JP2004066238A - Rotator for stirring molten metal - Google Patents

Rotator for stirring molten metal Download PDF

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Publication number
JP2004066238A
JP2004066238A JP2002224305A JP2002224305A JP2004066238A JP 2004066238 A JP2004066238 A JP 2004066238A JP 2002224305 A JP2002224305 A JP 2002224305A JP 2002224305 A JP2002224305 A JP 2002224305A JP 2004066238 A JP2004066238 A JP 2004066238A
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JP
Japan
Prior art keywords
molten metal
stirring
shaft
stirring disk
disk
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
JP2002224305A
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Japanese (ja)
Inventor
Shigeyuki Hamayoshi
濱吉 繁幸
Ichiji Furusho
古荘 一ニ
Shingo Nogami
野上 信悟
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Proterial Ltd
Original Assignee
Hitachi Metals Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Hitachi Metals Ltd filed Critical Hitachi Metals Ltd
Priority to JP2002224305A priority Critical patent/JP2004066238A/en
Publication of JP2004066238A publication Critical patent/JP2004066238A/en
Pending legal-status Critical Current

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Abstract

<P>PROBLEM TO BE SOLVED: To provide a rotator for stirring molten metal with which the development of the fracture or crack of a stirring disk is prevented by improving the conventional rotator for stirring the molten metal and also bubbles can be dispersed more uniformly. <P>SOLUTION: The ceramics-made stirring disk is fixed to a shaft having a gas supplying path in the inside. The lower end part of the shaft is protruded to the lower side from the bottom surface of the stirring disk and is closed. A plurality of gas exhausting holes are arranged on the side surface near the lower end part of the shaft. <P>COPYRIGHT: (C)2004,JPO

Description

【0001】
【発明の属する技術分野】
本発明は、アルミニウムなどの溶湯中に窒素やアルゴンガスのような不活性ガスを気泡状態に放出して、溶湯中の水素などのガスや酸化物などの不純物を除去する溶湯攪拌用回転体に関する。
【0002】
【従来の技術】
アルミニウムやアルミニウム合金などの溶湯では、溶湯中の不純物や水素ガスなどを浮遊させて除去するために、溶湯を攪拌しつつ、窒素やアルゴンガスなどの不活性ガスを溶湯中でバブリングさせて、気泡を微細化させるとともに溶湯中に均一に分散させる溶湯攪拌用回転体が用いられている。
【0003】
例えば、特公昭61−40737号公報には、気体供給路を内部に有する垂直回転軸(シャフト)の下端に、気泡微細化分散用回転体(撹拌ディスク)を取付け、気体供給路の下端が回転体の底面に開口させられ、回転体の底面に気体供給路の開口部から周縁に至る複数の溝が放射状に設けられ、回転体の周面における各溝の開口の間に、下端部が回転体の底面周縁部に開口した凹所を設けた溶湯攪拌用回転体が記載されている。
【0004】
また、特開平7−55365号公報には、気体供給路を内部に有するシャフトに、セラミックス製の撹拌ディスクを固定し、不活性ガス吹込み用開口部を撹拌ディスクの底面よりも下側に管状に突出させて形成し、撹拌ディスクの底面に気体供給路の開口部から周縁に至る複数の溝を放射状に設けた溶湯攪拌用回転体が記載されている。
【0005】
特開平7−55365号公報によれば、溶湯中に吹込まれたガスは、撹拌ディスクの回転による影響を受けた溶湯の流れとともに、撹拌ディスクの底面に向って上昇する。この間にガスは溶湯により加熱されて、撹拌ディスクの底面に到達するときは、もはや撹拌ディスクを急冷することがない。このため、撹拌ディスクの上面側と底面側との温度差による大きな熱応力を生じることがなく、割れやクラックの発生を防止できるものである。
【0006】
【発明が解決しようとする課題】
前記特開平7−55365号公報の溶湯攪拌用回転体は、撹拌ディスクの割れやクラックの発生を防止できるという利点を有するが、気泡が気体供給路の開口部から直下に放出されて撹拌ディスクの底面に向って上昇する間に層状に偏りやすく、気泡をより一層均一に分散させるには改善の余地が残されていた。
【0007】
したがって、本発明の目的は、従来の溶湯攪拌用回転体の改良を図り、撹拌ディスクの割れやクラックの発生を防止するとともに、気泡をより一層均一に分散させることができる溶湯攪拌用回転体を提供することである。
【0008】
【課題を解決するための手段】
本発明の溶湯攪拌用回転体は、気体供給路を内部に有するシャフトに、セラミックス製の撹拌ディスクを固定し、シャフトの下端部が撹拌ディスクの底面よりも下側に突出させられ、シャフトの下端部を閉塞するとともに、シャフトの下端部近傍の側面に複数個の気体放出孔を設けたことを特徴とする。
【0009】
【作用】
本発明は、従来のように気泡を気体供給路の開口部から直下に放出することは行なわず、シャフトの下端部を閉塞するとともに、シャフトの下端部近傍の側面に複数個の気体放出孔を設ける、望ましくはシャフトの下端部近傍の側面に円周方向に対し均等間隔に複数個の気体放出孔を設けるため、気泡はシャフトの円周方向に放出されて、撹拌ディスクの底面に向って上昇する間に層状に偏ることがなく均一に分散させられる。
【0010】
また、シャフトの下端部を撹拌ディスクの底面よりも下側に突出させているため、放出された気泡が撹拌ディスクの底面に向って上昇する間に、気泡が溶湯により加熱されて、撹拌ディスクの底面に到達するときは、もはや撹拌ディスクを急冷することがない。このため、撹拌ディスクの上面側と底面側との温度差による大きな熱応力を生じることがなく、割れやクラックの発生を防止できる。
【0011】
また、本発明の溶湯攪拌用回転体においては、従来の技術同様、気泡微細化作用を向上させるために、撹拌ディスクの底面に中央部から周縁部に至る複数の溝を放射状に設けることが好ましい。
【0012】
【発明の実施の形態】
図1は、本発明の溶湯攪拌用回転体の実施例を示す縦断面図である。図2は、その底面図である。図1および図2において、本発明の溶湯攪拌用回転体1は、中空管状のシャフト2の下端部23が撹拌ディスク3の底面31よりも下側に突出するように、シャフト2と撹拌ディスク3を固定して構成される。シャフト2の下端部23より上方に形成した雄ねじ部と、撹拌ディスク3の中央の孔部に形成した雌ねじ部とを螺合することにより固定した。
【0013】
シャフト2は、窒化ケイ素系セラミックス焼結体からなり、その内部に窒素やアルゴンガスなどの不活性ガスを供給するための中空の気体供給路21を有する。シャフト2はその下端部23を閉塞するとともに、シャフト2の下端部23近傍の側面24に、8個の気体放出孔25を円周方向45度間隔毎に設けた。気体供給路21から各々の気体放出孔25を経て撹拌ディスク3の底面31に不活性ガスが供給される。
【0014】
撹拌ディスク3は、シャフト2と同様に窒化ケイ素系セラミックス焼結体からなり、その外周部に、半径方向に突出する8個の突出部32を円周方向45度間隔毎に設けた。また、突出部32の回転方向前面が斜め上方を向くように、回転方向後面が斜め下方を向くように傾斜させた。これにより、前面の押圧力によって溶湯に揚力が働くと同時に、後面の吸引力によっても更に押圧力が働くから、溶湯表面での渦の発生が防止される。
【0015】
撹拌ディスク3の上面33は、中央の孔部から周縁部34に向って徐々に肉厚を減じるようにして、中央の孔部のシャフト2との螺合部位に必要な強度を確保させるとともに、熱応力による破損を受けないように薄肉に形成した。
【0016】
撹拌ディスク3の底面31に、気体供給路21の気体放出孔25に近い位置にある撹拌ディスク3の中央部から周縁部34に至る複数の溝35を放射状に設けた。
【0017】
本発明においては、撹拌ディスク3は特に耐溶損性を要求されるのでセラミックスで形成することが必要である。シャフト2はセラミックスで形成することが望ましいが、それ以外の材料で形成してもよい。また、突出部32の回転方向前面および後面は傾斜していなくてもかまわず、撹拌ディスク3も実施例の形状に限定されるものでない。
【0018】
ここで、本発明実施例の溶湯攪拌用回転体は次のように製造した。まず、平均粒径0.5μmの窒化ケイ素粉末に、焼結助剤として、平均粒径0.2μmの酸化マグネシウム粉末を2.8体積%、平均粒径0.2μmの酸化アルミニウム粉末を0.08体積%、平均粒径2.0μmの酸化イットリウム粉末を0.4体積%添加し、適量の分散剤を加えエタノール中で粉砕、混合した。ついで、真空乾燥後、篩を通して造粒した後、ゴム型に充填し、静水圧により冷間静水圧プレス(CIP)を行い、撹拌ディスクおよびシャフトとなる成形体を作製した。これらの成形体を1750℃、9気圧の窒素ガス雰囲気中で5時間焼成し、窒化ケイ素系セラミックス焼結体からなる本発明の撹拌ディスクおよびシャフトを得た。
【0019】
また、次の特性を調べるために、得られた窒化ケイ素系セラミックス焼結体から、直径10mm×厚さ3mmの密度および熱伝導率測定用の試験片、縦3mm×横4mm×長さ40mmの4点曲げ試験片を採取した。密度はマイクロメ−タによる寸法測定と重量測定の結果から求めた。熱伝導率はレーザーフラッシュ法により常温での比熱および熱拡散率を測定し熱伝導率を算出した。4点曲げ強度は常温にてJIS R1606に準拠して測定を行った。その結果、本発明実施例の窒化ケイ素系セラミックス焼結体は、密度が99.2%、常温における熱伝導率が85W/(m・K)、常温における4点曲げ強度が720MPaであった。
【0020】
本発明の撹拌ディスクおよびシャフトを形成するセラミックスとしては、窒化ケイ素系セラミックスが好ましい。なかでも、窒化ケイ素系セラミックス焼結体の常温における熱伝導率が60W/(m・K)以上であることが望ましい。熱伝導率を高めることにより、溶湯に浸漬する際、溶湯攪拌用回転体の表面から内部へ熱を迅速に伝達させることができ、回転体の表面と内部の温度差を緩和し、熱応力による割れを防止できる。また、使用中の機械的応力および衝撃に十分に耐えられるように、窒化ケイ素系セラミックス焼結体の常温における4点曲げ強度が600MPa以上であることが望ましい。
【0021】
このように構成した本発明実施例の溶湯攪拌用回転体を680℃のアルミニウム溶湯中に浸漬し、シャフトを駆動装置によって高速回転させるとともに、気体供給路から不活性ガスを供給して、溶湯中の不純物などを浮遊させるための回転攪拌に供したところ、気泡の微細化分散効果が十分に得られた。また、アルミニウム溶湯による侵食は殆どみられず、使用中の熱応力による割れやクラックも生じなかった。
【0022】
【発明の効果】
本発明の溶湯攪拌用回転体によれば、撹拌ディスクの割れやクラックの発生を防止するとともに、従来に比べ気泡をより一層均一に分散させることができる。
【図面の簡単な説明】
【図1】本発明の溶湯攪拌用回転体の実施例を示す縦断面図である。
【図2】本発明の溶湯攪拌用回転体の実施例を示す底面図である。
【符号の説明】
1 溶湯攪拌用回転体、 2 シャフト、 3 撹拌ディスク、
21 気体供給路、 23 下端部、 24 側面、 25 気体放出孔、
31 底面、 32 突出部、 33 上面、 34 周縁部、 35 溝
[0001]
TECHNICAL FIELD OF THE INVENTION
TECHNICAL FIELD The present invention relates to a rotating body for stirring a molten metal which releases an inert gas such as nitrogen or argon gas into a molten metal such as aluminum in a bubble state to remove impurities such as a gas such as hydrogen and oxides in the molten metal. .
[0002]
[Prior art]
In a molten metal such as aluminum or aluminum alloy, an inert gas such as nitrogen or argon gas is bubbled in the molten metal while stirring the molten metal to float and remove impurities and hydrogen gas in the molten metal. A rotary body for agitating a molten metal is used, which makes the particles finer and disperses them uniformly in the molten metal.
[0003]
For example, Japanese Patent Publication No. 61-40737 discloses that a rotating body (stirring disk) for atomizing and dispersing bubbles is attached to the lower end of a vertical rotating shaft (shaft) having a gas supply passage therein, and the lower end of the gas supply passage rotates. A plurality of grooves are radially provided on the bottom surface of the rotating body from the opening of the gas supply path to the periphery on the bottom surface of the rotating body, and the lower end rotates between the openings of the grooves on the circumferential surface of the rotating body. A molten metal stirring rotator having a recess opened at the periphery of the bottom surface of the body is described.
[0004]
Japanese Patent Application Laid-Open No. 7-55365 discloses that a stirring disk made of ceramics is fixed to a shaft having a gas supply passage therein, and an opening for blowing an inert gas is provided in a tubular shape below the bottom surface of the stirring disk. A rotating body for agitating a molten metal in which a plurality of grooves from the opening of the gas supply path to the periphery are radially provided on the bottom surface of the stirring disk.
[0005]
According to JP-A-7-55365, the gas blown into the molten metal rises toward the bottom surface of the stirring disk together with the flow of the molten metal affected by the rotation of the stirring disk. During this time, the gas is heated by the molten metal and, when it reaches the bottom surface of the stirring disk, no longer rapidly cools the stirring disk. For this reason, a large thermal stress due to a temperature difference between the upper surface side and the bottom surface side of the stirring disk does not occur, and the generation of cracks and cracks can be prevented.
[0006]
[Problems to be solved by the invention]
The rotating body for stirring a molten metal disclosed in Japanese Patent Application Laid-Open No. 7-55365 has an advantage that cracks and cracks of the stirring disk can be prevented. It tends to be layered while rising toward the bottom surface, and there is room for improvement in dispersing the bubbles more evenly.
[0007]
Accordingly, an object of the present invention is to improve a conventional rotating body for stirring a molten metal, to prevent generation of cracks and cracks in a stirring disk, and to provide a rotating body for stirring a molten metal capable of dispersing air bubbles more uniformly. To provide.
[0008]
[Means for Solving the Problems]
In the rotating body for stirring molten metal of the present invention, a ceramic stirring disk is fixed to a shaft having a gas supply passage therein, and a lower end portion of the shaft is protruded below a bottom surface of the stirring disk. And a plurality of gas discharge holes provided on a side surface near the lower end of the shaft.
[0009]
[Action]
The present invention does not discharge air bubbles directly below the opening of the gas supply path as in the related art, but closes the lower end of the shaft and forms a plurality of gas discharge holes on the side surface near the lower end of the shaft. In order to provide a plurality of gas discharge holes at equal intervals in the circumferential direction, preferably on the side surface near the lower end of the shaft, air bubbles are discharged in the circumferential direction of the shaft and rise toward the bottom surface of the stirring disk. During this process, the particles are uniformly dispersed without being deviated in layers.
[0010]
In addition, since the lower end of the shaft protrudes below the bottom surface of the stirring disk, while the released bubbles rise toward the bottom surface of the stirring disk, the bubbles are heated by the molten metal, and When reaching the bottom, the stirring disk is no longer quenched. For this reason, a large thermal stress due to a temperature difference between the upper surface side and the bottom surface side of the stirring disk does not occur, and generation of cracks and cracks can be prevented.
[0011]
Further, in the molten metal stirring rotating body of the present invention, similarly to the conventional technique, it is preferable to radially provide a plurality of grooves from the central portion to the peripheral edge on the bottom surface of the stirring disk in order to improve the bubble miniaturization action. .
[0012]
BEST MODE FOR CARRYING OUT THE INVENTION
FIG. 1 is a longitudinal sectional view showing an embodiment of a rotating body for stirring molten metal of the present invention. FIG. 2 is a bottom view thereof. 1 and 2, the molten metal stirring rotor 1 of the present invention comprises a shaft 2 and a stirring disk 3 such that the lower end 23 of the hollow tubular shaft 2 projects below the bottom surface 31 of the stirring disk 3. Is fixed. The male screw formed above the lower end 23 of the shaft 2 and the female screw formed in the center hole of the stirring disk 3 were fixed by screwing.
[0013]
The shaft 2 is made of a silicon nitride-based ceramics sintered body, and has a hollow gas supply path 21 for supplying an inert gas such as nitrogen or argon gas into the inside thereof. The shaft 2 has its lower end 23 closed, and eight gas discharge holes 25 are provided on the side surface 24 near the lower end 23 of the shaft 2 at intervals of 45 degrees in the circumferential direction. An inert gas is supplied from the gas supply path 21 to the bottom surface 31 of the stirring disk 3 via each gas discharge hole 25.
[0014]
The stirring disk 3 is made of a silicon nitride-based ceramics sintered body similarly to the shaft 2, and has eight protrusions 32 protruding in the radial direction on the outer periphery thereof at intervals of 45 degrees in the circumferential direction. In addition, the protrusion 32 is inclined such that the front surface in the rotation direction faces diagonally upward and the rear surface in the rotation direction faces diagonally downward. Accordingly, the lift force acts on the molten metal by the pressing force on the front surface, and the pressing force also acts on the molten metal by the suction force on the rear surface. Therefore, the generation of a vortex on the surface of the molten metal is prevented.
[0015]
The upper surface 33 of the stirring disk 3 is gradually reduced in thickness from the central hole toward the peripheral edge portion 34 to secure the necessary strength at a screwing portion of the central hole with the shaft 2. It was formed thin so as not to be damaged by thermal stress.
[0016]
On the bottom surface 31 of the stirring disk 3, a plurality of grooves 35 are formed radially from the central portion of the stirring disk 3 located at a position close to the gas discharge holes 25 of the gas supply passage 21 to the peripheral edge portion 34.
[0017]
In the present invention, since the stirring disk 3 is particularly required to have erosion resistance, it is necessary to form the stirring disk 3 from ceramics. The shaft 2 is desirably formed of ceramics, but may be formed of other materials. Further, the front surface and the rear surface in the rotation direction of the protrusion 32 may not be inclined, and the stirring disk 3 is not limited to the shape of the embodiment.
[0018]
Here, the rotating body for stirring the molten metal of the example of the present invention was manufactured as follows. First, 2.8% by volume of magnesium oxide powder having an average particle diameter of 0.2 μm and 0.2 μm of aluminum oxide powder having an average particle diameter of 0.2 μm were added to silicon nitride powder having an average particle diameter of 0.5 μm as a sintering aid. 0.4% by volume of yttrium oxide powder having an average particle size of 2.0 μm and a volume of 08% by volume were added, an appropriate amount of a dispersant was added, and the mixture was ground and mixed in ethanol. Then, after vacuum drying, the mixture was granulated through a sieve, filled in a rubber mold, and subjected to cold isostatic pressing (CIP) by hydrostatic pressure to produce a molded body to be a stirring disk and a shaft. These compacts were fired in a nitrogen gas atmosphere at 1750 ° C. and 9 atm for 5 hours to obtain a stirring disk and a shaft of the present invention comprising a silicon nitride ceramic sintered body.
[0019]
In addition, in order to examine the following characteristics, from the obtained silicon nitride-based ceramics sintered body, a test piece for measuring the density and thermal conductivity of 10 mm in diameter × 3 mm in thickness, and 3 mm in length × 4 mm in width × 40 mm in length Four-point bending test pieces were collected. The density was determined from the results of dimensional measurement and weight measurement using a micrometer. The thermal conductivity was determined by measuring the specific heat and the thermal diffusivity at room temperature by a laser flash method and calculating the thermal conductivity. The four-point bending strength was measured at room temperature in accordance with JIS R1606. As a result, the silicon nitride ceramic sintered body of the example of the present invention had a density of 99.2%, a thermal conductivity at room temperature of 85 W / (m · K), and a four-point bending strength at room temperature of 720 MPa.
[0020]
The ceramic forming the stirring disk and the shaft of the present invention is preferably a silicon nitride ceramic. In particular, the silicon nitride-based ceramics sintered body preferably has a thermal conductivity of 60 W / (m · K) or more at room temperature. By increasing the thermal conductivity, heat can be quickly transferred from the surface of the rotating body for stirring the molten metal to the inside when immersing in the molten metal. Cracks can be prevented. Further, it is desirable that the silicon nitride-based ceramics sintered body has a four-point bending strength at room temperature of 600 MPa or more so as to sufficiently withstand mechanical stress and impact during use.
[0021]
The rotating body for stirring the molten metal according to the embodiment of the present invention thus constructed is immersed in the molten aluminum at 680 ° C., and the shaft is rotated at a high speed by the driving device. When subjected to rotary stirring to suspend the impurities and the like, the effect of finely dispersing bubbles was sufficiently obtained. In addition, almost no erosion by the molten aluminum was observed, and no cracks or cracks occurred due to thermal stress during use.
[0022]
【The invention's effect】
ADVANTAGE OF THE INVENTION According to the rotating body for agitating a molten metal of this invention, while being able to prevent generation | occurrence | production of a crack and a crack of an agitating disk, a bubble can be disperse | distributed more uniformly than before.
[Brief description of the drawings]
FIG. 1 is a longitudinal sectional view showing an embodiment of a rotating body for stirring a molten metal of the present invention.
FIG. 2 is a bottom view showing an embodiment of a rotating body for stirring molten metal of the present invention.
[Explanation of symbols]
1 rotating body for stirring molten metal, 2 shaft, 3 stirring disk,
21 gas supply path, 23 lower end, 24 side surface, 25 gas discharge hole,
31 bottom surface, 32 protrusion, 33 top surface, 34 peripheral portion, 35 groove

Claims (1)

気体供給路を内部に有するシャフトに、セラミックス製の撹拌ディスクを固定し、シャフトの下端部が撹拌ディスクの底面よりも下側に突出させられ、シャフトの下端部を閉塞するとともに、シャフトの下端部近傍の側面に複数個の気体放出孔を設けたことを特徴とする溶湯攪拌用回転体。A stirring disk made of ceramics is fixed to a shaft having a gas supply passage therein, and the lower end of the shaft is projected below the bottom surface of the stirring disk to close the lower end of the shaft and the lower end of the shaft. A rotating body for stirring molten metal, wherein a plurality of gas discharge holes are provided on a side surface in the vicinity.
JP2002224305A 2002-08-01 2002-08-01 Rotator for stirring molten metal Pending JP2004066238A (en)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2010532427A (en) * 2007-07-05 2010-10-07 フォセコ・インターナショナル・リミテッド Rotary stirring device for processing molten metal
CN111438338A (en) * 2020-04-10 2020-07-24 宋丰艾 Aluminum alloy smelting and casting aluminum liquid diversion trench

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2010532427A (en) * 2007-07-05 2010-10-07 フォセコ・インターナショナル・リミテッド Rotary stirring device for processing molten metal
CN111438338A (en) * 2020-04-10 2020-07-24 宋丰艾 Aluminum alloy smelting and casting aluminum liquid diversion trench
CN111438338B (en) * 2020-04-10 2020-11-10 苏州镁瑞电子科技有限公司 Aluminum alloy smelting and casting aluminum liquid diversion trench

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