JP2001131866A - Antifungal and antibacterial treatment of fiber with turmeric extract - Google Patents
Antifungal and antibacterial treatment of fiber with turmeric extractInfo
- Publication number
- JP2001131866A JP2001131866A JP34516299A JP34516299A JP2001131866A JP 2001131866 A JP2001131866 A JP 2001131866A JP 34516299 A JP34516299 A JP 34516299A JP 34516299 A JP34516299 A JP 34516299A JP 2001131866 A JP2001131866 A JP 2001131866A
- Authority
- JP
- Japan
- Prior art keywords
- turmeric
- mordant
- extract
- fiber
- antifungal
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Landscapes
- Agricultural Chemicals And Associated Chemicals (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
Abstract
Description
【0001】[0001]
【発明の属する技術分野】本発明は、高い抗菌性を有す
るウコンの抽出物を有効成分として含有する事を特徴と
し優れた植物性抗菌加工製造に関するものである。BACKGROUND OF THE INVENTION 1. Field of the Invention The present invention relates to an excellent production of a plant antibacterial process characterized by containing an extract of turmeric having high antibacterial properties as an active ingredient.
【0002】[0002]
【従来の技術】従来の抗菌加工剤として有機系(36
群)と無機系(1群)があり、全体として約110種以
上の抗菌剤が使用されている。それぞれ一長一短があ
り、中には皮膚かぶれや環境高負荷かつ生態系に異常を
きたすものも見受けられる。染剤分子の構造により過剰
な抗菌加工が廃止され、選択殺菌(微生物の種類を判別
し、目的の有害微生物のみ殺菌する)が可能で、かつ地
球環境低負荷の抗菌剤、並びに抗菌加工技術の開発が望
まれる。2. Description of the Related Art As a conventional antibacterial processing agent, organic (36)
Group) and inorganic type (group 1), and about 110 or more antibacterial agents are used as a whole. Each has its pros and cons, and some of them have skin irritation, high environmental load, and ecosystem abnormalities. Excessive antibacterial processing is abolished by the structure of the dye molecule, and selective sterilization (discriminating the type of microorganism and sterilizing only the harmful microorganisms of interest) is possible. Development is desired.
【0003】[0003]
【発明が解決しようとする課題】本発明では、かかる状
況を鑑み、鋭意研究を重ねた結果、ウコンの抽出物に含
有するクルクミン及びタンニン及びサポニンが安定した
高い抗菌性を有し、従来の化学抗菌加工剤による人間の
皮膚に対する悪影響の改善、並びに化学抗菌剤の廃棄に
よる地球環境に対する生態系への悪影響の改善に貢献す
る方法を提供することを課題とする。In the present invention, curcumin, tannin and saponin contained in a turmeric extract have stable and high antibacterial properties, and as a result of intensive studies in view of such circumstances, conventional chemicals It is an object of the present invention to provide a method for improving the adverse effect on human skin caused by an antibacterial processing agent, and improving the adverse effect on the ecosystem due to the disposal of a chemical antibacterial agent on the global environment.
【0004】[0004]
【課題を解決するための手段】本発明のウコン抽出物溶
液による静菌及び制菌作用を有する抗菌繊維製品の製造
方法は、繊維製品をカチオン化剤を含む前処理液と接触
させてカチオン化処理した後、ウコンに含まれるクルク
ミン及びタンニン及びサポニンの抽出物を含む溶液と接
触させて反応させ、次に媒染剤を含む媒染液と接触を行
うものである。SUMMARY OF THE INVENTION According to the present invention, there is provided a method for producing an antibacterial fiber product having a bacteriostatic and bacteriostatic action using a turmeric extract solution. After the treatment, the turmeric is brought into contact with a solution containing an extract of curcumin, tannin and saponin to cause a reaction, and then is brought into contact with a mordant solution containing a mordant.
【0005】[0005]
【発明の実施の形態】本発明で使用するウコンの抽出物
とは、根部から抽出して得られるものである。BEST MODE FOR CARRYING OUT THE INVENTION The turmeric extract used in the present invention is obtained by extracting from a root.
【0006】本発明で使用するウコンは、ショウガ科の
Turmeric で、主に東南アジアが産地であ
る。この植物の乾燥品は市販品として入手でき、漢方薬
として血止剤、痔、創傷などに使用されており、食品で
あるカレー粉の主成分として多く用いられている。The turmeric used in the present invention is Turmeric, a ginger family, mainly from Southeast Asia. A dried product of this plant is available as a commercial product, and is used as a herbal medicine for hemostatic agents, hemorrhoids, wounds, and the like, and is often used as a main component of curry powder, which is a food.
【0007】繊維製品をカチオン化剤を含む前処理液と
接触させてカチオン化処理した後、ウコンの抽出物を含
む溶液と接触させて反応させ、次に媒染剤を含む媒染液
と接触させることによって、耐光堅牢度が向上する。[0007] The fiber product is subjected to a cationization treatment by contacting it with a pretreatment liquid containing a cationizing agent, followed by contact with a solution containing an extract of turmeric, followed by reaction with a mordant liquid containing a mordant. , Light fastness is improved.
【0008】本発明の方法に適用する繊維の材質は、木
綿、麻、絹、羊毛などの天然繊維が好ましい。繊維の形
状は、糸、織物、編み物、不織布のいずれであってもよ
い。The fiber material used in the method of the present invention is preferably a natural fiber such as cotton, hemp, silk and wool. The shape of the fiber may be any of yarn, woven fabric, knitted fabric and non-woven fabric.
【0009】本発明においては、繊維を必要に応じ糊抜
き、精練、漂白などを行ってから、カチオン化剤を含む
前処理液と接触させてカチオン化処理をする。市販の種
々のカチオン化剤を用いることが出来る。In the present invention, the fibers are subjected to desizing, scouring, bleaching and the like, if necessary, and then contacted with a pretreatment liquid containing a cationizing agent for cationization treatment. Various commercially available cationizing agents can be used.
【0010】カチオン化処理時の浴比は繊維製品の重量
に対し、20〜100倍程度、浴温は60℃〜90℃程
度、処理時間は30〜90分程度とすることが多い。カ
チオン化剤濃度は適宜に設定される。The bath ratio during the cationization treatment is often about 20 to 100 times the weight of the fiber product, the bath temperature is about 60 ° C. to 90 ° C., and the treatment time is about 30 to 90 minutes. The cationizing agent concentration is set appropriately.
【0011】ウコンによる抽出物を含む溶液による反応
処理時の浴比は繊維製品の重量に対し、20〜100倍
程度、浴温は60℃〜90℃、処理時間は30〜90分
とすることが多いが、必ずしもこの範囲に限定されな
い。ウコンによる抽出物を含む溶液濃度は抗菌製品の目
的に応じ広い範囲から選択しうる。The bath ratio during the reaction treatment with the solution containing the turmeric extract should be about 20 to 100 times the weight of the fiber product, the bath temperature should be 60 ° C. to 90 ° C., and the treatment time should be 30 to 90 minutes. , But is not necessarily limited to this range. The concentration of the solution containing the turmeric extract can be selected from a wide range depending on the purpose of the antimicrobial product.
【0012】反応処理後は、媒染剤を含む、媒染液と接
触反応させ、この工程は任意工程であるが、ウコン抽出
物溶液に含まれるクルクミン及びタンニン及びサポニン
の繊維に対する固着性及び染色堅牢度の点で設ける方が
好ましい。After the reaction treatment, it is contacted with a mordant solution containing a mordant, and this step is an optional step, and the curcumin, tannin, and saponin contained in the turmeric extract solution have a good fixation to the fiber and a high color fastness. It is more preferable to provide them at the point.
【0013】ここで、媒染剤としては酢酸アルミニウ
ム、硫酸アルミニウム、塩化アルミニウム、ミヨウバン
の他に、鉄媒染剤(木酢酸鉄、硫酸第一鉄、硝酸鉄)銅
媒染剤(銅塩)なども用いることができる。As the mordant, besides aluminum acetate, aluminum sulfate, aluminum chloride and alum, iron mordant (iron acetate, ferrous sulfate, iron nitrate), copper mordant (copper salt) and the like can also be used. .
【0014】媒染時の浴比は繊維製品の重量に対し、1
0〜100倍程度、浴温は常温ないし沸騰温度、処理時
間は10分〜1時間程度とすることが多いが、必ずしも
この範囲に限定されるものではない。The bath ratio at the time of mordant is 1 to the weight of the fiber product.
The bath temperature is usually about 0 to 100 times, the bath temperature is from normal temperature to boiling temperature, and the treatment time is about 10 minutes to 1 hour, but is not necessarily limited to this range.
【0015】ウコン抽出物溶液による繊維の抗菌加工工
程終了後は、適宜ソーピング、水洗いなどの後処理を行
ってから、日光乾燥、又は熱風乾燥する。After completion of the antibacterial processing step of the fiber with the turmeric extract solution, post-treatments such as soaping and washing with water are carried out as appropriate, and then sun drying or hot air drying.
【0016】[0016]
【実施例】次に実施例をあげて詳細に説明する。本説明
はこれに限定されるものではない。尚、実施例に示す
「%」とあるのは重量%を示す。EXAMPLES Next, examples will be described in detail. This description is not limited to this. It should be noted that "%" shown in the examples indicates% by weight.
【0017】ウコンの熱水抽出物 ウコンの粉末物100gに1000mlの水を加え、1
00℃で2時間煮沸、抽出した後、濾過しウコンの熱水
抽出物を得た。Turmeric hot water extract 1000 g of water is added to 100 g of turmeric powder,
After boiling and extraction at 00 ° C. for 2 hours, the mixture was filtered to obtain a hot water extract of turmeric.
【0018】綿生地の予備処理 綿生地100gと水道水2000ml(浴比1:20)
中に投入し、この液にカチオン化剤(日東紡績(株)製
のダンシェード185)2%o.w.fを加え、常温に
25分間浸透させた後、約10〜30分かけて65℃に
して5〜15分キープして、ついでNaOH(フレー
ク)3g/リットルを、はじめ3/10ついで7/10
加えて約85℃×30〜1時間加熱した。次に綿生地を
取り出して水洗いし、この液に酢酸1g/リットル(5
ml/リットル)を加えて中和し、40℃にして5分間
浸透させた。最後に水洗い、脱水してカチオン処理布を
得た。Pretreatment of cotton fabric 100 g of cotton fabric and 2000 ml of tap water (bath ratio 1:20)
And 2% o.c. of a cationizing agent (Danshade 185 manufactured by Nitto Boseki Co., Ltd.) w. f, infiltrate at room temperature for 25 minutes, keep at 65 ° C. for about 10 to 30 minutes, keep for 5 to 15 minutes, then add 3 g / liter of NaOH (flakes), 3/10 first, then 7/10
In addition, heating was performed at about 85 ° C. for 30 to 1 hour. Next, the cotton fabric is taken out and washed with water, and acetic acid 1 g / liter (5
(ml / liter), and the mixture was neutralized and permeated at 40 ° C. for 5 minutes. Finally, it was washed with water and dehydrated to obtain a cation-treated cloth.
【0019】染着―媒染反応 ウコン抽出物液に上記のカチオン処理布100gを入れ
てから加温し、85℃にて30分〜1時間加熱染着反応
させた後水洗いをし、酢酸アルミニウム液2g/リット
ルを10〜20倍の水に溶解し、この液に調整した染着
処理布を30℃20分加温し反応させた後水洗、脱水、
乾燥した。Dyeing-mordanting reaction 100 g of the above-mentioned cation-treated cloth is added to the turmeric extract solution, heated, and subjected to a heating dyeing reaction at 85 ° C. for 30 minutes to 1 hour, followed by washing with water and aluminum acetate solution. 2 g / liter is dissolved in 10 to 20 times the volume of water, and the dyeing-treated cloth adjusted to this solution is heated at 30 ° C. for 20 minutes to react, followed by washing with water, dehydration,
Dried.
【0020】抗菌性試験 上記で得られたウコン染着綿布を用いて黄色ぶどう球菌
(Staphylococcusaureus ATC
C 6538P)並びに肺炎桿菌(Klebsiell
a pneumoniae ATCC 4352)の抗
菌力試験を行った所、これらの菌に対して下記のような
抗菌性が認められた。結果を表1に示す。Antibacterial test Using the turmeric-dyed cotton cloth obtained above, Staphylococcus aureus ATC was used.
C 6538P) and Klebsiella (Klebsiell)
a. pneumoniae ATCC 4352) was tested for antibacterial activity, and the following antibacterial properties were observed for these bacteria. Table 1 shows the results.
【0021】[0021]
【表1】 試験方法:統一試験法(繊維製品新機能評価協議会) 供試菌:黄色ぶどう球菌(Staphylococcu
s aureus ATCC 6538P) 肺炎桿菌(Klebsiella pneumonia
e ATCC 4352) 洗濯方法:JIS L 0217 103号(但し、J
AFET標準洗剤を使用) 〈抗菌防臭の基準値:静菌活性値≧2.2以上〉 〈制菌加工基準値:殺菌活性値≧0.0以上〉[Table 1] Test method: Unified test method (Fiber Product New Function Evaluation Council) Test bacteria: Staphylococcus
s aureus ATCC 6538P) Klebsiella pneumonia
e ATCC 4352) Washing method: JIS L 0217 103 (however, J
(Use AFET standard detergent) <Standard value of antibacterial and deodorant: Bacteriostatic activity value> 2.2 or more><Bactericidal processing standard value: Bactericidal activity value> 0.0 or more>
Claims (1)
と接触させてカチオン化処理した後、ウコンに含まれる
クルクミン及びタンニン及びサポニンの抽出物を含む溶
液と接触させて反応させ、次に媒染剤を含む媒染液と接
触を行うことを特徴とするウコン抽出物溶液による静菌
及び制菌作用を有する抗菌繊維製品の製造方法。Claims 1. After cationizing a textile product by contacting it with a pretreatment solution containing a cationizing agent, the fiber product is contacted with a solution containing an extract of curcumin and tannin and saponin contained in turmeric, and reacted. A method for producing an antibacterial fiber product having a bacteriostatic and bacteriostatic action using a turmeric extract solution, which is brought into contact with a mordant solution containing a mordant.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP34516299A JP2001131866A (en) | 1999-10-29 | 1999-10-29 | Antifungal and antibacterial treatment of fiber with turmeric extract |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP34516299A JP2001131866A (en) | 1999-10-29 | 1999-10-29 | Antifungal and antibacterial treatment of fiber with turmeric extract |
Publications (1)
Publication Number | Publication Date |
---|---|
JP2001131866A true JP2001131866A (en) | 2001-05-15 |
Family
ID=18374712
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP34516299A Pending JP2001131866A (en) | 1999-10-29 | 1999-10-29 | Antifungal and antibacterial treatment of fiber with turmeric extract |
Country Status (1)
Country | Link |
---|---|
JP (1) | JP2001131866A (en) |
Cited By (11)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP2013542216A (en) * | 2010-10-29 | 2013-11-21 | シュバイツァー モウドゥイ インターナショナル インコーポレイテッド | Method for producing plant-derived products impregnated with liquid plant material |
CN105113071A (en) * | 2015-08-20 | 2015-12-02 | 湖州繁华绢纺有限公司 | High-count spun silk yarn production method |
JP2015218403A (en) * | 2014-05-15 | 2015-12-07 | 株式会社シオンテック | Method for producing antibacterial fiber, and the antibacterial fiber |
US10729662B2 (en) | 2013-08-20 | 2020-08-04 | Schweitzer-Mauduit International, Inc. | Product comprising a plant for medicinal, cosmetic, coloring or dermatologic use |
US10751282B2 (en) | 2013-08-02 | 2020-08-25 | Schweitzer-Mauduit International, Inc. | Edible product comprising reconstituted plant material |
US11035079B2 (en) | 2016-04-05 | 2021-06-15 | Schweitzer-Mauduit International, Inc. | Vegetable paper comprising fibres of a plant |
CN113863009A (en) * | 2021-10-15 | 2021-12-31 | 厦门勤嘉诚工贸有限公司 | Environment-friendly antibacterial split polyester fabric |
US11419347B2 (en) | 2013-02-28 | 2022-08-23 | Schweitzer-Mauduit International, Inc. | Composition for making a tea beverage or herbal and vegetable broths |
US11484497B2 (en) | 2013-02-28 | 2022-11-01 | Schweitzer-Mauduit International, Inc. | Composition for making a tea beverage or herbal and vegetable broths |
CN115897234A (en) * | 2022-12-09 | 2023-04-04 | 罗莱生活科技股份有限公司 | Antibacterial cotton fiber and preparation method and application thereof |
US11737472B2 (en) | 2015-03-02 | 2023-08-29 | Mativ Holdings, Inc. | Low bulk density composition for making a tea beverage having reduced dust or fines |
-
1999
- 1999-10-29 JP JP34516299A patent/JP2001131866A/en active Pending
Cited By (17)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP2013542216A (en) * | 2010-10-29 | 2013-11-21 | シュバイツァー モウドゥイ インターナショナル インコーポレイテッド | Method for producing plant-derived products impregnated with liquid plant material |
JP2017031187A (en) * | 2010-10-29 | 2017-02-09 | シュバイツァー モウドゥイ インターナショナル インコーポレイテッド | Production method of plant-derived product into which liquid plant substance is impregnated |
US10178872B2 (en) | 2010-10-29 | 2019-01-15 | Schweitzer-Manduit International, Inc. | Method for producing articles of plant origin impregnated with a liquid plant substance |
US11484497B2 (en) | 2013-02-28 | 2022-11-01 | Schweitzer-Mauduit International, Inc. | Composition for making a tea beverage or herbal and vegetable broths |
US11419347B2 (en) | 2013-02-28 | 2022-08-23 | Schweitzer-Mauduit International, Inc. | Composition for making a tea beverage or herbal and vegetable broths |
US11207268B2 (en) | 2013-08-02 | 2021-12-28 | Schweitzer-Mauduit International, Inc. | Edible product comprising reconstituted plant material |
US10751282B2 (en) | 2013-08-02 | 2020-08-25 | Schweitzer-Mauduit International, Inc. | Edible product comprising reconstituted plant material |
US11666530B2 (en) | 2013-08-02 | 2023-06-06 | Schweitzer-Mauduit International, Inc. | Edible product comprising reconstituted plant material |
US10729662B2 (en) | 2013-08-20 | 2020-08-04 | Schweitzer-Mauduit International, Inc. | Product comprising a plant for medicinal, cosmetic, coloring or dermatologic use |
JP2015218403A (en) * | 2014-05-15 | 2015-12-07 | 株式会社シオンテック | Method for producing antibacterial fiber, and the antibacterial fiber |
US11737472B2 (en) | 2015-03-02 | 2023-08-29 | Mativ Holdings, Inc. | Low bulk density composition for making a tea beverage having reduced dust or fines |
CN105113071A (en) * | 2015-08-20 | 2015-12-02 | 湖州繁华绢纺有限公司 | High-count spun silk yarn production method |
US11035079B2 (en) | 2016-04-05 | 2021-06-15 | Schweitzer-Mauduit International, Inc. | Vegetable paper comprising fibres of a plant |
US11619007B2 (en) | 2016-04-05 | 2023-04-04 | Mativ Holdings, Inc. | Vegetable paper comprising fibres of a plant |
CN113863009A (en) * | 2021-10-15 | 2021-12-31 | 厦门勤嘉诚工贸有限公司 | Environment-friendly antibacterial split polyester fabric |
CN115897234A (en) * | 2022-12-09 | 2023-04-04 | 罗莱生活科技股份有限公司 | Antibacterial cotton fiber and preparation method and application thereof |
CN115897234B (en) * | 2022-12-09 | 2024-01-30 | 罗莱生活科技股份有限公司 | Antibacterial cotton fiber and preparation method and application thereof |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
CN104396965B (en) | A kind of response type halogen amine antiseptic-germicide and its preparation method and application | |
CN100460590C (en) | Antimicrobial yarn having nanosilver particles and methods for manufacturing the same | |
CN101084343A (en) | Manufacturing methods and applications of antimicrobial plant fibers having silver particles | |
CN103554085B (en) | Reaction-type halogen amine antibacterial agent, and synthetic method and application thereof | |
JP2001131866A (en) | Antifungal and antibacterial treatment of fiber with turmeric extract | |
JPH0610272A (en) | Finishing agent for woven fabric | |
CN103058945A (en) | Halide amine antibacterial agent based on cyanuric acid and synthesis method and application thereof | |
JP3262875B2 (en) | Manufacturing method of tea-dyed fiber products | |
JP2000096433A (en) | Production of antibacterial fiber | |
KR101045388B1 (en) | A method of dyeing accomplishing antibiosis | |
CN112176725A (en) | Carboxyl esterification complex antibacterial fiber, preparation method and application | |
CN101153460B (en) | Ecological antimicrobial fabric and method for producing the same | |
JP2001131864A (en) | Method of antifungal and antibacterial treatment of fiber with tea extract | |
CN106702741A (en) | Antibacterial finishing liquid containing modified sericin protein and preparation method of antibacterial finishing liquid | |
JP3484520B2 (en) | Antimicrobial fiber product and method for producing the same | |
CN108708163A (en) | A kind of textile degerming method of simple process | |
CN115770203A (en) | Modified jojoba oil and preparation method and application thereof | |
JP2001131873A (en) | Method for producing antibacterial fiber finished by papaya extract solution | |
JP4166325B2 (en) | Antibacterial deodorant filter and production method thereof | |
JP2001131865A (en) | Antifungal and antibacterial treatment of fiber with red wine stum | |
WO2022099827A1 (en) | Method for preparing antimicrobial treatment agent for textile | |
JPH04185770A (en) | Treatment of textile product | |
JPH01213484A (en) | Deodorization processing of textile product | |
JPH06116879A (en) | Antibacterial dyeing of cotton | |
JP3268553B2 (en) | Processing method of cellulosic fiber |