JP2003137658A5 - - Google Patents

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JP2003137658A5
JP2003137658A5 JP2001325929A JP2001325929A JP2003137658A5 JP 2003137658 A5 JP2003137658 A5 JP 2003137658A5 JP 2001325929 A JP2001325929 A JP 2001325929A JP 2001325929 A JP2001325929 A JP 2001325929A JP 2003137658 A5 JP2003137658 A5 JP 2003137658A5
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aluminum oxide
parts
oxide powder
powder
mass
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JP2001325929A
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JP2003137658A (en
JP4017857B2 (en
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Claims (16)

平均一次粒子径の異なる少なくとも2種類以上の酸化アルミニウムを混合する工程と、混合した粉体を粉砕する工程とを含むことを特徴とする酸化アルミニウム粉体の製造方法。A method for producing an aluminum oxide powder, comprising: a step of mixing at least two types of aluminum oxides having different average primary particle sizes; and a step of pulverizing the mixed powder. 酸化アルミニウムを混合する工程と、粉砕する工程とを同時に行うことを特徴とする請求項1に記載の酸化アルミニウム粉体の製造方法。The method for producing an aluminum oxide powder according to claim 1, wherein the step of mixing aluminum oxide and the step of pulverizing are performed simultaneously. 平均一次粒子径の異なる少なくとも2種類以上の酸化アルミニウムが、平均一次粒子径が0.25μmを超え0.5μmまでの粉体Aと、0.5μmを超え1μmまでの粉体Bであることを特徴とする請求項1または2に記載の酸化アルミニウム粉体の製造方法。That at least two or more types of aluminum oxides having different average primary particle sizes are powder A having an average primary particle size of more than 0.25 μm to 0.5 μm and powder B of more than 0.5 μm to 1 μm. The method for producing an aluminum oxide powder according to claim 1 or 2. 平均一次粒子径の異なる少なくとも2種類以上の酸化アルミニウムが、酸化アルミニウム全体を100質量部とした場合の比率で、粉体Aが50〜90質量部の範囲内であり、粉体Bが10〜50質量部の範囲内であることを特徴とする請求項1〜3の何れか1項に記載の酸化アルミニウム粉体の製造方法。At least two or more kinds of aluminum oxides having different average primary particle diameters are in a ratio when the total aluminum oxide is 100 parts by mass, the powder A is in the range of 50 to 90 parts by mass, and the powder B is 10 to 10 parts by mass. It exists in the range of 50 mass parts, The manufacturing method of the aluminum oxide powder in any one of Claims 1-3 characterized by the above-mentioned. 平均一次粒子径の異なる少なくとも2種類以上の酸化アルミニウムが、酸化アルミニウム全体を100質量部とした場合の比率で、粉体Aと粉体Bとの合計が90質量部〜100質量部の範囲内であることを特徴とする請求項1〜4の何れか1項に記載の酸化アルミニウム粉体の製造方法。At least two or more types of aluminum oxides having different average primary particle diameters are in a ratio when the total aluminum oxide is 100 parts by mass, and the total of powder A and powder B is in the range of 90 parts by mass to 100 parts by mass. The method for producing an aluminum oxide powder according to any one of claims 1 to 4, wherein: 平均一次粒子径の異なる少なくとも2種類以上の酸化アルミニウムが、平均二次粒子径がそれぞれ30μm〜120μmの範囲内であることを特徴とする請求項1〜5の何れか1項に記載の酸化アルミニウム粉体の製造方法。The aluminum oxide according to any one of claims 1 to 5, wherein at least two kinds of aluminum oxides having different average primary particle diameters each have an average secondary particle diameter in the range of 30 µm to 120 µm. Powder manufacturing method. 混合した粉体を粉砕する工程での粉砕強度(R比×粉砕時間)が、90以上であることを特徴とする請求項1〜6の何れか1項に記載の酸化アルミニウム粉体の製造方法。The method for producing an aluminum oxide powder according to any one of claims 1 to 6, wherein a crushing strength (R ratio x crushing time) in the step of crushing the mixed powder is 90 or more. . グリコール類を添加することを特徴とする請求項1〜7の何れか1項に記載の酸化アルミニウム粉体の製造方法。Glycols are added, The manufacturing method of the aluminum oxide powder of any one of Claims 1-7 characterized by the above-mentioned. グリコール類の添加量が、酸化アルミニウム全体を100質量部とした場合の比率で、0.01質量部〜1質量部の範囲内であることを特徴とする請求項1〜8の何れか1項に記載の酸化アルミニウム粉体の製造方法。The amount of glycols added is in the range of 0.01 parts by weight to 1 part by weight, based on the total amount of aluminum oxide being 100 parts by weight. The manufacturing method of the aluminum oxide powder as described in 2. マグネシウム化合物類を添加することを特徴とする請求項1〜9の何れか1項に記載の酸化アルミニウム粉体の製造方法。Magnesium compounds are added, The manufacturing method of the aluminum oxide powder of any one of Claims 1-9 characterized by the above-mentioned. マグネシウム化合物類の添加量が、マグネシウム化合物類を酸化マグネシウムに換算した時の値で、酸化アルミニウム全体を100質量部とした場合の比率で、0.01質量部〜0.1質量部の範囲内であることを特徴とする請求項1〜10の何れか1項に記載の酸化アルミニウム粉体の製造方法。The amount of magnesium compounds added is the value when the magnesium compounds are converted to magnesium oxide, and the ratio when the total aluminum oxide is 100 parts by mass, in the range of 0.01 parts by mass to 0.1 parts by mass The method for producing an aluminum oxide powder according to any one of claims 1 to 10, wherein: 酸化アルミニウム粉体を98MPaで加圧成形し、1550℃以上で焼成した時の焼結密度が3.91g/cm3以上であり、かつ、収縮率が17.0%以下であることを特徴とする酸化アルミニウム粉体。The aluminum oxide powder is press-molded at 98 MPa and sintered at 1550 ° C. or higher, the sintered density is 3.91 g / cm 3 or higher, and the shrinkage is 17.0% or lower. Aluminum oxide powder to be used. 請求項1〜11の何れか1項に記載の製造方法によって製造された酸化アルミニウム粉体。The aluminum oxide powder manufactured by the manufacturing method of any one of Claims 1-11. 請求項12または請求項13に記載の酸化アルミニウム粉体を含む耐火物。A refractory containing the aluminum oxide powder according to claim 12 or 13. 請求項12または請求項13に記載の酸化アルミニウム粉体を含む電子部品。An electronic component comprising the aluminum oxide powder according to claim 12 or 13. 請求項12または請求項13に記載の酸化アルミニウム粉体を含む機械用部品。A machine part comprising the aluminum oxide powder according to claim 12 or 13.
JP2001325929A 2001-10-24 2001-10-24 Method for producing aluminum oxide powder and aluminum oxide powder Expired - Fee Related JP4017857B2 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP2001325929A JP4017857B2 (en) 2001-10-24 2001-10-24 Method for producing aluminum oxide powder and aluminum oxide powder

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Application Number Priority Date Filing Date Title
JP2001325929A JP4017857B2 (en) 2001-10-24 2001-10-24 Method for producing aluminum oxide powder and aluminum oxide powder

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JP2003137658A JP2003137658A (en) 2003-05-14
JP2003137658A5 true JP2003137658A5 (en) 2005-04-21
JP4017857B2 JP4017857B2 (en) 2007-12-05

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Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2007031163A (en) * 2004-07-02 2007-02-08 Showa Denko Kk Method of producing aluminum oxide powder, and aluminum oxide powder
JP2008041470A (en) * 2006-08-08 2008-02-21 Tokyo Electric Power Co Inc:The Interconnector of solid oxide fuel cell, its manufacturing method, and solid oxide fuel cell

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