JP2002119807A - Method of back washing filter device - Google Patents

Method of back washing filter device

Info

Publication number
JP2002119807A
JP2002119807A JP2000316816A JP2000316816A JP2002119807A JP 2002119807 A JP2002119807 A JP 2002119807A JP 2000316816 A JP2000316816 A JP 2000316816A JP 2000316816 A JP2000316816 A JP 2000316816A JP 2002119807 A JP2002119807 A JP 2002119807A
Authority
JP
Japan
Prior art keywords
backwash
water
backwashing
back washing
treatment layer
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
JP2000316816A
Other languages
Japanese (ja)
Inventor
Isamu Inoue
勇 井上
Kiyouichi Manabe
教市 真鍋
Keizo Murata
圭三 村田
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Sumitomo Heavy Industries Ltd
Original Assignee
Sumitomo Heavy Industries Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Sumitomo Heavy Industries Ltd filed Critical Sumitomo Heavy Industries Ltd
Priority to JP2000316816A priority Critical patent/JP2002119807A/en
Publication of JP2002119807A publication Critical patent/JP2002119807A/en
Pending legal-status Critical Current

Links

Landscapes

  • Filtration Of Liquid (AREA)

Abstract

PROBLEM TO BE SOLVED: To wash a cleaning layer in a desired degree by reducing the water quantity for back washing with back washing water after concurrent flow back washing. SOLUTION: Turbid matter is excellently and effectively stripped from a cleaning material by intermittently supplying back washing air in the concurrent flow back washing using the back washing water and a back washing gas in pulse state, cleaning the cleaning material with strong cleaning power to cause the collision effect of the cleaning material with each other in a period of supplying the back washing gas in pulse state. In a period of stopping the supply of the back washing gas in the pulse state, only the back washing water is supplied and in the meantime, the cleaning material floated by the combination back washing is precipitated to be separated by the difference of the specific gravity from the back washing water and the turbid substance stripped from the cleaning material is moved to the upper part of the cleaning treatment layer by the back washing water with the small difference of the specific gravity. The turbid substance is collected to the upper part without polluting the lower part and discharged easily outside a device by the back washing with the back washing water after the combination back washing by repeating a series of the excellent and effective stripping from the cleaning material and the movement to the upper part of the cleaning treatment layer with the pulse like intermittent supply of the back washing gas.

Description

【発明の詳細な説明】DETAILED DESCRIPTION OF THE INVENTION

【0001】[0001]

【発明の属する技術分野】本発明は、浄化材を積層して
成る濾過装置の逆洗方法に関する。
BACKGROUND OF THE INVENTION 1. Field of the Invention The present invention relates to a method for back-washing a filtration device comprising a stack of purification materials.

【0002】[0002]

【従来の技術】従来、浄化材として例えば砂、アンスラ
サイト等の濾材や例えば活性炭等の吸着材を備え、この
浄化材を積層して成る浄化処理層で被処理水の濁質を捕
捉して当該被処理水を浄化処理する濾過装置が知られて
いる。この濾過装置では、被処理水の濁質が、浄化処理
層の上層から下層に向かう被処理水の移動方向に沿って
指数的に減少するように捕捉される。そして、この濾過
装置にあっては、適宜浄化処理を停止した状態で、被処
理水の移動方向とは逆方向へ洗浄流体を流して浄化処理
層を洗浄し当該浄化処理層の閉塞を防止する逆洗が実施
されている。
2. Description of the Related Art Conventionally, a filtering material such as sand or anthracite or an adsorbing material such as activated carbon has been provided as a purifying material. A filtration device for purifying the water to be treated is known. In this filtration device, the turbid matter of the water to be treated is captured so as to decrease exponentially along the moving direction of the water to be treated from the upper layer to the lower layer of the purification treatment layer. In this filtration device, in a state where the purification treatment is appropriately stopped, a cleaning fluid is caused to flow in a direction opposite to the moving direction of the water to be treated to wash the purification treatment layer and prevent the purification treatment layer from being blocked. Backwashing has been implemented.

【0003】この逆洗方法としては種々の方法が採用さ
れるが、洗浄効果が高い方法として、浄化処理層に対し
て逆洗水と逆洗空気による併流逆洗(併洗)を実施し、
この併洗後に逆洗水による逆洗を実施する逆洗方法が知
られている。
[0003] Various methods are employed as this backwashing method. As a method having a high washing effect, a backwashing water and a backwashing air are used to carry out cocurrent backwashing (cowashing) on the purification treatment layer.
A backwashing method is known in which backwashing is performed with backwash water after the simultaneous washing.

【0004】この逆洗方法は、具体的には、浄化処理層
を形成する浄化材を展開可能とすべく当該浄化処理層が
多少膨張する程度の逆洗水を供給し、これと同時に所定
の流量の逆洗空気を供給して空洗し、この空洗による強
い洗浄力で浄化材に付着している濁質を剥離し、この剥
離した濁質を、併洗後の逆洗水による逆洗で容易に装置
外に排出するという方法である。
[0004] More specifically, in this backwashing method, backwash water is supplied to such an extent that the purification treatment layer is slightly expanded so that the purification material forming the purification treatment layer can be developed. Supply the backwash air at the flow rate to perform the empty washing, remove the turbidity adhering to the purification material with strong washing power by this empty washing, and remove the separated turbidity by the backwash water after the simultaneous washing. This is a method that discharges easily out of the device by washing.

【0005】[0005]

【発明が解決しようとする課題】ここで、上記方法にあ
っては、空洗は強い洗浄力を有しているため、併洗時に
は、逆洗水の供給と相俟って浄化処理層の上層と下層が
大きく混合する。このように浄化処理層の上層と下層が
大きく混合すると、上層の浄化材が下層に拡散して下層
の汚染が拡大されることになる。この下層に拡大した汚
染を、併洗後に実施される逆洗水による逆洗で上層を介
して装置外に排出して所望の度合いに浄化処理層を洗浄
するには、併洗後の逆洗水量を多量に要する。
Here, in the above method, since the empty washing has a strong detergency, at the time of simultaneous washing, the cleaning treatment layer is supplied together with the supply of the backwash water. The upper and lower layers are heavily mixed. When the upper layer and the lower layer of the purification treatment layer are greatly mixed in this way, the purification material of the upper layer is diffused into the lower layer, and the contamination of the lower layer is enlarged. In order to discharge the contamination that has spread to the lower layer to the outside through the upper layer by backwashing with backwash water that is performed after the co-washing and to clean the purification treatment layer to a desired degree, the backwashing after the co-washing is performed. Requires a large amount of water.

【0006】本発明は、このような課題を解決するため
になされたものであり、逆洗水と逆洗気体による併流逆
洗の後に実施される逆洗水による逆洗の水量を低減して
所望の度合いに浄化処理層を洗浄する濾過装置の逆洗方
法を提供することを目的とする。
SUMMARY OF THE INVENTION The present invention has been made to solve such a problem, and it is intended to reduce the amount of backwash water by backwash water which is performed after cocurrent backwash with backwash water and backwash gas. It is an object of the present invention to provide a method for backwashing a filtration device for washing a purification treatment layer to a desired degree.

【0007】[0007]

【課題を解決するための手段】本発明者らは、前述した
濾過装置の逆洗方法の問題点について検討した結果、併
流逆洗での逆洗気体による洗浄効果は、逆洗気体の供給
開始後数十秒程度が最も大きく、以降は、浄化材から濁
質を剥離させる浄化材同士の衝突効果が減少し、洗浄効
果が低下することを見出した。
Means for Solving the Problems The present inventors have examined the above-mentioned problems of the backwashing method of the filtration device and found that the effect of the backwashing gas in the cocurrent backwashing is as follows. After about several tens of seconds, the greatest effect was found, and thereafter, it was found that the effect of collision between the purifying materials for separating the suspended matter from the purifying material was reduced, and the cleaning effect was reduced.

【0008】そこで、本発明による濾過装置の逆洗方法
は、被処理水の濁質を捕捉する浄化材を積層して成る浄
化処理層に被処理水を通すことで当該被処理水を浄化処
理する濾過装置の浄化処理層を逆洗する方法であって、
浄化処理層に対して逆洗水と逆洗気体による併流逆洗を
実施してから逆洗水による逆洗を実施する逆洗方法にお
いて、併流逆洗での逆洗気体を、パルス状に間欠供給す
ることを特徴としている。
Therefore, the backwashing method for a filtration device according to the present invention is a process for purifying the water to be treated by passing the water to be treated through a purification treatment layer formed by laminating purification materials for trapping turbid substances of the water to be treated. Backwashing the purification treatment layer of the filtration device,
In the backwash method in which the backwash water and backwash gas are applied to the purification treatment layer in parallel, the backwash gas in the cocurrent backwash is intermittently pulsed. It is characterized by supplying.

【0009】このような濾過装置の逆洗方法によれば、
逆洗水と逆洗気体による併流逆洗での逆洗気体がパルス
状に間欠供給されるため、逆洗気体のパルス状供給期間
では、浄化材が強い洗浄力で洗浄されて浄化材同士の衝
突効果により当該浄化材から濁質が良好且つ効果的に剥
離され、逆洗気体のパルス状停止期間になると、逆洗水
のみが供給されて、この間では、併流逆洗で浮遊した浄
化材が比重差によって逆洗水に対して沈降分離し、一
方、浄化材から剥離した濁質は比重差が少ないので逆洗
水により浄化処理層の上部に移動し、この一連の浄化材
からの濁質の良好且つ効果的な剥離、濁質の浄化処理層
上部への移動が、逆洗気体のパルス状の間欠供給に従っ
て繰り返される。このため、濁質は、下部を汚染するこ
と無く上部に集合され、併流逆洗後の逆洗水による逆洗
で容易に装置外に排出される。
According to such a back washing method for a filtration device,
Since the backwash gas in the backwash water and the backwash gas in the cocurrent backwash is intermittently supplied in a pulsed manner, during the pulsed supply of the backwash gas, the purifying material is washed with strong cleaning power and the purifying materials are separated from each other. The turbid matter is effectively and effectively separated from the purifying material by the collision effect, and when the backwash gas is in a pulse stop period, only the backwash water is supplied. During this time, the purifying material floating in the cocurrent backwash is removed. The turbidity separated from the backwashing water due to the specific gravity difference, while the turbidity separated from the purification material moves to the upper part of the purification treatment layer by the backwashing water because the specific gravity difference is small, and the turbidity from this series of purification material And effective removal of turbidity and transfer of suspended matter to the upper part of the purification treatment layer are repeated in accordance with the pulsed intermittent supply of the backwash gas. Therefore, the turbid matter is collected at the upper portion without contaminating the lower portion, and is easily discharged out of the apparatus by backwashing with backwash water after co-current backwashing.

【0010】ここで、逆洗気体のパルス状の供給期間
は、10〜30秒間に設定されているのが好ましい。
Here, the pulse-like supply period of the backwash gas is preferably set to 10 to 30 seconds.

【0011】これは、逆洗気体のパルス状の供給期間が
30秒間を越えると、浄化処理層の上層と下層が大きく
混合され下層の汚染が拡大されて併流逆洗後の逆洗水に
よる逆洗水量を多量に要すると共に、浄化材同士が流動
化し衝突効果が低減されて洗浄効果が低下するからであ
り、一方、10秒間未満であると、浄化材からの濁質の
剥離が不十分となるからである。
This is because if the pulsed supply period of the backwash gas exceeds 30 seconds, the upper layer and the lower layer of the purification treatment layer are mixed greatly, and the contamination of the lower layer is enlarged, and the backwash water after the cocurrent backwash is used. This is because a large amount of water is required for washing, and the purifying materials are fluidized with each other, and the collision effect is reduced and the cleaning effect is reduced. On the other hand, if the cleaning time is less than 10 seconds, the removal of the turbidity from the purifying material is insufficient. Because it becomes.

【0012】また、逆洗気体のパルス状の停止期間は、
併流逆洗により浮上した浄化材が逆洗水に対して沈降分
離する迄の時間以上に設定されていると、浄化材の逆洗
水に対する沈降分離が十分に成され、浄化処理層下部の
汚染が一層防止される。
Further, the pulse-like stop period of the backwash gas is as follows:
If it is set longer than the time required for sedimentation of the purification material that floated by the cocurrent backwashing to the backwash water, sedimentation of the purification material to the backwash water will be sufficient, and contamination of the lower part of the purification treatment layer will occur. Is further prevented.

【0013】具体的には、逆洗気体のパルス状の停止期
間を、浄化処理層の膨張率が(逆洗水のみの供給で)5
%以下になる時間以上に設定することで、浄化材の逆洗
水に対する沈降分離が十分に成される。
[0013] Specifically, when the backwash gas is in a pulse-like stop period, the expansion rate of the purification layer is 5 (by supplying only backwash water).
%, The sedimentation and separation of the purification material with respect to the backwash water is sufficiently performed.

【0014】[0014]

【発明の実施の形態】以下、本発明に係る濾過装置の逆
洗方法の好適な実施形態について添付図面を参照しなが
ら説明する。図1は、本発明による逆洗方法を採用した
濾過装置を示す概略構成図である。
DETAILED DESCRIPTION OF THE PREFERRED EMBODIMENTS Preferred embodiments of a method for backwashing a filtration device according to the present invention will be described below with reference to the accompanying drawings. FIG. 1 is a schematic configuration diagram showing a filtration device employing a backwash method according to the present invention.

【0015】図1に示すように、濾過装置1は、浄化材
を収容する濾過槽2を備えている。濾過槽2は、仕切板
3で上部空間と下部空間とに分割され、この仕切板3に
は、上部空間と下部空間とを連通する集水ノズル4が複
数貫通して設置されている。上部空間には、被処理水
(例えば下水の二次処理水等)を供給する被処理水供給
ラインL1が接続されると共に、逆洗時の逆洗排水を外
部に排出する逆洗排水ラインL6が接続されるトラフ5
が複数設置されている。このトラフ5は、被処理水が流
入することで当該被処理水の濾過槽2内の供給を可能と
する一方で、逆洗時の逆洗排水が流入することで当該逆
洗排水の外部排出を可能とする。
As shown in FIG. 1, the filtration device 1 has a filtration tank 2 for accommodating a purifying material. The filtration tank 2 is divided into an upper space and a lower space by a partition plate 3, and a plurality of water collecting nozzles 4 that communicate the upper space and the lower space penetrate the partition plate 3. A treated water supply line L1 for supplying treated water (for example, sewage secondary treated water) is connected to the upper space, and a backwash drainage line L6 for discharging backwash wastewater during backwash to the outside. Is connected to trough 5
Are installed. The trough 5 enables the supply of the to-be-processed water into the filtration tank 2 when the to-be-processed water flows in, while the back-washing drainage at the time of the back-washing flows in when the to-be-processed water flows into the outside. Is possible.

【0016】また、仕切板3上であってトラフ5の下方
には、浄化材を積層して成る浄化処理層6が配設されて
いる。この浄化材としては、例えば砂、アンスラサイト
等の濾材や例えば活性炭等の吸着材が採用され、この濾
材や吸着材を敷き詰めて積層することで浄化処理層6が
形成されている。この浄化処理槽6は、被処理水が通過
することで当該被処理水を浄化処理する。
On the partition plate 3 and below the trough 5, a purification treatment layer 6 formed by laminating purification materials is provided. As this purifying material, for example, a filtering material such as sand or anthracite or an adsorbing material such as activated carbon is adopted, and the purifying treatment layer 6 is formed by spreading and laminating the filtering material and the adsorbent. The purification treatment tank 6 purifies the treatment water by passing the treatment water.

【0017】下部空間には、浄化処理層6で浄化処理さ
れ集中ノズル4を介して流下される濾過水を外部に排出
する濾過水排出ラインL2が接続されている。また、下
部空間には、散気用空気供給ラインL3を介して散気用
ブロワ7が接続されている。この散気用ブロワ7は、散
気用空気供給ラインL3、下部空間、集中ノズル4を介
して浄化処理層6に空気を供給し、当該浄化処理層6を
散気する。
The lower space is connected to a filtered water discharge line L2 for discharging filtered water that has been purified by the purification treatment layer 6 and flows down through the centralized nozzle 4. In addition, an air blower 7 is connected to the lower space via an air supply line L3 for air diffusion. The air blower 7 supplies air to the purification processing layer 6 through the air supply line L3 for diffusion, the lower space, and the centralized nozzle 4, and diffuses the purification processing layer 6.

【0018】さらに、下部空間には、逆洗水供給ライン
L4を介して逆洗用水源8が接続されると共に、逆洗空
気供給ラインL5を介して逆洗用ブロワ9が接続されて
いる。逆洗水供給ラインL4には逆洗ポンプ10が介装
され、この逆洗ポンプ10を駆動することで、逆洗用水
源8の水(逆洗水)を、逆洗水供給ラインL4、下部空
間、集中ノズル4を介して浄化処理層6に供給し、当該
浄化処理層6を水逆洗する。また、逆洗用ブロワ9は、
逆洗空気供給ラインL5、下部空間、集中ノズル4を介
して浄化処理層6に空気(逆洗空気)を供給し、当該浄
化処理層6を空気逆洗する。
Further, a backwash water source 8 is connected to the lower space via a backwash water supply line L4, and a backwash blower 9 is connected via a backwash air supply line L5. A backwash pump 10 is interposed in the backwash water supply line L4, and by driving the backwash pump 10, water (backwash water) from the backwash water source 8 is supplied to the backwash water supply line L4. The water is supplied to the purification treatment layer 6 through the space and the centralized nozzle 4, and the purification treatment layer 6 is backwashed with water. Also, the backwashing blower 9
Air (backwash air) is supplied to the purification treatment layer 6 through the backwash air supply line L5, the lower space, and the centralized nozzle 4, and the purification treatment layer 6 is backwashed with air.

【0019】この濾過装置1では、逆洗時には、水逆洗
と空気逆洗を併用する併流逆洗を実施し、この併流逆洗
後に水逆洗を実施する。併流逆洗では、逆洗用ブロワ9
及び逆洗ポンプ10を同時に駆動し、特に本実施形態の
併流逆洗では、逆洗用ブロワ9をパルス状に間欠駆動
し、逆洗空気をパルス状に間欠供給する空気逆洗(以下
パルス空気逆洗と呼ぶ)を、逆洗ポンプ10の駆動によ
る連続的な水逆洗と同時に実施する(詳しくは後述)。
また、併流逆洗後の水逆洗では、逆洗ポンプ10の単独
駆動による連続的な水逆洗を実施する。
In the filtration apparatus 1, at the time of backwashing, cocurrent backwashing using both water backwashing and air backwashing is performed, and after this cocurrent backwashing, water backwashing is performed. In cocurrent backwash, backwash blower 9
And the backwashing pump 10 is simultaneously driven. In particular, in the cocurrent backwashing of the present embodiment, the backwashing blower 9 is intermittently driven in a pulsed manner, and the backwashing air is intermittently supplied in a pulsed manner. Backwashing) is performed simultaneously with continuous water backwashing driven by the backwash pump 10 (to be described in detail later).
Further, in the water backwashing after the cocurrent backwashing, the continuous backwashing is performed by driving the backwashing pump 10 alone.

【0020】このような濾過装置1によれば、濾過時に
は、被処理水供給ラインL1、濾過水排出ラインL2、
散気用空気供給ラインL3が開にされると共に、逆洗水
供給ラインL4、逆洗空気供給ラインL5、逆洗排水ラ
インL6が閉にされる。この状態で、散気用ブロワ7が
駆動されて空気が浄化処理層6に供給され、当該浄化処
理層6が散気されて生物分解機能が与えられる一方で、
被処理水が濾過槽2内に供給される。この被処理水は、
流下に従って浄化処理層6で濁質が捕捉されると共に溶
解性有機物が酸化・分解処理される。この濁質は、浄化
処理層6の上層から下層に向かうに従って指数的に減少
するように捕捉され、濾過水は、集中ノズル4、下部空
間、濾過水排出ラインL2を介して外部に排出される。
According to such a filtration device 1, at the time of filtration, the treated water supply line L1, the filtered water discharge line L2,
The air supply line L3 for aeration is opened, and the backwash water supply line L4, the backwash air supply line L5, and the backwash drainage line L6 are closed. In this state, the air blower 7 is driven to supply air to the purification treatment layer 6, and the purification treatment layer 6 is diffused to provide a biodegradation function.
The water to be treated is supplied into the filtration tank 2. This treated water is
The suspended matter is captured by the purification treatment layer 6 as it flows down, and the soluble organic matter is oxidized and decomposed. This suspended matter is trapped so as to decrease exponentially from the upper layer to the lower layer of the purification treatment layer 6, and the filtered water is discharged to the outside via the centralized nozzle 4, the lower space, and the filtered water discharge line L2. .

【0021】ここで、所定の時期になると、浄化処理層
6を洗浄すべく、逆洗が実施される。この逆洗時には、
先ず、被処理水供給ラインL1、散気用空気供給ライン
L3が開から閉にされると共に散気用ブロワ7が停止さ
れ、濾過槽2内の水を濾過水排出ラインL2を介して外
部に抜く水抜きが実施される。
Here, at a predetermined time, back washing is performed to wash the purification treatment layer 6. During this backwash,
First, the water supply line L1 for treatment and the air supply line L3 for air diffusion are closed from open and the blower 7 for air diffusion is stopped, and the water in the filtration tank 2 is discharged to the outside via the filtration water discharge line L2. Draining is performed.

【0022】次いで、濾過水排出ラインL2が開から閉
にされると共に、逆洗水供給ラインL4、逆洗空気供給
ラインL5、逆洗排水ラインL6が閉から開にされる。
この状態で、逆洗ポンプ10が連続駆動されると共に逆
洗用ブロワ9がパルス状に間欠駆動され、浄化処理層6
に対して、水逆洗とパルス空気逆洗を併用する併流逆洗
が実施される。
Next, the filtered water discharge line L2 is changed from open to closed, and the backwash water supply line L4, the backwash air supply line L5, and the backwash drainage line L6 are changed from closed to open.
In this state, the backwashing pump 10 is continuously driven, and the backwashing blower 9 is intermittently driven in a pulsed manner.
On the other hand, cocurrent backwashing using both water backwashing and pulse air backwashing is performed.

【0023】ここで、本実施形態では、図2に示すよう
に、水逆洗の強度を12m/時、パルス空気逆洗の強度
を24m/時とする併流逆洗が3分間実施され、パルス
空気逆洗では、逆洗空気を20秒毎に供給(オン)/停
止(オフ)する間欠供給とされている。
In this embodiment, as shown in FIG. 2, cocurrent backwashing is performed for 3 minutes with a water backwashing intensity of 12 m / hour and a pulse air backwashing intensity of 24 m / hour. In the air backwashing, the backwash air is intermittently supplied (on) / stopped (off) every 20 seconds.

【0024】このように逆洗空気がパルス状に間欠供給
されるため、逆洗空気のパルス状供給期間では、浄化材
が強い洗浄力で洗浄されて浄化材同士の衝突効果により
当該浄化材から濁質が良好且つ効果的に剥離され、逆洗
空気のパルス状停止期間になると、逆洗水のみが供給さ
れて、この間では、併流逆洗で浮遊した浄化材が比重差
によって逆洗水に対して沈降分離し、一方、浄化材から
剥離した濁質は比重差が少ないので逆洗水により浄化処
理層6の上部に移動し、この一連の浄化材からの濁質の
良好且つ効果的な剥離、濁質の浄化処理層6上部への移
動が、逆洗空気のパルス状の間欠供給に従って繰り返さ
れる。従って、濁質は、下部を汚染すること無く上部に
集合される。
Since the backwash air is thus intermittently supplied in a pulsed manner, the purifying material is washed with a strong detergency during the pulsed supply period of the backwash air, and the purifying material is collided with the purifying material by an effect of collision between the purifying materials. When the suspended matter is successfully and effectively peeled off and the backwash air is in a pulse-stop period, only the backwash water is supplied. During this time, the purification material floating in the co-current backwash is converted into the backwash water by a difference in specific gravity. On the other hand, the turbid matter separated from the purifying material by sedimentation is moved to the upper part of the purifying treatment layer 6 by the backwashing water because the difference in specific gravity is small. The separation and the movement of the suspended matter to the upper part of the purification treatment layer 6 are repeated according to the pulsed intermittent supply of the backwash air. Therefore, the turbid matter is collected at the upper part without contaminating the lower part.

【0025】ここで、逆洗空気のパルス状の供給期間
は、本実施形態のように10〜30秒間(本実施形態で
は20秒間)に設定されているのが好ましい。これは、
逆洗空気のパルス状の供給期間が30秒間を越えると、
浄化処理層6の上層と下層が大きく混合され下層の汚染
が拡大されて後述の併流逆洗後の逆洗水による逆洗水量
を多量に要すると共に、浄化材同士が流動化し衝突効果
が低減されて洗浄効果が低下するからであり、一方、1
0秒間未満であると、浄化材からの濁質の剥離が不十分
となるからである。
Here, the pulse-like supply period of the backwash air is preferably set to 10 to 30 seconds (20 seconds in this embodiment) as in this embodiment. this is,
If the pulsed supply period of backwash air exceeds 30 seconds,
The upper layer and the lower layer of the purification treatment layer 6 are greatly mixed, and the contamination of the lower layer is enlarged, so that a large amount of backwash water is required by the backwash water after the cocurrent backwash described later, and the purifying materials are fluidized to reduce the collision effect. On the other hand, the cleaning effect is reduced.
If the time is less than 0 second, the turbidity is not sufficiently separated from the purifying material.

【0026】そして、逆洗用ブロワ9が停止されて併流
逆洗が終了すると、さらに逆洗ポンプ10が単独で連続
駆動される水逆洗が実施される。本実施形態では、図2
に示すように、水逆洗の強度を54m/時として10分
間実施される。
Then, when the backwashing blower 9 is stopped and the cocurrent backwashing is completed, water backwashing in which the backwash pump 10 is continuously driven independently is performed. In the present embodiment, FIG.
As shown in Fig. 8, the backwashing was performed for 10 minutes with the intensity of water backwashing at 54 m / hour.

【0027】この水逆洗で、併流逆洗により浄化処理層
6の上部に集合されている濁質が、逆洗排水と共にトラ
フ5、逆洗排水ラインL6を介して、容易に装置外に排
出される。
In this water backwashing, the turbid matter collected on the upper part of the purification treatment layer 6 by the cocurrent backwashing is easily discharged outside the apparatus together with the backwashing drainage through the trough 5 and the backwashing drainage line L6. Is done.

【0028】このように、本実施形態においては、水逆
洗との併流逆洗でパルス空気逆洗が実施されるため、浄
化材からの濁質の良好且つ効果的な剥離、濁質の浄化処
理層6上部への移動が、逆洗空気のパルス状の間欠供給
に従って繰り返され、濁質が、浄化処理層6下部を汚染
すること無く上部に集合されて、併流逆洗後の水逆洗で
容易に装置外に排出される。従って、併流逆洗後の水逆
洗の水量を低減して所望の度合いに浄化処理層6を洗浄
するのが可能とされている。
As described above, in this embodiment, the pulsed air backwash is carried out in the cocurrent backwash with the water backwash, so that the turbid material can be effectively and effectively separated from the purifying material, and the turbid material can be purified. The movement to the upper part of the treatment layer 6 is repeated according to the pulsed intermittent supply of the backwashing air, and the suspended matter is collected at the upper part without contaminating the lower part of the purification treatment layer 6, and the water is backwashed after the cocurrent backwashing. And is easily discharged out of the device. Therefore, it is possible to reduce the amount of water in the water backwashing after the cocurrent backwashing and to wash the purification treatment layer 6 to a desired degree.

【0029】なお、本実施形態においては、逆洗空気の
パルス状の停止期間を20秒としているが、併流逆洗で
の逆洗水量、浄化材の径、浄化材の比重等により異なる
ものであり、要は、併流逆洗により浮上した浄化材が併
流逆洗での逆洗水に対して沈降分離する迄の時間以上に
設定されていれば良い。これにより、浄化材の併流逆洗
での逆洗水に対する沈降分離が十分に成され、浄化処理
層6下部の汚染が一層防止されることになる。具体的に
は、逆洗空気のパルス状の停止期間を、浄化処理層6の
膨張率が(逆洗水のみの供給で)5%以下になる時間以
上に設定すれば、浄化材の逆洗水に対する沈降分離が十
分に成される。
In this embodiment, the pulse-like stop period of the backwash air is set to 20 seconds. However, the period differs depending on the backwash water amount, the diameter of the purifying material, the specific gravity of the purifying material, etc. in the co-current backwashing. In other words, it is only necessary that the time is set to be equal to or longer than the time required for the cleaning material floated by the cocurrent backwash to settle and separate from the backwash water in the cocurrent backwash. As a result, sedimentation and separation of the cleaning material in the backwash water in the cocurrent backwashing is sufficiently performed, and contamination of the lower part of the purification treatment layer 6 is further prevented. Specifically, if the pulse-like stop period of the backwashing air is set to be equal to or longer than the time when the expansion rate of the purification treatment layer 6 becomes 5% or less (by supplying only the backwash water), the backwashing of the purification material is performed. The sedimentation separation for water is sufficiently achieved.

【0030】以下、上記実施形態の効果を確認すべく、
本発明者が実施した実施例1、2及び比較例1、2につ
いて述べる。
Hereinafter, in order to confirm the effects of the above embodiment,
Examples 1 and 2 and Comparative Examples 1 and 2 performed by the inventor will be described.

【0031】(実施例1、2)河川水にPAC(ポリ塩
化アルミニウムクロライド:無機凝集剤)を混合して凝
集沈殿処理した処理水を、濾過した濾過装置を用い、こ
の濾過装置に対して、水逆洗とパルス空気逆洗の併流逆
洗を実施し、この後水逆洗を実施した。浄化処理層に
は、有効径1.2mm、均等係数1.3の活性炭を用
い、当該浄化処理層の面積を0.64m2、層厚を20
00mmとした。併流逆洗でのパルス空気逆洗の強度は
24m/時、併流逆洗での水逆洗の強度は18m/時と
し、パルス空気逆洗では、逆洗空気を20秒毎に供給/
停止する間欠供給として、このパルス空気逆洗と水逆洗
の併流逆洗を3分間実施した。併流逆洗終了後の水逆洗
は、その強度を54m/時とし、浄化処理層の膨張率を
35%として、15分間実施し、この時の逆洗排水濁度
の経時変化を調べた。実験は2回に分けて実施し、各々
を実施例1、実施例2とした。
(Examples 1 and 2) Using a filtration device for filtering treated water obtained by mixing river water with PAC (polyaluminum chloride: inorganic flocculant) and subjecting it to coagulation and sedimentation, Cocurrent backwashing of water backwashing and pulse air backwashing was performed, and then water backwashing was performed. Activated carbon having an effective diameter of 1.2 mm and a uniformity coefficient of 1.3 was used for the purification treatment layer. The area of the purification treatment layer was 0.64 m 2 , and the layer thickness was 20.
00 mm. The strength of the pulse air backwash in the cocurrent backwash is 24 m / hour, the strength of the water backwash in the cocurrent backwash is 18 m / hour, and the backwash air is supplied every 20 seconds in the pulse air backwash.
As an intermittent supply to stop, the cocurrent backwash of the pulse air backwash and water backwash was performed for 3 minutes. Water backwashing after the cocurrent backwashing was carried out for 15 minutes at an intensity of 54 m / hour and an expansion rate of the purification treatment layer of 35%, and the time-dependent change in backwash wastewater turbidity at this time was examined. The experiment was performed in two parts, each of which was referred to as Example 1 or Example 2.

【0032】(比較例1、2)併流逆洗で、逆洗空気を
継続して3分間供給する点以外は実施例1、2と同様と
した。実験は2回に分けて実施し、各々を比較例1、比
較例2とした。
(Comparative Examples 1 and 2) The procedure was the same as in Examples 1 and 2, except that backwash air was continuously supplied for 3 minutes in co-current backwashing. The experiment was performed in two parts, each of which was Comparative Example 1 and Comparative Example 2.

【0033】その結果を以下の表1に示すThe results are shown in Table 1 below.

【0034】[0034]

【表1】 [Table 1]

【0035】表1に示すように、例えば市場での要求値
とされている濁度1.5mg/Lを、実施例1、2で
は、併流逆洗後の水逆洗開始から10分で達成できるの
に対し、比較例1、2では15分でも達成できず、従っ
て、所望の度合いに浄化処理層を洗浄するのに必要な併
流逆洗後の逆洗水量が、実施例1、2の方が比較例1、
2に比して少なくて済むというのが分かる。
As shown in Table 1, for example, the turbidity of 1.5 mg / L, which is required in the market, was achieved in Examples 1 and 2 in 10 minutes from the start of water backwashing after cocurrent backwashing. On the other hand, in Comparative Examples 1 and 2, the amount of backwash water after co-current backwashing required to wash the purification treatment layer to a desired degree cannot be achieved even in 15 minutes. Is better in Comparative Example 1,
It can be seen that the number is smaller than that of 2.

【0036】さらに、本発明者らは、逆洗空気のパルス
状の供給期間を10〜30秒間とすることの効果を、以
下の実施例3で確認した。
Further, the present inventors confirmed the effect of setting the pulse-like supply period of the backwash air to 10 to 30 seconds in the following Example 3.

【0037】(実施例3)カオリン20mg/L、PA
C7.5mg/Lで調整した原水(被処理水)を、18
0m/日の濾過速度で15時間に亘って濾過した濾過装
置を用い、この濾過装置に対して、水逆洗とパルス空気
逆洗の併流逆洗を実施し、この後水逆洗を実施した。浄
化処理層には、有効径0.6mmの砂を用い、併流逆洗
でのパルス空気逆洗の強度は50m/時、併流逆洗での
水逆洗の強度は25m/時とし、逆洗空気のパルス状供
給期間を変数として併流逆洗を4分間実施した。併流逆
洗終了後の水逆洗は、その強度を50m/時として、1
0分間実施し、10分経過時の逆洗排水の濁度を調べ
た。この逆洗排水濁度と併流逆洗での逆洗空気のパルス
状供給期間との関係を図3に示す。図3に示すように、
逆洗空気のパルス状の供給期間を10〜30秒間とする
ことで、逆洗排水濁度が、前述した約1.5mg/L未
満に低減されるのが分かる。従って、逆洗空気のパルス
状の供給期間を10〜30秒間とすれば、所望の度合い
に浄化処理層を洗浄するのに必要な併流逆洗後の逆洗水
量を少なくできる。
Example 3 Kaolin 20 mg / L, PA
Raw water (treated water) adjusted at 7.5 mg / L C
Using a filtration device that was filtered at a filtration speed of 0 m / day for 15 hours, the filtration device was subjected to cocurrent backwashing of water backwashing and pulse air backwashing, and then water backwashing. . For the purification layer, sand with an effective diameter of 0.6 mm was used. The strength of pulse air backwash in cocurrent backwash was 50 m / h, and the strength of water backwash in cocurrent backwash was 25 m / hour. Cocurrent backwashing was performed for 4 minutes with the pulsed supply period of air as a variable. Water backwashing after co-current backwashing is performed with the strength of 50 m / hour and 1
It was carried out for 0 minutes, and the turbidity of the backwash wastewater after 10 minutes was examined. FIG. 3 shows the relationship between the backwash drainage turbidity and the pulsed supply period of the backwash air in the cocurrent backwash. As shown in FIG.
It can be seen that the backwash drainage turbidity is reduced to less than about 1.5 mg / L by setting the pulsed supply period of the backwash air to 10 to 30 seconds. Therefore, if the pulse-like supply period of the backwash air is set to 10 to 30 seconds, the amount of backwash water after co-current backwash necessary for washing the purification treatment layer to a desired degree can be reduced.

【0038】以上、本発明をその実施形態に基づき具体
的に説明したが、本発明は上記実施形態に限定されるも
のではなく、例えば、上記実施形態においては、併流逆
洗での逆洗空気のパルス状供給期間を、同一時間(実施
形態では20秒で全て同一)としているが、異なる時間
としても良い。同様に、逆洗空気のパルス状停止期間
も、同一時間(実施形態では20秒で全て同一)ではな
く異なる時間としても良い。また、併流逆洗でのパルス
空気逆洗の開始・終了が、併流逆洗での水逆洗の開始・
終了と必ずしも同期していなくても良い。
As described above, the present invention has been specifically described based on the embodiment. However, the present invention is not limited to the above embodiment. For example, in the above embodiment, the backwash air in the cocurrent backwash is used. Are set to the same time (all the same in 20 seconds in the embodiment), but may be set to different times. Similarly, the pulse-like stop period of the backwash air may be different from the same period (20 seconds in the embodiment, all the same). In addition, the start and end of pulse air backwash in cocurrent backwash are the same as the start and end of water backwash in cocurrent backwash.
It does not necessarily have to be synchronized with the end.

【0039】さらにまた、併流逆洗でパルス状に間欠供
給する逆洗気体は、空気に限定されるものではない。
Further, the backwash gas intermittently supplied in the form of pulses in the cocurrent backwash is not limited to air.

【0040】[0040]

【発明の効果】本発明による濾過装置の逆洗方法は、逆
洗水と逆洗気体による併流逆洗での逆洗気体をパルス状
に間欠供給し、逆洗気体のパルス状供給期間で、浄化材
を強い洗浄力で洗浄して浄化材同士の衝突効果により当
該浄化材から濁質を良好且つ効果的に剥離し、逆洗気体
のパルス状停止期間になると、逆洗水のみを供給して、
この間に、併流逆洗で浮遊した浄化材を比重差によって
逆洗水に対して沈降分離させ、一方、浄化材から剥離し
た濁質は比重差が少ないので逆洗水により浄化処理層の
上部に移動させ、この一連の浄化材からの濁質の良好且
つ効果的な剥離、濁質の浄化処理層上部への移動を、逆
洗気体のパルス状の間欠供給に従って繰り返し、濁質
を、下部を汚染すること無く上部に集合して、併流逆洗
後の逆洗水による逆洗で容易に装置外に排出するように
したものであるから、併流逆洗後の逆洗水による逆洗の
水量を低減して所望の度合いに浄化処理層を洗浄するの
が可能となる。
The method for backwashing a filtration device according to the present invention comprises intermittently supplying backwash gas in a cocurrent backwash with backwash water and backwash gas in a pulsed manner. The purifying material is washed with a strong cleaning power to turbidly separate the purifying material satisfactorily and effectively due to the collision effect between the purifying materials. When the backwash gas is in a pulse stop period, only the backwash water is supplied. hand,
During this time, the purification material suspended in the co-current backwash is settled and separated from the backwash water by the difference in specific gravity, while the turbidity separated from the purification material has a small difference in specific gravity. The turbidity is removed from the purifying material in a series of good and effective separation, and the turbidity is moved to the upper part of the purification treatment layer in accordance with the pulsed intermittent supply of the backwash gas. It is collected at the top without contaminating and is easily discharged outside the equipment by backwashing with backwash water after cocurrent backwashing, so the amount of backwash water by backwash water after cocurrent backwashing And it is possible to clean the purification treatment layer to a desired degree.

【図面の簡単な説明】[Brief description of the drawings]

【図1】本発明による逆洗方法を採用した濾過装置を示
す概略構成図である。
FIG. 1 is a schematic configuration diagram showing a filtration device employing a backwashing method according to the present invention.

【図2】本発明による逆洗方法を具体的に示す工程説明
図である。
FIG. 2 is a process explanatory view specifically showing a backwashing method according to the present invention.

【図3】本発明による逆洗方法で供給される逆洗空気の
パルス状供給期間と逆洗排水濁度との関係を示す図であ
る。
FIG. 3 is a diagram showing the relationship between the pulsed supply period of backwash air supplied by the backwash method according to the present invention and the backwash wastewater turbidity.

【符号の説明】[Explanation of symbols]

1…濾過装置、6…浄化処理層(浄化材積層)、8…逆
洗用水源、9…逆洗用ブロワ、10…逆洗ポンプ、L1
…被処理水供給ライン、L4…逆洗水供給ライン、L5
…逆洗空気供給ライン、L6…逆洗排水ライン。
DESCRIPTION OF SYMBOLS 1 ... Filtration apparatus, 6 ... Purification processing layer (purification material lamination), 8 ... Backwash water source, 9 ... Backwash blower, 10 ... Backwash pump, L1
… Treated water supply line, L4… backwash water supply line, L5
... Backwash air supply line, L6 ... Backwash drain line.

───────────────────────────────────────────────────── フロントページの続き (72)発明者 村田 圭三 東京都品川区北品川五丁目9番11号 住友 重機械工業株式会社内 Fターム(参考) 4D041 BA01 BB03 BB04 BC03 BC12 ────────────────────────────────────────────────── ─── Continuing on the front page (72) Inventor Keizo Murata F-term (reference) 4D041 BA01 BB03 BB04 BC03 BC12 within 5-9-1, Kita-Shinagawa, Shinagawa-ku, Tokyo

Claims (4)

【特許請求の範囲】[Claims] 【請求項1】 被処理水の濁質を捕捉する浄化材を積層
して成る浄化処理層に被処理水を通すことで当該被処理
水を浄化処理する濾過装置の前記浄化処理層を逆洗する
方法であって、前記浄化処理層に対して逆洗水と逆洗気
体による併流逆洗を実施してから逆洗水による逆洗を実
施する逆洗方法において、 前記併流逆洗での前記逆洗気体を、パルス状に間欠供給
することを特徴とする濾過装置の逆洗方法。
1. A purifying treatment layer of a filtration device for purifying a treated water by passing the treated water through a purifying treatment layer formed by laminating a purifying material for trapping a turbid substance of the treated water. A backwashing method for performing backwashing with backwash water and backwashing gas with respect to the purification treatment layer, and then performing backwashing with backwash water. A method for backwashing a filtration device, comprising intermittently supplying a backwash gas in a pulsed manner.
【請求項2】 前記逆洗気体の前記パルス状の供給期間
は、10〜30秒間に設定されていることを特徴とする
請求項1記載の濾過装置の逆洗方法。
2. The method according to claim 1, wherein the pulsed supply period of the backwash gas is set to 10 to 30 seconds.
【請求項3】 前記逆洗気体の前記パルス状の停止期間
は、前記併流逆洗により浮上した前記浄化材が前記逆洗
水に対して沈降分離する迄の時間以上に設定されている
ことを特徴とする請求項1または2記載の濾過装置の逆
洗方法。
3. The pulse-like stop period of the backwash gas is set to be equal to or longer than a time required for the cleaning material floated by the co-current backwash to settle and separate from the backwash water. The method for backwashing a filtration device according to claim 1 or 2,
【請求項4】 前記逆洗気体の前記パルス状の停止期間
は、前記浄化処理層の膨張率が5%以下になる時間以上
に設定されていることを特徴とする請求項1〜3の何れ
か一項に記載の濾過装置の逆洗方法。
4. The method according to claim 1, wherein the pulse-shaped stop period of the backwash gas is set to a time period at which an expansion rate of the purification treatment layer becomes 5% or less. The method for backwashing a filtration device according to claim 1.
JP2000316816A 2000-10-17 2000-10-17 Method of back washing filter device Pending JP2002119807A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP2000316816A JP2002119807A (en) 2000-10-17 2000-10-17 Method of back washing filter device

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP2000316816A JP2002119807A (en) 2000-10-17 2000-10-17 Method of back washing filter device

Publications (1)

Publication Number Publication Date
JP2002119807A true JP2002119807A (en) 2002-04-23

Family

ID=18795711

Family Applications (1)

Application Number Title Priority Date Filing Date
JP2000316816A Pending JP2002119807A (en) 2000-10-17 2000-10-17 Method of back washing filter device

Country Status (1)

Country Link
JP (1) JP2002119807A (en)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2014079665A (en) * 2012-10-12 2014-05-08 Swing Corp Cleaning method of water treatment device
CN104208928A (en) * 2013-06-05 2014-12-17 中国石油天然气集团公司 Pulse backwashing deep bed filter device and method

Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS5667511A (en) * 1979-11-07 1981-06-06 Kotobuki Kakoki Kk Washing method of filter layer which comprises particulate filter medium
JPS63185417A (en) * 1987-01-28 1988-08-01 ジンプロ/パサヴァント・インコーポレーテッド Removal of impurities from filtered fluid
JPH02191511A (en) * 1989-01-20 1990-07-27 Nkk Corp Filter and its back-washing method
JPH03293005A (en) * 1990-04-06 1991-12-24 Ngk Insulators Ltd Method and device for backwashing by siphoning
JPH04200604A (en) * 1990-11-30 1992-07-21 Tokyo Metropolis Washing method for packed bed equipment
JPH0751511A (en) * 1993-08-12 1995-02-28 Kurita Water Ind Ltd Filtering apparatus
JPH07313809A (en) * 1994-05-26 1995-12-05 Mitsui Mining Co Ltd Filter device
JPH09276610A (en) * 1996-04-12 1997-10-28 Suido Kiko Kaisha Ltd Valveless filtering device

Patent Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS5667511A (en) * 1979-11-07 1981-06-06 Kotobuki Kakoki Kk Washing method of filter layer which comprises particulate filter medium
JPS63185417A (en) * 1987-01-28 1988-08-01 ジンプロ/パサヴァント・インコーポレーテッド Removal of impurities from filtered fluid
JPH02191511A (en) * 1989-01-20 1990-07-27 Nkk Corp Filter and its back-washing method
JPH03293005A (en) * 1990-04-06 1991-12-24 Ngk Insulators Ltd Method and device for backwashing by siphoning
JPH04200604A (en) * 1990-11-30 1992-07-21 Tokyo Metropolis Washing method for packed bed equipment
JPH0751511A (en) * 1993-08-12 1995-02-28 Kurita Water Ind Ltd Filtering apparatus
JPH07313809A (en) * 1994-05-26 1995-12-05 Mitsui Mining Co Ltd Filter device
JPH09276610A (en) * 1996-04-12 1997-10-28 Suido Kiko Kaisha Ltd Valveless filtering device

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2014079665A (en) * 2012-10-12 2014-05-08 Swing Corp Cleaning method of water treatment device
CN104208928A (en) * 2013-06-05 2014-12-17 中国石油天然气集团公司 Pulse backwashing deep bed filter device and method
CN104208928B (en) * 2013-06-05 2015-12-23 中国石油天然气集团公司 A kind of pulse backwashing deep-bed filtration device and method

Similar Documents

Publication Publication Date Title
US3640387A (en) Removal of floc from settling device
KR101794195B1 (en) System for Recycling of Processed Waste Water
KR0166421B1 (en) Reverse washing method of waste water treating equipment by floatable filter media
JPH10109095A (en) Water purifying treatment device
JP3652567B2 (en) Cleaning method for filtration equipment
JP2745174B2 (en) Membrane filtration device
JPH11244870A (en) Flocculating and settling device for sewage and cleaning method thereof
JP2002119807A (en) Method of back washing filter device
JPS6216125B2 (en)
JP3384029B2 (en) Water purification device and water purification method
JP2002224543A (en) Water purification treatment method and apparatus therefor
JP3235740B2 (en) Solid-liquid separation device
JP2001347295A (en) Apparatus for cleaning seawater containing floating substance
DE3316480A1 (en) METHOD AND DEVICE FOR PURIFYING LIQUIDS
RU2238916C1 (en) Natural water purification process
JP3666065B2 (en) Biological filtration type nitrogen removal method
JPH0889709A (en) Separating and removing method of mixture in liquid
JP2002316183A (en) Method and apparatus for treating sewage
JPH07275610A (en) Precipitation filtration method and apparatus therefor
JPH01115500A (en) Slurry filtering method
JP2003117551A (en) Method and device for treating dioxins-containing waste water
JPH01171693A (en) Biomembrane filtration apparatus
JPH07323295A (en) Water purifier
JP3097164U (en) Integrated solid-liquid separation device
JPH044805Y2 (en)

Legal Events

Date Code Title Description
A711 Notification of change in applicant

Free format text: JAPANESE INTERMEDIATE CODE: A712

Effective date: 20070628

A625 Written request for application examination (by other person)

Free format text: JAPANESE INTERMEDIATE CODE: A625

Effective date: 20070919

RD01 Notification of change of attorney

Free format text: JAPANESE INTERMEDIATE CODE: A7421

Effective date: 20071011

A977 Report on retrieval

Free format text: JAPANESE INTERMEDIATE CODE: A971007

Effective date: 20090223

A131 Notification of reasons for refusal

Free format text: JAPANESE INTERMEDIATE CODE: A131

Effective date: 20100615

A521 Written amendment

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20100715

A02 Decision of refusal

Free format text: JAPANESE INTERMEDIATE CODE: A02

Effective date: 20101102