粉類やそれらの加工デンプン、小麦粉・きな粉等の穀粉類、ココア・抹茶等の食用粉末、グァーガム等の水溶性多糖類等が挙げられる。 The powder raw material in the Detailed Description of the Invention The present invention, when charged into the water, is not particularly limited as long as it has the above-mentioned problems, for example, powdered skim milk, such as whole milk powder milk powder, soy protein isolate, whey protein, sodium caseinate, albumin, water-soluble proteins such as gelatin, starches and their modified starches, such as potato, cereal flours such as wheat flour, soybean flour, edible powder such as cocoa, tea, water-soluble polysaccharides such as guar gum and the like. また、上記粉末原料の1種以上を含んだ粉体混合物であってもよい。 Further, it may be a powder mixture containing one or more of the above-mentioned powder material.
【0013】 [0013]
特に、粉末原料の粒子径が100μm以下になると飛散をおこし易くなるが、本発明のポリソルベートによる処理を行うことによって、飛散性による作業性改善、粉体への分散性が改善されると同時に、水への溶解性の改善が行われる。 In particular, although the particle size of the powder raw material is liable to cause a scatter 100μm or less, by performing the process according polysorbate present invention, workability improvement by fluffy, the dispersibility of the powder is improved at the same time, improvement of solubility in water is carried out.
【0014】 [0014]
本発明で用いるポリソルベートとは、ソルビタン脂肪酸エステルにエチレンオキシド20モルを付加させた親水性の非イオン界面活性剤で、優れた乳化性、可溶化性、分散性を示すため化粧品、医薬品をはじめ幅広い分野で使用されているものであればよいが、効果の点より、ポリソルベート80(ポリオキシエチレン(20)ソルビタンモノオレエート)、ポリソルベート60(ポリオキシエチレン(20)ソルビタンモノステアレート)を用いることが望ましい。 Polysorbate The used in the present invention, a non-ionic surfactant hydrophilic obtained by adding 20 moles of ethylene oxide to sorbitan fatty acid esters, good emulsifying, solubilizing, for indicating the dispersibility cosmetics, initially wide field of pharmaceuticals in as long as it is used, from the viewpoint of the effect, the use of polysorbate 80 (polyoxyethylene (20) sorbitan monooleate), polysorbate 60 (polyoxyethylene (20) sorbitan monostearate) desirable.
【0015】 [0015]
ポリソルベートの添加量は、粉末原料に対して0.01〜10重量%、好ましくは0.05〜10重量%である。 Amount of polysorbate is 0.01 to 10 wt% relative to the powder raw material, preferably 0.05 to 10 wt%. 0.01重量%より少ないと、飛散防止等の効果が低くなって好ましくない。 If less than 0.01 wt%, unfavorably lower the effect of scattering prevention. 上限は特に限定されないが10重量%より多いとポリソルベート自体の味やコストの面で問題が出る可能性がある。 The upper limit is not particularly limited it is possible that problems and leaving more than 10% by weight in terms of taste and cost of polysorbate itself.
【0016】 [0016]
粉末原料をポリソルベートで処理する方法は、粉末原料に、ポリソルベートを添加して混合し、均一に混ざる方法であれば特に制限はされない。 Method of processing a powdered raw material in polysorbate, a powder raw material, and mixed by adding polysorbate is not particularly limited as long as it is a method uniformly mixed. 例えば、粉末原料にポリソルベートを添加し、混練機を用いて粉体に均一に混ざるようにする方法があげられる。 For example, the addition of polysorbate in powder source, how to make uniformly mixed in powder using a kneading machine and the like.
【0017】 [0017]
混練機には、メランジャ等のホイール型混練機、ニーダー、オーガ、パドルミキサ、リボンミキサ、スクリューミキサ、タービュレントミキサ、マルチミックス、サーマルプロセッサ、ホーバーグミキサ及びフードミキサ、スパイラルミキサ、クッキングミキサ、ポニーミキサ、ユニミックス、ナウタミキサ、ファインミキサ及びコントラミックス等のブレード型混練機、ロールミル及びテーパーロール等のロール型混練機等があげられる。 The kneader wheel-type kneaders such as Meranja, kneader, auger, paddle mixers, ribbon mixers, screw mixers, Turbulent mixers, multi mix, thermal processor, Ho Berg mixers and food mixer, spiral mixer, cooking mixer, Ponimikisa, Uni mix, Nauta, fine mixers and contra mix like blade kneader, a roll mill, and taper roll or roll-type kneaders or the like can be mentioned.
【0018】 [0018]
また、水、メタノール、エタノール、イソプロピルアルコール、ヘキサン、アセトン等の溶剤に、予めポリソルベートを溶解したポリソルベート溶液を、粉体原料に添加して均一に混合後、必要に応じて乾燥等で溶剤を除去する方法でも良い。 Furthermore, removal of water, methanol, ethanol, isopropyl alcohol, hexane, a solvent such as acetone, polysorbate solution prepared by dissolving previously polysorbate, were uniformly mixed and added to the powder raw material, a solvent drying or the like, if necessary it may be a way to.
【0019】 [0019]
さらに、粉末原料にグァーガム、でん粉、デキストリン等のバインダーと共にポリソルベートを加えたバインダー溶液を用いて常法により粉末原料を造粒する方法でも良い。 Furthermore, the powdered material guar gum, starch, or a method of granulating a powder material by a conventional method using a binder solution prepared by adding polysorbate together with a binder such as dextrin.
【0020】 [0020]
また、粉体原料を常法により造粒したものに、上述したポリソルベート溶液を添加し、その造粒した粒子の表面をコーティングする方法でも良い。 Also, the powder raw material obtained by granulating a conventional manner, was added the above-mentioned polysorbate solution, or a method of coating the surface of the granulated particles.
【0021】 [0021]
本発明の飛散性、水への溶解性・分散性が改善された粉末組成物は、食品、例えば飲料、粉末飲料、デザート、チューインガム、錠菓、スナック菓子、水産加工品、畜産加工品、レトルト食品等の飲食品等や食品以外、例えば医薬品、医薬部外品、工業製品、化粧品、飼料等の原料として利用することができる。 Dispersible Powder composition the solubility, dispersibility in water has been improved according to the present invention, foods such beverages, powdered drinks, desserts, chewing gum, tablet candies, snacks, processed marine products, processed livestock products, retort foods other than food or drink and food and the like, for example pharmaceuticals, quasi-drugs, industrial products, cosmetics, can be used as a raw material for feed or the like.
【0022】 [0022]
【実施例】 【Example】
以下、実施例及び比較例を挙げて、本発明を具体的に説明するが、本発明はこれらの実施例に限定されるものではない。 Hereinafter, examples and comparative examples, the present invention will be described in detail, the present invention is not limited to these examples. なお、実施例中の部および%はいずれも重量部、重量%を意味する。 Even parts Any parts and percentages in the examples means weight%.
【0023】 [0023]
【実験例1】精製グァーガム100部にポリソルベート80 3部を添加し、万能撹拌機((株)品川工業所製)にて30分間撹拌混合を行って、精製グァーガム組成物1を得た。 [Experimental Example 1] was added to 80 3 parts Polysorbate purification guar gum 100 parts, universal agitator performing stirring and mixing for 30 minutes at (KK Shinagawa Industries) to obtain a purified guar gum composition 1.
【0024】 [0024]
【比較例1】精製グァーガム100部にショ糖ステアリン酸エステル(HLB11)3部を添加し、実験例1と同様の方法にて精製グァーガム組成物2を得た。 [Comparative Example 1] was added sucrose stearate (HLB11) 3 parts of purified guar gum 100 parts to obtain a purified guar gum composition 2 in the same manner as in Experimental Example 1.
【0025】 [0025]
【実験例2】流動造粒装置(大川原(株)社製)を用い、精製グァーガム100部にポリソルベート80 0.5部、水49.5部の水溶液からなるバインダー液を使用して、吸気温度は70℃、バインダー液のスプレー噴霧圧力は2kg/cm で造粒し、精製グァーガム造粒品1を得た。 Experiment 2 Using a fluidized granulator (manufactured by Okawara Co., Ltd.), 80 0.5 parts of polysorbate in purified guar gum 100 parts, using a binder solution comprising an aqueous solution of 49.5 parts of water, intake air temperature 70 ° C., the spraying pressure of binder solution is granulated with 2 kg / cm 2, to obtain a purified guar granulated product 1.
【0026】 [0026]
【実験例3】精製グァーガム100部にポリソルベート80 2部、水48部の水溶液からなるバインダー液を使用して、実験例2同様の方法で精製グァーガム造粒品2を得た。 Experiment 3] 80 2 parts polysorbate purification guar gum 100 parts, using a binder solution comprising an aqueous solution of water 48 parts, to obtain a purified guar granulated product 2 in Experimental Example 2 a similar manner.
【0027】 [0027]
【実験例4】精製グァーガム100部にポリソルベート60 2部、水48部の水溶液からなるバインダー液を使用して、実験例2と同様の方法で精製グァーガム造粒品3を得た。 Experiment 4] 60 2 parts polysorbate purification guar gum 100 parts, using a binder solution comprising an aqueous solution of water 48 parts, to obtain a purified guar granulated product 3 in the same manner as in Experimental Example 2.
【0028】 [0028]
【実験例5】流動造粒装置(大川原(株)社製)を用い、精製グァーガム100部に水50部をバインダー液に使用して、吸気温度は70℃、バインダー液のスプレー噴霧圧力は2kg/cm で造粒し、粒子径が約0.3mmと成長後、ポリソルベート80 2部、水48部の水溶液を、同条件で噴霧し、粒子の表面がポリソルベートで被覆された精製グァーガム造粒品4を得た。 [Experimental Example 5] use of a fluidized granulator (manufactured by Okawara Co., Ltd.), using 50 parts of water in the binder solution in purified guar gum 100 parts, inlet air temperature is 70 ° C., spray atomization pressure of the binder solution 2kg / granulated with cm 2, after growth to about 0.3mm particle size, 80 2 parts polysorbate, an aqueous solution of water 48 parts, was sprayed under the same conditions, purified guar gum granulating the surface of particles is coated with polysorbate to give the goods 4.
【0029】 [0029]
【比較例2】流動造粒装置(大川原(株)社製)を用い、精製グァーガム100部に酵素処理レシチン2部、水48部の水溶液からなるバインダー液を使用して、吸気温度は70℃、バインダー液のスプレー噴霧圧力は2kg/cm で造粒し、精製グァーガム造粒品5を得た。 Using [Comparative Example 2] fluidized granulator (manufactured by Okawara Co., Ltd.), enzyme-treated lecithin 2 parts of purified guar gum 100 parts, using a binder solution comprising an aqueous solution of water 48 parts of the inlet air temperature is 70 ° C. , spray atomization pressure of the binder solution is granulated with 2 kg / cm 2, to obtain a purified guar granulated product 5.
【0030】 [0030]
【比較例3】流動造粒装置(大川原(株)社製)を用い、精製グァーガム100部にソルビタンモノオレエート2部、水48部の水溶液からなるバインダー液を使用して、吸気温度は70℃、バインダー液のスプレー噴霧圧力は2kg/cm で造粒し、精製グァーガム造粒品6を得た。 [Comparative Example 3] using a fluid granulator (Okawara Co., Ltd.), 2 parts of sorbitan monooleate in purified guar gum 100 parts, using a binder solution comprising an aqueous solution of water 48 parts of the intake air temperature is 70 ° C., spraying pressure of binder solution is granulated with 2 kg / cm 2, to obtain a purified guar granulated product 6.
【0031】 [0031]
▲1▼溶解性改善テスト及び風味のテスト溶解性テストは、1000mlの水を、マグネテックスターラー(アズワン(株)社製)で撹拌しながら、精製グァーガム組成物1、2及び精製グァーガム造粒物1〜6 4gをそれぞれ一挙に投入し、目視で完全に溶解するまでの時間を測定した。 ▲ 1 ▼ Test Solubility Test Solubility improved testing and flavor, water 1000 ml, stirring with a magnetic Tech stirrer (manufactured by AS ONE Co., Ltd.), purified guar gum compositions 1, 2 and purified guar gum granules They were charged 1 to 6 4g at once respectively, to measure the time until complete dissolution visually. 溶解後の溶液の状態、及び官能評価を5段階で評価した。 Solution state after dissolution, and were evaluated sensory evaluation in five stages.
【0032】 [0032]
▲2▼作業時の粉立ちのテスト精製グァーガム組成物1、2及び精製グァーガム造粒物1〜6 30gをそれぞれ一挙に投入し、蓋をした後に、1分間激しく上下に振り、静置した時の粉立ちの状態を観察した。 ▲ 2 ▼ when working dusting test purified guar gum compositions 1, 2 and purified guar gum granules 1 to 6 30 g were charged at once, respectively, after the lid 1 minute vigorously shaken up and down, when allowed to stand state of dusting was observed.
【0033】 [0033]
【表1】 [Table 1]
溶液の風味1:異味異臭無し、2:わずかに異味異臭有り、3:異味異臭少し有り、4:異味異臭有り、5:異味異臭が強い【0034】 Flavor 1 of solution: off-taste without off-flavor, 2: slightly bad taste there unusual odor, 3: bad taste nasty smell there a little bit, 4: bad taste there unusual odor, 5: bad taste strange smell strong [0034]
上記のように、精製グァーガムをポリソルベートで処理すると、溶解性が向上し、透明に溶解し、また、異味異臭もない、さらに粉立ちもない精製グァーガム組成物となった。 As described above, when the purified guar gum treated with polysorbate, improved solubility, and transparent dissolve, nor foreign taste odor became more dusting nor purified guar gum composition.
【0035】 [0035]
【実施例1】 [Example 1]
天ぷら粉のダマ防止効果の確認市販の天ぷら粉に、ポリソルベート80を粉体の1%添加し、乳鉢でよく混合し、天ぷら粉組成物を得た。 Confirmation commercial tempura powder lumps preventing effect tempura flour, polysorbate 80 was added 1% of the powder, and mixed well in a mortar to obtain a tempura flour composition.
次いで、ボウルに水150gを入れ、天ぷら粉組成物100gを添加し、箸で良く天ぷら粉を溶いた。 Then placed 150g of water in a bowl, adding tempura flour composition 100 g, beaten well tempura flour with chopsticks.
【0036】 [0036]
無添加2分間よく溶き、状態を観察した所、天ぷら粉のダマが大小あわせ6個在った。 Beaten well no addition 2 minutes, observation of the state, lumps of tempura flour had six combined magnitude.
さらに2分間良く溶き状態を観察した所、完全にダマはなくならず小さなダマが2個在った。 Where it was further observed 2 min good beaten state, completely lumps are eliminated without small lumps were two up.
添加区1分間よく溶き、状態を観察した所、天ぷら粉のダマが、小さなもの3個在った。 Beaten well silage 1 minute, observation of the state, lumps of tempura powder was small things three up.
さらに1分間良く溶き状態を観察した所、完全になめらかな天ぷら粉となった。 Where it was further observed well beaten state 1 minute, it was a perfectly smooth tempura flour.
上記のように、天ぷら粉をポリソルベートで処理することによって、ダマになりにくい分散性良好な天ぷら粉を得ることができた。 As described above, by treating the tempura flour polysorbate, it was possible to obtain a dispersion having good tempura powder less likely to lumps.
【0037】 [0037]
【実施例2】 [Example 2]
スキンミルクの溶解性改善スキンミルクに、ポリソルベート60を粉体の3%添加し、乳鉢でよく混合し、スキンミルク組成物を得た。 Solubility improving skin milk skin milks, polysorbate 60 was added 3% of the powder, and mixed well in a mortar to obtain a skin milk composition.
次いで、カップに熱湯200gを入れ、スキンミルク組成物25gを添加し、攪拌棒で良く攪拌した。 Then placed hot water 200g cup, adding a skin milk composition 25 g, it was sufficiently stirred with a stirring bar.
無添加……6分間で完全溶解添加区……2分間で完全溶解上記のように、スキンミルクをポリソルベートで処理することによって、溶解性に優れたスキンミルクを得ることができた。 As complete dissolution above completely dissolved silage ...... 2 minutes at no addition ...... 6 minutes, by treating a skin milk polysorbate, it was possible to obtain an excellent skin milks solubility.
【0038】 [0038]
【発明の効果】本発明は、粉末原料を、ポリソルベートで処理することによって、飛散性、水への溶解性・分散性が改善された粉末組成物を得ることができる。 According to the present invention, a powder raw material, by treatment with polysorbate can be obtained scattering properties, the powder composition solubility, dispersibility in water is improved. この粉末組成物は、食品、医薬品、医薬部外品、工業製品、化粧品、飼料等の原料として利用することができる。 The powder composition, food, pharmaceutical, quasi-drugs, industrial products, cosmetics, can be used as a raw material feed and the like.

Claims (4)

  1. 粉末原料をポリソルベートで処理することを特徴とする粉末組成物の製造方法。 Method of producing a powder composition which comprises treating the powder material in polysorbate.
  2. ポリソルベートがポリソルベート80もしくはポリソルベート60またはそれらの混合物から選ばれる請求項1に記載の粉末組成物の製造方法。 Method of producing a powder composition according to claim 1, polysorbate is selected from polysorbate 80 or polysorbate 60, or mixtures thereof.
  3. 粉末原料をポリソルベートで処理することによって、水への溶解性・分散性が改善された粉末組成物。 By treating the powder material polysorbate, powder composition solubility, dispersibility in water is improved.
  4. 粉末原料をポリソルベートで処理することを特徴とする、粉末原料の水への溶解性・分散性の改善方法。 Characterized by treating the powder material polysorbate, solubility and dispersibility of the improved method of powder material in water.
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